CN108911510A - A kind of the effect glaze and its application method of architectural pottery incrustation - Google Patents
A kind of the effect glaze and its application method of architectural pottery incrustation Download PDFInfo
- Publication number
- CN108911510A CN108911510A CN201811033058.0A CN201811033058A CN108911510A CN 108911510 A CN108911510 A CN 108911510A CN 201811033058 A CN201811033058 A CN 201811033058A CN 108911510 A CN108911510 A CN 108911510A
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- China
- Prior art keywords
- glaze
- parts
- effect
- architectural pottery
- incrustation
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C8/00—Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
- C03C8/02—Frit compositions, i.e. in a powdered or comminuted form
- C03C8/04—Frit compositions, i.e. in a powdered or comminuted form containing zinc
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C8/00—Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
- C03C8/14—Glass frit mixtures having non-frit additions, e.g. opacifiers, colorants, mill-additions
- C03C8/16—Glass frit mixtures having non-frit additions, e.g. opacifiers, colorants, mill-additions with vehicle or suspending agents, e.g. slip
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/45—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements
- C04B41/50—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials
- C04B41/5022—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials with vitreous materials
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/80—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone of only ceramics
- C04B41/81—Coating or impregnation
- C04B41/85—Coating or impregnation with inorganic materials
- C04B41/86—Glazes; Cold glazes
Abstract
The invention discloses a kind of effect glaze of architectural pottery incrustation, the component including following parts by weight：Specific frit 70-75 parts, 10-13 parts of calcined earth, 10-13 parts of kaolin, 0-4 parts of potassium feldspar, 0.1-0.15 parts of carboxycellulose, 0.3-0.35 parts of sodium tripolyphosphate, 33-35 parts of water；The effect glaze of the above component is successively passed through into ball milling when use, tail over and removes iron and is handled, and is modulated into the effect glaze slip of certain weight proportion, glaze spraying is equably carried out in the glaze paint of architectural pottery, is fired after dry and obtains the architectural pottery with granulated sugar glaze paint.The glaze paint glossiness of architectural pottery prepared by the present invention is high, it is to have certain three-dimensional sense and have pico- glittering effect that glazing effect, which is similar to granulated sugar fritting, artistic effect is good, texture is strong, with good wear resistance and chemical-resistance, and compared to existing candy glaze technology, raw material, equipment research and development and production cost are substantially reduced, the raw material of use is environment-friendly materials, and application range is wider.
Description
Technical field
The present invention relates to the effect glaze of architectural pottery technical field more particularly to a kind of architectural pottery incrustation and
Its application method.
Background technique
Mostly brick glaze face is not all that very high tradition throws glaze or has certain wear resistance with wear resistance currently on the market
But based on the poor glaze paint modelled after an antique of decorative effect.Existing floor tile producer imitates to allow floor tile glaze paint to reach granulated sugar glaze glaze paint
Fruit needs corresponding dry granular can be only achieved, and needs to use the glazing of new material siccative, while researching and developing new glazing equipment, will increase in this way
Manufacturer's processing cost.
A kind of effect glaze can be researched and developed, raw material cost is low, can glaze spraying using traditional cloud machine and glaze spraying cabinet
The effect glaze paint of granulated sugar enamel-like out is the R&D direction of traditional ceramics floor tile developer.
It is common it is unwanted on the basis of need to purchase the granulated sugar glaze that our company researches and develops in new material technology be have both it is good
The glaze paint of wear resistance and certain decorative effect, and do not need to research and develop new glazing equipment, it is good with traditional cloud machine and atomization
Good glaze spraying cabinet, compared to the use that can reduce glaze slip amount for traditional glaze volume.Floor tile will reach this at present
The effect of glaze paint needs corresponding dry granular can be only achieved.For production and technique, the glazing process of this product is opposite
Simply, producing can reach good effect with seldom amount
Summary of the invention
The present invention provides a kind of effect glaze of architectural pottery incrustation and its application methods.Use this glaze fabric
The glossiness of the glazed tile of firing can achieve 20 ° or so, and anti-pollution is good, have good resist chemical performance.
To achieve the goals above, present invention employs following technical solutions：
A kind of effect glaze of architectural pottery incrustation, which is characterized in that the component including following parts by weight：It is special
Determine 70-75 parts of frit, 10-13 parts of calcined earth, 10-13 parts of kaolin, 0-4 parts of potassium feldspar, 0.1-0.15 parts of carboxycellulose, three
0.3-0.35 parts of polyphosphate sodium, 33-35 parts of water.
A kind of effect glaze of the architectural pottery incrustation, which is characterized in that the specific frit by with
The component raw material of lower parts by weight is made：SiO250-60 parts, Al2O30-4 parts, 10-15 parts of CaO, R20-4 parts of O, MgO 0-2
Part, 5-7 parts of ZnO, B2O30-1 parts.
A kind of effect glaze of the architectural pottery incrustation, it is characterised in that：The R2O is selected from Na2O、
K2O、Li2One of O three or a variety of mixing.
A kind of effect glaze of architectural pottery incrustation, which is characterized in that the system of the specific frit
Preparation Method carries out according to the following steps：(1) formula material is mixed in proportion；(2) by the raw material mixed in 1560-
Uniform glass melt is melted at 1580 DEG C；(3) resulting glass melt is flowed into water, water quenching becomes disintegrating slag shape, then
By dehydration, dries, obtains finished product, packaging.
The application method of the effect glaze, which is characterized in that include the following steps：
S1, the modulation of effect glaze slip：By the specific frit of formula ratio, calcined earth, kaolin, potassium feldspar, carboxycellulose,
Sodium tripolyphosphate and water are added in ball mill, and after a certain period of time, the slurry ground out tails over ball milling by sieve, by removing iron
Processing, obtains effect glaze slip；
S2, the glaze spraying processing of architectural pottery：Using glaze spraying equipment, in the architectural pottery by overglaze processing and decorative pattern spray printing
Glaze paint on, by S1 modulation certain weight proportion the equably glaze spraying of effect glaze slip, it is to be dried spare；
S3, the firing of granulated sugar glaze paint：The architectural pottery that S2 is obtained is fired in kiln, obtains having building for granulated sugar glaze paint
Build ceramics.
The application method of the effect glaze of a kind of architectural pottery incrustation, which is characterized in that in the S1
Ball-milling Time 13-16h, effect glaze slip use 325 mesh screens, screen over-size 0.3-0.5%,.
The application method of the effect glaze of a kind of architectural pottery incrustation, which is characterized in that in the S2
Effect glaze slip glaze slip specific gravity be 1.40-1.45g/cm3, glaze spraying amount is 85g ± 5g/m2。
A kind of application method of the effect glaze of the architectural pottery incrustation, it is characterised in that：In the S2
Glaze spraying equipment be cloud glaze spraying machine and glaze spraying cabinet in any one, the glaze spraying cabinet atomization use compressed air pressure
0.5-1MPa。
A kind of application method of the effect glaze of the architectural pottery incrustation, it is characterised in that：In the S3
Kiln temperature be 1181-1199 DEG C, the firing time be 50-60 minutes.
The application method of the effect glaze of a kind of architectural pottery incrustation, which is characterized in that in the S3
The glossiness of obtained granulated sugar glaze paint is 20 ± 2 °.
Compared with prior art, the beneficial effects of the invention are as follows：
1, effect glaze cost of material of the invention is low：The present invention uses common calcined earth, kaolin, potassium feldspar, and
Self-control frit is added, effect glaze is made, cost of material is low；
2, glaze spraying simple process, glaze volume are few：Effect glaze of the invention sprays to ceramic tile glaze with simple traditional equipment
On face, reached glazing effect be using innovation equipment and the effect that can just make of new material, and effect glaze paint have both it is good
Wear resistance and certain decorative effect, and do not need to research and develop new glazing equipment, with traditional cloud machine and wellatomized spray
Glaze cabinet, compared to the use that can reduce glaze slip amount for traditional glaze volume.
3, the glazing effect of finished product is good：Effect glaze of the invention is sprayed application into architectural pottery face using conventional equipment
On, it is to have certain three-dimensional sense and have pico- glittering effect, glaze paint light that the glazing effect for being burnt into out, which is similar to granulated sugar fritting,
Damp degree is 20 ° or so, and has good wear resistance and chemical-resistance, this glaze paint is suitable for glaze paint modelled after an antique, plays wear-resisting and dress
Adorn double effects.
4. carboxycellulose and sodium tripolyphosphate is added in the present invention in effect glaze slip, carboxycellulose is that anionic is fine
Plain ethers is tieed up, has certain viscosity after being dissolved in water, is to be easy to get and the glaze suspending agent of environmental protection, sodium tripolyphosphate is a kind of chelating
Agent can be effectively prevented the deposition of glaze powder；It is glutinous that carboxycellulose and sodium tripolyphosphate make glaze slip form stable middle height
The colloidal solution of degree, to simplify glaze spraying work, without spraying equipment expensive in existing candy glaze technology, using common
Cloud glaze spraying machine or the good glaze spraying cabinet of atomization, further save cost, and uniformity of the glaze slip in glaze paint
More preferably, glaze spraying amount is few, and the quality of glaze paint is high.
Specific embodiment
Below in conjunction with embodiment, further clear, complete description is carried out to technical solution of the present invention, it is clear that institute
The embodiment of description is only the description of the invention, rather than limiting the invention.
Embodiment 1：
The preparation of specific frit, includes the following steps：
(1) following components raw material is weighed by weight：SiO255 parts, Al2O32.5 parts, 12 parts of CaO, R22 parts of O, MgO
1 part, 6 parts of ZnO, B2O30.5 part, wherein R2O is Na2O、K2O、Li2The mixture of O three；
(2) weighed formula material is mixed in proportion；(3) raw material mixed is melted at 1560-1580 DEG C
It is melted into uniform glass melt；(4) resulting glass melt is flowed into water, water quenching becomes disintegrating slag shape, then will dehydration, baking
It does, obtain finished product frit, packaging.
Embodiment 2
A kind of ornamental effect glaze of tile surface, the component including following parts by weight：Frit made from embodiment 1
72 parts, 12 parts of calcined earth, 12 parts of kaolin, 3 parts of potassium feldspar, 0.12 part of carboxycellulose, 0.34 part of sodium tripolyphosphate, 34 parts
Water,
Application method includes the following steps：
S1, the modulation of effect glaze slip：By the component raw material of above-mentioned formula ratio, it is added in ball mill, after ball milling 15h, grinds out
Obtained slurry tails over 0.3-0.5% by 325 sieves, and specific gravity is adjusted to 1.40g/cm3, by being handled except iron, imitated
Fruit glaze slip；
S2, effect glaze spray：By effect glaze slip made from S1, use the pressure of atomization compressed air for 0.6-
The glaze spraying cabinet of 0.7MPa equably sprays effect glaze in the floor tile glaze paint by overglaze processing and the good decorative pattern of spray printing, and glaze spraying amount is
85g/m2, it is to be dried；
S3, the firing of granulated sugar glaze paint：The S2 floor tile for having sprayed effect glaze is sent into kiln, is gradually warming up to 1185 DEG C,
60min is fired, the granulated sugar glazed floor tile that glossiness is 20 ° is obtained.
The glazing effect for the floor tile that the present embodiment is burnt out, which is similar to granulated sugar fritting, to be had certain three-dimensional sense and has micro-
Micro- glittering effect, glaze paint glossiness is 20 ° or so, and has good wear resistance and chemical-resistance.
Embodiment 3：
A kind of ornamental effect glaze of tile surface, the component including following parts by weight：Frit made from embodiment 1
74 parts, 11 parts of calcined earth, 13 parts of kaolin, 3 parts of potassium feldspar, 0.14 part of carboxycellulose, 0.34 part of sodium tripolyphosphate, 35 parts
Water,
Application method includes the following steps：
S1, the modulation of effect glaze slip：By the component raw material of above-mentioned formula ratio, it is added in ball mill, after ball milling 14h, grinds out
Obtained slurry tails over 0.3-0.5% by 325 sieves, and specific gravity is adjusted to 1.45g/cm3, by being handled except iron, imitated
Fruit glaze slip；
S2, by effect glaze slip made from S1, using cloud glaze spraying machine, in the floor tile by overglaze processing and the good decorative pattern of spray printing
Effect glaze is equably sprayed in glaze paint, glaze spraying amount is 84g/m2, to be dried；
S3, the firing of granulated sugar glaze paint：The glaze spraying floor tile that S2 is obtained is placed in kiln, is gradually warming up to 1195 DEG C, is fired
50min obtains the granulated sugar glazed floor tile that glossiness is 23 °.
The glazing effect for the floor tile that the present embodiment is burnt out, which is similar to granulated sugar fritting, to be had certain three-dimensional sense and has micro-
Micro- glittering effect, glaze paint glossiness is 23 °, and has good wear resistance and chemical-resistance.
Embodiment 4：
A kind of ornamental effect glaze of tile surface, the component including following parts by weight：Frit made from embodiment 1
75 parts, 13 parts of calcined earth, 10 parts of kaolin, 4 parts of potassium feldspar, 0.15 part of carboxycellulose, 0.33 part of sodium tripolyphosphate, 35 parts
Water,
Application method includes the following steps：
S1, the modulation of effect glaze slip：By the component raw material of above-mentioned formula ratio, it is added in ball mill, after ball milling 13h, grinds out
Obtained slurry tails over 0.3-0.5% by 325 sieves, and specific gravity is adjusted to 1.44g/cm3, by being handled except iron, imitated
Fruit glaze slip；
S2, by effect glaze slip made from S1, using cloud glaze spraying machine, in the floor tile by overglaze processing and the good decorative pattern of spray printing
Effect glaze is equably sprayed in glaze paint, glaze spraying amount is 83g/m2, to be dried；
S3, the firing of granulated sugar glaze paint：The glaze spraying floor tile that S2 is obtained is placed in kiln, is gradually warming up to 1194 DEG C, is fired
55min obtains the granulated sugar glazed floor tile that glossiness is 22 °.
The glazing effect for the floor tile that the present embodiment is burnt out, which is similar to granulated sugar fritting, to be had certain three-dimensional sense and has micro-
Micro- glittering effect, glaze paint glossiness is 22 °, and has good wear resistance and chemical-resistance.
Comparative example
A kind of ornamental glaze material of tile surface, the component including following parts by weight：50 parts of feldspar, 4.2 parts of quartz,
11 parts of calcite, 22 parts of zircon, 1.5 parts of zinc oxide, 4 parts of talcum powder, 32 parts of water,
Application method includes the following steps：
S1, the modulation of glaze slip：The component raw material of above-mentioned formula ratio is added in ball mill, after ball milling 15h, mill is obtained out
Slurry tail over 0.3-0.5% by 325 sieves, and specific gravity is adjusted to 1.5g/cm3, by handling except iron, obtain glaze slip；
S2, overglaze spray：Glaze slip made from S1 is spent well using cloud glaze spraying machine by overglaze processing and spray printing
Equably glaze spraying in the floor tile glaze paint of line, glaze spraying amount are 100g/m2, to be dried；
S3, the firing of glaze paint：The S2 floor tile for having sprayed glaze is sent into kiln, 1185 DEG C is gradually warming up to, fires
60min obtains the general glazed floor tile of glossiness.
The glazed floor tile burnt out using effect glaze fabric of the invention and conventional glaze fabric, which is compared, the results are shown in Table
1。
Table 1
Effect glaze fabric of the invention burns out the glaze of glazed floor tile compared with common glaze material as can be seen from Table 1
Face effect is significantly different, and glazing effect of the invention is good, has three-dimensional sense and has pico- glittering effect, glaze paint glossiness is high, single
The glaze volume of plane product is low, and glaze paint wear resistance is high.
The foregoing is only a preferred embodiment of the present invention, but scope of protection of the present invention is not limited thereto,
Anyone skilled in the art in the technical scope disclosed by the present invention, according to the technique and scheme of the present invention and its
Inventive concept is subject to equivalent substitution or change, should be covered by the protection scope of the present invention.
Claims (10)
1. a kind of effect glaze of architectural pottery incrustation, which is characterized in that the component including following parts by weight：It is specific
70-75 parts of frit, 10-13 parts of calcined earth, 10-13 parts of kaolin, 0-4 parts of potassium feldspar, 0.1-0.15 parts of carboxycellulose, trimerization
0.3-0.35 parts of sodium phosphate, 33-35 parts of water.
2. a kind of effect glaze of architectural pottery incrustation according to claim 1, which is characterized in that the spy
Determine frit to be made by the component raw material of following parts by weight：SiO250-60 parts, Al2O30-4 parts, 10-15 parts of CaO, R2O 0-4
Part, 0-2 parts of MgO, 5-7 parts of ZnO, B2O30-1 parts.
3. a kind of effect glaze of architectural pottery incrustation according to claim 2, it is characterised in that：The R2O
Selected from Na2O、K2O、Li2One of O three or a variety of mixing.
4. a kind of effect glaze of architectural pottery incrustation according to claim 2, which is characterized in that the spy
Determine the preparation method of frit, carries out according to the following steps：(1) formula material is mixed in proportion；(2) raw material that will be mixed
Uniform glass melt is melted at 1560-1580 DEG C；(3) resulting glass melt is flowed into water, water quenching becomes disintegrating slag
Shape, then by dehydration, dry, obtain finished product, packaging.
5. the application method of effect glaze according to claim 1, which is characterized in that include the following steps：
S1, the modulation of effect glaze slip：By specific frit, calcined earth, kaolin, potassium feldspar, carboxycellulose, the trimerization of formula ratio
Sodium phosphate and water are added in ball mill, and after a certain period of time, the slurry ground out tails over ball milling by sieve, by except at iron
Reason, obtains effect glaze slip；
S2, the glaze spraying processing of architectural pottery：Using glaze spraying equipment, in the glaze by overglaze processing and the architectural pottery of decorative pattern spray printing
It is to be dried spare by the effect glaze slip equably glaze spraying of S1 modulation certain weight proportion on face；
S3, the firing of granulated sugar glaze paint：The architectural pottery that S2 is obtained is fired in kiln, obtains having the building of granulated sugar glaze paint to make pottery
Porcelain.
6. a kind of application method of the effect glaze of architectural pottery incrustation according to claim 5, feature exist
In Ball-milling Time 13-16h in the S1, effect glaze slip uses 325 mesh screens, screen over-size 0.3-0.5%.
7. a kind of application method of the effect glaze of architectural pottery incrustation according to claim 5, feature exist
In the glaze slip specific gravity of the effect glaze slip in the S2 is 1.40-1.45g/cm3, glaze spraying amount is 85g ± 5g/m2。
8. a kind of application method of the effect glaze of architectural pottery incrustation according to claim 5, feature exist
In：Glaze spraying equipment in the S2 is any one in cloud glaze spraying machine and glaze spraying cabinet, the atomization compression of the glaze spraying cabinet
The pressure 0.5-1MPa of air.
9. a kind of application method of the effect glaze of architectural pottery incrustation according to claim 5, feature exist
In：Kiln temperature in the S3 is 1181-1199 DEG C, and the firing time is 50-60 minutes.
10. a kind of application method of the effect glaze of architectural pottery incrustation according to claim 5, feature exist
In the glossiness of granulated sugar glaze paint obtained in the S3 is 20 ± 10 °.
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| CN201811033058.0A CN108911510A (en) | 2018-09-05 | 2018-09-05 | A kind of the effect glaze and its application method of architectural pottery incrustation |
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Family
ID=64407578
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|---|---|---|---|---|
| JPS5490224A (en) * | 1977-12-27 | 1979-07-17 | Akira Oguri | Production of lighttweight ceramic panel |
| CN103102181A (en) * | 2012-12-19 | 2013-05-15 | 广东东鹏控股股份有限公司 | Method for preparing flash glazed wall tile |
| CN103497007A (en) * | 2013-09-17 | 2014-01-08 | 佛山市五月玫瑰陶瓷有限公司 | Ceramic tile with dispersed shimmering powder and manufacturing method thereof |
| CN104261880A (en) * | 2014-09-23 | 2015-01-07 | 广东道氏技术股份有限公司 | Novel sand crystal glaze utilizing mica iron oxide and preparation process of sand crystal glaze |
| CN104829267A (en) * | 2015-05-04 | 2015-08-12 | 广东蒙娜丽莎新型材料集团有限公司 | High wear resistance in-glaze decoration ceramic brick and preparation method thereof |
| CN105218158A (en) * | 2015-08-27 | 2016-01-06 | 广东博华陶瓷有限公司 | A kind of happy ceramic tile |
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2018
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|---|---|---|---|---|
| JPS5490224A (en) * | 1977-12-27 | 1979-07-17 | Akira Oguri | Production of lighttweight ceramic panel |
| CN103102181A (en) * | 2012-12-19 | 2013-05-15 | 广东东鹏控股股份有限公司 | Method for preparing flash glazed wall tile |
| CN103497007A (en) * | 2013-09-17 | 2014-01-08 | 佛山市五月玫瑰陶瓷有限公司 | Ceramic tile with dispersed shimmering powder and manufacturing method thereof |
| CN104261880A (en) * | 2014-09-23 | 2015-01-07 | 广东道氏技术股份有限公司 | Novel sand crystal glaze utilizing mica iron oxide and preparation process of sand crystal glaze |
| CN104829267A (en) * | 2015-05-04 | 2015-08-12 | 广东蒙娜丽莎新型材料集团有限公司 | High wear resistance in-glaze decoration ceramic brick and preparation method thereof |
| CN105218158A (en) * | 2015-08-27 | 2016-01-06 | 广东博华陶瓷有限公司 | A kind of happy ceramic tile |
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| Title |
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| 周晓燕主编: "《陶瓷坯釉料制备技术》", 31 August 2017, 江西高校出版社 * |
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