CN108840811A - The method that vegetable oil extracts calciferol in mushroom powder - Google Patents
The method that vegetable oil extracts calciferol in mushroom powder Download PDFInfo
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- CN108840811A CN108840811A CN201810764699.7A CN201810764699A CN108840811A CN 108840811 A CN108840811 A CN 108840811A CN 201810764699 A CN201810764699 A CN 201810764699A CN 108840811 A CN108840811 A CN 108840811A
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- mushroom
- oil
- calciferol
- vegetable oil
- mushroom powder
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- 235000001674 Agaricus brunnescens Nutrition 0.000 title claims abstract description 83
- 238000000034 method Methods 0.000 title claims abstract description 55
- 239000000843 powder Substances 0.000 title claims abstract description 34
- 235000015112 vegetable and seed oil Nutrition 0.000 title claims abstract description 33
- 239000008158 vegetable oil Substances 0.000 title claims abstract description 32
- MECHNRXZTMCUDQ-UHFFFAOYSA-N Vitamin D2 Natural products C1CCC2(C)C(C(C)C=CC(C)C(C)C)CCC2C1=CC=C1CC(O)CCC1=C MECHNRXZTMCUDQ-UHFFFAOYSA-N 0.000 title claims abstract description 28
- 229960002061 ergocalciferol Drugs 0.000 title claims abstract description 28
- MECHNRXZTMCUDQ-RKHKHRCZSA-N vitamin D2 Chemical compound C1(/[C@@H]2CC[C@@H]([C@]2(CCC1)C)[C@H](C)/C=C/[C@H](C)C(C)C)=C\C=C1\C[C@@H](O)CCC1=C MECHNRXZTMCUDQ-RKHKHRCZSA-N 0.000 title claims abstract description 28
- 235000001892 vitamin D2 Nutrition 0.000 title claims abstract description 28
- 239000011653 vitamin D2 Substances 0.000 title claims abstract description 28
- 239000000284 extract Substances 0.000 title claims abstract description 11
- 238000000605 extraction Methods 0.000 claims abstract description 30
- 239000004519 grease Substances 0.000 claims abstract description 21
- 239000003921 oil Substances 0.000 claims abstract description 18
- 235000019198 oils Nutrition 0.000 claims abstract description 18
- 238000000926 separation method Methods 0.000 claims abstract description 16
- 238000001035 drying Methods 0.000 claims abstract description 12
- 239000000203 mixture Substances 0.000 claims abstract description 10
- 235000011194 food seasoning agent Nutrition 0.000 claims description 8
- 238000004108 freeze drying Methods 0.000 claims description 7
- 235000019486 Sunflower oil Nutrition 0.000 claims description 6
- 235000013305 food Nutrition 0.000 claims description 6
- 239000002600 sunflower oil Substances 0.000 claims description 6
- 244000251953 Agaricus brunnescens Species 0.000 claims description 5
- JEIPFZHSYJVQDO-UHFFFAOYSA-N iron(III) oxide Inorganic materials O=[Fe]O[Fe]=O JEIPFZHSYJVQDO-UHFFFAOYSA-N 0.000 claims description 5
- 238000004519 manufacturing process Methods 0.000 claims description 5
- 238000001914 filtration Methods 0.000 claims description 4
- 238000012792 lyophilization process Methods 0.000 claims description 4
- 238000003801 milling Methods 0.000 claims description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 4
- 241000222532 Agrocybe Species 0.000 claims description 3
- 241000726811 Carpinus betulus Species 0.000 claims description 3
- 244000234623 Coprinus comatus Species 0.000 claims description 3
- 235000004439 Coprinus comatus Nutrition 0.000 claims description 3
- 240000000588 Hericium erinaceus Species 0.000 claims description 3
- 235000007328 Hericium erinaceus Nutrition 0.000 claims description 3
- 235000019483 Peanut oil Nutrition 0.000 claims description 3
- 244000252132 Pleurotus eryngii Species 0.000 claims description 3
- 235000001681 Pleurotus eryngii Nutrition 0.000 claims description 3
- 241000318836 Pleurotus nebrodensis Species 0.000 claims description 3
- 240000001462 Pleurotus ostreatus Species 0.000 claims description 3
- 235000001603 Pleurotus ostreatus Nutrition 0.000 claims description 3
- 235000008452 baby food Nutrition 0.000 claims description 3
- 239000010495 camellia oil Substances 0.000 claims description 3
- 235000009508 confectionery Nutrition 0.000 claims description 3
- 235000005687 corn oil Nutrition 0.000 claims description 3
- 239000002285 corn oil Substances 0.000 claims description 3
- 239000000796 flavoring agent Substances 0.000 claims description 3
- 235000019634 flavors Nutrition 0.000 claims description 3
- 238000000227 grinding Methods 0.000 claims description 3
- ZQPPMHVWECSIRJ-KTKRTIGZSA-N oleic acid group Chemical group C(CCCCCCC\C=C/CCCCCCCC)(=O)O ZQPPMHVWECSIRJ-KTKRTIGZSA-N 0.000 claims description 3
- 239000004006 olive oil Substances 0.000 claims description 3
- 235000008390 olive oil Nutrition 0.000 claims description 3
- 239000000312 peanut oil Substances 0.000 claims description 3
- 238000002203 pretreatment Methods 0.000 claims description 3
- 239000003549 soybean oil Substances 0.000 claims description 3
- 235000012424 soybean oil Nutrition 0.000 claims description 3
- 235000019484 Rapeseed oil Nutrition 0.000 claims description 2
- 239000003240 coconut oil Substances 0.000 claims description 2
- 235000019864 coconut oil Nutrition 0.000 claims description 2
- 241000196324 Embryophyta Species 0.000 claims 1
- 238000004821 distillation Methods 0.000 claims 1
- 239000003960 organic solvent Substances 0.000 abstract description 10
- 239000000126 substance Substances 0.000 abstract description 6
- 102000004190 Enzymes Human genes 0.000 abstract description 5
- 108090000790 Enzymes Proteins 0.000 abstract description 5
- 239000013043 chemical agent Substances 0.000 abstract description 5
- 238000011109 contamination Methods 0.000 abstract description 5
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 6
- 150000002148 esters Chemical class 0.000 description 3
- 235000014113 dietary fatty acids Nutrition 0.000 description 2
- 229930195729 fatty acid Natural products 0.000 description 2
- 239000000194 fatty acid Substances 0.000 description 2
- 150000004665 fatty acids Chemical class 0.000 description 2
- 239000004615 ingredient Substances 0.000 description 2
- 238000000053 physical method Methods 0.000 description 2
- 239000002904 solvent Substances 0.000 description 2
- 239000001149 (9Z,12Z)-octadeca-9,12-dienoate Substances 0.000 description 1
- WTTJVINHCBCLGX-UHFFFAOYSA-N (9trans,12cis)-methyl linoleate Natural products CCCCCC=CCC=CCCCCCCCC(=O)OC WTTJVINHCBCLGX-UHFFFAOYSA-N 0.000 description 1
- LNJCGNRKWOHFFV-UHFFFAOYSA-N 3-(2-hydroxyethylsulfanyl)propanenitrile Chemical compound OCCSCCC#N LNJCGNRKWOHFFV-UHFFFAOYSA-N 0.000 description 1
- 239000004215 Carbon black (E152) Substances 0.000 description 1
- 244000060011 Cocos nucifera Species 0.000 description 1
- 235000013162 Cocos nucifera Nutrition 0.000 description 1
- PKIXXJPMNDDDOS-UHFFFAOYSA-N Methyl linoleate Natural products CCCCC=CCCC=CCCCCCCCC(=O)OC PKIXXJPMNDDDOS-UHFFFAOYSA-N 0.000 description 1
- 150000001335 aliphatic alkanes Chemical class 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 150000001720 carbohydrates Chemical class 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000004332 deodorization Methods 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 235000019197 fats Nutrition 0.000 description 1
- 229930195733 hydrocarbon Natural products 0.000 description 1
- 150000002430 hydrocarbons Chemical class 0.000 description 1
- 238000009776 industrial production Methods 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 230000004060 metabolic process Effects 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 239000003346 palm kernel oil Substances 0.000 description 1
- 102000004169 proteins and genes Human genes 0.000 description 1
- 108090000623 proteins and genes Proteins 0.000 description 1
- 238000011084 recovery Methods 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 150000003626 triacylglycerols Chemical class 0.000 description 1
- 235000013311 vegetables Nutrition 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C401/00—Irradiation products of cholesterol or its derivatives; Vitamin D derivatives, 9,10-seco cyclopenta[a]phenanthrene or analogues obtained by chemical preparation without irradiation
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D11/00—Solvent extraction
- B01D11/02—Solvent extraction of solids
- B01D11/0288—Applications, solvents
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
Abstract
The present invention relates to oil extraction technical fields, and in particular to the method that a vegetable oil extracts calciferol in mushroom powder includes the following steps, mushroom is dried in STP1；STP2 is milled to the mushroom after drying；STP3 extracts calciferol in the mushroom powder in STP2 with vegetable oil；The method that STP4 uses physical separation, separates the mixture of grease and mushroom powder in STP3, obtains grease.Calciferol content in oil produced by the invention is not handled using chemical agents such as organic solvent or enzymes in entire separation process between 20-20000IU/g, therefore chemical contamination is not present in grease obtained.
Description
Technical field
The present invention relates to oil extraction technical fields, and in particular to a vegetable oil extracts the side of calciferol in mushroom powder
Method.
Background technique
Grease is the general designation of oil & fat.Chemically grease is all that higher fatty acids is formed with glycerol from ingredient
Ester.Grease is the derivative of hydrocarbon.Grease is a kind of special ester.Grease in nature is the mixture of many kinds of substance, master
Wanting ingredient is that a molecule glycerol and three molecule higher fatty acids are dehydrated the ester to be formed, referred to as triglycerides.The major physiological of grease
Function is storage and supply thermal energy, and the energy ratio carbohydrate and protein that can be provided in metabolism about double.One gram of grease exists
When internal complete oxidation, the thermal energy of 39.8 kilojoules about can produce.In the patent document of Patent No. CN201610011291
In, disclose a kind of method for extracting natural VE using two step stripping process comprising following steps：Deodorization is distillated
Extraction phase of the object after ion liquid abstraction carries out two step back extraction；Wherein, the extractant of first step back extraction is organic
Solvent, the dosage of organic solvent are the 10%~100% of extraction phase quality；Second step back extraction extractant be organic solvent and
The mass ratio of water, the organic solvent and the water is (0.1~0.6):(0.3~1.2)；The organic solvent is saturation
Alkane.Extracting method disclosed by the invention, extraction efficiency with higher greatly reduce the dosage of extractant, acquisition
The purity of natural VE is up to 99.2%, while its rate of recovery is 97.5%, methyl linoleate concentration is 0.8%；This
The method for inventing offer is easy to operate, and the equal reproducible utilization of related solvents is conducive to industrial production.
The above-mentioned patent valence of asking solves the extracting process of natural VE, and the equal reproducible utilization of related solvents is conducive to work
Industry production；But for how to provide a kind of separation for carrying out calciferol using physical method, guarantee that calciferol content exists
Between 20-20000IU/g, do not handled using chemical agents such as organic solvent or enzymes in entire separation process, the oil of acquisition
There is no the extracting process of chemical contamination to lack technical solution for rouge.
Summary of the invention
In view of the deficiencies of the prior art, the invention discloses a vegetable oil extraction mushroom powder in calciferol method,
For solving how to provide a kind of separation for carrying out calciferol using physical method, guarantee calciferol content in 20-
Between 20000IU/g, do not handled using chemical agents such as organic solvent or enzymes in entire separation process, the grease of acquisition is not
There are problems that the extracting process of chemical contamination.
The present invention is achieved by the following technical programs：
The method that one vegetable oil extracts calciferol in mushroom powder, it is characterised in that：It the described method comprises the following steps：
Mushroom is dried in STP1；
STP2 is milled to the mushroom after drying；
STP3 extracts calciferol in the mushroom powder in STP2 with vegetable oil；
The method that STP4 uses physical separation, separates the mixture of grease and mushroom powder in STP3, obtains oil
Rouge.
Preferably, the mushroom is agaricus bisporus or oyster mushroom, crab flavour mushroom, Pleurotus eryngii, white beech mushroom, agrocybe, double spores
Mushroom, mushroom, sliding Hericium erinaceus, Pleurotus nebrodensis and coprinus comatus.
Preferably, mushroom is carried out pre-treatment or is not processed before the STP1 directly to carry out next step operation, it is described
Pretreatment mode includes：Slice；Fresh mushroom is ground.
Preferably, there are two types of the drying pretreatment modes of the STP1 mushroom, respectively：
(1) convection drying, so that moisture≤15% in mushroom；
(2) predrying is first carried out, so that in mushroom then moisture is dried again between 30~70%, so that mushroom
Middle moisture is below 15%.
Preferably, the STP1 dry method includes hot-air seasoning and vacuum lyophilization, the hot-air seasoning, work
Skill condition is：30~260 DEG C, 10~300min of time；The vacuum lyophilization process conditions are：Cryogenic temperature -80~0 DEG C,
Vacuum degree is 0.3~2MPa, lyophilization temperature is 10~150 DEG C.
Preferably, the method for the milling includes Universalpulverizer method, Double roll crusher comminuting method and ball mill grinding method.
Preferably, the vegetable oil in the STP3 is sunflower oil, high oleic sunflower oil, olive oil, corn oil, vegetable seed
Oil, soybean oil, peanut oil, coconut oil, tea-seed oil, DHA oil or ARA oil in any one.
Preferably, it is mushroom powder that the extraction, which is added to component ratio range,：Vegetable oil=1:0.1-1：100, extraction temperature
Spending range is 0-300 DEG C, and extraction time range is -100 hours 10 minutes.
Preferably, the separation of the vegetable oil and mushroom powder mixture is realized by the way of filtering, process conditions
For：0.05~6MPa of pressure, 0~180 DEG C of temperature.
Preferably, the grease, which is used as, is used for gel candy, pregnant and lying-in women's food, infant food or person in middle and old age's food production
Purposes.
Beneficial effects of the present invention are：
Calciferol content in oil produced by the invention does not use in entire separation process between 20-20000IU/g
The chemical agents such as organic solvent or enzyme are handled, therefore chemical contamination is not present in grease obtained.
Detailed description of the invention
In order to more clearly explain the embodiment of the invention or the technical proposal in the existing technology, to embodiment or will show below
There is attached drawing needed in technical description to be briefly described, it should be apparent that, the accompanying drawings in the following description is only this
Some embodiments of invention for those of ordinary skill in the art without creative efforts, can be with
It obtains other drawings based on these drawings.
Fig. 1 is the step block diagram of the method for the present invention.
Specific embodiment
In order to make the object, technical scheme and advantages of the embodiment of the invention clearer, below in conjunction with the embodiment of the present invention
In attached drawing, technical scheme in the embodiment of the invention is clearly and completely described, it is clear that described embodiment is
A part of the embodiment of the present invention, instead of all the embodiments.Based on the embodiments of the present invention, those of ordinary skill in the art
Every other embodiment obtained without creative efforts, shall fall within the protection scope of the present invention.
Embodiment 1
Specific implementation step：
Mushroom is dried in STP1；
STP2 is milled to the mushroom after drying；
STP3 extracts calciferol in the mushroom powder in STP2 with vegetable oil；
The method that STP4 uses physical separation, separates the mixture of grease and mushroom powder in STP3, obtains oil
Rouge.
Above-mentioned mushroom is agaricus bisporus.
Pre-treatment is carried out to mushroom before STP1, the pretreatment mode includes：Slice；Fresh mushroom is ground.
The drying pretreatment mode of STP1 mushroom is：
Convection drying, so that moisture≤15% in mushroom；
STP1 dry method includes hot-air seasoning and vacuum lyophilization, the hot-air seasoning, and process conditions are：30
~260 DEG C, 10~300min of time；The vacuum lyophilization process conditions are：Cryogenic temperature -80~0 DEG C, vacuum degree 0.3
~2MPa, lyophilization temperature are 10~150 DEG C.
The method of milling is Universalpulverizer method.
Vegetable oil in STP3 is sunflower oil.
It is mushroom powder that extraction, which is added to component ratio,：Vegetable oil=1:20, extraction temperature is 80 DEG C, extraction time range
It is 50 minutes.
The separation of vegetable oil and mushroom powder mixture is realized by the way of filtering, and process conditions are：Pressure 0.05
~6MPa, 0~180 DEG C of temperature.
Grease is as the purposes for gel candy production.
Embodiment 2
Specific implementation step：
Mushroom is dried in STP1；
STP2 is milled to the mushroom after drying；
STP3 extracts calciferol in the mushroom powder in STP2 with vegetable oil；
The method that STP4 uses physical separation, separates the mixture of grease and mushroom powder in STP3, obtains oil
Rouge.
Mushroom be oyster mushroom, crab flavour mushroom, Pleurotus eryngii, white beech mushroom, agrocybe, agaricus bisporus, mushroom, sliding Hericium erinaceus, Pleurotus nebrodensis and
Any one in coprinus comatus.
It is not processed before STP1 and directly carries out next step operation.
The drying pretreatment mode of STP1 mushroom is：
Predrying is first carried out, so that in mushroom then moisture is dried again between 30~70%, so that water in mushroom
Divide below 15%.
STP1 dry method includes hot-air seasoning and vacuum lyophilization, the hot-air seasoning, and process conditions are：30
~260 DEG C, 10~300min of time；The vacuum lyophilization process conditions are：Cryogenic temperature -80~0 DEG C, vacuum degree 0.3
~2MPa, lyophilization temperature are 10~150 DEG C.
The method of milling is Double roll crusher comminuting method or ball mill grinding method.
Vegetable oil in STP3 is high oleic sunflower oil, olive oil, corn oil, rapeseed oil, soybean oil, peanut oil, coconut palm
Seed oil, tea-seed oil, DHA oil or ARA oil in any one.
It is mushroom powder that extraction, which is added to component ratio range,：Vegetable oil=1:0.1-1：100, extraction temperature range is 0-
300 DEG C, extraction time range is -100 hours 10 minutes.
The separation of vegetable oil and mushroom powder mixture is realized by the way of filtering, and process conditions are：Pressure 0.05
~6MPa, 0~180 DEG C of temperature.
Grease is as the purposes for being used for pregnant and lying-in women's food, infant food or person in middle and old age's food production.
Calciferol content in oil produced by the invention does not use in entire separation process between 20-20000IU/g
The chemical agents such as organic solvent or enzyme are handled, therefore chemical contamination is not present in grease obtained.
The above embodiments are merely illustrative of the technical solutions of the present invention, rather than its limitations；Although with reference to the foregoing embodiments
Invention is explained in detail, those skilled in the art should understand that：It still can be to aforementioned each implementation
Technical solution documented by example is modified or equivalent replacement of some of the technical features；And these modification or
Replacement, the spirit and scope for technical solution of various embodiments of the present invention that it does not separate the essence of the corresponding technical solution.
Claims (10)
1. the method that a vegetable oil extracts calciferol in mushroom powder, it is characterised in that：It the described method comprises the following steps：
Mushroom is dried in STP1；
STP2 is milled to the mushroom after drying；
STP3 extracts calciferol in the mushroom powder in STP2 with vegetable oil；
The method that STP4 uses physical separation, separates the mixture of grease and mushroom powder in STP3, obtains grease.
2. the method for calciferol in vegetable oil extraction mushroom powder according to claim 1, it is characterised in that：The mushroom
It is agaricus bisporus or oyster mushroom, crab flavour mushroom, Pleurotus eryngii, white beech mushroom, agrocybe, agaricus bisporus, mushroom, sliding Hericium erinaceus, Pleurotus nebrodensis
And coprinus comatus.
3. the method for calciferol in vegetable oil extraction mushroom powder according to claim 1, it is characterised in that：The STP1
Mushroom is carried out pre-treatment or is not processed before directly to carry out next step operation, the pretreatment mode includes：Slice；Fresh mushroom
Mushroom grinds.
4. the method for calciferol in vegetable oil extraction mushroom powder according to claim 1, it is characterised in that：The STP1
There are two types of the drying pretreatment modes of mushroom, respectively：
(1) convection drying, so that moisture≤15% in mushroom；
(2) predrying is first carried out, so that in mushroom then moisture is dried again between 30~70%, so that water in mushroom
Divide below 15%.
5. the method for calciferol in vegetable oil extraction mushroom powder according to claim 1, it is characterised in that：The STP1
Dry method includes hot-air seasoning and vacuum lyophilization, the hot-air seasoning, and process conditions are：30~260 DEG C, the time
10~300min；The vacuum lyophilization process conditions are：Cryogenic temperature -80~0 DEG C, vacuum degree are 0.3~2MPa, distillation is dry
Dry temperature is 10~150 DEG C.
6. the method for calciferol in vegetable oil extraction mushroom powder according to claim 1, it is characterised in that：The milling
Method include Universalpulverizer method, Double roll crusher comminuting method and ball mill grinding method.
7. the method for calciferol in vegetable oil extraction mushroom powder according to claim 1, it is characterised in that：The STP3
In vegetable oil be sunflower oil, high oleic sunflower oil, olive oil, corn oil, rapeseed oil, soybean oil, peanut oil, coconut
Oil, tea-seed oil, DHA oil or ARA oil in any one.
8. the method for calciferol in vegetable oil extraction mushroom powder according to claim 1, it is characterised in that：The extraction
Being added to component ratio range is mushroom powder：Vegetable oil=1:0.1-1：100, extraction temperature range is 0-300 DEG C, when extraction
Between range be -100 hours 10 minutes.
9. the method for calciferol in vegetable oil extraction mushroom powder according to claim 1, it is characterised in that：The plant
The separation of oil and mushroom powder mixture is realized by the way of filtering, and process conditions are：0.05~6MPa of pressure, temperature 0
~180 DEG C.
10. the method for calciferol in vegetable oil extraction mushroom powder according to claim 1, it is characterised in that：The oil
Rouge is as gel candy, pregnant and lying-in women's food, infant food or the purposes of person in middle and old age's food production.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810764699.7A CN108840811A (en) | 2018-07-12 | 2018-07-12 | The method that vegetable oil extracts calciferol in mushroom powder |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810764699.7A CN108840811A (en) | 2018-07-12 | 2018-07-12 | The method that vegetable oil extracts calciferol in mushroom powder |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN108840811A true CN108840811A (en) | 2018-11-20 |
Family
ID=64197137
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201810764699.7A Pending CN108840811A (en) | 2018-07-12 | 2018-07-12 | The method that vegetable oil extracts calciferol in mushroom powder |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109527121A (en) * | 2018-12-10 | 2019-03-29 | 瞿瀚鹏 | Mushroom vitamin D2The preparation method and application of oil |
| CN109527122A (en) * | 2018-12-10 | 2019-03-29 | 瞿瀚鹏 | A kind of vitamin D containing mushroom2The food of oil |
| CN109601679A (en) * | 2019-01-10 | 2019-04-12 | 广州富诺健康科技股份有限公司 | A kind of natural calcium D soft sweets and preparation method thereof |
| CN109601678A (en) * | 2019-01-10 | 2019-04-12 | 广州富诺健康科技股份有限公司 | A kind of pure plant type calcium D gel candy and preparation method thereof |
| CN109619214A (en) * | 2019-01-15 | 2019-04-16 | 广州富诺健康科技股份有限公司 | A kind of mushroom oil droplet agent and preparation method thereof rich in vegetalitas VD2 |
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| CN109601679A (en) * | 2019-01-10 | 2019-04-12 | 广州富诺健康科技股份有限公司 | A kind of natural calcium D soft sweets and preparation method thereof |
| CN109601678A (en) * | 2019-01-10 | 2019-04-12 | 广州富诺健康科技股份有限公司 | A kind of pure plant type calcium D gel candy and preparation method thereof |
| CN109619214A (en) * | 2019-01-15 | 2019-04-16 | 广州富诺健康科技股份有限公司 | A kind of mushroom oil droplet agent and preparation method thereof rich in vegetalitas VD2 |
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