CN203768508U - Spinning nozzle device for mixture nanofibers - Google Patents

Spinning nozzle device for mixture nanofibers Download PDF

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Publication number
CN203768508U
CN203768508U CN201420166873.5U CN201420166873U CN203768508U CN 203768508 U CN203768508 U CN 203768508U CN 201420166873 U CN201420166873 U CN 201420166873U CN 203768508 U CN203768508 U CN 203768508U
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CN
China
Prior art keywords
nozzle
shower nozzle
syringe needle
hollow cone
spray
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Withdrawn - After Issue
Application number
CN201420166873.5U
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Chinese (zh)
Inventor
王太宏
黄辉
刘源
刘彬
蔡道平
李寒
王晨霞
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Xiamen University
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Xiamen University
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Filing date
Publication date
Application filed by Xiamen University filed Critical Xiamen University
Priority to CN201420166873.5U priority Critical patent/CN203768508U/en
Application granted granted Critical
Publication of CN203768508U publication Critical patent/CN203768508U/en
Anticipated expiration legal-status Critical
Withdrawn - After Issue legal-status Critical Current

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Abstract

The utility model discloses a spinning nozzle device for mixture nanofibers and relates to electrostatic spinning nozzles. The spinning nozzle device comprises a nozzle support, a hollow conical nozzle, a nozzle cavity, a nozzle coupling shaft, a transmission gear, a bearing, an internal needle head, an internal needle head sleeve, an internal need head, an internal needle head seat, an electrode, a motor and a driving gear. The nozzle cavity is fixedly connected with the nozzle support, the rear portion of the hollow conical nozzle penetrates through the front end of the nozzle support and is matched with the nozzle cavity rotatably, and the rear end of the hollow conical nozzle is connected with the front end of the nozzle coupling shaft. The internal needle head sleeve is sleeved with the rear portion of the internal needle head and matched with a central through hole in the rear end of the nozzle coupling shaft rotatably, the internal needle head penetrates through a nozzle coupler to be positioned in the hollow conical nozzle, and the transmission gear is arranged on the outer wall of the rear end of the nozzle coupling shaft. The internal needle head seat is fixedly connected with the nozzle cavity, the external needle head faces the outer wall of the hollow conical nozzle, the electrode contacts with the hollow conical nozzle, the motor is arranged on the nozzle support, the driving gear on the output shaft of the motor is meshed with the transmission gear, and the internal needle head, the external needle head and the electrode are connected with a power supply externally.

Description

A kind of mixture nanofiber spinning nozzle device
Technical field
The utility model relates to a kind of electrostatic spinning nozzle, especially relates to a kind of mixture nanofiber spinning nozzle device.
Background technology
Along with the development of nanometer technology in recent years, electrostatic spinning has become to be prepared the important method of nanofiber and receives much concern.Method of electrostatic spinning is widely used, from industrial synthetic polymer to cellulose, the various raw materials such as ossein, protein, DNA complex can carry out spinning, and can in spinning process, add antibiotics, nano particle etc., prepare various functional fibers.
Traditional electrostatic spinning technique is one and prepares the most widely used technology of nanofiber, its utilize HV generator produce several kilovolts even the high-pressure electrostatic of tens kilovolts in polymer solution or melt, exert pressure, make needle tip drop deformation form taylor cone.In the time that electric field force reaches critical value, can overcome surface tension, jetting stream, jet is reeled in electric field, bending, final curing is on dash receiver.But, in traditional electrostatic spinning, the electrostatic spinning output of needle point spray nozzle type is little, though adopt Multi-tip spray nozzle type electrostatic spinning apparatus to improve to a certain extent output, but because the spacing between spinning head is little, easily produce electrostatic interference, make spinning process unstable, and the spinning head having does not carry out spinning.Low-yield, homogeneity is poor is that Electrospun can not large-scale industrial production or the main cause of application.Document [1] ([1] OODosunmu, GGChase, WKataphinan, et al.Nanotechnology.2006; 11:1123-7.) prepared nanofiber with antipriming pipe as shower nozzle, output has improved 250 times of left and right than traditional electrostatic spinning in this way.But the preparation process of this method is unsettled, and the problem that antipriming pipe stops up is also difficult to solve.Document [2] ([2] Weitz RT, Hamau L, Rauschenbach S, et al.Nano Lett.2008; 8:1187-91.) use pointed cone without shower nozzle as shower nozzle, provide a kind of efficient, the device of easy electrostatic spinning.But the fibre diameter of making is by this way disunity, from 25nm to 500mm, not etc., homogeneity is not lower.Chinese patent CN200810153891.9 has reported a kind of non-woven not electric spinning equipment in batches, the metal roller that the circumference appearance that this device employing is immersed in polymer solution is cast with tapered thread is injector head, to replace traditional needle point shower nozzle to carry out spinning, though output significantly improves, but it exists the shortcoming that injection electric threshold value is high, and can not spin the nanofiber that contains two kinds of materials simultaneously.
In view of this, the utility model proposes a kind of novel electrostatic spinning nozzle device, use this shower nozzle to carry out spinning, the more traditional needle point electrospinning of productive rate shower nozzle has great raising, and without shower nozzle blockage problem, the homogeneity of spun nanofiber diameter is good.And can spin the nanofiber that contains two kinds of different materials simultaneously.
Summary of the invention
The purpose of this utility model is to provide and can improves electrospinning device productive rate and spin fiber homogeneity, can spin a kind of mixture nanofiber spinning nozzle device of the mixture nanofiber that contains two kinds of different materials simultaneously.
The utility model comprises Spray-nozzle carrier, hollow cone shower nozzle, shower nozzle cavity, shower nozzle coupling spindle, travelling gear, bearing, interior syringe needle, interior pinhead sleeve, outer syringe needle, outer needle holder, electrode, motor and driven wheel;
Described shower nozzle cavity and Spray-nozzle carrier are connected, hollow cone shower nozzle rear portion is through Spray-nozzle carrier front end, hollow cone shower nozzle rear portion and shower nozzle cavity are rotatably assorted, hollow cone shower nozzle rear end is connected with shower nozzle coupling spindle front end, shower nozzle shaft coupling is provided with central through hole, interior pinhead sleeve is sheathed on interior syringe needle rear portion, interior pinhead sleeve and shower nozzle coupling spindle rear end central through hole are rotatably assorted, interior syringe needle is through shower nozzle shaft coupling, interior syringe needle is positioned at hollow cone shower nozzle, travelling gear is located at shower nozzle coupling spindle rear end outer wall, outer syringe needle is located in outer needle holder, outer needle holder and shower nozzle cavity are connected, outer syringe needle is in the face of hollow cone shower nozzle outer wall, electrode and hollow cone shower nozzle touch, motor is arranged on Spray-nozzle carrier, motor output shaft is provided with driven wheel, driven wheel engages with travelling gear, interior syringe needle, outer syringe needle and electrode be external DC high-voltage power supply all.
Described Spray-nozzle carrier front end is provided with through hole, and hollow cone shower nozzle rear portion is arranged in the through hole of Spray-nozzle carrier.
Described hollow cone shower nozzle rear portion is rotatably assorted by bearing and shower nozzle cavity.
Described interior pinhead sleeve and shower nozzle coupling spindle rear end central through hole are also rotatably assorted by bearing.
Described motor is arranged on Spray-nozzle carrier by electric machine support.
Described electrode is the carbon electrode with spring, is arranged in the electrode sleeve of being located at Spray-nozzle carrier bottom with the carbon electrode of spring.
Compared with the prior art, operation principle of the present utility model and beneficial effect are as follows:
When spinning, interior syringe needle (outer syringe needle) is connect to high-voltage DC power supply positive pole, spinning collecting board is connect to high-voltage DC power supply negative pole, solution or melt from interior syringe needle or syringe needle flow to hollow cone shower nozzle, solution is evenly spin-coated on cone surface, under the acting in conjunction due to centrifugal force and adhesion in rotary course, and liquid meeting deformation, and flow to large end circumference from cone shower nozzle small end, after under electrostatic force, form Electrospun.The utility model, owing to having inside and outside two syringe needles, therefore can inject spinning solution by inside and outside syringe needle to the inside and outside wall of hollow cone shower nozzle simultaneously or separately.When use inside and outside syringe needle can spin mixture nanofiber in the time that hollow cone shower nozzle injects solution simultaneously, comprise two kinds of different types of nanofiber products.Outer syringe needle is fixed on Spray-nozzle carrier by outer needle holder, and maintenance is relative static with Spray-nozzle carrier.When the rotation of shower nozzle coupling spindle, it is static that interior syringe needle keeps.Shower nozzle shaft coupling when rotated shower nozzle cavity keeps static.Motor rotation, by gear transmission, drives shower nozzle shaft coupling and the rotation of hollow cone shower nozzle.In the time that hollow cone shower nozzle rotates, the cylinder ledge surface of electrode and hollow cone shower nozzle keeps in touch, and conducts electricity.Owing to can forming a large amount of taylor cone of evenly arranging (being equivalent to traditional needle point shower nozzle circle ring array arranges) therefore on the large end circumference of cone shower nozzle, the utility model can improve electrospinning device productive rate, simultaneously because the electric field action that on circumference, each taylor cone is subject to is almost identical, therefore spin fiber homogeneity high, and can spin a kind of mixture nanofiber spinning nozzle device of the mixture nanofiber that contains two kinds of different materials simultaneously.
Brief description of the drawings
Fig. 1 is one of the utility model example structure schematic perspective view.
Fig. 2 is two of the utility model example structure schematic perspective view.
Fig. 3 is the utility model example structure decomposing schematic representation.
Detailed description of the invention
Referring to Fig. 1~3, the present embodiment comprises Spray-nozzle carrier 12, hollow cone shower nozzle 1, shower nozzle cavity 2, shower nozzle coupling spindle 4, travelling gear 7, bearing 8, interior syringe needle 9, interior pinhead sleeve 10, outer syringe needle 5, outer needle holder 6, electrode, motor 14 and driven wheel 15.
Shower nozzle cavity 2 is connected with Spray-nozzle carrier 12, and Spray-nozzle carrier 12 front ends are provided with through hole, and hollow cone shower nozzle 1 rear portion is arranged in the through hole of Spray-nozzle carrier 12.Hollow cone shower nozzle 1 rear portion is through Spray-nozzle carrier 12 front ends, and hollow cone shower nozzle 1 rear portion is rotatably assorted by 2 bearings 3 and shower nozzle cavity 2.Hollow cone shower nozzle 1 rear end is connected with shower nozzle coupling spindle 4 front ends, and shower nozzle shaft coupling 4 is provided with central through hole, and interior pinhead sleeve 10 is sheathed on interior syringe needle 9 rear portions, and interior pinhead sleeve 10 is rotatably assorted by bearing 8 with shower nozzle coupling spindle 4 rear end central through holes.Interior syringe needle 9 is through shower nozzle shaft coupling 4, interior syringe needle 9 is positioned at hollow cone shower nozzle 1, travelling gear 7 is located at shower nozzle coupling spindle 4 rear end outer walls, and outer syringe needle 5 is located in outer needle holder 6, and outer needle holder 6 is connected with shower nozzle cavity 2, outer syringe needle 5 is in the face of hollow cone shower nozzle 1 outer wall, electrode and hollow cone shower nozzle 1 touch, and electrode connects DC high-voltage power supply, and motor 14 is arranged on Spray-nozzle carrier 12, motor 14 output shafts are provided with driven wheel 15, and driven wheel 15 engages with travelling gear 7.Interior syringe needle 9, outer syringe needle 5 and electrode be external DC high-voltage power supply (not shown) all.
Described motor 14 is arranged on Spray-nozzle carrier 12 by electric machine support 13.
Described electrode is the carbon electrode with spring, is arranged in the electrode sleeve 11 of being located at Spray-nozzle carrier 12 bottoms with the carbon electrode of spring.

Claims (6)

1. a mixture nanofiber spinning nozzle device, it is characterized in that, comprise Spray-nozzle carrier, hollow cone shower nozzle, shower nozzle cavity, shower nozzle coupling spindle, travelling gear, bearing, interior syringe needle, interior pinhead sleeve, outer syringe needle, outer needle holder, electrode, motor and driven wheel;
Shower nozzle cavity and Spray-nozzle carrier are connected, hollow cone shower nozzle rear portion is through Spray-nozzle carrier front end, hollow cone shower nozzle rear portion and shower nozzle cavity are rotatably assorted, hollow cone shower nozzle rear end is connected with shower nozzle coupling spindle front end, shower nozzle shaft coupling is provided with central through hole, interior pinhead sleeve is sheathed on interior syringe needle rear portion, interior pinhead sleeve and shower nozzle coupling spindle rear end central through hole are rotatably assorted, interior syringe needle is through shower nozzle shaft coupling, interior syringe needle is positioned at hollow cone shower nozzle, travelling gear is located at shower nozzle coupling spindle rear end outer wall, outer syringe needle is located in outer needle holder, outer needle holder and shower nozzle cavity are connected, outer syringe needle is in the face of hollow cone shower nozzle outer wall, electrode and hollow cone shower nozzle touch, motor is arranged on Spray-nozzle carrier, motor output shaft is provided with driven wheel, driven wheel engages with travelling gear, interior syringe needle, outer syringe needle and electrode be external DC high-voltage power supply all.
2. a kind of mixture nanofiber spinning nozzle device as claimed in claim 1, is characterized in that, described Spray-nozzle carrier front end is provided with through hole, and hollow cone shower nozzle rear portion is arranged in the through hole of Spray-nozzle carrier.
3. a kind of mixture nanofiber spinning nozzle device as claimed in claim 1, is characterized in that, described hollow cone shower nozzle rear portion is rotatably assorted by bearing and shower nozzle cavity.
4. a kind of mixture nanofiber spinning nozzle device as claimed in claim 1, is characterized in that, described interior pinhead sleeve and shower nozzle coupling spindle rear end central through hole are also rotatably assorted by bearing.
5. a kind of mixture nanofiber spinning nozzle device as claimed in claim 1, is characterized in that, described motor is arranged on Spray-nozzle carrier by electric machine support.
6. a kind of mixture nanofiber spinning nozzle device as claimed in claim 1, is characterized in that, described electrode is the carbon electrode with spring, is arranged in the electrode sleeve of being located at Spray-nozzle carrier bottom with the carbon electrode of spring.
CN201420166873.5U 2014-04-09 2014-04-09 Spinning nozzle device for mixture nanofibers Withdrawn - After Issue CN203768508U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201420166873.5U CN203768508U (en) 2014-04-09 2014-04-09 Spinning nozzle device for mixture nanofibers

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201420166873.5U CN203768508U (en) 2014-04-09 2014-04-09 Spinning nozzle device for mixture nanofibers

Publications (1)

Publication Number Publication Date
CN203768508U true CN203768508U (en) 2014-08-13

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Family Applications (1)

Application Number Title Priority Date Filing Date
CN201420166873.5U Withdrawn - After Issue CN203768508U (en) 2014-04-09 2014-04-09 Spinning nozzle device for mixture nanofibers

Country Status (1)

Country Link
CN (1) CN203768508U (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103866404A (en) * 2014-04-09 2014-06-18 厦门大学 Spinning sprayer device for compound nano-fiber
CN105568410A (en) * 2016-02-03 2016-05-11 厦门大学 Gas-assisted nanofiber conveying device

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103866404A (en) * 2014-04-09 2014-06-18 厦门大学 Spinning sprayer device for compound nano-fiber
CN105568410A (en) * 2016-02-03 2016-05-11 厦门大学 Gas-assisted nanofiber conveying device

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Date Code Title Description
C14 Grant of patent or utility model
GR01 Patent grant
AV01 Patent right actively abandoned

Granted publication date: 20140813

Effective date of abandoning: 20160106

C25 Abandonment of patent right or utility model to avoid double patenting