CN108912919A - A kind of preparation method of multi-color - Google Patents
A kind of preparation method of multi-color Download PDFInfo
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- CN108912919A CN108912919A CN201810860783.9A CN201810860783A CN108912919A CN 108912919 A CN108912919 A CN 108912919A CN 201810860783 A CN201810860783 A CN 201810860783A CN 108912919 A CN108912919 A CN 108912919A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D133/00—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Coating compositions based on derivatives of such polymers
- C09D133/04—Homopolymers or copolymers of esters
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D143/00—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and containing boron, silicon, phosphorus, selenium, tellurium, or a metal; Coating compositions based on derivatives of such polymers
- C09D143/04—Homopolymers or copolymers of monomers containing silicon
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/29—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes for multicolour effects
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/65—Additives macromolecular
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
- C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
Abstract
The present invention provides a kind of preparation methods of multi-color, including：(1) colloidal solution is prepared；(2) preparation toning base-material；(3) toning point processed：It is that toning base-material is tuned into required each color, is matched colors with reference to toning with actual effect；Toning base-material and colloidal solution are pressed 5：3 ratio is uniformly mixed, and obtains colloidal mixture, colloidal mixture is sheared colloidal particle；(4) continuous；(5) it mixes：Colloidal particle obtained in step (3) is added in continuous mixed liquor obtained in step (4), is stirred evenly to get multi-color is arrived.Colorful paint formula of the invention is reasonable, particularly with the addition of enhancing modified cellulose, can effectively improve the hardness toughness of particle, it is made to be not easy to disperse in transit.
Description
Technical field
The present invention relates to decorating inner and external walls technical field of coatings, and in particular to a kind of preparation method of multi-color.
Background technique
Multi-color is that two or more aqueous colored particle is suspended in aqueous interlayer, more by once spraying generation
The one-component coating for exterior walls of buildings of kind color is applied to copy stone effect, therefore also known as liquid stone more.It is to adopt
It is painted with base-material with acrylic silicon resin lotion and fluorocarbon resin cream, in conjunction with high-quality inorganic pigment and high performance adjuvant, breaks through coating
Chemical industry scientific principle, the water-based exterior wall multi-color being process through special process.
The hardness toughness of the multi-color applied in the field of construction at present, particle is insufficient, during transportation, multi-color
Easily disperse between particle.
Summary of the invention
It is easy in transportational process technical problem to be solved by the present invention lies in the hardness toughness deficiency of existing multi-color particle
The problem of dispersion.
The present invention solves above-mentioned technical problem by the following technical programs：
A kind of preparation method of multi-color, including：
(1) colloidal solution is prepared
Prepare deionized water 890-960 parts by weight, aqueous colorful protective glue 60-70 parts by weight, by the two mix and it is abundant
Dissolution, obtains colloidal solution；
(2) preparation toning base-material
Following raw material is successively added into water：5-10 parts of cellulose, enhance modified cellulose 20-40 parts, more function
Can be 1-3 parts of auxiliary agent, 1-3 parts of dispersing agent, 1-2 parts of wetting agent, 1-3 parts of defoaming agent, 10-20 parts of titanium dioxide, 40-60 parts of kaolin,
1-3 parts of fungicide, 9-12 parts of coalescing agent, 8-10 parts of propylene glycol, 180-240 parts of pure acrylic latex, colloidal solution 80-110
Part；It is stirred continuously mixed liquor in adding procedure, finally adds 1-2 parts of defoaming agent, 1-3 parts of thickener are continued to stir evenly, and are obtained
To toning base-material；
(3) toning point processed
It is that toning base-material is tuned into required each color, is matched colors with reference to toning with actual effect；To mix colours base-material
5 are pressed with colloidal solution：3 ratio is uniformly mixed, and obtains colloidal mixture, colloidal mixture is sheared colloidal particle；
(4) continuous
Prepare water 60-70 parts, side stirs and successively adds following raw material into water：0.3-1 parts of fungicide, defoaming
0.1-0.5 parts of agent, 6-7 parts of coalescing agent, 1-4 parts of propylene glycol, 100-140 parts of silicone acrylic emulsion, 0.1-0.3 parts of multifunctional assistant,
0-0.4 parts of thickener, obtain continuous mixed liquor；
(5) it mixes
Colloidal particle obtained in step (3) is added in continuous mixed liquor obtained in step (4), is stirred evenly, i.e.,
Obtain multi-color.
Preferably, in the step (1), prepare 935 parts by weight of deionized water, 65 parts by weight of aqueous colorful protective glue.
Preferably, in the step (2), following raw material is successively added into water：7 parts of cellulose, enhancing is modified
30 parts of cellulose, 2 parts of multifunctional assistant, 2 parts of dispersing agent, 1.5 parts of wetting agent, 2 parts of defoaming agent, 15 parts of titanium dioxide, kaolin 50
Part, 2 parts of fungicide, 10 parts of coalescing agent, 9 parts of propylene glycol, 200 parts of pure acrylic latex, 100 parts of colloidal solution；Adding procedure
In be stirred continuously mixed liquor, finally add 1.5 parts of defoaming agent, 2 parts of thickener.
Preferably, in the step (2), cellulose selects cellulose HBR-250, and multifunctional assistant selects AMP-95, institute
It states dispersing agent and selects ammonium salt dispersing agent, the wetting agent selects non-anion wetting agent, and the titanium dioxide selects golden red titanium dioxide,
It is 6.5% S-482 solution that the colloidal solution, which selects mass fraction, and the pure acrylic latex selects pure acrylic latex
2788。
Preferably, in the step (2), enhancing modified cellulose selects enhancing modified cellulose AF-40.
Preferably, in the step (3), toning base-material is 500 parts by weight, and colloidal solution is 300 parts by weight.
Preferably, in the step (3), the particle size of colloidal particle is -30 mesh of 10 mesh.
Preferably, in the step (4), prepare 65 parts by weight of water, side stirs and successively adds following parts by weight into water
Raw material：0.5 part of fungicide, 0.2 part of defoaming agent, 6.5 parts of coalescing agent, 2 parts of propylene glycol, 125 parts of silicone acrylic emulsion, multifunctional assistant
0.2 part, 0.2 part of thickener.
Preferably, in the step (4), multifunctional assistant selects AMP-95, and thickener selects thickener 936.
Compared with prior art, the present invention having following beneficial effect：
Colorful paint formula of the invention is reasonable, particularly with the addition of enhancing modified cellulose, can effectively improve the hard of particle
Toughness is spent, while it being made to be not easy to disperse between particle in transit, color is more bright-coloured bright after brushing.
Specific embodiment
Below with reference to embodiment, the invention will be further described.
Embodiment 1
A kind of preparation method of multi-color, including：
(1) colloidal solution is prepared
Prepare 890 parts by weight of deionized water, the two is mixed and sufficiently dissolved, obtained by 60 parts by weight of aqueous colorful protective glue
To colloidal solution；
(2) preparation toning base-material
Following raw material is successively added into water：5 parts of cellulose, enhance 20 parts of modified cellulose, multifunctional assistant 1
Part, 1 part of dispersing agent, 1 part of wetting agent, 1 part of defoaming agent, 10 parts of titanium dioxide, 40 parts of kaolin, 1 part of fungicide, 9 parts of coalescing agent,
8 parts of propylene glycol, 180 parts of pure acrylic latex, 80 parts of colloidal solution；It is stirred continuously mixed liquor in adding procedure, finally adds
1 part of defoaming agent, 1 part of thickener is continued to stir evenly, and obtains toning base-material；
Above-mentioned cellulose selects cellulose HBR-250, and multifunctional assistant selects AMP-95, and the dispersing agent selects ammonium salt point
Powder, the wetting agent select non-anion wetting agent, and the titanium dioxide selects golden red titanium dioxide, and the colloidal solution selects matter
The S-482 solution that score is 6.5% is measured, the pure acrylic latex selects pure acrylic latex 2788.Enhance modified cellulose
Select enhancing modified cellulose AF-40.
(3) toning point processed
It is that toning base-material is tuned into required each color, is matched colors with reference to toning with actual effect；To mix colours base-material
5 are pressed with colloidal solution：3 ratio is uniformly mixed, and obtains colloidal mixture, and it is 10 that colloidal mixture, which is sheared glue into particle size,
Mesh colloidal particle；
(4) continuous
Prepare 60 parts of water, side stirs and successively adds following raw material into water：0.3 part of fungicide, defoaming agent 0.1
Part, 6 parts of coalescing agent, 1 part of propylene glycol, 100 parts of silicone acrylic emulsion, 0.1 part of multifunctional assistant, obtain continuous mixed liquor；It is described more
Function additive selects AMP-95, and thickener selects thickener 936；
(5) it mixes
Colloidal particle obtained in step (3) is added in continuous mixed liquor obtained in step (4), is stirred evenly, i.e.,
Obtain multi-color.
Embodiment 2
A kind of preparation method of multi-color, including：
(1) colloidal solution is prepared
Prepare 935 parts by weight of deionized water, the two is mixed and sufficiently dissolved, obtained by 65 parts by weight of aqueous colorful protective glue
To colloidal solution；
(2) preparation toning base-material
Following raw material is successively added into water：7 parts of cellulose, enhance 30 parts of modified cellulose, multifunctional assistant 2
Part, 2 parts of dispersing agent, 1.5 parts of wetting agent, 2 parts of defoaming agent, 15 parts of titanium dioxide, 50 parts of kaolin, 2 parts of fungicide, coalescing agent 10
Part, 9 parts of propylene glycol, 200 parts of pure acrylic latex, 100 parts of colloidal solution；Mixed liquor is stirred continuously in adding procedure, finally again
1.5 parts of defoaming agent are added, 2 parts of thickener are continued to stir evenly, and obtain toning base-material；
Above-mentioned cellulose selects cellulose HBR-250, and multifunctional assistant selects AMP-95, and the dispersing agent selects ammonium salt point
Powder, the wetting agent select non-anion wetting agent, and the titanium dioxide selects golden red titanium dioxide, and the colloidal solution selects matter
The S-482 solution that score is 6.5% is measured, the pure acrylic latex selects pure acrylic latex 2788.Enhance modified cellulose
Select enhancing modified cellulose AF-40.
(3) toning point processed
It is that toning base-material is tuned into required each color, is matched colors with reference to toning with actual effect；To mix colours base-material
5 are pressed with colloidal solution：3 ratio is uniformly mixed, wherein toning base-material is 500 parts by weight, colloidal solution is 300 parts by weight, is obtained
To colloidal mixture, it is -30 mesh colloidal particle of 10 mesh that colloidal mixture, which is sheared glue into particle size,；
(4) continuous
Prepare 65 parts of water, side stirs and successively adds following raw material into water：0.5 part of fungicide, defoaming agent 0.2
Part, it 6.5 parts of coalescing agent, 2 parts of propylene glycol, 125 parts of silicone acrylic emulsion, 0.2 part of multifunctional assistant, 0.2 part of thickener, obtains continuous
Mixed liquor；The multifunctional assistant selects AMP-95, and thickener selects thickener 936；
(5) it mixes
Colloidal particle obtained in step (3) is added in continuous mixed liquor obtained in step (4), is stirred evenly, i.e.,
Obtain multi-color.
Embodiment 3
A kind of preparation method of multi-color, including：
(1) colloidal solution is prepared
Prepare 960 parts by weight of deionized water, the two is mixed and sufficiently dissolved, obtained by 70 parts by weight of aqueous colorful protective glue
To colloidal solution；
(2) preparation toning base-material
Following raw material is successively added into water：10 parts of cellulose, enhance 40 parts of modified cellulose, multifunctional assistant
3 parts, 3 parts of dispersing agent, 2 parts of wetting agent, 3 parts of defoaming agent, 20 parts of titanium dioxide, 60 parts of kaolin, 3 parts of fungicide, coalescing agent 12
Part, 10 parts of propylene glycol, 240 parts of pure acrylic latex, 110 parts of colloidal solution；Mixed liquor is stirred continuously in adding procedure, finally again
2 parts of defoaming agent are added, 3 parts of thickener are continued to stir evenly, and obtain toning base-material；
Above-mentioned cellulose selects cellulose HBR-250, and multifunctional assistant selects AMP-95, and the dispersing agent selects ammonium salt point
Powder, the wetting agent select non-anion wetting agent, and the titanium dioxide selects golden red titanium dioxide, and the colloidal solution selects matter
The S-482 solution that score is 6.5% is measured, the pure acrylic latex selects pure acrylic latex 2788.Enhance modified cellulose
Select enhancing modified cellulose AF-40.
(3) toning point processed
It is that toning base-material is tuned into required each color, is matched colors with reference to toning with actual effect；To mix colours base-material
5 are pressed with colloidal solution：3 ratio is uniformly mixed, and obtains colloidal mixture, and it is 30 that colloidal mixture, which is sheared glue into particle size,
Mesh colloidal particle；
(4) continuous
Prepare 70 parts of water, side stirs and successively adds following raw material into water：1 part of fungicide, defoaming agent 0.5
Part, it 7 parts of coalescing agent, 4 parts of propylene glycol, 140 parts of silicone acrylic emulsion, 0.3 part of multifunctional assistant, 0.4 part of thickener, is continuously mixed
Close liquid；The multifunctional assistant selects AMP-95, and thickener selects thickener 936；
(5) it mixes
Colloidal particle obtained in step (3) is added in continuous mixed liquor obtained in step (4), is stirred evenly, i.e.,
Obtain multi-color.
The foregoing is only a preferred embodiment of the present invention, is not intended to restrict the invention, although referring to aforementioned reality
Applying example, invention is explained in detail, for those skilled in the art, still can be to aforementioned each implementation
Technical solution documented by example is modified or equivalent replacement of some of the technical features.It is all in essence of the invention
Within mind and principle, any modification, equivalent replacement, improvement and so on be should all be included in the protection scope of the present invention.
Claims (9)
1. a kind of preparation method of multi-color, which is characterized in that including：
(1) colloidal solution is prepared
Preparing deionized water 890-960 parts by weight, the two is mixed and is sufficiently dissolved by aqueous colorful protective glue 60-70 parts by weight,
Obtain colloidal solution；
(2) preparation toning base-material
Following raw material is successively added into water：5-10 parts of cellulose, enhance modified cellulose 20-40 parts, multifunctional assistant
1-3 parts of agent, 1-3 parts of dispersing agent, 1-2 parts of wetting agent, 1-3 parts of defoaming agent, 10-20 parts of titanium dioxide, 40-60 parts of kaolin, sterilization
1-3 parts of agent, 9-12 parts of coalescing agent, 8-10 parts of propylene glycol, 180-240 parts of pure acrylic latex, 80-110 parts of colloidal solution；Add
It is stirred continuously mixed liquor during adding, finally adds 1-2 parts of defoaming agent, 1-3 parts of thickener are continued to stir evenly, and are mixed colours
Base-material；
(3) toning point processed
It is that toning base-material is tuned into required each color, is matched colors with reference to toning with actual effect；It will toning base-material and glue
Liquid solution presses 5：3 ratio is uniformly mixed, and obtains colloidal mixture, colloidal mixture is sheared colloidal particle；
(4) continuous
Prepare water 60-70 parts, side stirs and successively adds following raw material into water：0.3-1 parts of fungicide, defoaming agent
0.1-0.5 parts, 6-7 parts of coalescing agent, 1-4 parts of propylene glycol, 100-140 parts of silicone acrylic emulsion, 0.1-0.3 parts of multifunctional assistant, increase
Thick dose 0-0.4 parts, obtain continuous mixed liquor；
(5) it mixes
Colloidal particle obtained in step (3) is added in continuous mixed liquor obtained in step (4), is stirred evenly to get arriving
Multi-color.
2. a kind of preparation method of multi-color according to claim 1, which is characterized in that in the step (1), be ready to
935 parts by weight of ionized water, 65 parts by weight of aqueous colorful protective glue.
3. a kind of preparation method of multi-color according to claim 1, which is characterized in that in the step (2), successively to
Following raw material is added in water：7 parts of cellulose, 30 parts of modified cellulose of enhancing, 2 parts of multifunctional assistant, 2 parts of dispersing agent,
1.5 parts of wetting agent, 2 parts of defoaming agent, 15 parts of titanium dioxide, 50 parts of kaolin, 2 parts of fungicide, 10 parts of coalescing agent, 9 parts of propylene glycol,
200 parts of pure acrylic latex, 100 parts of colloidal solution；It is stirred continuously mixed liquor in adding procedure, finally adds defoaming agent 1.5
Part, 2 parts of thickener.
4. a kind of preparation method of multi-color according to claim 1, which is characterized in that in the step (2), cellulose
Cellulose HBR-250 is selected, multifunctional assistant selects AMP-95, and the dispersing agent selects ammonium salt dispersing agent, the wetting agent choosing
With non-anion wetting agent, the titanium dioxide selects golden red titanium dioxide, and it is 6.5% S- that the colloidal solution, which selects mass fraction,
482 solution, the pure acrylic latex select pure acrylic latex 2788.
5. a kind of preparation method of multi-color according to claim 1, which is characterized in that in the step (2), enhancing changes
Property cellulose select enhancing modified cellulose AF-40.
6. a kind of preparation method of multi-color according to claim 1, which is characterized in that in the step (3), base of mixing colours
Material is 500 parts by weight, and colloidal solution is 300 parts by weight.
7. a kind of preparation method of multi-color according to claim 1, which is characterized in that in the step (3), gluey
The particle size of grain is -30 mesh of 10 mesh.
8. a kind of preparation method of multi-color according to claim 1, which is characterized in that in the step (4), prepare water
65 parts by weight, side stir and successively add following raw material into water：0.5 part of fungicide, 0.2 part of defoaming agent, film forming helps
6.5 parts of agent, 2 parts of propylene glycol, 125 parts of silicone acrylic emulsion, 0.2 part of multifunctional assistant, 0.2 part of thickener.
9. a kind of preparation method of multi-color according to claim 1, which is characterized in that multi-functional in the step (4)
Selection of auxiliary AMP-95, thickener select thickener 936.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201810860783.9A CN108912919A (en) | 2018-08-01 | 2018-08-01 | A kind of preparation method of multi-color |
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| CN201810860783.9A CN108912919A (en) | 2018-08-01 | 2018-08-01 | A kind of preparation method of multi-color |
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| CN108912919A true CN108912919A (en) | 2018-11-30 |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109735185A (en) * | 2018-12-27 | 2019-05-10 | 兰州梓苑环保科技有限公司 | A kind of novel water-in-water multicolor coating and preparation method thereof |
-
2018
- 2018-08-01 CN CN201810860783.9A patent/CN108912919A/en active Pending
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109735185A (en) * | 2018-12-27 | 2019-05-10 | 兰州梓苑环保科技有限公司 | A kind of novel water-in-water multicolor coating and preparation method thereof |
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Application publication date: 20181130 |