CN108839163A - A kind of mildew and insect proof processing method of wicker plaiting article raw material - Google Patents
A kind of mildew and insect proof processing method of wicker plaiting article raw material Download PDFInfo
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- CN108839163A CN108839163A CN201810559517.2A CN201810559517A CN108839163A CN 108839163 A CN108839163 A CN 108839163A CN 201810559517 A CN201810559517 A CN 201810559517A CN 108839163 A CN108839163 A CN 108839163A
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B27—WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
- B27K—PROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
- B27K3/00—Impregnating wood, e.g. impregnation pretreatment, for example puncturing; Wood impregnation aids not directly involved in the impregnation process
- B27K3/02—Processes; Apparatus
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B27—WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
- B27K—PROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
- B27K3/00—Impregnating wood, e.g. impregnation pretreatment, for example puncturing; Wood impregnation aids not directly involved in the impregnation process
- B27K3/16—Inorganic impregnating agents
- B27K3/20—Compounds of alkali metals or ammonium
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B27—WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
- B27K—PROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
- B27K3/00—Impregnating wood, e.g. impregnation pretreatment, for example puncturing; Wood impregnation aids not directly involved in the impregnation process
- B27K3/34—Organic impregnating agents
- B27K3/50—Mixtures of different organic impregnating agents
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B27—WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
- B27K—PROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
- B27K5/00—Treating of wood not provided for in groups B27K1/00, B27K3/00
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B27—WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
- B27K—PROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
- B27K5/00—Treating of wood not provided for in groups B27K1/00, B27K3/00
- B27K5/003—Treating of wood not provided for in groups B27K1/00, B27K3/00 by using electromagnetic radiation or mechanical waves
- B27K5/0065—Ultrasonic treatment
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B27—WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
- B27K—PROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
- B27K5/00—Treating of wood not provided for in groups B27K1/00, B27K3/00
- B27K5/04—Combined bleaching or impregnating and drying of wood
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B27—WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
- B27K—PROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
- B27K9/00—Chemical or physical treatment of reed, straw, or similar material
- B27K9/002—Cane, bamboo
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B27—WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
- B27K—PROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
- B27K2240/00—Purpose of the treatment
- B27K2240/20—Removing fungi, molds or insects
Abstract
The invention discloses a kind of mildew and insect proof processing methods of wicker plaiting article raw material, include the following steps：（1）Raw material cleaning treatment,（2）Steam explosion treatment,（3）Immersion treatment,（4）Secondary immersion treatment,（5）It is dried.Processing method processing step of the present invention is simple, easy to promote and utilize, and treated, and wicker plaiting article raw material has very strong, very stable mildew and insect proof ability, and has the characteristics that green, nontoxic, environmentally friendly, great application value.
Description
Technical field
The invention belongs to wicker plaiting article working process technical fields, and in particular to a kind of mildew and insect proof processing side of wicker plaiting article raw material
Method.
Background technique
Funan County is under the jurisdiction of Anhui Province's Fuyang City, belongs to inland exploitation area earlier, on the Anhui Province northwestward, Huaihe River
Middle reaches engaging portion north bank.Funan County is known as the title in " famous-brand and high-quality specialty county ", " Natural resources reservoir ", be national grain-production great Xian, in
The unique agricultural in township, the whole nation of state's wicker plaiting article（Forestry）Circular economy demonstration pilot project county, Funan are the township of national wicker plaiting article, wicker products
It is sold abroad.
The raw material of wicker products can be wicker, timber, bamboo wood etc., and product may include：Wicker plaiting article case（Packet）, meal basket, food basket
（Circle, ellipse）, bamboo strainer, needlework shallow basket made of wicker or thin bamboo strips, kang mat, reed matting etc..The reason of because of wicker plaiting article raw material self-characteristic, cause it in atmospheric environment
When middle use easily by moisture and entomogenous fungi etc. corrode, eventually lead to its it is mouldy rot, not only affect appearance condition, while also dropping
Its low mechanics etc. uses characteristic.For characteristics such as the mildew and insect proofs that improves wicker products, someone is carried out using chemical antibacterial agent
Spraying, although good effect can be played, how irritant ingredient is, toxic, unfavorable to the health of human body, needs one kind more
The processing method of environmental protection.
Summary of the invention
The purpose of the present invention is being directed to existing problem, a kind of mildew and insect proof processing method of wicker plaiting article raw material is provided.
The present invention is achieved by the following technical solutions：
A kind of mildew and insect proof processing method of wicker plaiting article raw material, includes the following steps：
（1）Raw material cleaning treatment：
Wicker plaiting article raw material is put into 20 ~ 25min of immersion treatment in sodium hydroxide solution, taking-up is rinsed with clear water to neutrality after the completion
It is spare afterwards；
（2）Steam explosion treatment：
By step（1）Wicker plaiting article raw material, which is put into steam blasting tank, after processing carries out Steam explosion treatment, takes out after the completion spare；
（3）Immersion treatment：
A. by chitosan, silane coupling agent, dodecyl trimethyl ammonium chloride, odium stearate, ethylenediamine tetraacetic acetyl disodium, go from
Sub- water is corresponding according to weight ratio 7 ~ 10:14~16：18~20:3~6:0.5~1：100 ~ 110, which carry out mixing, puts into reaction kettle, adds
It is 77 ~ 82 DEG C that heat, which keeps the temperature in reaction kettle, and it is spare to obtain a soak after 4 ~ 5h of high-speed stirred processing；By chitosan and ten
It while dialkyl group trimethyl ammonium chloride is reacted, and is added to silane coupling agent ingredient and is mixed, be finally made one
The silane-modified chitosan quaternary ammonium salt composite parts of kind, its absorption is incorporated into wicker plaiting article under the action ofs ethylenediamine tetraacetic acetyl disodium etc.
On raw fibre surface, its fiber surface activity is improved, improves the change to effective component of chinese medicine in subsequent secondary soak
It learns absorption and absorbs fixed amount, improve the effect of pest-resistant bacterium, the chemically fixed energy power of more untreated wicker plaiting article raw material improves
35% or more, enhance the effect of subsequent processing；
B. by step（2）Treated, and wicker plaiting article raw material is immersed in the operation resulting soak of a, and heating keeps primary and impregnates
The temperature of liquid is 45 ~ 50 DEG C, is taken out after 2 ~ 3h of immersion treatment spare；
（4）Secondary immersion treatment：
A. chinaberry, dried peppermint leaf, Radix Isatidis, rhizoma menispermi, radix scutellariae, the Chinese bulbul, oldenlandia diffusa is corresponding according to following weight ratio 9
~12:5~7:4~6:2~5:3~6:1~3:5 ~ 8, which carry out mixing, puts into pot, and the clear of 5 ~ 7 times of its gross mass is then added into pot
Water, heating boiling are filtered after boiling 1 ~ 2h of processing, then resulting filtrate is concentrated into behind the 1/8 ~ 1/6 of original volume secondary soak is standby
With；
B. by step（3）Treated, and wicker plaiting article raw material immerses in the operation resulting secondary soak of a, after being ultrasonically treated 35 ~ 40min
It takes out spare；
（5）It is dried：
By step（4）Treated, and wicker plaiting article raw material is put into progress vacuum drying treatment in vacuum oven, and taking-up after the completion is
It can.
Further, step（1）Described in sodium hydroxide solution mass fraction be 4 ~ 6%.
Further, step（2）Described in Steam explosion treatment when concrete operations be：It is passed through into steam blasting tank
The vapor that temperature is 105 ~ 110 DEG C, while the pressure in steam blasting tank is increased into 0.45 ~ 0.50MPa, heat-insulation pressure keeping processing
After 10 ~ 12min, it will be unloaded in steam blasting tank to normal temperature and pressure in 1min.
Further, step（3）Operating silane coupling agent described in a is silane coupling agent kh550, silane coupling agent
Any one in kh560, silane coupling agent kh570.
Further, step（3）Speed of agitator when operating the processing of high-speed stirred described in a is 2000 ~ 2300 revs/min
Clock, it is 0.2 ~ 0.25MPa that during which pressurization, which keeps the pressure in reaction kettle,.
Further, step（4）Ultrasonic frequency when operating ultrasonic treatment described in b is 340 ~ 380kHz.
Further, step（5）Described in vacuum drying treatment when control vacuum oven in temperature be 75 ~ 80
℃。
The present invention provides a kind of special treatment method of wicker plaiting article raw material, its mildew and insect proof characteristic is effectively improved,
It is middle that cleaning treatment first has been carried out to it, surface impurity ingredient is eliminated, then carries out Steam explosion treatment, loose wicker plaiting article raw material
Wood fibre structure, expand fibre gap, improve whole adsorption reaction ability, then carried out at primary immersion
Reason, impregnates wicker plaiting article raw material with a special soak, improves the surface-active of wicker plaiting article raw fibre, improve it
To the chemisorption binding ability of subsequent effective component of chinese medicine, the mildew and insect proof characteristic of itself is enhanced, has carried out two again later
Secondary immersion treatment has been obtained through refining into secondary soak with the traditional Chinese medicine ingredients water of several special collocation, with very strong mildew and insect proof
Performance, and to human body, environmentally friendly.
The present invention has the following advantages that compared with prior art：
Processing method processing step of the present invention is simple, easy to promote and utilize, and treated wicker plaiting article raw material has very strong, very stable
Mildew and insect proof ability, and have the characteristics that green, nontoxic, environmentally friendly, great application value.
Specific embodiment
Embodiment 1
A kind of mildew and insect proof processing method of wicker plaiting article raw material, includes the following steps：
（1）Raw material cleaning treatment：
Wicker plaiting article raw material is put into immersion treatment 20min in sodium hydroxide solution, taking-up is rinsed with clear water to neutrality after the completion
It is spare；
（2）Steam explosion treatment：
By step（1）Wicker plaiting article raw material, which is put into steam blasting tank, after processing carries out Steam explosion treatment, takes out after the completion spare；
（3）Immersion treatment：
A. by chitosan, silane coupling agent, dodecyl trimethyl ammonium chloride, odium stearate, ethylenediamine tetraacetic acetyl disodium, go from
Sub- water is corresponding according to weight ratio 7:14：18:3:0.5：100, which carry out mixing, puts into reaction kettle, and heating is kept in reaction kettle
Temperature is 77 DEG C, and it is spare to obtain a soak after high-speed stirred processing 4h；
B. by step（2）Treated, and wicker plaiting article raw material is immersed in the operation resulting soak of a, and heating keeps primary and impregnates
The temperature of liquid is 45 DEG C, is taken out after immersion treatment 2h spare；
（4）Secondary immersion treatment：
A. chinaberry, dried peppermint leaf, Radix Isatidis, rhizoma menispermi, radix scutellariae, the Chinese bulbul, oldenlandia diffusa is corresponding according to following weight ratio
9:5:4:2:3:1:5, which carry out mixing, puts into pot, and the clear water of 5 times of its gross mass is then added into pot, and processing is boiled in heating boiling
Filtered after 1h, then resulting filtrate is concentrated into behind the 1/8 of original volume secondary soak is spare；
B. by step（3）Treated, and wicker plaiting article raw material immerses in the operation resulting secondary soak of a, takes after being ultrasonically treated 35min
It is spare out；
（5）It is dried：
By step（4）Treated, and wicker plaiting article raw material is put into progress vacuum drying treatment in vacuum oven, and taking-up after the completion is
It can.
Further, step（1）Described in sodium hydroxide solution mass fraction be 4%.
Further, step（2）Described in Steam explosion treatment when concrete operations be：It is passed through into steam blasting tank
The vapor that temperature is 105 DEG C, while the pressure in steam blasting tank is increased into 0.45MPa, after heat-insulation pressure keeping handles 10min,
It will be unloaded in steam blasting tank to normal temperature and pressure in 1min.
Further, step（3）Operating silane coupling agent described in a is silane coupling agent kh550.
Further, step（3）Speed of agitator when operating the processing of high-speed stirred described in a is 2000 revs/min, the phase
Between pressurization keep reaction kettle in pressure be 0.2MPa.
Further, step（4）Ultrasonic frequency when operating ultrasonic treatment described in b is 340kHz.
Further, step（5）Described in vacuum drying treatment when control vacuum oven in temperature be 75 DEG C.
Embodiment 2
A kind of mildew and insect proof processing method of wicker plaiting article raw material, includes the following steps：
（1）Raw material cleaning treatment：
Wicker plaiting article raw material is put into immersion treatment 23min in sodium hydroxide solution, taking-up is rinsed with clear water to neutrality after the completion
It is spare；
（2）Steam explosion treatment：
By step（1）Wicker plaiting article raw material, which is put into steam blasting tank, after processing carries out Steam explosion treatment, takes out after the completion spare；
（3）Immersion treatment：
A. by chitosan, silane coupling agent, dodecyl trimethyl ammonium chloride, odium stearate, ethylenediamine tetraacetic acetyl disodium, go from
Sub- water is corresponding according to weight ratio 9:15：19:5:0.8：105, which carry out mixing, puts into reaction kettle, and heating is kept in reaction kettle
Temperature is 80 DEG C, and it is spare to obtain a soak after high-speed stirred processing 4.5h；
B. by step（2）Treated, and wicker plaiting article raw material is immersed in the operation resulting soak of a, and heating keeps primary and impregnates
The temperature of liquid is 47 DEG C, is taken out after immersion treatment 2.6h spare；
（4）Secondary immersion treatment：
A. chinaberry, dried peppermint leaf, Radix Isatidis, rhizoma menispermi, radix scutellariae, the Chinese bulbul, oldenlandia diffusa is corresponding according to following weight ratio
11:6:5:4:5:2:7, which carry out mixing, puts into pot, and the clear water of 6 times of its gross mass is then added into pot, and processing is boiled in heating boiling
Filtered after 1.5h, then resulting filtrate is concentrated into behind the 1/7 of original volume secondary soak is spare；
B. by step（3）Treated, and wicker plaiting article raw material immerses in the operation resulting secondary soak of a, takes after being ultrasonically treated 38min
It is spare out；
（5）It is dried：
By step（4）Treated, and wicker plaiting article raw material is put into progress vacuum drying treatment in vacuum oven, and taking-up after the completion is
It can.
Further, step（1）Described in sodium hydroxide solution mass fraction be 5%.
Further, step（2）Described in Steam explosion treatment when concrete operations be：It is passed through into steam blasting tank
The vapor that temperature is 108 DEG C, while the pressure in steam blasting tank is increased into 0.47MPa, after heat-insulation pressure keeping handles 11min,
It will be unloaded in steam blasting tank to normal temperature and pressure in 1min.
Further, step（3）Operating silane coupling agent described in a is silane coupling agent kh560.
Further, step（3）Speed of agitator when operating the processing of high-speed stirred described in a is 2200 revs/min, the phase
Between pressurization keep reaction kettle in pressure be 0.23MPa.
Further, step（4）Ultrasonic frequency when operating ultrasonic treatment described in b is 360kHz.
Further, step（5）Described in vacuum drying treatment when control vacuum oven in temperature be 77 DEG C.
Embodiment 3
A kind of mildew and insect proof processing method of wicker plaiting article raw material, includes the following steps：
（1）Raw material cleaning treatment：
Wicker plaiting article raw material is put into immersion treatment 25min in sodium hydroxide solution, taking-up is rinsed with clear water to neutrality after the completion
It is spare；
（2）Steam explosion treatment：
By step（1）Wicker plaiting article raw material, which is put into steam blasting tank, after processing carries out Steam explosion treatment, takes out after the completion spare；
（3）Immersion treatment：
A. by chitosan, silane coupling agent, dodecyl trimethyl ammonium chloride, odium stearate, ethylenediamine tetraacetic acetyl disodium, go from
Sub- water is corresponding according to weight ratio 10:16：20:6:1：110, which carry out mixing, puts into reaction kettle, and heating keeps the temperature in reaction kettle
Degree is 82 DEG C, and it is spare to obtain a soak after high-speed stirred processing 5h；
B. by step（2）Treated, and wicker plaiting article raw material is immersed in the operation resulting soak of a, and heating keeps primary and impregnates
The temperature of liquid is 50 DEG C, is taken out after immersion treatment 3h spare；
（4）Secondary immersion treatment：
A. chinaberry, dried peppermint leaf, Radix Isatidis, rhizoma menispermi, radix scutellariae, the Chinese bulbul, oldenlandia diffusa is corresponding according to following weight ratio
12:7:6:5:6:3:8, which carry out mixing, puts into pot, and the clear water of 7 times of its gross mass is then added into pot, and processing is boiled in heating boiling
Filtered after 2h, then resulting filtrate is concentrated into behind the 1/6 of original volume secondary soak is spare；
B. by step（3）Treated, and wicker plaiting article raw material immerses in the operation resulting secondary soak of a, takes after being ultrasonically treated 40min
It is spare out；
（5）It is dried：
By step（4）Treated, and wicker plaiting article raw material is put into progress vacuum drying treatment in vacuum oven, and taking-up after the completion is
It can.
Further, step（1）Described in sodium hydroxide solution mass fraction be 6%.
Further, step（2）Described in Steam explosion treatment when concrete operations be：It is passed through into steam blasting tank
The vapor that temperature is 110 DEG C, while the pressure in steam blasting tank is increased into 0.50MPa, after heat-insulation pressure keeping handles 12min,
It will be unloaded in steam blasting tank to normal temperature and pressure in 1min.
Further, step（3）Operating silane coupling agent described in a is silane coupling agent kh570.
Further, step（3）Speed of agitator when operating the processing of high-speed stirred described in a is 2300 revs/min, the phase
Between pressurization keep reaction kettle in pressure be 0.25MPa.
Further, step（4）Ultrasonic frequency when operating ultrasonic treatment described in b is 380kHz.
Further, step（5）Described in vacuum drying treatment when control vacuum oven in temperature be 80 DEG C.
Comparative example 1
This comparative example 1 compared with Example 2, eliminates step（3）Constituent of chitosan in immersion treatment operation a,
Method and step in addition to this is all the same.
Comparative example 2
This comparative example 2 compared with Example 2, eliminates step（3）The whole operation of immersion treatment, side in addition to this
Method step is all the same.
In order to compare effect of the present invention, selects with the purple willow of a batch harvesting as wicker plaiting article raw material, be used as experimental subjects, respectively
It is handled with above-described embodiment 2, comparative example 1, the corresponding method of comparative example 2, to each group, treated after the completion
Purple willow raw material carries out antibacterial experiment, and specific correlation data is as shown in table 1 below：
Table 1
| Mould proof duration（It） | |
| Embodiment 2 | 147 |
| Comparative example 1 | 86 |
| Comparative example 2 | 58 |
Note：Corresponding antibacterial experiment is specifically in upper table 1：By each group, treated that purple willow raw material is respectively put into chamber, control
Temperature in chamber processed is 30 DEG C, and normal pressure, relative humidity 95% is inoculated with Trichoderma viride, aspergillus niger, soil in chamber
Total duration experienced when aspergillus, green ochre mould and white rake teeth bacterium, statistics by mycotic infection area are 8%, with mould proof duration table
Show, to characterize anti-mold effect.
The characteristics such as mould proof of the present invention treated wicker plaiting article raw material significantly enhance it can be seen from upper table 1, are obviously improved
The using effect and service life, the great market competitiveness and application value of wicker products.
Claims (7)
1. a kind of mildew and insect proof processing method of wicker plaiting article raw material, which is characterized in that include the following steps：
（1）Raw material cleaning treatment：
Wicker plaiting article raw material is put into 20 ~ 25min of immersion treatment in sodium hydroxide solution, taking-up is rinsed with clear water to neutrality after the completion
It is spare afterwards；
（2）Steam explosion treatment：
By step（1）Wicker plaiting article raw material, which is put into steam blasting tank, after processing carries out Steam explosion treatment, takes out after the completion spare；
（3）Immersion treatment：
A. by chitosan, silane coupling agent, dodecyl trimethyl ammonium chloride, odium stearate, ethylenediamine tetraacetic acetyl disodium, go from
Sub- water is corresponding according to weight ratio 7 ~ 10:14~16：18~20:3~6:0.5~1：100 ~ 110, which carry out mixing, puts into reaction kettle, adds
It is 77 ~ 82 DEG C that heat, which keeps the temperature in reaction kettle, and it is spare to obtain a soak after 4 ~ 5h of high-speed stirred processing；
B. by step（2）Treated, and wicker plaiting article raw material is immersed in the operation resulting soak of a, and heating keeps primary and impregnates
The temperature of liquid is 45 ~ 50 DEG C, is taken out after 2 ~ 3h of immersion treatment spare；
（4）Secondary immersion treatment：
A. chinaberry, dried peppermint leaf, Radix Isatidis, rhizoma menispermi, radix scutellariae, the Chinese bulbul, oldenlandia diffusa is corresponding according to following weight ratio 9
~12:5~7:4~6:2~5:3~6:1~3:5 ~ 8, which carry out mixing, puts into pot, and the clear of 5 ~ 7 times of its gross mass is then added into pot
Water, heating boiling are filtered after boiling 1 ~ 2h of processing, then resulting filtrate is concentrated into behind the 1/8 ~ 1/6 of original volume secondary soak is standby
With；
B. by step（3）Treated, and wicker plaiting article raw material immerses in the operation resulting secondary soak of a, after being ultrasonically treated 35 ~ 40min
It takes out spare；
（5）It is dried：
By step（4）Treated, and wicker plaiting article raw material is put into progress vacuum drying treatment in vacuum oven, and taking-up after the completion is
It can.
2. a kind of mildew and insect proof processing method of wicker plaiting article raw material according to claim 1, which is characterized in that step（1）In
The mass fraction of the sodium hydroxide solution is 4 ~ 6%.
3. a kind of mildew and insect proof processing method of wicker plaiting article raw material according to claim 1, which is characterized in that step（2）In
Concrete operations when the described Steam explosion treatment are：The vapor that temperature is 105 ~ 110 DEG C is passed through into steam blasting tank, together
When the pressure in steam blasting tank increased into 0.45 ~ 0.50MPa, after heat-insulation pressure keeping handles 10 ~ 12min, will be steamed in 1min
It is unloaded in vapour cavity charge containers to normal temperature and pressure.
4. a kind of mildew and insect proof processing method of wicker plaiting article raw material according to claim 1, which is characterized in that step（3）Behaviour
Make silane coupling agent described in a as appointing in silane coupling agent kh550, silane coupling agent kh560, silane coupling agent kh570
It anticipates one kind.
5. a kind of mildew and insect proof processing method of wicker plaiting article raw material according to claim 1, which is characterized in that step（3）Behaviour
Speed of agitator when making the processing of high-speed stirred described in a is 2000 ~ 2300 revs/min, and during which pressurization is kept in reaction kettle
Pressure is 0.2 ~ 0.25MPa.
6. a kind of mildew and insect proof processing method of wicker plaiting article raw material according to claim 1, which is characterized in that step（4）Behaviour
Ultrasonic frequency when making ultrasonic treatment described in b is 340 ~ 380kHz.
7. a kind of mildew and insect proof processing method of wicker plaiting article raw material according to claim 1, which is characterized in that step（5）In
Temperature when the described vacuum drying treatment in control vacuum oven is 75 ~ 80 DEG C.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810559517.2A CN108839163A (en) | 2018-06-02 | 2018-06-02 | A kind of mildew and insect proof processing method of wicker plaiting article raw material |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810559517.2A CN108839163A (en) | 2018-06-02 | 2018-06-02 | A kind of mildew and insect proof processing method of wicker plaiting article raw material |
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| Publication Number | Publication Date |
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| CN108839163A true CN108839163A (en) | 2018-11-20 |
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| CN201810559517.2A Pending CN108839163A (en) | 2018-06-02 | 2018-06-02 | A kind of mildew and insect proof processing method of wicker plaiting article raw material |
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| CN111791327A (en) * | 2020-06-22 | 2020-10-20 | 安徽省家好家节能门窗有限公司 | Timber renewing and corrosion preventing process for ancient building moving |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN106182265A (en) * | 2016-08-27 | 2016-12-07 | 阜南县永兴工艺品有限公司 | A kind of mildew-proof treatment method of straw plaited |
| CN107457853A (en) * | 2017-09-12 | 2017-12-12 | 阜南县永兴工艺品有限公司 | A kind of processing technology for lifting wicker characteristic |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN106182265A (en) * | 2016-08-27 | 2016-12-07 | 阜南县永兴工艺品有限公司 | A kind of mildew-proof treatment method of straw plaited |
| CN107457853A (en) * | 2017-09-12 | 2017-12-12 | 阜南县永兴工艺品有限公司 | A kind of processing technology for lifting wicker characteristic |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111791327A (en) * | 2020-06-22 | 2020-10-20 | 安徽省家好家节能门窗有限公司 | Timber renewing and corrosion preventing process for ancient building moving |
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