CN108835770A - A kind of environmental-protecting insoles and preparation method thereof - Google Patents
A kind of environmental-protecting insoles and preparation method thereof Download PDFInfo
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- CN108835770A CN108835770A CN201810757780.2A CN201810757780A CN108835770A CN 108835770 A CN108835770 A CN 108835770A CN 201810757780 A CN201810757780 A CN 201810757780A CN 108835770 A CN108835770 A CN 108835770A
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- A—HUMAN NECESSITIES
- A43—FOOTWEAR
- A43B—CHARACTERISTIC FEATURES OF FOOTWEAR; PARTS OF FOOTWEAR
- A43B17/00—Insoles for insertion, e.g. footbeds or inlays, for attachment to the shoe after the upper has been joined
- A43B17/003—Insoles for insertion, e.g. footbeds or inlays, for attachment to the shoe after the upper has been joined characterised by the material
- A43B17/006—Insoles for insertion, e.g. footbeds or inlays, for attachment to the shoe after the upper has been joined characterised by the material multilayered
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Abstract
The invention discloses a kind of environmental-protecting insoles and preparation method thereof, it is related to insole field, including insole upper and lower level cotton, insole upper and lower level cotton inner surface is coated with antibiotic layer, insole upper and lower level is closed by adhesive layer, and antibiotic layer includes the raw material of the parts by weight meters such as 1-3 parts of cloves, 1-3 parts of lemon peel, 2-5 parts of grape pip, 2-5 parts of ginkgo leaf, 4-9 parts of camphortree bark, 2-5 parts of short-tube lycoris, 1-3 parts of profound spar powder, 2-5 parts of negative ion powder；Adhesive layer includes 30-40 parts of PVC paste resin, 0.2-0.6 parts of crosslinking agent, 1-3 parts of emulsifier, 0.1-0.3 parts of potassium peroxide and 15-22 parts of water；The present invention by be made after crushing natural plants with other components coordinated antimicrobial emulsion be applied to insole internal layer solidification after, using bonding lotion bonding, the mating reactions such as natural plants and negative ion powder, profound spar powder have good antibacterial and deodouring ability, long action time does not contain any noxious material.
Description
Technical field
The present invention relates to insole fields, and in particular to a kind of environmental-protecting insoles and preparation method thereof.
Background technique
Insole is the layer of material being laid between sole and shoes, has the dual function of protection both feet and shoes.Foot is people
Running body qi and blood, through the important starting position of upper and lower internal organs and channels and collaterals, by modest movement sweat can be discharged in sole in human body,
Especially after strenuous exercise, a large amount of sweat can be discharged in the small space of worn shoes airtightness in foot, if these sweat
It cannot exclude in time, bacterium can be bred in moist shoes, lead to the generation of foot odour and tinea pedis, and endanger the health of foot in turn,
Therefore can have the insole of a pair of antibacterial and good hygroscopicity when wearing shoes, for adjust microenvironment that foot lives in shoes,
Inhibit the generation of bacterium, and finally protection human health is very important.
Chinese patent CN201410265692.2 discloses a kind of with absorbing sweat, antibacterial and deodorant function insole, including insole
Ontology, insole body are from top to bottom disposed with precoat, spongy layer and PU foamed cotton layer composition, and the spray of fabric layer surface is equipped with anti-
Bacterium absorbing sweat liquid, wherein the preparation method of insole is to be coated with Environment-friendlyglue glue in PU foamed cotton layer upper surface and spongy layer upper surface, then
It is bonding by three layers；The insole bonded is dried at a temperature of 150~180 degree again, until Environment-friendlyglue glue is dried.Though the invention
So there is preferable biocidal property, but precoat, spongy layer and PU foamed cotton layer three-decker are bonded together with glue, are affected
Gas, therefore the sweat on foot is conducted can not quickly, comfort is not good enough.
The processing method that Chinese patent CN201310570211.4 discloses a kind of ventilated respiration shoes, wherein the preparation of insole walks
Suddenly include：First the precoat of insole upper epidermis is connected by silica gel piece and elastic balloon green tack in the front end of elastic balloon
It is connected to air inlet pipe, is corresponded on insole mold and is equipped with locating slot at the air inlet pipe closed end, positioning is inserted into the closed end of air inlet pipe
In slot, the exhaust valve position of mounting hole is corresponded on insole mold and is equipped with positioning convex column, it will by positioning convex column and locating slot
Elastic balloon, air inlet pipe, precoat and silica gel piece are fixed on insole mold, and the material of main part PU of insole is finally poured into shoes
Foaming in mold is padded, insole shaping and demoulding again cuts the closed end of air inlet pipe after taking out, insole after molding followed by place
Equipped with pillar, pillar is matched with the pit on sole.The patent of realization technics comparing in to(for) stomata is complicated.
Summary of the invention
Aiming at the problems existing in the prior art, the present invention provides a kind of environmental-protecting insoles and preparation method thereof, the present invention
The insole present invention is applied to insole internal layer by the way that antimicrobial emulsion is made after crushing natural plants with other components coordinated and consolidates
After change, using bonding lotion bonding, the mating reactions such as natural plants and negative ion powder, profound spar powder have good antibacterial and deodouring
Ability, long action time do not contain any noxious material, environmentally protective.
In order to achieve the above object, the present invention is achieved through the following technical solutions：
A kind of environmental-protecting insoles, including insole upper and lower level cotton, insole upper and lower level cotton inner surface are coated with antibiotic layer, shoes
Upper and lower level is padded to be closed by adhesive layer；
The antibiotic layer includes following raw material by weight：1-3 parts of cloves, 1-3 parts of lemon peel, 2-5 parts of grape pip,
2-5 parts of ginkgo leaf, 4-9 parts of camphortree bark, 2-5 parts of short-tube lycoris, 1-3 parts of profound spar powder, 2-5 parts of negative ion powder, nano silica 5-
10 parts, 1-2 parts of dodecyl pyrrolidone, 1-2.2 parts of eucalyptus oil, 1-1.8 parts of rose extract, 3-5 parts of emulsion adjuvant and water
8-12 parts；
The adhesive layer includes the raw material of following parts by weight meter：30-40 parts of PVC paste resin, 0.2-0.6 parts of crosslinking agent, cream
1-3 parts of agent, 0.1-0.3 parts of potassium peroxide and 15-22 parts of water.
Preferably, the antibiotic layer includes following raw material by weight：1.5-2.5 parts of cloves, lemon peel 1.5-2.5
Part, 3-4 parts of grape pip, 3-4 parts of ginkgo leaf, 5-8 parts of camphortree bark, 3-4 parts of short-tube lycoris, 1.5-2.5 parts of profound spar powder, negative ion powder 3-
4 parts, 6-9 parts of nano silica, 1.2-1.8 parts of dodecyl pyrrolidone, 1.5-1.8 parts of eucalyptus oil, rose extract
1.2-1.6 parts, 3.5-4.5 parts of emulsion adjuvant and 9-11 parts of water；
The adhesive layer includes the raw material of following parts by weight meter：32-38 parts of PVC paste resin, 0.3-0.5 parts of crosslinking agent, cream
1.5-2.5 parts of agent, 0.15-0.25 parts of potassium peroxide and 17-20 parts of water.
Preferably, the antibiotic layer includes following raw material by weight：2 parts of cloves, 2 parts of lemon peel, grape pip 3.5
Part, 3.5 parts of ginkgo leaf, 7 parts of camphortree bark, 3.5 parts of short-tube lycoris, 2 parts of profound spar powder, 3.5 parts of negative ion powder, 8 parts of nano silica,
1.6 parts of dodecyl pyrrolidone, 1.6 parts of eucalyptus oil, 1.5 parts of rose extract, 4 parts of emulsion adjuvant and 10 parts of water；
The adhesive layer includes the raw material of following parts by weight meter：36 parts of PVC paste resin, 0.4 part of crosslinking agent, 2 parts of emulsifier,
0.2 part and 18 parts of water of potassium peroxide.
Preferably, the emulsion adjuvant in the antibiotic layer is fat alcohol polyethylene ether and cornstarch according to mass ratio 1:5
Mixing composition.
Preferably, the emulsifier in the adhesive layer is different tridecanol polyoxyethylene ether, fatty alcohol polyoxyethylene ether, tristearin
One or more of sour polyoxyethylene ester and rosin polyoxyethylene ester combine.
Preferably, the crosslinking agent in the adhesive layer is cumyl peroxide, benzoyl peroxide, di-t-butyl peroxide
One or more of compound and di-isopropylbenzene hydroperoxide combine.
The preparation method that a kind of above-mentioned environmental-protecting insoles are also disclosed in the present invention specifically includes the following steps：
(1) preparation of antibiotic layer：
Cloves, lemon peel, grape pip, ginkgo leaf, camphortree bark, short-tube lycoris, profound spar powder are mixed to be added in pulverizer and carried out
It crushes, crosses 100-200 mesh, obtain sterilization powder；
Negative ion powder, nano silica, dodecyl pyrrolidone, eucalyptus oil, rose are sequentially added into sterilization powder
After extract, emulsion adjuvant and water are uniformly mixed, be placed in ultrasonic wave separating apparatus in disperse 40 minutes to get；
(2) preparation of adhesive layer：After PVC paste resin, crosslinking agent, emulsifier, potassium peroxide and water are mixed, with 400-
After 600 revs/min of speed is stirred 10-15 minutes, with the power of 10-15KW under 40-50 degrees Celsius, disperse 30-40
Minute, obtain bonding lotion；
(3) adhesive layer is uniformly brushed on insole upper and lower level cotton inner surface, the ultraviolet light of 265-272 nanometers of merging
Under, under 50-60 degree celsius temperature, dry solidification；
(4) adhesive layer is uniformly smeared on the adhesive layer after step (3) solidifies, after upper and lower level cotton is merged bonding, used
After roller roll-in is smooth, dry to get the environmental-protecting insoles.
Preferably, the drying in the step (4) is to dry 60-100 seconds under 130 degrees Celsius.
Preferably, the antibiotic layer with a thickness of 0.1-1 millimeters.
Preferably, the adhesive layer with a thickness of 0.05-0.3 millimeters.
The present invention has following beneficial effect：
(1) the insole present invention of the present invention is by being made antimicrobial emulsion with other components coordinated after crushing natural plants
After being applied to the solidification of insole internal layer, using bonding lotion bonding, the mating reactions such as natural plants and negative ion powder, profound spar powder tool
There is good antibacterial and deodouring ability, long action time does not contain any noxious material, environmentally protective.
(2) present invention addition cloves, lemon peel, grape pip, ginkgo leaf, camphortree bark, short-tube lycoris, profound several natural goods of spar powder
Matter has good antibiotic property, while lemon peel distributes natural faint scent, there is improving peculiar smell, the present invention also add bear from
Sub- powder, nano silica, dodecyl pyrrolidone, eucalyptus oil, rose extract, fat alcohol polyethylene ether, cornstarch
It is stirred with water, negative ion powder has the function of that sterilization removes odors, while negative ion powder discharges infrared ray, facilitates foot
Health, nano silica have damping effect.
(3) present invention bonding lotion selects PVC paste resin, and caking property is good, and chemical property is stablized, and is applied to deodorizing antibiotic cream
On liquid, has the function of protection, while it is simple to bond emulsion preparation method, high income, controllability is good.
(4) preparation method of the present invention is simple, and operability is high, and controllability is good, is suitable for industrialized production.
Specific embodiment
Below with reference to embodiment, further description of the specific embodiments of the present invention, and following embodiment is only used for more
Technical solution of the present invention is clearly demonstrated, and not intended to limit the protection scope of the present invention.
Embodiment 1
A kind of environmental-protecting insoles, including insole upper and lower level cotton, insole upper and lower level cotton inner surface are coated with antibiotic layer, shoes
Upper and lower level is padded to be closed by adhesive layer；
The antibiotic layer includes following raw material by weight：3 parts of cloves, 3 parts of lemon peel, 5 parts of grape pip, ginkgo leaf
5 parts, 9 parts of camphortree bark, 5 parts of short-tube lycoris, 3 parts of profound spar powder, 5 parts of negative ion powder, 10 parts of nano silica, dodecyl pyrrolidine
2 parts of ketone, 2.2 parts of eucalyptus oil, 1.8 parts of rose extract, 5 parts of emulsion adjuvant and 12 parts of water；
Adhesive layer includes the raw material of following parts by weight meter：40 parts of PVC paste resin, 0.6 part of crosslinking agent, 3 parts of emulsifier, peroxide
0.3 part and 22 parts of water of potassium sulfate.
Emulsion adjuvant in antibiotic layer is fat alcohol polyethylene ether and cornstarch according to mass ratio 1:5 mixing compositions.
Emulsifier in adhesive layer is different tridecanol polyoxyethylene ether.
Crosslinking agent in adhesive layer is cumyl peroxide.
The preparation method of environmental-protecting insoles in the present embodiment specifically includes the following steps：
(1) preparation of antibiotic layer：
Cloves, lemon peel, grape pip, ginkgo leaf, camphortree bark, short-tube lycoris, profound spar powder are mixed to be added in pulverizer and carried out
It crushes, sieves with 100 mesh sieve, obtain sterilization powder；
Negative ion powder, nano silica, dodecyl pyrrolidone, eucalyptus oil, rose are sequentially added into sterilization powder
After extract, emulsion adjuvant and water are uniformly mixed, be placed in ultrasonic wave separating apparatus in disperse 40 minutes to get；
(2) preparation of adhesive layer：After PVC paste resin, crosslinking agent, emulsifier, potassium peroxide and water are mixed, with 400
Rev/min speed be stirred after ten minutes, with the power of 10KW under 40 degrees Celsius, disperse 30 minutes, obtain bonding lotion；
(3) adhesive layer is uniformly brushed on insole upper and lower level cotton inner surface, under the ultraviolet light of 265 nanometers of merging,
Under 50 degree celsius temperatures, dry solidification；
(4) adhesive layer is uniformly smeared on the adhesive layer after step (3) solidifies, after upper and lower level cotton is merged bonding, used
After roller roll-in is smooth, dry to get the environmental-protecting insoles.
Drying in step (4) is to dry 60 seconds under 130 degrees Celsius.
Antibiotic layer with a thickness of 0.1 millimeter.
Adhesive layer with a thickness of 0.05 millimeter.
Embodiment 2
A kind of environmental-protecting insoles, including insole upper and lower level cotton, insole upper and lower level cotton inner surface are coated with antibiotic layer, shoes
Upper and lower level is padded to be closed by adhesive layer；
Antibiotic layer includes following raw material by weight：1.5 parts of cloves, 1.5 parts of lemon peel, 3 parts of grape pip, ginkgo leaf
3 parts, 5 parts of camphortree bark, 3 parts of short-tube lycoris, 1.5 parts of profound spar powder, 3 parts of negative ion powder, 6 parts of nano silica, dodecyl pyrroles
1.2 parts of alkanone, 1.5 parts of eucalyptus oil, 1.2 parts of rose extract, 3.5 parts of emulsion adjuvant and 9 parts of water；
Adhesive layer includes the raw material of following parts by weight meter：32 parts of PVC paste resin, 0.3 part of crosslinking agent, 1.5 parts of emulsifier, mistake
0.15 part and 17 parts of water of oxygen potassium sulfate.
Emulsion adjuvant in antibiotic layer is fat alcohol polyethylene ether and cornstarch according to mass ratio 1:5 mixing compositions.
Emulsifier in adhesive layer is fatty alcohol polyoxyethylene ether.
Crosslinking agent in adhesive layer is benzoyl peroxide.
The preparation method of environmental-protecting insoles in the present embodiment specifically includes the following steps：
(1) preparation of antibiotic layer：
Cloves, lemon peel, grape pip, ginkgo leaf, camphortree bark, short-tube lycoris, profound spar powder are mixed to be added in pulverizer and carried out
It crushes, crosses 200 meshes, obtain sterilization powder；
Negative ion powder, nano silica, dodecyl pyrrolidone, eucalyptus oil, rose are sequentially added into sterilization powder
After extract, emulsion adjuvant and water are uniformly mixed, be placed in ultrasonic wave separating apparatus in disperse 40 minutes to get；
(2) preparation of adhesive layer：After PVC paste resin, crosslinking agent, emulsifier, potassium peroxide and water are mixed, with 600
Rev/min speed be stirred 15 minutes after, at 50 c with the power of 15KW, disperse 40 minutes, obtain bonding lotion；
(3) adhesive layer is uniformly brushed on insole upper and lower level cotton inner surface, under the ultraviolet light of 272 nanometers of merging,
Under 60 degree celsius temperatures, dry solidification；
(4) adhesive layer is uniformly smeared on the adhesive layer after step (3) solidifies, after upper and lower level cotton is merged bonding, used
After roller roll-in is smooth, dry to get the environmental-protecting insoles.
Drying in step (4) is to dry 100 seconds under 130 degrees Celsius.
Antibiotic layer with a thickness of 1 millimeter.
Adhesive layer with a thickness of 0.3 millimeter.
Embodiment 3
A kind of environmental-protecting insoles, including insole upper and lower level cotton, insole upper and lower level cotton inner surface are coated with antibiotic layer, shoes
Upper and lower level is padded to be closed by adhesive layer；
Antibiotic layer includes following raw material by weight：1 part of cloves, 1 part of lemon peel, 2 parts of grape pip, 2 parts of ginkgo leaf,
4 parts of camphortree bark, 2 parts of short-tube lycoris, 1 part of profound spar powder, 2 parts of negative ion powder, 5 parts of nano silica, dodecyl pyrrolidone 1
Part, 1 part of eucalyptus oil, 1 part of rose extract, 3 parts of emulsion adjuvant and 8 parts of water；
Adhesive layer includes the raw material of following parts by weight meter：30 parts of PVC paste resin, 0.2 part of crosslinking agent, 1 part of emulsifier, peroxide
0.1 part and 15 parts of water of potassium sulfate.
Emulsion adjuvant in antibiotic layer is fat alcohol polyethylene ether and cornstarch according to mass ratio 1:5 mixing compositions.
Emulsifier in adhesive layer is polyoxyethylene stearic acid ester.
Crosslinking agent in adhesive layer is di-tert-butyl peroxide.
The preparation method of environmental-protecting insoles in the present embodiment specifically includes the following steps：
(1) preparation of antibiotic layer：
Cloves, lemon peel, grape pip, ginkgo leaf, camphortree bark, short-tube lycoris, profound spar powder are mixed to be added in pulverizer and carried out
It crushes, crosses 150 meshes, obtain sterilization powder；
Negative ion powder, nano silica, dodecyl pyrrolidone, eucalyptus oil, rose are sequentially added into sterilization powder
After extract, emulsion adjuvant and water are uniformly mixed, be placed in ultrasonic wave separating apparatus in disperse 40 minutes to get；
(2) preparation of adhesive layer：After PVC paste resin, crosslinking agent, emulsifier, potassium peroxide and water are mixed, with 460
Rev/min speed be stirred 13 minutes after, with the power of 12KW under 48 degrees Celsius, disperse 35 minutes, obtain bonding lotion；
(3) adhesive layer is uniformly brushed on insole upper and lower level cotton inner surface, the ultraviolet light of 265-272 nanometers of merging
Under, under 56 degree celsius temperatures, dry solidification；
(4) adhesive layer is uniformly smeared on the adhesive layer after step (3) solidifies, after upper and lower level cotton is merged bonding, used
After roller roll-in is smooth, dry to get the environmental-protecting insoles.
Drying in step (4) is to dry 80 seconds under 130 degrees Celsius.
Antibiotic layer with a thickness of 0.6 millimeter.
Adhesive layer with a thickness of 0.15 millimeter.
Embodiment 4
A kind of environmental-protecting insoles, including insole upper and lower level cotton, insole upper and lower level cotton inner surface are coated with antibiotic layer, shoes
Upper and lower level is padded to be closed by adhesive layer；
Antibiotic layer includes following raw material by weight：2.5 parts of cloves, 2.5 parts of lemon peel, 4 parts of grape pip, ginkgo leaf
4 parts, 8 parts of camphortree bark, 4 parts of short-tube lycoris, 2.5 parts of profound spar powder, 4 parts of negative ion powder, 9 parts of nano silica, dodecyl pyrroles
1.8 parts of alkanone, 1.8 parts of eucalyptus oil, 1.6 parts of rose extract, 4.5 parts of emulsion adjuvant and 11 parts of water；
Adhesive layer includes the raw material of following parts by weight meter：38 parts of PVC paste resin, 0.5 part of crosslinking agent, 2.5 parts of emulsifier, mistake
0.25 part and 20 parts of water of oxygen potassium sulfate.
Emulsion adjuvant in antibiotic layer is fat alcohol polyethylene ether and cornstarch according to mass ratio 1:5 mixing compositions.
Emulsifier in adhesive layer is rosin polyoxyethylene ester.
Crosslinking agent in adhesive layer is di-isopropylbenzene hydroperoxide.
The preparation method of environmental-protecting insoles in the present embodiment specifically includes the following steps：
(1) preparation of antibiotic layer：
Cloves, lemon peel, grape pip, ginkgo leaf, camphortree bark, short-tube lycoris, profound spar powder are mixed to be added in pulverizer and carried out
It crushes, crosses 170 meshes, obtain sterilization powder；
Negative ion powder, nano silica, dodecyl pyrrolidone, eucalyptus oil, rose are sequentially added into sterilization powder
After extract, emulsion adjuvant and water are uniformly mixed, be placed in ultrasonic wave separating apparatus in disperse 40 minutes to get；
(2) preparation of adhesive layer：After PVC paste resin, crosslinking agent, emulsifier, potassium peroxide and water are mixed, with 520
Rev/min speed be stirred 14 minutes after, with the power of 10-15KW under 42 degrees Celsius, disperse 38 minutes, cream must be bonded
Liquid；
(3) adhesive layer is uniformly brushed on insole upper and lower level cotton inner surface, under the ultraviolet light of 268 nanometers of merging,
Under 57 degree celsius temperatures, dry solidification；
(4) adhesive layer is uniformly smeared on the adhesive layer after step (3) solidifies, after upper and lower level cotton is merged bonding, used
After roller roll-in is smooth, dry to get the environmental-protecting insoles.
Drying in step (4) is to dry 90 seconds under 130 degrees Celsius.
Antibiotic layer with a thickness of 0.6 millimeter.
Adhesive layer with a thickness of 0.25 millimeter.
Embodiment 5
A kind of environmental-protecting insoles, including insole upper and lower level cotton, insole upper and lower level cotton inner surface are coated with antibiotic layer, shoes
Upper and lower level is padded to be closed by adhesive layer；
Antibiotic layer includes following raw material by weight：2 parts of cloves, 2 parts of lemon peel, 3.5 parts of grape pip, ginkgo leaf
3.5 parts, 7 parts of camphortree bark, 3.5 parts of short-tube lycoris, 2 parts of profound spar powder, 3.5 parts of negative ion powder, 8 parts of nano silica, dodecyl
1.6 parts of pyrrolidones, 1.6 parts of eucalyptus oil, 1.5 parts of rose extract, 4 parts of emulsion adjuvant and 10 parts of water；
Adhesive layer includes the raw material of following parts by weight meter：36 parts of PVC paste resin, 0.4 part of crosslinking agent, 2 parts of emulsifier, peroxide
0.2 part and 18 parts of water of potassium sulfate.
Emulsion adjuvant in antibiotic layer is fat alcohol polyethylene ether and cornstarch according to mass ratio 1:5 mixing compositions.
Emulsifier in adhesive layer is different tridecanol polyoxyethylene ether.
Crosslinking agent in adhesive layer is peroxidating diisopropyl.
The preparation method of environmental-protecting insoles in the present embodiment specifically includes the following steps：
(1) preparation of antibiotic layer：
Cloves, lemon peel, grape pip, ginkgo leaf, camphortree bark, short-tube lycoris, profound spar powder are mixed to be added in pulverizer and carried out
It crushes, crosses 180 meshes, obtain sterilization powder；
Negative ion powder, nano silica, dodecyl pyrrolidone, eucalyptus oil, rose are sequentially added into sterilization powder
After extract, emulsion adjuvant and water are uniformly mixed, be placed in ultrasonic wave separating apparatus in disperse 40 minutes to get；
(2) preparation of adhesive layer：After PVC paste resin, crosslinking agent, emulsifier, potassium peroxide and water are mixed, with 560
Rev/min speed be stirred 13 minutes after, with the power of 14KW under 48 degrees Celsius, disperse 34 minutes, obtain bonding lotion；
(3) adhesive layer is uniformly brushed on insole upper and lower level cotton inner surface, under the ultraviolet light of 271 nanometers of merging,
Under 54 degree celsius temperatures, dry solidification；
(4) adhesive layer is uniformly smeared on the adhesive layer after step (3) solidifies, after upper and lower level cotton is merged bonding, used
After roller roll-in is smooth, dry to get the environmental-protecting insoles.
Drying in step (4) is to dry 86 seconds under 130 degrees Celsius.
Antibiotic layer with a thickness of 0.7 millimeter.
Adhesive layer with a thickness of 0.15 millimeter.
Comparative example 1：In addition to being not provided with antibiotic layer, remaining preparation method and raw material are same as Example 1；
Insole made from environmental-protecting insoles made from embodiment 1-4 and ratio 1 is tested for the property, as a result such as the following table 1：
| Experimental group | Antibiotic property | Removing odors property |
| Embodiment 1 | ○ | ○ |
| Embodiment 2 | ○ | ○ |
| Embodiment 3 | ○ | ○ |
| Embodiment 4 | ○ | ○ |
| Embodiment 5 | ○ | ○ |
| Comparative example 1 | × | × |
To sum up locating, the present invention has the following advantages that：
(1) the insole present invention of the present invention is by being made antimicrobial emulsion with other components coordinated after crushing natural plants
After being applied to the solidification of insole internal layer, using bonding lotion bonding, the mating reactions such as natural plants and negative ion powder, profound spar powder tool
There is good antibacterial and deodouring ability, long action time does not contain any noxious material, environmentally protective.
(2) present invention addition cloves, lemon peel, grape pip, ginkgo leaf, camphortree bark, short-tube lycoris, profound several natural goods of spar powder
Matter has good antibiotic property, while lemon peel distributes natural faint scent, there is improving peculiar smell, the present invention also add bear from
Sub- powder, nano silica, dodecyl pyrrolidone, eucalyptus oil, rose extract, fat alcohol polyethylene ether, cornstarch
It is stirred with water, negative ion powder has the function of that sterilization removes odors, while negative ion powder discharges infrared ray, facilitates foot
Health, nano silica have damping effect.
(3) present invention bonding lotion selects PVC paste resin, and caking property is good, and chemical property is stablized, and is applied to deodorizing antibiotic cream
On liquid, has the function of protection, while it is simple to bond emulsion preparation method, high income, controllability is good.
(4) preparation method of the present invention is simple, and operability is high, and controllability is good, is suitable for industrialized production.
The foregoing is only a preferred embodiment of the present invention, is not intended to restrict the invention, although referring to aforementioned reality
Applying example, invention is explained in detail, for those skilled in the art, still can be to aforementioned each implementation
Technical solution documented by example is modified or equivalent replacement of some of the technical features.It is all in essence of the invention
Within mind and principle, any modification, equivalent replacement, improvement and so on be should all be included in the protection scope of the present invention.
Claims (10)
1. a kind of environmental-protecting insoles, including insole upper and lower level cotton, insole upper and lower level cotton inner surface is coated with antibiotic layer, insole
Upper and lower level is closed by adhesive layer, which is characterized in that the antibiotic layer includes following raw material by weight：1-3 parts of cloves,
1-3 parts of lemon peel, 2-5 parts of grape pip, 2-5 parts of ginkgo leaf, 4-9 parts of camphortree bark, 2-5 parts of short-tube lycoris, 1-3 parts of profound spar powder, bear from
Sub- powder 2-5 parts, 5-10 parts of nano silica, 1-2 parts of dodecyl pyrrolidone, 1-2.2 parts of eucalyptus oil, rose extract 1-
1.8 parts, 3-5 parts of emulsion adjuvant and 8-12 parts of water；
The adhesive layer includes the raw material of following parts by weight meter：30-40 parts of PVC paste resin, 0.2-0.6 parts of crosslinking agent, emulsifier
1-3 parts, 0.1-0.3 parts of potassium peroxide and 15-22 parts of water.
2. environmental-protecting insoles according to claim 1, which is characterized in that the antibiotic layer includes following original by weight
Material：1.5-2.5 parts of cloves, 1.5-2.5 parts of lemon peel, 3-4 parts of grape pip, 3-4 parts of ginkgo leaf, 5-8 parts of camphortree bark, short-tube lycoris 3-4
Part, 1.5-2.5 parts of profound spar powder, 3-4 parts of negative ion powder, 6-9 parts of nano silica, dodecyl pyrrolidone 1.2-1.8
Part, 1.5-1.8 parts of eucalyptus oil, 1.2-1.6 parts of rose extract, 3.5-4.5 parts of emulsion adjuvant and 9-11 parts of water；
The adhesive layer includes the raw material of following parts by weight meter：32-38 parts of PVC paste resin, 0.3-0.5 parts of crosslinking agent, emulsifier
1.5-2.5 parts, 0.15-0.25 parts of potassium peroxide and 17-20 parts of water.
3. environmental-protecting insoles according to claim 1, which is characterized in that the antibiotic layer includes following original by weight
Material：2 parts of cloves, 2 parts of lemon peel, 3.5 parts of grape pip, 3.5 parts of ginkgo leaf, 7 parts of camphortree bark, 3.5 parts of short-tube lycoris, 2 parts of profound spar powder,
3.5 parts of negative ion powder, 8 parts of nano silica, 1.6 parts of dodecyl pyrrolidone, 1.6 parts of eucalyptus oil, rose extract 1.5
Part, 4 parts of emulsion adjuvant and 10 parts of water；
The adhesive layer includes the raw material of following parts by weight meter：36 parts of PVC paste resin, 0.4 part of crosslinking agent, 2 parts of emulsifier, peroxide
0.2 part and 18 parts of water of potassium sulfate.
4. environmental-protecting insoles according to claim 1, which is characterized in that the emulsion adjuvant in the antibiotic layer is poly alkyl alcohol
Vinethene and cornstarch are according to mass ratio 1:5 mixing compositions.
5. environmental-protecting insoles according to claim 1, which is characterized in that the emulsifier in the adhesive layer is poly- for different tridecanol
One or more of ethylene oxide ether, fatty alcohol polyoxyethylene ether, polyoxyethylene stearic acid ester and rosin polyoxyethylene ester combine.
6. environmental-protecting insoles according to claim 1, which is characterized in that the crosslinking agent in the adhesive layer is that peroxidating two is different
One or more of propyl benzene, benzoyl peroxide, di-tert-butyl peroxide and di-isopropylbenzene hydroperoxide combine.
7. a kind of preparation method of environmental-protecting insoles as claimed in any one of claims 1 to 6, which is characterized in that including following step
Suddenly：
(1) preparation of antibiotic layer：
Cloves, lemon peel, grape pip, ginkgo leaf, camphortree bark, short-tube lycoris, profound spar powder are mixed to be added in pulverizer and crushed,
100-200 mesh is crossed, sterilization powder is obtained；
Negative ion powder, nano silica, dodecyl pyrrolidone, eucalyptus oil, rose is sequentially added into sterilization powder to extract
After object, emulsion adjuvant and water are uniformly mixed, be placed in ultrasonic wave separating apparatus in disperse 40 minutes to get；
(2) preparation of adhesive layer：After PVC paste resin, crosslinking agent, emulsifier, potassium peroxide and water are mixed, with 400-600
Rev/min speed be stirred 10-15 minutes after, with the power of 10-15KW under 40-50 degrees Celsius, dispersion 30-40 point
Clock obtains bonding lotion；
(3) adhesive layer is uniformly brushed on insole upper and lower level cotton inner surface, under the ultraviolet light of 265-272 nanometers of merging,
Under 50-60 degree celsius temperature, dry solidification；
(4) adhesive layer is uniformly smeared on the adhesive layer after step (3) solidifies, after upper and lower level cotton is merged bonding, uses roller
After roll-in is smooth, dry to get the environmental-protecting insoles.
8. environmental-protecting insoles Preparation Method according to claim 7, which is characterized in that the drying in the step (4) is 130
It is dried 60-100 seconds under degree Celsius.
9. the preparation method of environmental-protecting insoles according to claim 7, which is characterized in that the antibiotic layer with a thickness of 0.1-
1 millimeter.
10. the preparation method of environmental-protecting insoles according to claim 7, which is characterized in that the adhesive layer with a thickness of
0.05-0.3 millimeters.
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| CN201810757780.2A CN108835770A (en) | 2018-07-11 | 2018-07-11 | A kind of environmental-protecting insoles and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201810757780.2A CN108835770A (en) | 2018-07-11 | 2018-07-11 | A kind of environmental-protecting insoles and preparation method thereof |
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| CN110946365A (en) * | 2019-12-27 | 2020-04-03 | 起步股份有限公司 | Breathable antibacterial self-heating memory cotton children shoe insole and preparation method thereof |
| CN111227433A (en) * | 2020-02-12 | 2020-06-05 | 常德集智生物科技有限公司 | Green antibacterial and bactericidal insole |
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| CN110946365A (en) * | 2019-12-27 | 2020-04-03 | 起步股份有限公司 | Breathable antibacterial self-heating memory cotton children shoe insole and preparation method thereof |
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