CN108893788A - A kind of electrostatic spinning apparatus - Google Patents

A kind of electrostatic spinning apparatus Download PDF

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Publication number
CN108893788A
CN108893788A CN201810916006.1A CN201810916006A CN108893788A CN 108893788 A CN108893788 A CN 108893788A CN 201810916006 A CN201810916006 A CN 201810916006A CN 108893788 A CN108893788 A CN 108893788A
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CN
China
Prior art keywords
hollow needle
liquid
spinning
jet
electrostatic spinning
Prior art date
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Granted
Application number
CN201810916006.1A
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Chinese (zh)
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CN108893788B (en
Inventor
许国杰
王晗
曾俊
林雅茹
梁烽
林洪鑫
庞应龙
辛正
辛正一
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Guangdong Houhai Environmental Protection New Material Co ltd
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Guangdong University of Technology
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Priority to CN201810916006.1A priority Critical patent/CN108893788B/en
Publication of CN108893788A publication Critical patent/CN108893788A/en
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Classifications

    • DTEXTILES; PAPER
    • D01NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01DMECHANICAL METHODS OR APPARATUS IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS
    • D01D5/00Formation of filaments, threads, or the like
    • D01D5/0007Electro-spinning
    • D01D5/0061Electro-spinning characterised by the electro-spinning apparatus
    • D01D5/0069Electro-spinning characterised by the electro-spinning apparatus characterised by the spinning section, e.g. capillary tube, protrusion or pin

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  • Engineering & Computer Science (AREA)
  • Mechanical Engineering (AREA)
  • Textile Engineering (AREA)
  • Spinning Methods And Devices For Manufacturing Artificial Fibers (AREA)
  • Nonwoven Fabrics (AREA)

Abstract

The application belong to electrostatic spinning technical field more particularly to a kind of electrostatic spinning apparatus.The application discloses a kind of electrostatic spinning apparatus, including:Collection device;High voltage power supply, high voltage power supply are connect with collection device;Spinning liquid pool;Spinning ejection assemblies, spinning ejection assemblies are built in spinning liquid pool comprising:The liquid inlet of liquid injection apparatus and hollow needle group, hollow needle group is connect with liquid injection apparatus pipeline;Gas supply assembly, gas supply assembly are built in spinning liquid pool comprising jet column assembly and air pump, the hollow needle of the jet column package hollow needle group of jet column assembly, air pump are connect with jet column assembly.This application discloses a kind of electrostatic spinning apparatus, it can solve syringe needle existing for existing spininess electrostatic spinning technique and be easy to appear blocking and the low technological deficiency of production efficiency.

Description

A kind of electrostatic spinning apparatus
Technical field
The application belong to electrostatic spinning technical field more particularly to a kind of electrostatic spinning apparatus.
Background technique
Electrostatic spinning technique is a kind of technology using electrostatic field force production nanofiber, and principle is in high-voltage electrostatic field In, charged polymer solution forms taylor cone under the action of electric field force, when electric field force is sufficiently large, so that charged drop overcomes table Face tension formed electrified jet, finally on collecting mechanism deposition cure at nanofibrous structures.Since electrospinning process is It produces that nanofiber is the simplest and low-cost method, has biggish utilization in various fields, such as filter industry, electricity The fields such as son, the energy, catalysis, biological medicine have broad application prospects.Wherein Electrospun nano-fibers prepare filter membrane There is the features such as filter efficiency is high, and technical costs is low, and low energy consumption.
Currently, electrostatic spinning technique is mainly used in scientific research field, hinder the one of its industrialization development big the reason is that being based on The nano fiber batch production method of the technology.Electrostatic spinning production method is broadly divided into spininess spinning at present and needleless is spun Two kinds of silk in needleless spining technology, there is mangneto gunite, antipriming pipe spinning method, disk spinning method, bubble spinning method etc., although The production efficiency of needleless spining technology has obtained greatly being promoted compared to spininess spining technology, but due to needleless spinning jet Direction and amount it is uncontrollable, lead to the nano fibrous membrane for being difficult to produce high quality, the nano fibrous membrane of spininess spinning production exists It is more excellent than needleless spinning in terms of uniformity, but the production efficiency of spininess spinning is not so good as needleless spinning.
In conclusion in existing spininess spining technology, due to that can be realized by the arrangement of syringe needle between syringe needle When the uniformity of field distribution, but during the spinning process, especially spinning rheological property bad material, syringe needle is easy It now blocks, will lead to the uneven of nano fibrous membrane in this way;Moreover, existing spininess spining technology is also difficult to meet industrialization Required production efficiency.
Apply for content
In view of this, can solve existing spininess electrostatic spinning technique this application discloses a kind of electrostatic spinning apparatus and deposit Syringe needle be easy to appear blocking and the low technological deficiency of production efficiency.
This application provides a kind of electrostatic spinning apparatus, including:
Collection device;
High voltage power supply, the high voltage power supply are connect with the collection device;
Spinning liquid pool;
Spinning ejection assemblies, the spinning ejection assemblies are built in the spinning liquid pool comprising;Liquid injection apparatus With hollow needle group, the liquid inlet of the hollow needle group is connect with the liquid injection apparatus pipeline;
Gas supply assembly, the gas supply assembly are built in the spinning liquid pool comprising jet column assembly and air pump, it is described The jet column of jet column assembly wraps up the hollow needle of the hollow needle group, and the air pump is connect with the jet column assembly.
Preferably, the hollow needle group includes more hollow needles and liquid injection pipe;The more hollow needles are equidistant It is connected to the jet port of the liquid injection pipe.
Preferably, the jet column assembly includes more jet columns and gas injection tube;The more jet columns are equidistant Be connected to the jet port of the gas injection tube.
Preferably, the liquid injection apparatus includes motor, liquid pump and inlet tube;
The motor is connect with the liquid pump;
The inlet tube is connect with the liquid pump;
The liquid outlet of the liquid pump is connect with the liquid inlet pipeline of the hollow needle group.
Preferably, the hollow needle that the jet column of the jet column assembly wraps up the hollow needle group is specially:The spray The jet column of air column component wraps up the hollow needle of the hollow needle group, and the top syringe needle of the hollow needle protrudes from the jet The top of column.
Preferably, the shape of the collection device is tabular, convex-shaped or concave shape.
Preferably, the hollow needle of the hollow needle group is metal hollow needle.
The syringe needle that the purpose of the application occurs for the spininess spining technology of the prior art is easy to appear blocking, and is difficult to Meet production efficiency required by industrialization.Therefore, the application discloses a kind of electrostatic spinning apparatus, including:Collection device;High pressure Power supply, high voltage power supply are connect with collection device;Spinning liquid pool;Spinning ejection assemblies, spinning ejection assemblies are built in spinning liquid pool It is interior comprising;The liquid inlet of liquid injection apparatus and hollow needle group, hollow needle group is connect with liquid injection apparatus pipeline;For Pneumatic module, gas supply assembly are built in spinning liquid pool comprising jet column assembly and air pump, the jet column package of jet column assembly The hollow needle of hollow needle group, air pump are connect with jet column assembly.Electrostatic spinning apparatus is placed in spinning liquid pool and is spun in spinning Silk solution, the liquid level of spinning solution are lower than the top of jet column and are supplied after high voltage power supply starting by the high speed of liquid injection apparatus Liquid, by the spinning solution in spinning liquid pool through duct injection into hollow needle group, spinning solution is routinely from hollow needle group Hollow needle eject fluid column, from the tip of hollow needle to the top of fluid column, there is spinning appearance, meanwhile, air pump duration pair The jet column of jet column assembly supplies, and can efficiently avoid tradition has the problem of spinneret of needle spinning blocks, and also mentions significantly The high efficiency of spinning.
Detailed description of the invention
In order to illustrate the technical solutions in the embodiments of the present application or in the prior art more clearly, to embodiment or will show below There is attached drawing needed in technical description to be briefly described.
Fig. 1 shows the structural schematic diagram of electrostatic spinning apparatus provided by the embodiments of the present application;
Wherein, appended drawing reference, collection device 1, high voltage power supply 2, spinning liquid pool 3, hollow needle 4, hollow needle top syringe needle 4-1, liquid injection pipe 4-2, liquid pump 5, motor 6, inlet tube 7, jet column assembly 8, jet column 8-1, jet column top 8-2, Gas injection tube 8-3, air pump 9, the collecting terminal A of collection device, the liquid inlet B of hollow needle group, liquid injection pipe jet port C, the liquid level D of spinning solution.
Specific embodiment
This application provides a kind of electrostatic spinning apparatus, for solving syringe needle existing for existing spininess electrostatic spinning technique It is easy to appear blocking and the low technological deficiency of production efficiency.
Below by the technical scheme in the embodiment of the application is clearly and completely described, it is clear that described implementation Example is merely a part but not all of the embodiments of the present application.Based on the embodiment in the application, this field is common Technical staff's every other embodiment obtained without making creative work belongs to the model of the application protection It encloses.
This application discloses a kind of electrostatic spinning apparatus, including:Collection device 1;High voltage power supply 2, high voltage power supply 2 and collection Device 1 connects;The collecting terminal A of collection device is arranged in spinning liquid pool 3, spinning liquid pool 3;Spinning ejection assemblies, spinning injection group Part is built in spinning liquid pool 3 comprising;Liquid injection apparatus and hollow needle group, the liquid inlet B and liquid of hollow needle group spray The connection of injection device pipeline;Gas supply assembly, gas supply assembly are built in spinning liquid pool 3 comprising jet column assembly 8 and air pump 9, spray The hollow needle 4 of the jet column 8-1 package hollow needle group of air column component, air pump 9 are connect with jet column assembly.
The present embodiment places spinning solution in spinning in spinning liquid pool 3, and the liquid level D of spinning solution is lower than jet column Top 8-2, high voltage power supply 2 start after, by the high speed feed flow of liquid injection apparatus, by the spinning solution in spinning liquid pool 3 Through duct injection into hollow needle group, spinning solution routinely ejects fluid column from the hollow needle 4 of hollow needle group, from hollow The top syringe needle 4-1 of needle has spinning appearance to the top of fluid column, meanwhile, jet column of 9 duration of air pump to jet column assembly 8-1 gas supply.
In the present embodiment, hollow needle group includes more hollow needles 4 and liquid injection pipe 4-2;More hollow needles 4 are equidistant It is connected to the jet port C of liquid injection pipe 4-2.Jet column assembly 8 includes more jet column 8-1 and gas injection tube 8-3;More Jet column 8-1 is equidistant to be connected to the jet port of gas injection tube 8-3.It is special by being carried out to hollow needle 4 in liquid injection pipe 4-2 Fixed arrangement, to realize the uniformity of fluid column tip electric field, so that spinning goes out the nano fibrous membrane of high quality, meanwhile, in order to make It obtains jet column 8-1 and wraps up hollow needle 4, so, position of the jet column 8-1 on gas injection tube 8-3 will be arranged with hollow needle 4 exist The position of liquid injection pipe 4-2 matches.
In the present embodiment, liquid injection apparatus includes motor 6, liquid pump 5 and inlet tube 7;Motor 6 is connect with liquid pump 5;Into Liquid pipe 7 is connect with liquid pump 5;The liquid outlet of liquid pump 5 is connect with the liquid inlet B pipeline of hollow needle group, the liquid of inlet tube 7 into The bottom of pond of spinning liquid pool 3 is arranged in mouth, and liquid pump 5 is facilitated to pump spinning solution to hollow needle 4 by inlet tube 7.When work, motor 6 driving liquid pumps 5 pump the spinning solution of spinning liquid pool 3 to hollow needle 4 by inlet tube 7.
In the present embodiment, the every hollow needle 4 of the every jet column 8-1 package hollow needle group of jet column assembly is specific For:The hollow needle 4 of the jet column 8-1 package hollow needle group of jet column assembly, and the prominent jet column of top needle 4-1 of hollow needle Top 8-2.
In the present embodiment, the shape of collection device 1 is tabular;In addition to tabular, collection device 1 can also be convex-shaped Or concave shape.
In the present embodiment, the hollow needle 4 of hollow needle group is metal hollow needle, and the hollow needle 4 of metal material can be more preferable Carry out electrostatic spinning.
The above is only the preferred embodiment of the application, it is noted that for the ordinary skill people of the art For member, under the premise of not departing from the application principle, several improvements and modifications can also be made, these improvements and modifications are also answered It is considered as the protection scope of the application.

Claims (7)

1. a kind of electrostatic spinning apparatus, which is characterized in that including:
Collection device;
Spinning liquid pool;
High voltage power supply, the high voltage power supply are connect with the collection device;
Spinning ejection assemblies, the spinning ejection assemblies are built in the spinning liquid pool comprising;Liquid injection apparatus and sky Heart needle group, the liquid inlet of the hollow needle group are connect with the liquid injection apparatus pipeline;
Gas supply assembly, the gas supply assembly are built in the spinning liquid pool comprising jet column assembly and air pump, the jet The jet column of column assembly wraps up the hollow needle of the hollow needle group, and the air pump is connect with the jet column assembly.
2. electrostatic spinning apparatus according to claim 1, which is characterized in that the hollow needle group include more hollow needles and Liquid injection pipe;The more hollow needles are equidistant to be connected to the jet port of the liquid injection pipe.
3. electrostatic spinning apparatus according to claim 1, which is characterized in that the jet column assembly includes more jet columns And gas injection tube;The more jet columns are equidistant to be connected to the jet port of the gas injection tube.
4. electrostatic spinning apparatus according to claim 1, which is characterized in that the liquid injection apparatus includes motor, liquid Pump and inlet tube;
The motor is connect with the liquid pump;
The inlet tube is connect with the liquid pump;
The liquid outlet of the liquid pump is connect with the liquid inlet pipeline of the hollow needle group.
5. electrostatic spinning apparatus according to claim 1, which is characterized in that the jet column of the jet column assembly wraps up institute The hollow needle for stating hollow needle group is specially:The jet column of the jet column assembly wraps up the hollow needle of the hollow needle group, and institute State the top of the prominent jet column of top syringe needle of hollow needle.
6. electrostatic spinning apparatus according to claim 1, which is characterized in that the shape of the collection device be tabular, Convex-shaped or concave shape.
7. electrostatic spinning apparatus according to claim 1, which is characterized in that the hollow needle of the hollow needle group is that metal is empty Heart needle.
CN201810916006.1A 2018-08-13 2018-08-13 Electrostatic spinning device Active CN108893788B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201810916006.1A CN108893788B (en) 2018-08-13 2018-08-13 Electrostatic spinning device

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201810916006.1A CN108893788B (en) 2018-08-13 2018-08-13 Electrostatic spinning device

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CN108893788B CN108893788B (en) 2021-09-17

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111005077A (en) * 2019-12-02 2020-04-14 厦门纳莱科技有限公司 Core-string type multi-needle electrostatic spinning nozzle and electrostatic spinning device

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102534822A (en) * 2012-02-18 2012-07-04 上海工程技术大学 Device and method for preparing polysulfonamide nanometer fiber nets by means of airflow-electrostatic combination
CN103173873A (en) * 2013-05-03 2013-06-26 中原工学院 Multiple spray-head combined type air-injection electrostatic spinning machine
KR20140106874A (en) * 2013-02-27 2014-09-04 코오롱패션머티리얼 (주) Porous support, method for manufacturing the same and membrane for gas or liquid filter comprising the same
CN205275796U (en) * 2016-01-15 2016-06-01 厦门大学 Even minute liquid electrostatic spinning shower nozzle of independent power supply in area
CN107245763A (en) * 2017-07-19 2017-10-13 广东工业大学 A kind of electrostatic spinning array shower nozzle
KR20170133643A (en) * 2016-05-26 2017-12-06 황도혁 A Nano-fiber spun yarn manufacture equipment for continuous production.

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Publication number Priority date Publication date Assignee Title
CN102534822A (en) * 2012-02-18 2012-07-04 上海工程技术大学 Device and method for preparing polysulfonamide nanometer fiber nets by means of airflow-electrostatic combination
KR20140106874A (en) * 2013-02-27 2014-09-04 코오롱패션머티리얼 (주) Porous support, method for manufacturing the same and membrane for gas or liquid filter comprising the same
CN103173873A (en) * 2013-05-03 2013-06-26 中原工学院 Multiple spray-head combined type air-injection electrostatic spinning machine
CN205275796U (en) * 2016-01-15 2016-06-01 厦门大学 Even minute liquid electrostatic spinning shower nozzle of independent power supply in area
KR20170133643A (en) * 2016-05-26 2017-12-06 황도혁 A Nano-fiber spun yarn manufacture equipment for continuous production.
CN107245763A (en) * 2017-07-19 2017-10-13 广东工业大学 A kind of electrostatic spinning array shower nozzle

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拉马克瑞斯纳·西拉姆: "《静电纺丝与纳米纤维导论》", 30 September 2012, 东华大学出版社 *

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111005077A (en) * 2019-12-02 2020-04-14 厦门纳莱科技有限公司 Core-string type multi-needle electrostatic spinning nozzle and electrostatic spinning device

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Effective date of registration: 20240516

Address after: 529738 No. 6-2, Zone 8, Sanlian Industrial Zone, Gulao Town, Heshan City, Jiangmen City, Guangdong Province

Patentee after: Guangdong Houhai environmental protection new material Co.,Ltd.

Country or region after: China

Address before: 510006 No. 100 West Ring Road, Panyu District University, Guangdong, Guangzhou

Patentee before: GUANGDONG University OF TECHNOLOGY

Country or region before: China

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