CN108850331A - A kind of tibetan crabapple tea cream and its preparation process - Google Patents
A kind of tibetan crabapple tea cream and its preparation process Download PDFInfo
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- A23F—COFFEE; TEA; THEIR SUBSTITUTES; MANUFACTURE, PREPARATION, OR INFUSION THEREOF
- A23F3/00—Tea; Tea substitutes; Preparations thereof
- A23F3/34—Tea substitutes, e.g. matè; Extracts or infusions thereof
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Abstract
The present invention provides a kind of tibetan crabapple tea cream and its preparation processes, are related to the field of deep of tibetan crabapple leaf.The preparation process, including：Treated filters after tibetan crabapple leaf mixes 4~6min with 80~95 DEG C of water by fermented, obtains Aqueous extracts；It is again the alcoholic solution of 1~10Vol% according to solid-liquid ratio 1 by filter residue resulting after filtering and ethanol content：30~70 mixing, are extracted 1~3 time, 8~20min, obtains alcohol extract every time using solvent extraction method；Alcohol extract is mixed with Aqueous extracts again, obtains crude extract；After crude extract 60~100 μm of filter paper filtering, it is concentrated into the medicinal extract of dilute syrupy shape, after drying and crushing, briquet.Obtained tibetan crabapple tea cream, small in size, light-weight, without tea grounds after brewing, and the coloration of millet paste, brightness, transparency are higher, have back sweet, mellow, lubricious mouthfeel.
Description
Technical field
The present invention relates to the field of deep of tibetan crabapple, in particular to a kind of tibetan crabapple tea cream and its preparation
Technique.
Background technique
Qinghai Tibetan tea is made of the tender leaf of tibetan crabapple, and ancient times only circulates in living Buddha stratum, belongs to a kind of high-grade drink.Solution
It puts rear use scope to be gradually expanded, will be widely welcomed in the Tibetan people masses.Tibetan crabapple tea flavour sweetness and bitterness, mouthfeel are aromatic,
Rich in macronutrients such as tea polyphenols, vitamin C, flavonoids, quite liked by the Tibetan masses.Tibetan crabapple to modern three
It is high：Hyperlipidemia, high-fat, hypertension and diuresis toxin expelling have significant curative effect, get consumer reception again, sales volume is increasing.
Why tibetan crabapple becomes one of the fine work in numerous tealeaves, is because of its distinctive geographical growing environment and system
Make technique and as the extension fragrance mouthfeel of storage time is better.Tibetan crabapple has solution grease, aid digestion, warm in addition
Stomach, promote the production of body fluid, quench the thirst, the multi-functionals such as relieve the effect of alcohol of sobering up are liked deeply by the vast people that drinks tea.But tibetan crabapple brews technique, uses
Utensil have special requirement, it usually needs take a significant amount of time according to stringency procedures tea-making, can fully demonstrate
The characteristic of tibetan crabapple, thus itself and its be not suitable for drinking in hotel, public arena and out on tours, and its make tea it is cumbersome
Process seriously constrains numerous consumer groups.
Summary of the invention
The first object of the present invention is to provide a kind of tibetan crabapple tea cream, which is mutually tied using water extraction with alcohol extracting method
The mode of conjunction dissolves out the big effective component of dissolubility in tibetan crabapple leaf, and yield is high, and aroma substance is largely protected
It stays, and the utilization rate of raw material is big,.
The second object of the present invention is to provide a kind of tibetan crabapple tea cream as made from above-mentioned preparation process, the tea cream body
Product is small, light-weight, easy to carry and drink.Without tea grounds after brewing, and the coloration of millet paste, brightness, transparency are higher, have
Return sweet, mellow, lubricious mouthfeel.
In order to realize above-mentioned purpose of the invention, spy uses following technical scheme：
A kind of preparation process of tibetan crabapple tea cream comprising：
Treated filters after tibetan crabapple leaf mixes 4~6min with 80~95 DEG C of water by fermented, obtains Aqueous extracts；Again
It is the alcoholic solution of 1~10Vol% according to solid-liquid ratio 1 by filter residue resulting after filtering and ethanol content：30~70 mixing, use are molten
Agent extraction method is extracted 1~3 time, and 8~20min, obtains alcohol extract every time；Alcohol extract is mixed with Aqueous extracts again, obtains crude extract；
After crude extract 60~100 μm of filter paper filtering, it is concentrated into the medicinal extract of dilute syrupy shape, after drying and crushing, compacting
It is blocking.
A kind of tibetan crabapple tea cream as obtained by above-mentioned preparation process.
Compared with prior art, beneficial effects of the present invention for example including：
Present disclosure provide this tibetan crabapple tea cream preparation process, first with brewed in hot water tibetan crabapple leaf 4~
6min simulates the process made tea, and makes big polar substances Fast Stripping contained in tibetan crabapple leaf；Ethanol content is then used again
Lower alcoholic solution carries out alcohol extracting, dissolves out the active principle that polarity is slightly lower in medicinal material successively, so as to improve the yield of leachable
With the amount retained of dissolubility and raising fragrance matter.After obtained crude extract is filtered again again, it is concentrated into paste, is made
Obtain tibetan crabapple tea cream.In this way, the dissolution rate of chemical substance is big in tibetan crabapple leaf, yield is high, so that raw material
Utilization rate is big, is suitble to the tibetan crabapple tea cream of scale, batch production.
Obtained this tibetan crabapple tea cream, it is small in size, light-weight, dissolubility is good, it conveniently brews and drinks；After brewing
Without tea grounds, and the coloration of millet paste, brightness, transparency are preferable, have back sweet, mellow, lubricious mouthfeel.
Specific embodiment
Embodiment of the present invention is described in detail below in conjunction with embodiment, but those skilled in the art will
Understand, the following example is merely to illustrate the present invention, and is not construed as limiting the scope of the invention.It is not specified in embodiment specific
Condition person carries out according to conventional conditions or manufacturer's recommended conditions.Reagents or instruments used without specified manufacturer is
The conventional products that can be obtained by commercially available purchase.
Present embodiment provides a kind of tibetan crabapple tea cream, and preparation process includes：
Step S1:Treated filters after tibetan crabapple leaf mixes 4~6min with 80~95 DEG C of water by fermented, obtains water
Extract.
Step brewed in hot water tibetan crabapple leaf keeps big polar substances contained in tibetan crabapple leaf fast in a short time
It is instant go out, be conducive to the efficiency for improving extract obtained dissolubility and subsequent alcohol extracting.The temperature of hot water is 80~95 DEG C,
Perhaps it is 82~93 DEG C to be perhaps 85~90 DEG C and be perhaps 87~89 DEG C or be 88 DEG C.The time of brewed in hot water be 4~
6min, or be 5min.
Further, before with brewed in hot water, further include the steps that crushing on tibetan crabapple leaf, smashed tibetan crabapple
Leaf be it is powdered, granularity be 20~40 mesh, or be 25~35 mesh.The tibetan crabapple leaf powder of this partial size, with water or
When person's alcohol water extracts, the contact area of tibetan crabapple leaf and Extraction solvent is big, the dissolution of chemical substance contained by tibetan crabapple leaf
Rate is high, but its granularity can not be too thin, to avoid subsequent filter overlong time.
Further, tibetan crabapple leaf is made by fermentation process, and fermentation temperature is 20~25 DEG C, the air of fermentation
Humidity is 90~99%, and fermentation time is 0.5~3h.
When fermentation, ferment indoor temperature, humidity need to meet the oxidative polymerization of tea polyphenols oxidizing ferment.More preferably
, fermenting cellar temperature is controlled at 20~25 DEG C or so, and the temperture of leaves of fermentation, which are maintained at 30 DEG C or so, to be advisable.If temperture of leaves are more than 40 DEG C,
Carry out turning heat dissipation, in order to avoid fermentation is excessively fierce, make gross tea it is fragrant it is low it is lightly seasoned, color is dark.It to be taken especially in high temperature season
Cooling measure, booth leaf wants thin, with sharp radiating and cooling；Conversely, spreading out Ye Yaohou when temperature is lower, some heat preservations is taken to arrange when necessary
It applies.
In fermenting cellar, air humidity is maintained at 90% or more the activity for being conducive to improve polyphenol oxidase, is conducive to tea Huang
The formation and accumulation of element；Conversely, fermentation space-time air humidity is spent low, it is unfavorable for the enzymatic oxidation of tea polyphenols, adds non-enzymatic oxidation
Play causes soup look and tea residue all dimmed, and flavour is thin.
When fermentation, leaf-spreading thickness is generally at 8~12 centimetres.Tender leaf and blade profile it is small want thin booth；Old leaf and blade profile are big to be wanted
Thickness booth.Thick booth is wanted when temperature is low；Thin booth is answered when temperature is high.But no matter thick booth or thin booth, ventilation when keeping fermentation that spreads leaf
Well.It should be turned in fermentation process once, with benefit heat dissipation ventilation.
Fermentation time is usually 0.5~3h, is perhaps 0.5~2.5h or is 1~2h.Fermentated leaves green grass gas disappears, out
A kind of existing fresh, pure and fresh flowers and fruits are fragrant, the red change of leaf color, as fermentation appropriateness.
Step S2:It is again the alcoholic solution of 1~10Vol% according to solid-liquid ratio 1 by filter residue resulting after filtering and ethanol content：
30~70 mixing, are extracted 1~3 time, 8~20min, obtains alcohol extract every time using solvent extraction method.
Ethanol content is used (to be perhaps 2~8Vol% or be 4~6Vol%, Huo Zhewei for 1~10Vol%
Alcoholic solution 5Vol%) carries out alcohol extracting can make the polarity of water decrease although the content of ethyl alcohol is lower, be mentioned with this
The effective component that polarity is slightly lower is taken, and retains some aroma substances.If it is extracted completely with pure water, then it cannot will be big absolutely
Partial fragrance matter brings tea cream into, it is therefore necessary to a small amount of ethyl alcohol be added in extracting solution, just can guarantee depositing for fragrance matter
It stays.And the most important feature of tibetan crabapple tea is its soup look in Chinese red, bright beauty.Solid-liquid ratio when extraction is 1：30~
70, or be 1：40~60, or be 1：45~55；It or is 1：50.
Further, filter residue is extracted into 1~3 time (being chosen as 2 times) using solvent extraction method, the 1st extraction time is 8
~12min is perhaps 9~11min or is 10min；2nd~3 extraction time is 15~20min, or for 16~
19min, or be 17~18min.By the extraction of short period first time, polarity in tibetan crabapple leaf can be made more slightly lower
Ingredient Fast Stripping, reduce filter residue in polar substances content；Then pass through the extraction of second and third secondary long period, so that
Consider the slightly lower ingredient dissolution as much as possible of polarity in slag, thus improve the efficiency of extraction, the dissolubility of extract with
And content.
Further, the alcoholic solution that ethanol content is 1~10Vol% be with alcoholic strength be 45~55 degree (or for 48~
52 degree, or be 50 degree) grain wine be mixed to prepare with water.Alcoholic solution is mixed with using grain wine and water, is unfavorable for increasing
Aroma substance in alcoholic solution, so that the flavor and taste of last prepared tibetan crabapple are preferable.Grain wine, such as can
To be liquor made from sorghum, rice wine, barley wine etc..
Further, solvent extraction method includes heating and refluxing extraction method, ultrasonic vibration extraction method, decocting method, percolation, leaching
Stain method.
Further, solvent extraction method is heating and refluxing extraction method, and heating temperature is 80~90 DEG C, or is 82~88
DEG C, perhaps it is 84~86 DEG C or is 85 DEG C.
Further, solvent extraction method is ultrasonic vibration extraction method, and supersonic frequency is 500~1000Hz, or for 600~
900Hz is perhaps 700~800Hz or is 850Hz.
Further, solvent extraction method is decocting method, and decocting temperature is 80~95 DEG C, or is 82~92 DEG C, Huo Zhewei
84~90 DEG C are perhaps 86~88 DEG C or are 87 DEG C.
Step S3:Alcohol extract is mixed with Aqueous extracts again, obtains crude extract.
Step S4:After 60~100 μm of filter paper filtering of crude extract, it is concentrated into the medicinal extract of dilute syrupy shape, drying and crushing
Afterwards, briquet.
It is for re-filtering to crude extract using 60~100 μm of filter paper in order to improve the dissolubility of obtained tea cream,
Remove the substance and mixed filter residue of slightly solubility.The aperture of filter paper is 60~100 μm, be perhaps 70~90 μm or be 75~
85 μm, or be 80 μm.
Further, before being filtered crude extract, further include：By crude extract be concentrated under reduced pressure into original volume 0.4~
After 0.6 times, natural cooling.After the volume reduction of crude extract and extracting solution temperature reduce, the lesser substance meeting of partial solubility
It separates out, filters at this time, the lesser substance of solubility in crude extract can be removed, further increase the dissolution of prepared tea cream
Property.
Further, dry method includes boulton process, freeze-drying.Obtained medicinal extract is done under vacuum
It is dry, it helps avoid the structure in high-temperature drying procedures of chemical substance contained in tealeaves and changes, influence mouthfeel and tea
Health-care effect.Water content after drying in resulting tea cream is 10~15%, is perhaps 12~14% or is 13%.
Feature and performance of the invention are described in further detail with reference to embodiments：
Embodiment 1
The present embodiment provides a kind of tibetan crabapple tea cream, preparation method includes：
It will be filtered after the resulting tibetan crabapple leaf of fermentation process and 90 DEG C of water mixing 5min, obtain Aqueous extracts；It again will filtering
Resulting filter residue and ethanol content are the alcoholic solution of 10Vol% according to solid-liquid ratio 1 afterwards：70 mixing, are extracted 2 times using decocting method,
Each 14min, obtains alcohol extract；Alcohol extract is mixed with Aqueous extracts again, obtains crude extract.
After crude extract 80 μm of filter paper filtering, it is concentrated into the medicinal extract of dilute syrupy shape, after drying and crushing, briquet,
Up to tibetan crabapple tea cream.
Embodiment 2
The present embodiment provides a kind of tibetan crabapple tea cream, preparation method includes：
It will be filtered after the resulting tibetan crabapple leaf of fermentation process and 95 DEG C of water mixing 4min, obtain Aqueous extracts；It again will filtering
Resulting filter residue and ethanol content are the alcoholic solution of 10Vol% according to solid-liquid ratio 1 afterwards：70 mixing, using heating and refluxing extraction method
It is extracted 1 time at 85 DEG C, extraction time 20min obtains alcohol extract；Alcohol extract is mixed with Aqueous extracts again, obtains crude extract；
After crude extract 100 μm of filter paper filtering, it is concentrated into the medicinal extract of dilute syrupy shape, after drying and crushing, briquet,
Up to tibetan crabapple tea cream.
Embodiment 3
The present embodiment provides a kind of tibetan crabapple tea cream, preparation method includes：
By fermentation process gained and granularity is filters after the tibetan crabapple leaf and 80 DEG C of water mixing 6min of 28~32 mesh,
Obtain Aqueous extracts；It is again the alcoholic solution of 1.0Vol% according to solid-liquid ratio 1 by filter residue resulting after filtering and ethanol content：30 mixing,
It is extracted 2 times using ultrasonic vibration extraction method in 850Hz, each 8min obtains alcohol extract；Alcohol extract is mixed with Aqueous extracts again,
Obtain crude extract；
After crude extract 60 μm of filter paper filtering, it is concentrated into the medicinal extract of dilute syrupy shape, after drying and crushing, briquet,
Up to tibetan crabapple tea cream.
Embodiment 4
The present embodiment provides a kind of tibetan crabapple tea cream, preparation method includes：
It will be obtained by fermentation process and granularity is tibetan crabapple leaf powder and the mistake after 88 DEG C of water mixing 5min of 35~40 mesh
Filter, obtains Aqueous extracts；It is again the alcoholic solution of 7Vol% according to solid-liquid ratio 1 by filter residue resulting after filtering and ethanol content：40 mixing,
It is extracted at 95 DEG C 2 times using decocting method, the 1st time extraction 10min, the 2nd extraction 18min obtain alcohol extract；Again by alcohol extract
It is mixed with the Aqueous extracts, obtains crude extract；
Crude extract is concentrated under reduced pressure into 0.5 times of original volume, the natural cooling when color of crude extract becomes claret, with
Afterwards with after 70 μm of filter paper filtering, it is concentrated into the medicinal extract of dilute syrupy shape, is dried using boulton process, and after crushing, pressure
Block is made to get tibetan crabapple tea cream.
Embodiment 5
The present embodiment provides a kind of tibetan crabapple tea cream, preparation method includes：
It will be obtained by fermentation process and granularity is tibetan crabapple leaf powder and the mistake after 92 DEG C of water mixing 5min of 20~25 mesh
Filter, obtains Aqueous extracts；It is again the alcoholic solution of 4Vol% according to solid-liquid ratio 1 by filter residue resulting after filtering and ethanol content：60 mixing,
It is extracted at 90 DEG C 3 times using heating and refluxing extraction method, the 1st time extraction 8min, the 2nd, 3 extraction 15min obtain alcohol extract；
Alcohol extract is mixed with Aqueous extracts again, obtains crude extract；
Crude extract is concentrated under reduced pressure into 0.4 times of original volume, the natural cooling when color of crude extract becomes claret, with
Afterwards with after 90 μm of filter paper filtering, it is concentrated into the medicinal extract of dilute syrupy shape, is dried using boulton process, and after crushing, pressure
Block is made to get tibetan crabapple tea cream.
Embodiment 6
The present embodiment provides a kind of tibetan crabapple tea cream, preparation method includes：
It will be obtained by fermentation process and granularity is tibetan crabapple leaf powder and the mistake after 85 DEG C of water mixing 5min of 25~30 mesh
Filter, obtains Aqueous extracts；It is again the alcoholic solution of 6Vol% according to solid-liquid ratio 1 by filter residue resulting after filtering and ethanol content：80 mixing,
It is extracted 2 times using ultrasonic vibration extraction method in 1000Hz, the 1st time extraction 12min, the 2nd extraction 20min obtain alcohol extract；Again
Alcohol extract is mixed with Aqueous extracts, obtains crude extract；
Crude extract is concentrated under reduced pressure into 0.6 times of original volume, the natural cooling when color of crude extract becomes claret, with
Afterwards with after 65 μm of filter paper filtering, it is concentrated into the medicinal extract of dilute syrupy shape, after dry at 80~100 DEG C and crushing, is pressed into
Block is to get tibetan crabapple tea cream.
Experimental example
Influence of the alcoholic solution of different Extracting temperature, different content to yield and solubility：
Extracting method：
A. it will be filtered after the resulting tibetan crabapple leaf (5Kg) of fermentation process and 90 DEG C of water mixing 5min, obtain Aqueous extracts；
B. resulting filter residue is from alcohol-water solution (ethanol content is different) according to solid-liquid ratio 1 after filtering again：45 mixing, are adopted
It is extracted at different temperatures 2 times with heating and refluxing extraction method, each 14min obtains alcohol extract；Alcohol extract and Aqueous extracts are mixed again
It closes, obtains crude extract；
C. by after 80 μm of filter paper filtering of crude extract, it is concentrated into the medicinal extract of dilute syrupy shape, is carried out using boulton process
It is dried.
Resulting dry cream load-bearing after will be dry, and solubility is tested in 80 DEG C of hot water, as a result see in table 1.
Influence of the 1. different tests condition of table to yield and solubility
| Technique number | Ethanol content (%) in alcohol-water solution | Extracting temperature (DEG C) | Yield (%) | Dissolubility |
| 1 | 0 | 75 | 8.37 | It is high |
| 2 | 0 | 85 | 8.75 | It is high |
| 3 | 0 | 95 | 9.84 | In |
| 4 | 5 | 75 | 11.71 | It is high |
| 5 | 5 | 85 | 12.58 | It is high |
| 6 | 5 | 95 | 12.90 | In |
| 7 | 15 | 75 | 12.47 | In |
| 8 | 15 | 85 | 13.50 | In |
| 9 | 15 | 95 | 14.07 | Difference |
As can be seen from Table 1, the ethanol content in alcohol-water solution and Extracting temperature have the yield of dry cream and dissolubility
It influences, specifically, the ethanol content in alcohol-water solution is bigger, dry spun is bigger, but dissolubility is gradually deteriorated；Extracting temperature
Higher, dry spun is bigger, but dissolubility is gradually deteriorated.Meanwhile technique number be 5 the resulting dry spun of method it is big and
Dissolubility is good.
In conclusion the preparation process for this tibetan crabapple tea cream that present embodiment provides, first uses brewed in hot water floral leaf
Malus spectabilis 4~6min of leaf, simulates the process made tea, and makes big polar substances Fast Stripping contained in tibetan crabapple leaf；Then adopt again
Alcohol extracting is carried out with the lower alcoholic solution of ethanol content, dissolves out the active principle that polarity is slightly lower in medicinal material successively, so as to improve molten
The yield and dissolubility of object and the amount retained of raising fragrance matter out.After obtained crude extract is filtered again again, concentration
To paste, tibetan crabapple tea cream is made.In this way, the dissolution rate of chemical substance is big in tibetan crabapple leaf, yield is high, makes
The utilization rate for obtaining raw material is big, is suitble to the tibetan crabapple tea cream of scale, batch production.Obtained this tibetan crabapple tea cream,
It is small in size, light-weight, dissolubility is good, conveniently brew and drink；Without tea grounds after brewing, and the coloration of millet paste, brightness, transparency are equal
Preferably, there is back sweet, mellow, lubricious mouthfeel.
Although illustrate and describing the present invention with specific embodiment, it will be appreciated that without departing substantially from of the invention
Many other change and modification can be made in the case where spirit and scope.It is, therefore, intended that in the following claims
Including belonging to all such changes and modifications in the scope of the invention.
Claims (10)
1. a kind of preparation process of tibetan crabapple tea cream, which is characterized in that it includes：
Treated filters after tibetan crabapple leaf mixes 4~6min with 80~95 DEG C of water by fermented, obtains Aqueous extracts；It incited somebody to action again
Resulting filter residue and ethanol content are the alcoholic solution of 1~10Vol% according to solid-liquid ratio 1 after filter：30~70 mixing, are mentioned using solvent
It follows the example of extraction 1~3 time, 8~20min, obtains alcohol extract every time；The alcohol extract is mixed with the Aqueous extracts again, is obtained thick
Extract；
After the crude extract 60~100 μm of filter paper filtering, it is concentrated into the medicinal extract of dilute syrupy shape, after drying and crushing, compacting
It is blocking.
2. the preparation process of tibetan crabapple tea cream according to claim 1, which is characterized in that the fermentation of the fermentation process
Temperature is 20~25 DEG C, and the air humidity of fermentation is 90~99%, and fermentation time is 0.5~3h.
3. the preparation process of tibetan crabapple tea cream according to claim 1, which is characterized in that will be described in filter residue use
Solvent extraction method extracts 1~3 time, and the 1st extraction time is 8~12min, and the 2nd~3 extraction time is 15~20min.
4. the preparation process of tibetan crabapple tea cream according to claim 1, which is characterized in that the ethanol content be 1~
The alcoholic solution of 10Vol% is that the grain wine for being 45~55 degree with alcoholic strength is mixed to prepare with water.
5. the preparation process of tibetan crabapple tea cream according to claim 1, which is characterized in that carried out by the crude extract
Before filtering, further include：After the crude extract to be concentrated under reduced pressure into 0.4~0.6 times of original volume, natural cooling.
6. the preparation process of tibetan crabapple tea cream according to claim 1, which is characterized in that the method for the drying includes
Boulton process, freeze-drying.
7. the preparation process of tibetan crabapple tea cream according to claim 1, which is characterized in that the solvent extraction method includes
Heating and refluxing extraction method, ultrasonic vibration extraction method, decocting method, percolation.
8. the preparation process of tibetan crabapple tea cream according to claim 1, which is characterized in that the solvent extraction method is to add
Water bath reflux method, heating temperature are 80~90 DEG C.
9. the preparation process of tibetan crabapple tea cream according to claim 1, which is characterized in that the solvent extraction method is super
Extraction method is swung in acoustic shock, and supersonic frequency is 500~1000Hz.
10. tibetan crabapple tea cream obtained by a kind of preparation process as described in any one of claims 1 to 9.
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