CN108836906B - Powdery scalp environment conditioner and fermentation method and application thereof - Google Patents

Powdery scalp environment conditioner and fermentation method and application thereof Download PDF

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CN108836906B
CN108836906B CN201810771608.2A CN201810771608A CN108836906B CN 108836906 B CN108836906 B CN 108836906B CN 201810771608 A CN201810771608 A CN 201810771608A CN 108836906 B CN108836906 B CN 108836906B
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CN108836906A (en
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刘聚磊
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Beijing Danhang Biotechnology Development Co ltd
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9789Magnoliopsida [dicotyledons]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/02Cosmetics or similar toiletry preparations characterised by special physical form
    • A61K8/0216Solid or semisolid forms
    • A61K8/022Powders; Compacted Powders
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9794Liliopsida [monocotyledons]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/80Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
    • A61K2800/85Products or compounds obtained by fermentation, e.g. yoghurt, beer, wine

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Abstract

The invention relates to a powdery scalp environment conditioner and a fermentation method and application thereof. The raw material components of the conditioner comprise: 300 parts of white paeony root, 150 parts of Chinese date, 150 parts of cassia twig, 100 parts of honey-fried licorice root, 150 parts of ginger, 50 parts of mint, 50 parts of lightyellow sophora root, 50 parts of belvedere fruit, 50 parts of grassleaf sweelflag rhizome, 50 parts of amur corktree bark, 50 parts of mulberry leaf, 130 parts of yeast and 130 parts of white sugar. The scalp environment conditioner is prepared from dozens of herbaceous plants, is pure natural and free of additives, integrates various nutrients required by hair growth, does not hurt hair and scalp, does not generate any side effect on a human body, has a natural maintenance effect, and can effectively regulate the scalp ecological environment. In addition, the conditioner is in a powder state, does not contain water, essence, pigment, thickening agent, preservative and the like, completely uses natural plants to replace chemical components, and has obvious effect.

Description

Powdery scalp environment conditioner and fermentation method and application thereof
Technical Field
The invention relates to the technical field of washing and caring products, in particular to a powdery scalp environment conditioner and a fermentation method and application thereof.
Background
As a fine chemical product, the traditional commercially available shampoo is a hair care product with the functions of removing dandruff, treating oil, dyeing hair and the like. At present, all shampoo manufacturers focus on the problems of making hair more smooth, smooth and healthy and the like in the global scope, and the root causes of the problems are not traced.
The following manufacturers are concerned with solving the appearance problem, such as: how do the hair dry? How do hair perm damaged? How do the hair get damaged? How to make the fragrance of the product more like a bit, the softness of the hair washing is soft and smooth, the packaging is more graded, and the design is beautiful. Only then, only few manufacturers or enterprises have to trace deeply, which results in imbalance of scalp ecological environment and high alopecia rate in the present society. According to incomplete statistics: china currently has two hundred million people with severe alopecia and baldness, and the rate of alopecia and baldness are continuously rising and have become rapidly younger.
It is well known that a healthy scalp ecosystem is maintained by three major balances: oil, flora and metabolic balance. When the secretion of oil and fat of scalp is unbalanced, the oil of scalp is greasy; when the scalp flora is unbalanced in environment and a large amount of harmful bacteria are bred, the phenomenon of itching can occur; the stratum corneum of the scalp is metabolized too quickly and falls off to form dandruff. Scalp problems caused by imbalance of ecological environment of scalp include oily hair, itching hair, dandruff, dry hair, alopecia, etc. The most easily caused problems are dandruff, oily hair and alopecia.
Based on this, it is important to provide a novel, natural, safe and non-toxic product for scalp care that can effectively regulate the ecological environment of the scalp.
Disclosure of Invention
Aiming at the defects in the prior art, the invention aims to provide a powdery scalp environment conditioner and a fermentation method and application thereof. The powdery scalp environment conditioner provided by the invention is prepared from dozens of herbaceous plants, is pure natural and free of additives, integrates various nutrients required by hair growth, does not damage hair and scalp, does not generate any side effect on human health, has a natural maintenance effect, and can effectively adjust the scalp ecological environment. In addition, the conditioner is in a powder state, does not contain water, essence, pigment, thickening agent, preservative and the like, completely uses natural plants to replace chemical components, and has obvious effect.
Therefore, the invention provides the following technical scheme:
in a first aspect, the invention provides a conditioner, which comprises the following raw material components in parts by weight: 200-400 parts of white peony root, 100-200 parts of Chinese date, 100-200 parts of cassia twig, 50-150 parts of honey-fried licorice root, 100-200 parts of ginger, 30-60 parts of mint, 30-60 parts of radix sophorae flavescentis and 30-60 parts of amur corktree.
Preferably, the raw material components of the conditioner further comprise: 40-60 parts of fructus kochiae, 30-60 parts of rhizoma acori graminei and 30-60 parts of folium mori.
Preferably, the raw material components of the conditioner further comprise: 120-140 parts of yeast and 120-140 parts of white sugar. The inventors should select relevant commercially available yeast products according to actual needs.
Preferably, the conditioner is prepared from the following raw material components: 300 parts of white paeony root, 150 parts of Chinese date, 150 parts of cassia twig, 100 parts of honey-fried licorice root, 150 parts of ginger, 50 parts of mint, 50 parts of lightyellow sophora root, 50 parts of belvedere fruit, 50 parts of grassleaf sweelflag rhizome, 50 parts of amur corktree bark, 50 parts of mulberry leaf, 130 parts of yeast and 130 parts of white sugar.
Preferably, the conditioning agent is in a powder form.
The raw material components for preparing the powdery scalp environment conditioner are taken as the mixture ratio according to the parts by mass, and can be increased or reduced according to the corresponding ratio during production, for example, the mass production can be in kilogram or ton units, the small-scale production can also be in gram units, the weight can be increased or reduced, but the mass mixture ratio of the raw material components among the components is not changed.
In a second aspect, the present invention provides a process for preparing a conditioner, comprising the steps of: s1: weighing the raw material components in proportion, removing impurities, and then drying; crushing the dried raw material components; s2: mixing the crushed raw material components with water and then steaming for a preset time; s3: mixing the product obtained in S2 with warm water, adding yeast and white sugar, and fermenting in a sealed container; s4: and filtering the fermented product, collecting filter residues, drying and crushing the filter residues into powder to obtain the conditioner.
Preferably, in S2: the ratio of the amount of the crushed raw material components to the amount of water is 1: (0.2 to 0.8), preferably 1: 0.5, and the preset time is 20-40 min, preferably 30 min.
Preferably, in S3: before adding the yeast and the white sugar, the method preferably further comprises the following steps: taking a proper amount of warm water, adding yeast and white sugar, and uniformly mixing; the fermentation temperature is 20-25 ℃, and the fermentation time is 5-7 d. It should be noted that, the amount of warm water used in the dissolving process can be determined by those skilled in the art according to actual conditions, and the amount of warm water is preferably equal to the amount of the pulverized raw material components.
Preferably, the product obtained in S2 is mixed with warm water in a ratio of 1: (1-3) mixing in a mass ratio; the temperature of the warm water is 40-50 ℃, and preferably 45 ℃.
In a third aspect, the invention provides the use of a conditioner in the manufacture of a personal care product and in particular a product and/or product additive for the care of the scalp environment.
Compared with the prior art, the technical scheme of the invention has the following advantages:
(1) the applicant has found through a great deal of research that: the powdery scalp environment conditioner provided by the invention is prepared from dozens of herbaceous plants, is pure natural and free of additives, integrates various nutrients required by hair growth, does not damage hair and scalp, does not generate any side effect on human health, has a natural maintenance effect, and can effectively adjust the scalp ecological environment.
(2) The hair conditioner provided by the invention is in a powder state, does not contain water, essence, pigment, thickening agent, preservative and the like, completely uses natural plants to replace chemical components, and has an obvious effect. In addition, the hair conditioner disclosed by the invention is low in raw material component cost, simple and convenient to operate in a preparation method, excellent in using effect and very beneficial to industrial mass production.
Additional aspects and advantages of the invention will be set forth in part in the description which follows and, in part, will be obvious from the description, or may be learned by practice of the invention.
Detailed Description
Hereinafter, embodiments of the present invention will be described in detail. The following examples are only for illustrating the technical solutions of the present invention more clearly, and therefore are only examples, and the protection scope of the present invention is not limited thereby.
The experimental procedures in the following examples are conventional unless otherwise specified. The test materials used in the following examples were purchased from a conventional reagent store unless otherwise specified. In the quantitative tests in the following examples, three replicates were set, and the data are the mean or the mean ± standard deviation of the three replicates.
The invention provides a powdery conditioner which comprises the following raw material components in parts by weight: 200-400 parts of white peony root, 100-200 parts of Chinese date, 100-200 parts of cassia twig, 50-150 parts of honey-fried licorice root, 100-200 parts of ginger, 30-60 parts of mint, 30-60 parts of radix sophorae flavescentis and 30-60 parts of amur corktree. The raw material components preferably further comprise: 40-60 parts of fructus kochiae, 30-60 parts of rhizoma acori graminei and 30-60 parts of folium mori; more preferably, the method further comprises: 120-140 parts of yeast and 120-140 parts of white sugar.
In addition, the applicant has specifically designed a preparation method for the powdery scalp environment conditioner of the present invention, which comprises the steps of:
s1: weighing the raw material components in proportion, removing impurities, and then drying; pulverizing the dried raw material components.
S2: mixing the crushed raw material components with water according to the ratio of 1: (0.2 to 0.8), and preferably 1: 0.5 mixing, and then steaming for 20-40 min by using steam.
S3: mixing the product obtained in S2 with warm water according to the weight ratio of 1: (1-3), adding yeast and white sugar, and fermenting in a closed container. Wherein the fermentation temperature is 20-25 ℃ and the fermentation time is 5-7 days.
S4: and filtering the fermented product, collecting filter residues, drying and crushing the filter residues into powder to obtain the conditioner.
In a further embodiment of the present invention, before adding yeast and white sugar, it is preferable to further comprise the steps of: taking a proper amount of warm water, adding yeast and white sugar, and uniformly mixing.
The following description is made with reference to specific embodiments:
example one
The embodiment provides a powdery scalp environment conditioner which is prepared from the following raw material components: 300 parts of white peony root, 150 parts of Chinese date, 150 parts of cassia twig, 100 parts of honey-fried licorice root, 150 parts of ginger, 50 parts of mint, 50 parts of radix sophorae flavescentis, 50 parts of amur corktree, 130 parts of yeast and 130 parts of white sugar.
The powdery scalp environment conditioner is prepared by adopting the components as follows:
s1: weighing the raw material components in proportion, removing impurities, drying, and crushing into coarse powder.
S2: mixing the coarse powder with water according to the weight ratio of 1: 0.5 mass ratio, followed by steaming for 30min with steam.
S3: mixing the steamed coarse powder with 45 deg.C warm water according to a ratio of 1: 2, adding a yeast and white sugar mixed solution (obtained by dissolving yeast and white sugar in 45 ℃ warm water), and fermenting in a closed container; placing the container in a space with constant temperature of 25 deg.C, and fermenting for 5 d.
S4: and filtering the fermented product to obtain liquid, collecting filter residues, drying and crushing the filter residues into powder to obtain the conditioner.
Example two
The embodiment provides a powdery scalp environment conditioner which is prepared from the following raw material components: 400 parts of white peony root, 100 parts of Chinese date, 200 parts of cassia twig, 50 parts of honey-fried licorice root, 200 parts of ginger, 30 parts of mint, 60 parts of radix sophorae flavescentis, 30 parts of amur corktree bark, 60 parts of mulberry leaf, 120 parts of yeast and 140 parts of white sugar.
The powdery scalp environment conditioner is prepared by adopting the components as follows:
s1: weighing the raw material components in proportion, removing impurities, drying, and crushing into coarse powder.
S2: mixing the coarse powder with water according to the weight ratio of 1: 0.8 mass ratio, followed by steaming for 40min with steam.
S3: mixing the steamed coarse powder with warm water according to the weight ratio of 1: 3, adding a yeast and white sugar mixed solution (obtained by dissolving yeast and white sugar in 45 ℃ warm water), and fermenting in a closed container; placing the container in a space with constant temperature of 20 deg.C, and fermenting for 7 d.
S4: and filtering the fermented product to obtain liquid, collecting filter residues, drying and crushing the filter residues into powder to obtain the conditioner.
EXAMPLE III
The embodiment provides a powdery scalp environment conditioner which is prepared from the following raw material components: 300 parts of white paeony root, 150 parts of Chinese date, 150 parts of cassia twig, 100 parts of honey-fried licorice root, 150 parts of ginger, 50 parts of mint, 50 parts of lightyellow sophora root, 50 parts of belvedere fruit, 50 parts of grassleaf sweelflag rhizome, 50 parts of amur corktree bark, 50 parts of mulberry leaf, 130 parts of yeast and 130 parts of white sugar.
The powdery scalp environment conditioner is prepared by adopting the components as follows:
s1: weighing the raw material components in proportion, removing impurities, drying, and crushing into coarse powder.
S2: mixing the coarse powder with water according to the weight ratio of 1: 0.5 mass ratio, followed by steaming for 30min with steam.
S3: mixing the steamed coarse powder with 45 deg.C warm water according to a ratio of 1: 2, adding a yeast and white sugar mixed solution (obtained by dissolving yeast and white sugar in 45 ℃ warm water), and fermenting in a closed container; placing the container in a space with constant temperature of 25 deg.C, and fermenting for 5 d.
S4: and filtering the fermented product to obtain liquid, collecting filter residues, drying and crushing the filter residues into powder to obtain the conditioner.
Example four
The embodiment provides a powdery scalp environment conditioner which is prepared from the following raw material components: 400 parts of white peony root, 100 parts of Chinese date, 200 parts of cassia twig, 50 parts of honey-fried licorice root, 200 parts of ginger, 30 parts of mint, 60 parts of radix sophorae flavescentis, 30 parts of amur corktree bark, 40 parts of fructus kochiae, 60 parts of rhizoma acori graminei, 30 parts of mulberry leaf, 120 parts of yeast and 140 parts of white sugar.
The powdery scalp environment conditioner is prepared by adopting the components as follows:
s1: weighing the raw material components in proportion, removing impurities, drying, and crushing into coarse powder.
S2: mixing the coarse powder with water according to the weight ratio of 1: 0.8 mass ratio, followed by steaming for 40min with steam.
S3: mixing the steamed coarse powder with warm water according to the weight ratio of 1: 3, adding a yeast and white sugar mixed solution (obtained by dissolving yeast and white sugar in 45 ℃ warm water), and fermenting in a closed container; placing the container in a space with constant temperature of 20 deg.C, and fermenting for 7 d.
S4: and filtering the fermented product to obtain liquid, collecting filter residues, drying and crushing the filter residues into powder to obtain the conditioner.
In addition, in order to further highlight the advantages of the technical solution of the present invention, the following comparative examples were provided. The following comparative examples were all set on the basis of example three.
Comparative example 1
The comparison example provides a powdery scalp environment conditioner which is prepared from the following raw material components: 300 parts of white peony root, 150 parts of Chinese date, 150 parts of cassia twig, 100 parts of honey-fried licorice root, 150 parts of ginger, 50 parts of mint, 50 parts of radix sophorae flavescentis and 50 parts of phellodendron amurense.
The powdery scalp environment conditioner is prepared by adopting the components as follows:
weighing the raw material components in proportion, removing impurities, drying, and crushing into coarse powder. Mixing the coarse powder with water according to the weight ratio of 1: 0.5 mass ratio, followed by steaming for 30min with steam. Filtering out liquid from the steamed coarse powder, collecting filter residues, drying and crushing into powder to obtain the conditioner.
Comparative example No. two
The comparison example provides a powdery scalp environment conditioner which is prepared from the following raw material components: 300 parts of white peony root, 150 parts of Chinese date, 150 parts of cassia twig, 100 parts of honey-fried licorice root, 150 parts of ginger, 50 parts of mint, 50 parts of radix sophorae flavescentis, 50 parts of fructus kochiae, 50 parts of rhizoma acori graminei, 50 parts of amur corktree bark and 50 parts of mulberry leaf.
The powdery scalp environment conditioner is prepared by adopting the components as follows:
weighing the raw material components in proportion, removing impurities, drying, and crushing into coarse powder. Mixing the coarse powder with water according to the weight ratio of 1: 0.5 mass ratio, followed by steaming for 30min with steam. Filtering out liquid from the steamed coarse powder, collecting filter residues, drying and crushing into powder to obtain the conditioner.
In addition, in order to further explain the effects of the examples of the present invention, the powdery detergents obtained in the examples were subjected to performance tests.
One or more embodiments of the method for detecting the sanitation and safety of the powdery cleaning agent
The microbial content and the heavy metal content of the powdery cleaners of the examples and comparative examples of the present invention were measured according to the technical specification for cosmetic safety (2015 edition), and the results are shown in table 1.
Table 1 sanitation safety test of powdery detergent in each example
Figure BDA0001730403930000071
Figure BDA0001730403930000081
Second, evaluation of trial Performance of powdery detergent of each example
The performance of the powder cleaning agent of each embodiment of the invention is tested by referring to the test and evaluation methods in GB/T29679-2013, and the results are shown in Table 2. The scoring criterion is 5 points, 1 point is the worst, 5 points are the best, and the higher the score is, the better the score is.
Specifically, 60 volunteers aged 18-50 years were recruited, and the volunteers were divided into 6 groups of 10 each. The first group to the fourth group respectively use the powdery hair cleaning agent of the first embodiment to the fourth embodiment of the invention, and the fifth group and the sixth group respectively use the powdery hair cleaning agent of the first embodiment and the second embodiment of the invention, and the using method is similar to that of shampoo; if the patient carelessly enters the eye, the patient can be washed by clear water.
TABLE 2 List of the properties of the powdered hair cleansers of the examples
Figure BDA0001730403930000082
Of course, other kinds and weight percentages of the raw material components, conditions and parameters in the production process, and the like are also possible in addition to those exemplified in each example.
The powdery scalp environment conditioner provided by the invention is prepared from dozens of herbaceous plants, is pure natural and free of additives, integrates various nutrients required by hair growth, does not damage hair and scalp, does not generate any side effect on human health, has a natural maintenance effect, and can effectively adjust the scalp ecological environment. In addition, the conditioner is in a powder state, does not contain water, essence, pigment, thickening agent, preservative and the like, completely uses natural plants to replace chemical components, and has obvious effect.
In the description herein, it is understood that reference to the description of the terms "one embodiment," "some embodiments," "an example," "a specific example," or "some examples," etc., means that a particular feature, structure, material, or characteristic described in connection with the embodiment or example is included in at least one embodiment or example of the invention. In this specification, the schematic representations of the terms used above are not necessarily intended to refer to the same embodiment or example. Furthermore, the particular features, structures, materials, or characteristics described may be combined in any suitable manner in any one or more embodiments or examples. Furthermore, various embodiments or examples and features of different embodiments or examples described in this specification can be combined and combined by one skilled in the art without contradiction.
Although embodiments of the present invention have been shown and described above, it is understood that the above embodiments are exemplary and should not be construed as limiting the present invention, and that variations, modifications, substitutions and alterations can be made to the above embodiments by those of ordinary skill in the art within the scope of the present invention.

Claims (6)

1. The preparation method of the scalp care conditioner is characterized in that the scalp care conditioner is prepared by fermenting the following traditional Chinese medicine components:
200-400 parts of white peony root, 100-200 parts of Chinese date, 100-200 parts of cassia twig, 50-150 parts of honey-fried licorice root, 100-200 parts of ginger, 30-60 parts of mint, 30-60 parts of radix sophorae flavescentis, 30-60 parts of amur corktree bark, 40-60 parts of fructus kochiae, 30-60 parts of rhizoma acori graminei, 30-60 parts of mulberry leaf, 120-140 parts of yeast and 120-140 parts of white sugar;
the preparation method comprises the following steps:
s1: weighing the raw material components in proportion, removing impurities, and then drying; crushing the dried raw material components;
s2: mixing the crushed raw material components with water and then steaming for a preset time;
s3: mixing the product obtained in the step S2 with warm water, adding yeast and white sugar, and fermenting in a closed container;
s4: filtering the fermented product, collecting filter residues, drying and crushing the filter residues into powder to obtain the conditioner;
in said S3:
the method also comprises the following steps before adding the yeast and the white sugar: taking a proper amount of warm water, adding yeast and white sugar, and uniformly mixing;
the fermentation temperature is 20-25 ℃, and the fermentation time is 5-7 d;
mixing the product obtained in the step S2 with warm water according to the weight ratio of 1: (1-3) mixing in a mass ratio; the temperature of the warm water is 40-50 ℃;
the conditioning agent is in a powder state.
2. The method of preparing the conditioner according to claim 1, wherein the scalp care conditioner is prepared from the following raw material components:
300 parts of white paeony root, 150 parts of Chinese date, 150 parts of cassia twig, 100 parts of honey-fried licorice root, 150 parts of ginger, 50 parts of mint, 50 parts of lightyellow sophora root, 50 parts of belvedere fruit, 50 parts of grassleaf sweelflag rhizome, 50 parts of amur corktree bark, 50 parts of mulberry leaf, 130 parts of yeast and 130 parts of white sugar.
3. A process for preparing a conditioning agent according to claim 1, characterized in that:
in said S2:
the ratio of the crushed raw material components to the water is 1: (0.2-0.8), wherein the preset time is 20-40 min.
4. A process for preparing a conditioning agent according to claim 1, characterized in that:
in said S2:
the ratio of the crushed raw material components to the water is 1: 0.5.
5. a process for preparing a conditioning agent according to claim 1, characterized in that:
in said S2:
the preset time is 30 min.
6. A process for preparing a conditioning agent according to claim 1, characterized in that:
the temperature of the warm water is 45 ℃.
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