CN108813742A - A kind of electronics tobacco tar and preparation method thereof fragrant with cocoa baking - Google Patents

A kind of electronics tobacco tar and preparation method thereof fragrant with cocoa baking Download PDF

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Publication number
CN108813742A
CN108813742A CN201811040689.5A CN201811040689A CN108813742A CN 108813742 A CN108813742 A CN 108813742A CN 201811040689 A CN201811040689 A CN 201811040689A CN 108813742 A CN108813742 A CN 108813742A
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China
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cocoa
fragrant
tobacco tar
electronics tobacco
preparation
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CN201811040689.5A
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CN108813742B (en
Inventor
王晋
张承明
张涛
陈建华
向明
孔维松
杨叶昆
魏玉玲
田丽梅
蒋次清
王小龙
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China Tobacco Yunnan Industrial Co Ltd
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China Tobacco Yunnan Industrial Co Ltd
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    • A24F47/008

Abstract

The present invention relates to a kind of electronics tobacco tar and preparation method thereof fragrant with cocoa baking, belong to new tobacco products technical field.This method is that polyalcohol and calcium salt complex are added into the powder sample of Buddhist Lars spy's Luo Keke criollo cocoa and Trinida cocoa, stirring is to after mixing, 0.5~3h is reacted at 150~250 DEG C, then product is added in organic solvent, after 10~60min of ultrasonic extraction, then shakes 10~60min of extraction, it is centrifugated later, after taking the organic membrane filtration of supernatant liquid, filtrate decompression distillation obtains cocoa and toasts fragrant fragrance;It cocoa is toasted into fragrant fragrance, polydextrose and atomized liquid is again stirred at room temperature to after mixing, being placed in and be protected from light shady place and refine 24~48h, obtain the electronics tobacco tar for having cocoa baking fragrant.Electronics tobacco tar preparation method of the present invention is simple, at low cost, and baking note is prominent, in use, comfort improves, respiratory tract irritation is substantially reduced.

Description

A kind of electronics tobacco tar and preparation method thereof fragrant with cocoa baking
Technical field
The invention belongs to new tobacco products technical fields, and in particular to a kind of electronics tobacco tar fragrant with cocoa baking and Preparation method.
Background technique
As cigarette consumption person is to the growing interest of own health, and the requirement to cigarette interior quality is higher and higher, Low tar high-quality cigarette has become the emphasis studied at present.However, being necessarily accompanied with cigarette flavor damage while low tar It loses and comfort level is deteriorated.And in quality, country's cigarette product has one in terms of sucking quality and sense organ at present Fixed deficiency, such as fragrance is faint, dry sensation is strong, sweet degree is inadequate, comfort level is poor.
In order to improve the quality of cigarette, can by perfuming cigarette feeding technique, come set off, added volume cigarette perfume taste, increase Flue gas concentration, improvement is jealous, removes and cover miscellaneous gas, reduces irritation, assigns the good characteristic chicken flavor of product, and prominent cigarette produces The personalized style of product, promote cigarette sucks satisfaction and pleasure degree.
Toasting fragrant note is to bake one of perfume (or spice) note, is the important component of cigarette flavor.In recent years, there is research Flavouring is carried out to traditional red date extract using zymotechnic, microbial fermentation technology, Maillard reaction etc., produces fragrant processing, The note for enriching red date extract to a certain extent increases the content of flavor component.There are also normal using malt extract etc. With cigarette additive, it is fragrant to increase flue gas baking.But the baking perfume (or spice) note of gained the said goods does not protrude, and wherein still Generation so can be cracked during cigarette is burnt and sucked containing macromolecular substances, these substances such as a certain amount of protein, pectin, polysaccharide Some harmful components, increase cigarette smoking irritation and miscellaneous gas.
One of big soft drink in the world three can be can be, there is the nutritive value compared with quotient, be widely used in chocolate, beverage, cake With the industries such as ice cream.Cocoa bean due to its process, formed its solely its with unique flavor and nutriment abundant, It is also widely used for also being applied in tobacco, cosmetics and pharmaceuticals.How the prior art is overcome using cocoa not The problem of foot is current new tobacco products technical field urgent need to resolve.
Summary of the invention
It is an object of the present invention to solve the deficiency of the existing technology and provide a kind of electronics tobacco tar fragrant with cocoa baking And preparation method thereof, the electronics tobacco tar preparation method for having cocoa baking fragrant is simple, and it is at low cost, for toasting in electronic cigarette Note is prominent, and comfort increases, and respiratory tract irritation is substantially reduced.
To achieve the above object, the technical solution adopted by the present invention is as follows:
A kind of preparation method of the electronics tobacco tar fragrant with cocoa baking, includes the following steps:
Step (1) weighs 10~60 parts of Buddhist Lars spy Luo Keke, 1~5 part of criollo cocoa in parts by weight With the powder sample of 5~50 parts of Trinida cocoas, 100~500 parts of polyalcohols and 0.01~1 part of calcium salt are then added thereto Complex compound, stirring react 0.5~3h to after mixing at 150~250 DEG C;
The polyalcohol is the combination of one or more of ethylene glycol, propylene glycol and glycerol;
The calcium salt complex is calcium glycine complex compound or Ca-EDTA complex compound;
The product that step (1) obtains is added in organic solvent, after 10~60min of ultrasonic extraction, then shakes by step (2) Swing 10~60min of extraction, be centrifugated later, after taking the organic membrane filtration of supernatant liquid, to filtrate be evaporated under reduced pressure with Organic solvent is removed, cocoa is obtained and toasts fragrant fragrance;
Step (3) weighs cocoa and toasts fragrant 1~5 part of fragrance, 5~20 parts of polydextrose and atomization in parts by weight 75~94 parts of liquid, be stirred at room temperature to after mixing, be placed in be protected from light shady place refine 24~48h, obtain with cocoa baking Bake fragrant electronics tobacco tar.It is further preferred that the Buddhist Lars spy Luo Keke is brazilian cocoa, Ghana in step (1) The combination of one or more of cocoa and Hainan cocoa.
It is further preferred that the criollo cocoa is Mexico's cocoa, Ecuador's cocoa in step (1) With the combination of one or more of Taiwan cocoa.
It is further preferred that the Trinida cocoa is that Venezuela's cocoa and/or Indonesia can in step (1) It can.
It is further preferred that the organic solvent is petroleum ether, n-hexane, ethyl alcohol, chloroform, two in step (2) The combination of one or more of chloromethanes, ethyl acetate and methyl acetate;Consumption of organic solvent is 200~2000 parts by weight.
It is further preferred that the centrifuge separation time is 4~15min in step (2).Further, preferably It is that in step (3), the mixing time is 20~30min.
It is further preferred that the atomized liquid is propylene glycol or glycerol in step (3).
Present invention simultaneously provides the electronics tobacco tar with cocoa baking perfume made from above-mentioned preparation method.
The present invention is progress Maillard reaction using calcium salt complex as catalyst, later by product specific organic molten Extraction and separation in agent obtain the dense cocoa of cocoa baking note and toast fragrant fragrance, and are practically free of protein, fruit in the substance Glue and polysaccharide compound electronics tobacco tar obtained with polydextrose, atomized liquid when in use, can reduce irritation and miscellaneous gas.
Compared with prior art, the present invention its advantages are:
Selected cocoa by specific modulated process, is generated the perfume (or spice) that there is distinctive cocoa to toast fragrant note by the present invention Material, in modulated process, carries out targeting extraction using certain solvent, and can remove macromolecular substances etc. can generate flue gas stimulation Property, miscellaneous gas substance, it is later, multiple with polydextrose, atomized liquid using it so that obtaining pure cocoa toasts fragrant note substance Match, obtains the electronics tobacco tar for having cocoa baking fragrant, it is prominent which toasts note, and due to compounding with polydextrose, So stimulation of the tobacco tar to respiratory tract can be substantially reduced.
Electronics tobacco tar of the present invention can improve the baking fragrance and suction mouthfeel of electronic cigarette, can effectively improve Novel tobacco The baking perfume (or spice) quality of straw-made articles, reduces miscellaneous tolerance, and comfort and the harmony preparation method for improving electronic cigarette are easy to operate, produces Product safety, is with a wide range of applications.
Specific embodiment
Below with reference to embodiment, the present invention is described in further detail.
It will be understood to those of skill in the art that the following example is merely to illustrate the present invention, and it should not be regarded as limiting this hair Bright range.In the examples where no specific technique or condition is specified, described technology or conditions according to the literature in the art Or it is carried out according to product description.Production firm person is not specified in material therefor or equipment, is that can be obtained by purchase Conventional products.
Embodiment 1
A kind of preparation method of the electronics tobacco tar fragrant with cocoa baking, includes the following steps:
Step (1) weighs 10 parts of Buddhist Lars spy Luo Keke, 1 part of criollo cocoa and 5 parts of spies in parts by weight The powder sample of Li Nida cocoa, is then added 100 parts of polyalcohols and 0.01 part of calcium salt complex thereto, and stirring is equal to mixing After even, 3h is reacted at 150 DEG C;
The polyalcohol is ethylene glycol;
The calcium salt complex is calcium glycine complex compound;
The product that step (1) obtains is added in 200 parts of organic solvents, after ultrasonic extraction 60min, then shakes by step (2) Swing extraction 60min, be centrifugated 15min later, after taking the organic membrane filtration of supernatant liquid, to filtrate be evaporated under reduced pressure with Organic solvent is removed, cocoa is obtained and toasts fragrant fragrance;
Step (3) weighs cocoa and toasts fragrant 1 part of fragrance, 5 parts of polydextrose and 94 parts of atomized liquid in parts by weight, 20min is stirred at room temperature, is placed in and is protected from light shady place alcoholization for 24 hours, obtains the electronics tobacco tar for having cocoa baking fragrant.
In step (1), the Buddhist Lars spy Luo Keke is brazilian cocoa.The criollo cocoa is that Mexico can It can.The Trinida cocoa is Venezuela's cocoa.
In step (2), the organic solvent is petroleum ether.
In step (3), the atomized liquid is propylene glycol.
Later, the electronics tobacco tar for toasting fragrant fragrance without cocoa using the preparation of step (3) method, as control.And it incite somebody to action this The electronics tobacco tar that embodiment has cocoa baking fragrant is placed in identical electronic cigarette with the electronics tobacco tar for toasting fragrant fragrance without cocoa In, it smokes panel test, the results showed that:Compared with the control group, the present embodiment electronic cigarette baking note is more prominent, and comfort improves, Respiratory tract irritation is substantially reduced.
The sensory evaluation of all embodiments is all carried out according to GB5606.4-2005.
Embodiment 2
A kind of preparation method of the electronics tobacco tar fragrant with cocoa baking, includes the following steps:
Step (1) weighs 60 parts of Buddhist Lars spy Luo Keke, 5 parts of criollo cocoas and 50 parts of spies in parts by weight The powder sample of Li Nida cocoa, is then added 500 parts of polyalcohols and 0.01 part of calcium salt complex thereto, and stirring is equal to mixing After even, 0.5h is reacted at 250 DEG C;
The polyalcohol is ethylene glycol and propylene glycol (mass ratio 1:1);
The Ca-EDTA complex compound;
The product that step (1) obtains is added in 2000 parts of organic solvents by step (2), after ultrasonic extraction 10min, then Concussion extraction 10min, is centrifugated 4min later, after taking the organic membrane filtration of supernatant liquid, is evaporated under reduced pressure to filtrate To remove organic solvent, obtains cocoa and toast fragrant fragrance;
Step (3) weighs cocoa and toasts fragrant 5 parts of fragrance, 20 parts of polydextrose and atomized liquid 75 in parts by weight Part, 30min is stirred at room temperature, is placed in and is protected from light shady place alcoholization 48h, obtain the electronics tobacco tar for having cocoa baking fragrant.
In step (1), the Buddhist Lars spy Luo Keke is Ghana's cocoa and Hainan cocoa (mass ratio 1:1).
The criollo cocoa is Ecuador's cocoa and Taiwan cocoa (mass ratio 1:1).
The Trinida cocoa is Venezuela's cocoa and Indonesia's cocoa (mass ratio 1:1).
In step (2), the organic solvent is n-hexane and chloroform (mass ratio 1:1).
In step (3), the atomized liquid is glycerol.
Later, the electronics tobacco tar for toasting fragrant fragrance without cocoa using the preparation of step (3) method, as control.And it incite somebody to action this The electronics tobacco tar that embodiment has cocoa baking fragrant is placed in identical electronic cigarette with the electronics tobacco tar for toasting fragrant fragrance without cocoa In, it smokes panel test, the results showed that:Compared with the control group, the present embodiment electronic cigarette baking note is dense, and miscellaneous gas is reduced, harmony Increase, respiratory tract irritation is substantially reduced.
Embodiment 3
A kind of preparation method of the electronics tobacco tar fragrant with cocoa baking, includes the following steps:
Step (1) weighs 30 parts of Buddhist Lars spy Luo Keke, 2 parts of criollo cocoas and 18 parts of spies in parts by weight The powder sample of Li Nida cocoa, is then added 200 parts of polyalcohols and 0.1 part of calcium salt complex thereto, and stirring is equal to mixing After even, 1h is reacted at 200 DEG C;
The polyalcohol is glycerol;
The calcium salt complex is calcium glycine complex compound;
The product that step (1) obtains is added in 1000 parts of organic solvents by step (2), after ultrasonic extraction 30min, then Concussion extraction 30min, is centrifugated 4min later, after taking the organic membrane filtration of supernatant liquid, is evaporated under reduced pressure to filtrate To remove organic solvent, obtains cocoa and toast fragrant fragrance;
Step (3) weighs cocoa and toasts fragrant 3 parts of fragrance, 10 parts of polydextrose and atomized liquid 87 in parts by weight Part, 25min is stirred at room temperature, is placed in and is protected from light shady place alcoholization 30h, obtain the electronics tobacco tar for having cocoa baking fragrant.
In step (1), the Buddhist Lars spy Luo Keke is brazilian cocoa and Hainan cocoa (mass ratio 1:1).It is described Criollo cocoa be Ecuador's cocoa.The Trinida cocoa is Venezuela's cocoa.
In step (2), the organic solvent is ethyl acetate.
In step (3), the atomized liquid is propylene glycol.
Later, the electronics tobacco tar for toasting fragrant fragrance without cocoa using the preparation of step (3) method, as control.And it incite somebody to action this The electronics tobacco tar that embodiment has cocoa baking fragrant is placed in identical electronic cigarette with the electronics tobacco tar for toasting fragrant fragrance without cocoa In, it smokes panel test, the results showed that:Compared with the control group, the present embodiment electronic cigarette baking note foot, in good taste, respiratory tract Property is substantially reduced.
Embodiment 4
A kind of preparation method of the electronics tobacco tar fragrant with cocoa baking, includes the following steps:
Step (1) weighs 20 parts of Buddhist Lars spy Luo Keke, 2 parts of criollo cocoas and 30 parts of spies in parts by weight The powder sample of Li Nida cocoa, is then added 300 parts of polyalcohols and 0.2 part of calcium salt complex thereto, and stirring is equal to mixing After even, 2h is reacted at 210 DEG C;
The polyalcohol is propylene glycol;
The calcium salt complex is Ca-EDTA complex compound;
The product that step (1) obtains is added in 2000 parts of organic solvents by step (2), after ultrasonic extraction 20min, then Concussion extraction 15min, is centrifugated 8min later, after taking the organic membrane filtration of supernatant liquid, is evaporated under reduced pressure to filtrate To remove organic solvent, obtains cocoa and toast fragrant fragrance;
Step (3) weighs cocoa and toasts fragrant 5 parts of fragrance, 15 parts of polydextrose and atomized liquid 80 in parts by weight Part, 24min is stirred at room temperature, is placed in and is protected from light shady place alcoholization 40h, obtain the electronics tobacco tar for having cocoa baking fragrant.
In step (1), the Buddhist Lars spy Luo Keke is brazilian cocoa and Ghana's cocoa (mass ratio 1:1).
The criollo cocoa is Mexico's cocoa.
The Trinida cocoa is Venezuela's cocoa and Indonesia's cocoa (mass ratio 1:2).
In step (2), the organic solvent is ethyl alcohol, methylene chloride and methyl acetate (mass ratio 1:2:1).
In step (3), the atomized liquid is propylene glycol.
Later, the electronics tobacco tar for toasting fragrant fragrance without cocoa using the preparation of step (3) method, as control.And it incite somebody to action this The electronics tobacco tar that embodiment has cocoa baking fragrant is placed in identical electronic cigarette with the electronics tobacco tar for toasting fragrant fragrance without cocoa In, it smokes panel test, the results showed that:Compared with the control group, the present embodiment electronic cigarette baking note is prominent, and flue gas is fine and smooth, respiratory tract Irritation is substantially reduced.
Comparative test 1
Comparative sample 1 is prepared according to method in embodiment 1, but calcium salt complex is added without in preparation process, is detected respectively Cocoa toasts the macromoleculars content such as protein, pectin and polysaccharide in fragrant fragrance in comparative sample 1 and embodiment 1.As shown in Table 1, add Enter cocoa after calcium salt complex and toast the macromoleculars content such as protein, pectin and polysaccharide in fragrant fragrance to be substantially reduced.
Table 1
Protein content % Pectin mg/g Polysaccharide mg/g
Control 1 0.3% 31 22
Embodiment 1 0 0 0.1
While electronic cigarette 1 is compareed according to being prepared into described in embodiment 1.Shown by smokeing panel test:Opposite 1 electronic cigarette of embodiment, Control electronic cigarette 1 has certain cocoa baking note but not enough protrudes, while miscellaneous gas is obvious, and irritation is strong, and comfort is poor.
Comparative test 2
Comparative sample 2 is prepared according to method in embodiment 1, but calcium salt complex is changed to calcium chloride in preparation process, respectively It detects cocoa in comparative sample 2 and embodiment 1 and toasts the macromoleculars content such as protein, pectin and polysaccharide in fragrant fragrance.It can by table 2 Know, the macromoleculars content such as protein, pectin and polysaccharide in fragrant fragrance is toasted using cocoa after calcium salt complex and is substantially reduced.
Table 2
While electronic cigarette 2 is compareed according to being prepared into described in embodiment 1.Shown by smokeing panel test:Opposite 1 electronic cigarette of embodiment, Control electronic cigarette 2 has certain cocoa baking note but does not protrude, while miscellaneous gas is obvious, and irritation is strong, and comfort is poor.
Comparative test 3
Comparative sample 3 is prepared according to method in embodiment 1, but reaction temperature is 120 DEG C, detects comparative sample 3 and reality respectively It applies cocoa in example 1 and toasts the macromoleculars content such as protein, pectin and polysaccharide in fragrant fragrance.As shown in Table 3,1 cocoa of embodiment dries The macromoleculars content such as protein, pectin and polysaccharide is substantially reduced in roasting perfume fragrance.
Table 3
Protein content % Pectin mg/g Polysaccharide mg/g
Comparative sample 3 0.3% 22 15
Embodiment 1 0 0 0.1
While electronic cigarette 3 is compareed according to being prepared into described in embodiment 1.Shown by smokeing panel test:Opposite 1 electronic cigarette of embodiment, Control electronic cigarette 3 has certain cocoa baking note but does not protrude very much, while miscellaneous gas is obvious, and irritation is strong, and comfort is poor.
Comparative test 4
Comparative sample 4 is prepared according to method in embodiment 1, but solvent changes tetrahydrofuran into, detects comparative sample 4 and reality respectively It applies cocoa in example 1 and toasts the macromoleculars content such as protein, pectin and polysaccharide in fragrant fragrance.As shown in Table 4,1 cocoa of embodiment dries The macromoleculars content such as protein, pectin and polysaccharide is substantially reduced in roasting perfume fragrance.
Table 4
Protein content % Pectin mg/g Polysaccharide mg/g
Comparative sample 4 0.5% 32 20
Embodiment 1 0 0 0.1
While electronic cigarette 4 is compareed according to being prepared into described in embodiment 1.Shown by smokeing panel test:Opposite 1 electronic cigarette of embodiment, Control electronic cigarette 4 has certain cocoa baking note but does not protrude very much, while miscellaneous gas is obvious, and irritation is strong, and comfort is poor.
Comparative test 5
Comparative sample 5 is prepared according to method in embodiment 1, but ultrasonic extraction, concussion extraction and step with centrifugal separation are changed to Conventional extraction is carried out using separatory funnel, cocoa in comparative sample 5 and embodiment 1 is detected respectively and toasts protein, fruit in fragrant fragrance The macromoleculars content such as glue and polysaccharide.As shown in Table 5,1 cocoa of embodiment toasts big point of protein, pectin and polysaccharide etc. in fragrant fragrance Sub- content is substantially reduced.
Table 5
Protein content % Pectin mg/g Polysaccharide mg/g
Comparative sample 5 0.4% 10 8
Embodiment 1 0 0 0.1
While electronic cigarette 5 is compareed according to being prepared into described in embodiment 1.Shown by smokeing panel test:Opposite 1 electronic cigarette of embodiment, Control electronic cigarette 5 has certain cocoa baking note but does not protrude very much, while miscellaneous gas is obvious, and irritation is strong, and comfort is poor.
Comparative test 6
Comparative sample 6 is prepared according to method in embodiment 1, but polydextrose is added without in preparation process.Simultaneously according to reality It applies described in example 1, is prepared into control electronic cigarette 6.Shown by smokeing panel test:Control electronic cigarette in opposite embodiment 1, compares electronic cigarette 6 cocoas toast note and protrude, and comfort is slightly good, and respiratory tract irritation decreases, but bright without the reduction of 1 electronic cigarette of embodiment It is aobvious.
The basic principles, main features and advantages of the present invention have been shown and described above.The technology of the industry Personnel are it should be appreciated that the present invention is not limited to the above embodiments, and the above embodiments and description only describe this The principle of invention, without departing from the spirit and scope of the present invention, various changes and improvements may be made to the invention, these changes Change and improvement all fall within the protetion scope of the claimed invention.The claimed scope of the invention by appended claims and its Equivalent thereof.

Claims (9)

1. a kind of preparation method of the electronics tobacco tar fragrant with cocoa baking, which is characterized in that include the following steps:
Step(1), in parts by weight, weigh 10~60 parts of Buddhist Lars spy Luo Keke, 1~5 part of criollo cocoa and 5~ Then 100~500 parts of polyalcohols and 0.01~1 part of calcium salt complexing are added in the powder sample of 50 parts of Trinida cocoas thereto Object, stirring react 0.5~3h to after mixing at 150~250 DEG C;
The polyalcohol is the combination of one or more of ethylene glycol, propylene glycol and glycerol;
The calcium salt complex is calcium glycine complex compound or Ca-EDTA complex compound;
Step(2), by step(1)Obtained product is added in organic solvent, after 10~60min of ultrasonic extraction, then shakes extraction 10~60min is taken, is centrifugated later, after taking the organic membrane filtration of supernatant liquid, filtrate is evaporated under reduced pressure to remove Organic solvent obtains cocoa and toasts fragrant fragrance;
Step(3), in parts by weight, weigh cocoa and toast fragrant 1~5 part of fragrance, 5~20 parts of polydextrose and atomized liquid 75 It~94 parts, is stirred at room temperature to after mixing, being placed in and is protected from light shady place and refines 24~48h, obtain toasting with cocoa fragrant Electronics tobacco tar.
2. the preparation method of the electronics tobacco tar fragrant with cocoa baking according to claim 1, which is characterized in that step (1)In, the Buddhist Lars spy Luo Keke is the combination of one or more of brazilian cocoa, Ghana's cocoa and Hainan cocoa.
3. the preparation method of the electronics tobacco tar fragrant with cocoa baking according to claim 1, which is characterized in that step (1)In, the criollo cocoa is the group of one or more of Mexico's cocoa, Ecuador's cocoa and Taiwan cocoa It closes.
4. the preparation method of the electronics tobacco tar fragrant with cocoa baking according to claim 1, which is characterized in that step (1)In, the Trinida cocoa is Venezuela's cocoa and/or Indonesia's cocoa.
5. the preparation method of the electronics tobacco tar fragrant with cocoa baking according to claim 1, which is characterized in that step (2)In, the organic solvent is in petroleum ether, n-hexane, ethyl alcohol, chloroform, methylene chloride, ethyl acetate and methyl acetate One or more of combinations;Consumption of organic solvent is 200~2000 parts by weight.
6. the preparation method of the electronics tobacco tar fragrant with cocoa baking according to claim 1, which is characterized in that step (2)In, the centrifuge separation time is 4~15min.
7. the preparation method of the electronics tobacco tar fragrant with cocoa baking according to claim 1, which is characterized in that step (3)In, the mixing time is 20~30min.
8. the preparation method of the electronics tobacco tar fragrant with cocoa baking according to claim 1, which is characterized in that step (3)In, the atomized liquid is propylene glycol or glycerol.
9. having made from the preparation method with the fragrant electronics tobacco tar of cocoa baking described in claim 1-8 any one can Fragrant electronics tobacco tar can be toasted.
CN201811040689.5A 2018-09-07 2018-09-07 Electronic cigarette oil with cocoa baking fragrance and preparation method thereof Active CN108813742B (en)

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CN106723302A (en) * 2016-12-20 2017-05-31 深圳昱朋科技有限公司 Tobacco tar and preparation method thereof
CN107846971A (en) * 2015-08-13 2018-03-27 菲利普莫里斯生产公司 Flavour capsule for smoking product
CN108113048A (en) * 2017-12-12 2018-06-05 湖北中烟工业有限责任公司 A kind of tobacco juice for electronic smoke of sophora flower odor type and preparation method thereof

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4995407A (en) * 1989-07-25 1991-02-26 International Flavors & Fragrances, Inc. Non-combustible artificial cigarette
WO1999044448A1 (en) * 1998-03-03 1999-09-10 Brown & Williamson Tobacco Corporation A smoking device
CN103284319A (en) * 2013-06-20 2013-09-11 昌宁德康生物科技有限公司 Oral cavity atomized liquid with cytosine replacing nicotine and preparation method thereof
CN104585861A (en) * 2015-01-15 2015-05-06 中国烟草总公司郑州烟草研究院 Preparation method of low-sugar electronic cigarette liquid
CN104824834A (en) * 2015-05-26 2015-08-12 郑悦 Electronic cigarette liquid and preparing method thereof
CN105021727A (en) * 2015-07-10 2015-11-04 云南中烟工业有限责任公司 Accurate characterization and evaluation method of cocoa aroma characteristics of cigarette aroma
CN107846971A (en) * 2015-08-13 2018-03-27 菲利普莫里斯生产公司 Flavour capsule for smoking product
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CN106723315A (en) * 2016-12-01 2017-05-31 华宝香精股份有限公司 A kind of preparation method of electronic cigarette raw material
CN106723302A (en) * 2016-12-20 2017-05-31 深圳昱朋科技有限公司 Tobacco tar and preparation method thereof
CN108113048A (en) * 2017-12-12 2018-06-05 湖北中烟工业有限责任公司 A kind of tobacco juice for electronic smoke of sophora flower odor type and preparation method thereof

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