CN108911593A - A kind of lacquer and preparation method thereof - Google Patents
A kind of lacquer and preparation method thereof Download PDFInfo
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- CN108911593A CN108911593A CN201810648828.6A CN201810648828A CN108911593A CN 108911593 A CN108911593 A CN 108911593A CN 201810648828 A CN201810648828 A CN 201810648828A CN 108911593 A CN108911593 A CN 108911593A
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- lacquer
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B26/00—Compositions of mortars, concrete or artificial stone, containing only organic binders, e.g. polymer or resin concrete
- C04B26/30—Compounds having one or more carbon-to-metal or carbon-to-silicon linkages ; Other silicon-containing organic compounds; Boron-organic compounds
- C04B26/32—Compounds having one or more carbon-to-metal or carbon-to-silicon linkages ; Other silicon-containing organic compounds; Boron-organic compounds containing silicon
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2111/00—Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
- C04B2111/00474—Uses not provided for elsewhere in C04B2111/00
- C04B2111/00482—Coating or impregnation materials
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2111/00—Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
- C04B2111/20—Resistance against chemical, physical or biological attack
- C04B2111/27—Water resistance, i.e. waterproof or water-repellent materials
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2111/00—Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
- C04B2111/80—Optical properties, e.g. transparency or reflexibility
- C04B2111/82—Coloured materials
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Ceramic Engineering (AREA)
- Materials Engineering (AREA)
- Structural Engineering (AREA)
- Organic Chemistry (AREA)
- Paints Or Removers (AREA)
Abstract
The present invention relates to field of material technology, especially a kind of lacquer and preparation method thereof；Its mass parts composition is as follows：10-20 parts of hydroxypropyl methyl cellulose, TD66110-20 parts of silicone acrylic emulsion, 2-10 parts of coalescing agent, 0.05-0.5 parts of thickened systems, 0.1-0.5 parts of hydrophober, 0.1-0.2 parts of sterilization antiseptic, 80-200 parts of quartz sand, 0.1-0.3 parts of adsorbent modifier, 10-40 parts of deionized water；Lacquer wall surface coating color of the invention is uniform, without color difference, under exposing to the weather, fades for a long time, lotion is water-fast, good weatherability, is not easy xanthochromia；Lotion in the present invention uses silicone acrylic emulsion TD661, so that lacquer of the invention water resistance with higher and alkali resistance；Tool closes whitening resistance waterproof outstanding, anti-after-tackiness and the general salt of alkali resistant, fabulous adhesive force, cohesion.
Description
Technical field
The present invention relates to field of material technology, especially a kind of lacquer and preparation method thereof.
Background technique
Lacquer is that a kind of decorative effect exactly likes marble, granite, and the building after lacquer decoration has natural true
Real natural colour gives graceful harmonious, serious aesthetic feeling, is suitable for the interior/exterior decoration of various buildings, can receive
Vividly, the effect of true to nature, back to nature, exterior wall true stone paint is reaching almost phase compared with granite lithotome finishing material
In the case where same decoration grain effect, have the following advantages that：1. it is at low cost, it is equivalent to cladding marmorean 1/4 or so；2. applying
Work technique is relatively simple；It can be achieved personalized aesthetic.3. safety, granite self weight conference increases wall load-bearing, exists not
Safety factor.4. health, part granite building material can also discharge the micro radioactive element harmful to human health；5. real
With property, can be widely used on the various basic materials such as cement wall, outer wall heat preservation system, asbestos board.To comply with building energy conservation
Development trend and meet security requirement, decorative effect is abundant and has excellent performance, highly-safe lacquer coating just gradually generation
For exterior wall lithotome facing, become the mainstream of external wall decorative material.
In practical engineering applications, the problems such as easily there is color difference in lacquer, the accumulation of salt in the surface soil whitens, floating is cracked, and stain resistance is poor,
This project is set about from constituent, the mechanism of action, the preparation method of research lacquer, by raw material types, volume progress
A large amount of comparative experiments, obtains different base-material kinds and grading of aggregates, auxiliary agent volume, and finish selects the shadow to lacquer performance
It rings, determination obtains a kind of lacquer exterior coating system that effect is optimal.
Summary of the invention
The purpose of the present invention is：There is provided that a kind of caking property is good, is not easy to form hollowing, true stone with long service life after use
Paint, another object of the present invention are to provide a kind of preparation method of lacquer.
In order to solve the above technical problems, the technical solution adopted by the present invention is as follows：
A kind of lacquer, mass parts composition are as follows：10-20 parts of hydroxypropyl methyl cellulose, silicone acrylic emulsion TD66110-
20 parts, 2-10 parts of coalescing agent, 0.05-0.5 parts of thickened systems, 0.1-0.5 parts of hydrophober, 0.1-0.2 parts of sterilization antiseptic, stone
80-200 parts of sand, 0.1-0.3 parts of adsorbent modifier, 10-40 parts of deionized water.
Preferably, the coalescing agent select glycerine Block polyoxyethylene oleic acid ester, silane based modified porous starch,
The mixture of allyl methyl phenyl ether, mass ratio 1:1.2-1.5:1.
Preferably, the dispersing agent selects the mixture of sodium tripolyphosphate and acrylate copolymer, mass ratio 1:
1.5-2。
Preferably, the thickened systems use the mixture of hydroxyethyl ether cellulose and the non-swollen ASE60 of association type alkali soluble,
Mass ratio is 1:1.2-3.
Preferably, the hydrophober selects organosiloxane, the agent of LLD super-hydrophobicity nano-interface, one in polysiloxanes
Kind is several.
Preferably, the hydrophober selects the nano-interface agent of LLD super-hydrophobicity.
Preferably, in the quartz sand 40-80 mesh mass fraction be quartz sand total amount 60%, 100-120 mesh matter
Measure 40% that score is quartz sand total amount.
Preferably, the defoaming agent is selected from one or more of metal soap NXZ, paraffin class 1340, EFKA8580.
A method of the lacquer prepared the described method comprises the following steps：
(1) it is added deionized water in high speed disperser, control mixing speed is 300-400rpm, is successively slowly added to point
Powder, part defoaming agent, hydroxypropyl methyl cellulose add rear revolving speed and improve to 1000rpm, stirs 5-10min, be in slurry
Then transparent g., jelly-like adjusts revolving speed 600rpm, pigments and fillers are added in uniform speed slow, adds rear revolving speed and is adjusted to 1200rpm, high speed point
10min is dissipated,
(2) control revolving speed is 500rpm, is slowly added to coalescing agent, silicone acrylic emulsion TD66, hydrophober, adsorbent modifier,
PH value is adjusted to 8.5-9 with NaOH, is stirred 10min, is obtained slurry；
(3) it is successively slowly added to quartz sand while stirring, it is that 600-800rpm stirs 10min that revolving speed is controlled after adding, according to
Secondary addition sterilization antiseptic and remaining defoaming agent, are finally added dropwise thickened systems while stirring, add and continue to stir 10min, adjust
It discharges after section appropriate viscosity.
Preferably, the defoaming agent added in the step (1) is the half that dosage is defoamed in formula.
It is using the beneficial effect of technical solution of the present invention：
1, lacquer wall surface coating color of the invention is uniform, without color difference, under exposing to the weather, fades for a long time, cream
Liquid is water-fast, good weatherability, is not easy xanthochromia；
2, the lotion in the present invention uses silicone acrylic emulsion TD661, so that lacquer of the invention water resistance with higher
And alkali resistance；Tool closes whitening resistance waterproof outstanding, anti-after-tackiness and the general salt of alkali resistant, fabulous adhesive force, cohesion；
3, for the present invention using the quartz sand of different grain size size as filler material, reasonable proportion imitates the emulation of lacquer
Fruit reaches optimal state, can get the effect mixed the spurious with the genuine.
Specific embodiment
The invention will be further described With reference to embodiment.
Embodiment 1
A kind of lacquer, mass parts composition are as follows：10 parts of hydroxypropyl methyl cellulose, TD66110 parts of silicone acrylic emulsion, at
2 parts of film auxiliary agent, 0.05 part of thickened systems, 0.1 part of hydrophober, 0.1 part of sterilization antiseptic, 80 parts of quartz sand, adsorbent modifier 0.1
Part, 10 parts of deionized water.
In the present embodiment coalescing agent select glycerine Block polyoxyethylene oleic acid ester, silane based modified porous starch,
The mixture of allyl methyl phenyl ether, mass ratio 1:1.2:1.
The mixture of sodium tripolyphosphate and acrylate copolymer, mass ratio 1 are selected in the present embodiment:1.5.
Thickened systems use the mixture of hydroxyethyl ether cellulose and the non-swollen ASE60 of association type alkali soluble in the present embodiment,
Mass ratio is 1:1.2.
Hydrophober selects organosiloxane in the present embodiment.
The mass fraction of 40-80 mesh is the quality of 60%, the 100-120 mesh of quartz sand total amount in quartz sand in the present embodiment
Score is the 40% of quartz sand total amount.
Defoaming agent is selected from metal soap NXZ in the present embodiment.
The method of lacquer, includes the following steps in the present embodiment：
(1) it is added deionized water in high speed disperser, control mixing speed is 300-400rpm, is successively slowly added to point
Powder, part defoaming agent, hydroxypropyl methyl cellulose add rear revolving speed and improve to 1000rpm, stirs 5-10min, be in slurry
Then transparent g., jelly-like adjusts revolving speed 600rpm, pigments and fillers are added in uniform speed slow, adds rear revolving speed and is adjusted to 1200rpm, high speed point
10min is dissipated, defoaming agent is the half that dosage is defoamed in formula；
(2) control revolving speed is 500rpm, is slowly added to coalescing agent, silicone acrylic emulsion TD66, hydrophober, adsorbent modifier,
PH value is adjusted to 8.5-9 with NaOH, is stirred 10min, is obtained slurry；
(3) it is successively slowly added to quartz sand while stirring, it is that 600-800rpm stirs 10min that revolving speed is controlled after adding, according to
Secondary addition sterilization antiseptic and remaining defoaming agent, are finally added dropwise thickened systems while stirring, add and continue to stir 10min, adjust
It discharges after section appropriate viscosity.
Embodiment 2
A kind of lacquer, mass parts composition are as follows：15 parts of hydroxypropyl methyl cellulose, TD66115 parts of silicone acrylic emulsion, at
6 parts of film auxiliary agent, 0.3 part of thickened systems, 0.3 part of hydrophober, 0.15 part of sterilization antiseptic, 100 parts of quartz sand, adsorbent modifier
0.2 part, 25 parts of deionized water.
In the present embodiment coalescing agent select glycerine Block polyoxyethylene oleic acid ester, silane based modified porous starch,
The mixture of allyl methyl phenyl ether, mass ratio 1:1.3:1.
The mixture of sodium tripolyphosphate and acrylate copolymer, mass ratio 1 are selected in the present embodiment:1.8.
Thickened systems use the mixture of hydroxyethyl ether cellulose and the non-swollen ASE60 of association type alkali soluble in the present embodiment,
Mass ratio is 1:2.
Hydrophober selects the nano-interface agent of LLD super-hydrophobicity in the present embodiment.
The mass fraction of 40-80 mesh is the quality of 60%, the 100-120 mesh of quartz sand total amount in quartz sand in the present embodiment
Score is the 40% of quartz sand total amount.
Defoaming agent is selected from the mixture of metal soap NXZ, paraffin class 1340, mass ratio 1 in the present embodiment:1.
The method of lacquer, includes the following steps in the present embodiment：
(1) it is added deionized water in high speed disperser, control mixing speed is 300-400rpm, is successively slowly added to point
Powder, part defoaming agent, hydroxypropyl methyl cellulose add rear revolving speed and improve to 1000rpm, stirs 5-10min, be in slurry
Then transparent g., jelly-like adjusts revolving speed 600rpm, pigments and fillers are added in uniform speed slow, adds rear revolving speed and is adjusted to 1200rpm, high speed point
10min is dissipated, defoaming agent is the half that dosage is defoamed in formula；
(2) control revolving speed is 500rpm, is slowly added to coalescing agent, silicone acrylic emulsion TD66, hydrophober, adsorbent modifier,
PH value is adjusted to 8.5-9 with NaOH, is stirred 10min, is obtained slurry；
(3) it is successively slowly added to quartz sand while stirring, it is that 600-800rpm stirs 10min that revolving speed is controlled after adding, according to
Secondary addition sterilization antiseptic and remaining defoaming agent, are finally added dropwise thickened systems while stirring, add and continue to stir 10min, adjust
It discharges after section appropriate viscosity.
Embodiment 3
A kind of lacquer, mass parts composition are as follows：20 parts of hydroxypropyl methyl cellulose, TD66120 parts of silicone acrylic emulsion, at
10 parts of film auxiliary agent, 0.5 part of thickened systems, 0.5 part of hydrophober, 0.2 part of sterilization antiseptic, 200 parts of quartz sand, adsorbent modifier
0.3 part, 40 parts of deionized water.
In the present embodiment coalescing agent select glycerine Block polyoxyethylene oleic acid ester, silane based modified porous starch,
The mixture of allyl methyl phenyl ether, mass ratio 1:1.5:1.
The mixture of sodium tripolyphosphate and acrylate copolymer, mass ratio 1 are selected in the present embodiment:2.
Thickened systems use the mixture of hydroxyethyl ether cellulose and the non-swollen ASE60 of association type alkali soluble in the present embodiment,
Mass ratio is 1:3.
Hydrophober selects the mixing of organosiloxane, the LLD agent of super-hydrophobicity nano-interface and polysiloxanes in the present embodiment
Object, mass ratio 1:1:1.
The mass fraction of 40-80 mesh is the quality of 60%, the 100-120 mesh of quartz sand total amount in quartz sand in the present embodiment
Score is the 40% of quartz sand total amount.
Defoaming agent is selected from the mixture of metal soap NXZ, paraffin class 1340 and EFKA8580, mass ratio in the present embodiment
It is 1:1:1.
The method of lacquer, includes the following steps in the present embodiment：
(1) it is added deionized water in high speed disperser, control mixing speed is 300-400rpm, is successively slowly added to point
Powder, part defoaming agent, hydroxypropyl methyl cellulose add rear revolving speed and improve to 1000rpm, stirs 5-10min, be in slurry
Then transparent g., jelly-like adjusts revolving speed 600rpm, pigments and fillers are added in uniform speed slow, adds rear revolving speed and is adjusted to 1200rpm, high speed point
10min is dissipated, defoaming agent is the half that dosage is defoamed in formula；
(2) control revolving speed is 500rpm, is slowly added to coalescing agent, silicone acrylic emulsion TD66, hydrophober, adsorbent modifier,
PH value is adjusted to 8.5-9 with NaOH, is stirred 10min, is obtained slurry；
(3) it is successively slowly added to quartz sand while stirring, it is that 600-800rpm stirs 10min that revolving speed is controlled after adding, according to
Secondary addition sterilization antiseptic and remaining defoaming agent, are finally added dropwise thickened systems while stirring, add and continue to stir 10min, adjust
It discharges after section appropriate viscosity.
Performance detection：
The production and maintenance of mortar block, according to People's Republic of China (PRC) building material industry standard JC/T1024_2007《Wall decorations
Facing sand slurry》Regulation carry out.JG/T24.2000 is pressed in the preparation and maintenance of test plate (panel)《SAND SLURRY SYNTHETIC EMULSION ARCHITECTURAL COATINGS》
It carries out
(1) water-resistant coating：The resistivity that water resistance, that is, film acts on water does not absorb water, impermeable performance.It applies
Film has certain water resistance, that is, refers to that dry film is not in whiting after meeting water, blisters phenomena such as falling off, expanding,
And from water after moisture evaporation, coating can restore original appearance.By GB/T1733.1993《Building coating water-resistance property of coating
Measuring method》Regulation carries out.
(2) that is, under prescribed conditions film test plate (panel) is immersed in centainly by the resistivity that alkali resistance, that is, film corrodes alkali
In the lye of concentration, observing it, whether there is or not whiten, loss of gloss, blister, fall off.Test method presses GB9265.1988《Building applies
Expect the measuring method of coating alkali resistance》It carries out.
(3) tensile bond strength：By test specimen to be measured under conditions of the fog room of laboratory, i.e. 23 DEG C of temperature, humidity 65%
Then JG/T24.2000 is pressed in maintenance 14 days《SAND SLURRY SYNTHETIC EMULSION ARCHITECTURAL COATINGS》Carry out the test of tensile bond strength
And the test of test specimen immersion post-tensioning bond strength.
(4) impact resistance：The performance that impact resistance refers to flawless after coating is impacted, peels off and obviously deform.
Test method presses JG/T24.2000《SAND SLURRY SYNTHETIC EMULSION ARCHITECTURAL COATINGS》The regulation of impact resistance is carried out.
(5) storage at normal temperature stability：Coating passes through the property changed without agglomeration, cohesion and constituent certain time at normal temperature
Energy.By standard JG/T24.2000《SAND SLURRY SYNTHETIC EMULSION ARCHITECTURAL COATINGS》It carries out.
Above-mentioned experimental result in embodiment 1-3 is shown in Table 1.
Table 1
In conclusion lacquer wall surface coating color of the invention is uniform, without color difference, under exposing to the weather, for a long time
It fades, lotion is water-fast, good weatherability, is not easy xanthochromia；Lotion in the present invention uses silicone acrylic emulsion TD661, so that of the invention
Lacquer water resistance with higher and alkali resistance；Tool closes whitening resistance waterproof outstanding, anti-after-tackiness and the general salt of alkali resistant, pole
Adhesive force well, cohesion；For the present invention using the quartz sand of different grain size size as filler material, reasonable proportion makes lacquer
Simulated effect reach optimal state, can get the effect mixed the spurious with the genuine.
Taking the above-mentioned ideal embodiment according to the present invention as inspiration, through the above description, relevant staff is complete
Various changes and amendments can be carried out without departing from the scope of the technological thought of the present invention' entirely.The technology of this invention
Property range is not limited to the contents of the specification, it is necessary to which the technical scope thereof is determined according to the scope of the claim.
Claims (10)
1. a kind of lacquer, it is characterised in that：Its mass parts composition is as follows：10-20 parts of hydroxypropyl methyl cellulose, silicone acrylic emulsion
TD66110-20 parts, 2-10 parts of coalescing agent, 0.05-0.5 parts of thickened systems, 0.1-0.5 parts of hydrophober, sterilization antiseptic 0.1-
0.2 part, 80-200 parts of quartz sand, 0.1-0.3 parts of adsorbent modifier, 10-40 parts of deionized water.
2. a kind of lacquer according to claim 1, it is characterised in that：The coalescing agent selects glycerine block polyoxy
Ethylene oleic acid ester, silane based modified porous starch, allyl methyl phenyl ether mixture, mass ratio 1:1.2-1.5:
1。
3. a kind of lacquer according to claim 1, it is characterised in that：The dispersing agent selects sodium tripolyphosphate and propylene
The mixture of acid ester copolymer, mass ratio 1:1.5-2.
4. a kind of lacquer according to claim 1, it is characterised in that：The thickened systems use hydroxyethyl ether cellulose
With the mixture of the non-swollen ASE60 of association type alkali soluble, mass ratio 1:1.2-3.
5. a kind of lacquer according to claim 1, it is characterised in that：The hydrophober selects organosiloxane, LLD super
One or more of hydrophobic nano interfacial agents, polysiloxanes.
6. a kind of lacquer according to claim 5, it is characterised in that：The hydrophober selects LLD super-hydrophobicity nanometer
Interfacial agents.
7. a kind of lacquer according to claim 1, it is characterised in that：The mass fraction of 40-80 mesh in the quartz sand
Mass fraction for 60%, the 100-120 mesh of quartz sand total amount is the 40% of quartz sand total amount.
8. a kind of lacquer according to claim 1, it is characterised in that：The defoaming agent is selected from metal soap NXZ, paraffin
One or more of class 1340, EFKA8580.
9. a kind of method of the lacquer prepared, which is characterized in that the described method comprises the following steps：
(1) deionized water is added in high speed disperser, control mixing speed is 300-400rpm, is successively slowly added to disperse
Agent, part defoaming agent, hydroxypropyl methyl cellulose add rear revolving speed and improve to 1000rpm, 5-10min stirred, to slurry in saturating
Bright g., jelly-like, then adjusts revolving speed 600rpm, and uniform speed slow is added pigments and fillers, adds rear revolving speed and be adjusted to 1200rpm, high speed dispersion
10min,
(2) control revolving speed is 500rpm, is slowly added to coalescing agent, silicone acrylic emulsion TD66, hydrophober, adsorbent modifier, is used
NaOH adjusts pH value to 8.5-9, stirs 10min, obtains slurry；
(3) be successively slowly added to quartz sand while stirring, after adding control revolving speed be 600-800rpm stir 10min, successively plus
Enter sterilization antiseptic and remaining defoaming agent, thickened systems are finally added dropwise while stirring, adds and continue to stir 10min, adjust and close
It discharges after suitable viscosity.
10. a kind of method for preparing lacquer according to claim 9, it is characterised in that：It is added in the step (1)
Defoaming agent is the half that dosage is defoamed in formula.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201810648828.6A CN108911593A (en) | 2018-06-22 | 2018-06-22 | A kind of lacquer and preparation method thereof |
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| CN113908821A (en) * | 2020-07-08 | 2022-01-11 | 河南润世界新型涂料科技有限公司 | Preparation method of photocatalytic composite material, environment-friendly self-cleaning real stone paint and preparation method thereof |
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| CN113908821A (en) * | 2020-07-08 | 2022-01-11 | 河南润世界新型涂料科技有限公司 | Preparation method of photocatalytic composite material, environment-friendly self-cleaning real stone paint and preparation method thereof |
| CN113908821B (en) * | 2020-07-08 | 2024-03-19 | 河南润世界新型涂料科技有限公司 | Preparation method of photocatalysis composite material, environment-friendly self-cleaning stone-like paint and preparation method thereof |
| CN114149702A (en) * | 2021-12-23 | 2022-03-08 | 广东美家美福科技有限公司 | Inorganic stone-like paint |
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Application publication date: 20181130 |