CN108797125A - A kind of method of spinning sizing agent recycling - Google Patents

A kind of method of spinning sizing agent recycling Download PDF

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Publication number
CN108797125A
CN108797125A CN201810688867.9A CN201810688867A CN108797125A CN 108797125 A CN108797125 A CN 108797125A CN 201810688867 A CN201810688867 A CN 201810688867A CN 108797125 A CN108797125 A CN 108797125A
Authority
CN
China
Prior art keywords
desizing
fabric
ultrasonic cleaning
desizing liquid
sizing agent
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201810688867.9A
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Chinese (zh)
Inventor
吴明
刘亚
马志瑞
陈俊
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Huaian Shengda Weaving Co Ltd
Original Assignee
Huaian Shengda Weaving Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Huaian Shengda Weaving Co Ltd filed Critical Huaian Shengda Weaving Co Ltd
Priority to CN201810688867.9A priority Critical patent/CN108797125A/en
Publication of CN108797125A publication Critical patent/CN108797125A/en
Pending legal-status Critical Current

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Classifications

    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M15/00Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
    • D06M15/19Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
    • D06M15/21Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
    • D06M15/327Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds of unsaturated alcohols or esters thereof
    • D06M15/333Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds of unsaturated alcohols or esters thereof of vinyl acetate; Polyvinylalcohol
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06LDRY-CLEANING, WASHING OR BLEACHING FIBRES, FILAMENTS, THREADS, YARNS, FABRICS, FEATHERS OR MADE-UP FIBROUS GOODS; BLEACHING LEATHER OR FURS
    • D06L1/00Dry-cleaning or washing fibres, filaments, threads, yarns, fabrics, feathers or made-up fibrous goods
    • D06L1/12Dry-cleaning or washing fibres, filaments, threads, yarns, fabrics, feathers or made-up fibrous goods using aqueous solvents
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06LDRY-CLEANING, WASHING OR BLEACHING FIBRES, FILAMENTS, THREADS, YARNS, FABRICS, FEATHERS OR MADE-UP FIBROUS GOODS; BLEACHING LEATHER OR FURS
    • D06L1/00Dry-cleaning or washing fibres, filaments, threads, yarns, fabrics, feathers or made-up fibrous goods
    • D06L1/12Dry-cleaning or washing fibres, filaments, threads, yarns, fabrics, feathers or made-up fibrous goods using aqueous solvents
    • D06L1/14De-sizing
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M2200/00Functionality of the treatment composition and/or properties imparted to the textile material
    • D06M2200/40Reduced friction resistance, lubricant properties; Sizing compositions

Abstract

The invention discloses a kind of methods of spinning sizing agent recycling, include the following steps:Textile processing, the surface floating dust of textile raw material is cleared up, and textile raw material is dried, PVA slurry sizings, textile raw material is immersed in PVA slurries, carry out starching processing, then it completes dry and weaving and obtains fabric A, ultrasonic cleaning, fabric A is put into ultrasonic cleaning pond, and suitable pure water is added into ultrasonic cleaning pond, it controls supersonic cleaning pond and carries out low frequency cleaning, desizing, desizing processing is carried out to the fabric A Jing Guo ultrasonic cleaning, obtain desizing liquid and fabric B, desizing liquid filters, desizing liquid is put into pumping and filtering device and is filtered.The present invention can remove the partial impurities in fabric, be conducive to the purity for improving desizing liquid, facilitate the recycling of desizing liquid, improve probability of recycling success, improve desizing rate, reduce discharging of waste liquid, be conducive to environmental protection.

Description

A kind of method of spinning sizing agent recycling
Technical field
The present invention relates to spinning sizing agent recovery technology field more particularly to a kind of methods of spinning sizing agent recycling.
Background technology
The starching of yarn is to weave a significant process of preamble work, and sizing quality directly influences follow-up weaving.On Slurry can improve wearability, strength, the patch of the filoplume volt of warp thread, reduce degree of stretching, surface is smooth, to bear warp thread in weaving process In the mechanicals efforts that are subject to, make it have good weavability.The factor for influencing starching mainly has selected slurry and starching side Method.Polyvinyl alcohol(Hereinafter referred to as PVA)Slurry has good effect to yarn, this is also current most of enterprise in sizing Process still uses the major reason of PVA slurries.It realizes the recycling to PVA spinning sizing agents, production cost can be saved, reduce Environmental pollution.
Existing spinning sizing agent recovery method, inefficient, the introducing of desizing liquid impurity is more, so now proposing a kind of spinning The method for knitting slurry recycling.
Invention content
Technical problems based on background technology, the present invention propose a kind of method of spinning sizing agent recycling.
A kind of method of spinning sizing agent recycling proposed by the present invention, includes the following steps:
S1:Textile processing, the surface floating dust of textile raw material is cleared up, and is dried to textile raw material;
S2:Textile raw material is immersed in PVA slurries by PVA slurry sizings, carries out starching processing, is then completed dry and is spun It knits to obtain fabric A;
S3:Ultrasonic cleaning puts into fabric A in ultrasonic cleaning pond, and is added into ultrasonic cleaning pond suitable pure Water, control supersonic cleaning pond carry out low frequency cleaning;
S4:Desizing carries out desizing processing to the fabric A Jing Guo ultrasonic cleaning, obtains desizing liquid and fabric B;
S5:Desizing liquid filter, desizing liquid is put into pumping and filtering device and is filtered, and injects suitable pure water, to waste residue into Row rinses;
S6:Acid-base property is adjusted, and carries out pH value detection to the desizing liquid by filtering, and put into reagent and pH value is adjusted;
S7:Desizing liquid recycles, and the desizing liquid adjusted by acid-base property is mixed with PVA slurries, serves as sizing material use.
Preferably, fabric A is put into ultrasonic cleaning pond in the S4, by strong illumination, carries out photocatalytic, It is used in combination flow to be rinsed, controls certain water level, then control the work of ultrasonic cleaning pond, carry out ultrasonication, accelerate to move back Slurry.
Preferably, in the S3, the temperature for injecting pure water is controlled at 15 DEG C or less.
Preferably, in the S1, the moisture for controlling textile raw material is less than 15%.
Preferably, the S4, the water temperature in supersonic cleaning pond control between 70 to 90 DEG C.
Preferably, in the S7, the desizing liquid and the PVA slurry mixed proportions that are adjusted by acid-base property are 1 to 1.
Having the beneficial effect that in the present invention:
1. by the supersonic cleaning of progress, coordinate low-temperature pure water, it is possible to reduce PVA is dissolved in water, can remove the portion in fabric Divide impurity, is conducive to the purity for improving desizing liquid, facilitates the recycling of desizing liquid.
2. by the photocatalytic of progress, the impurity introduction volume in desizing liquid is reduced, the recycling quality of desizing liquid is improved, carries High probability of recycling success coordinates ultrasonication, improves desizing rate, reduces discharging of waste liquid, is conducive to environmental protection.
Description of the drawings
Fig. 1 is a kind of flow diagram of the method for spinning sizing agent recycling proposed by the present invention;
Fig. 2 is a kind of flow diagram of the method desizing of spinning sizing agent recycling proposed by the present invention.
Specific implementation mode
Following will be combined with the drawings in the embodiments of the present invention, and technical solution in the embodiment of the present invention carries out clear, complete Site preparation describes, it is clear that described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.
Embodiment 1, referring to Fig.1-2, a kind of method of spinning sizing agent recycling includes the following steps:
S1:Textile processing, the surface floating dust of textile raw material is cleared up, and is dried to textile raw material;
S2:Textile raw material is immersed in PVA slurries by PVA slurry sizings, carries out starching processing, is then completed dry and is spun It knits to obtain fabric A;
S3:Ultrasonic cleaning puts into fabric A in ultrasonic cleaning pond, and is added into ultrasonic cleaning pond suitable pure Water, control supersonic cleaning pond carry out low frequency cleaning;
S4:Desizing carries out desizing processing to the fabric A Jing Guo ultrasonic cleaning, obtains desizing liquid and fabric B;
S5:Desizing liquid filter, desizing liquid is put into pumping and filtering device and is filtered, and injects suitable pure water, to waste residue into Row rinses;
S6:Acid-base property is adjusted, and carries out pH value detection to the desizing liquid by filtering, and put into reagent and pH value is adjusted;
S7:Desizing liquid recycles, and the desizing liquid adjusted by acid-base property is mixed with PVA slurries, serves as sizing material use.
In the present invention, fabric A is put into ultrasonic cleaning pond in S4, by strong illumination, carries out photocatalytic, and It is rinsed with flow, controls certain water level, then controlled the work of ultrasonic cleaning pond, carry out ultrasonication, accelerate desizing, In S3, the temperature for injecting pure water is controlled at 15 DEG C hereinafter, in S1, and the moisture for controlling textile raw material is less than 15%, S4, ultrasound Wave cleans the water temperature in pond and controls at 70 DEG C, and in S7, the desizing liquid and the PVA slurry mixed proportions that are adjusted by acid-base property are 1 ratio 1。
Embodiment 2, referring to Fig.1-2, a kind of method of spinning sizing agent recycling includes the following steps:
S1:Textile processing, the surface floating dust of textile raw material is cleared up, and is dried to textile raw material;
S2:Textile raw material is immersed in PVA slurries by PVA slurry sizings, carries out starching processing, is then completed dry and is spun It knits to obtain fabric A;
S3:Ultrasonic cleaning puts into fabric A in ultrasonic cleaning pond, and is added into ultrasonic cleaning pond suitable pure Water, control supersonic cleaning pond carry out low frequency cleaning;
S4:Desizing carries out desizing processing to the fabric A Jing Guo ultrasonic cleaning, obtains desizing liquid and fabric B;
S5:Desizing liquid filter, desizing liquid is put into pumping and filtering device and is filtered, and injects suitable pure water, to waste residue into Row rinses;
S6:Acid-base property is adjusted, and carries out pH value detection to the desizing liquid by filtering, and put into reagent and pH value is adjusted;
S7:Desizing liquid recycles, and the desizing liquid adjusted by acid-base property is mixed with PVA slurries, serves as sizing material use.
In the present invention, fabric A is put into ultrasonic cleaning pond in S4, by strong illumination, carries out photocatalytic, and It is rinsed with flow, controls certain water level, then controlled the work of ultrasonic cleaning pond, carry out ultrasonication, accelerate desizing, In S3, the temperature for injecting pure water is controlled at 15 DEG C hereinafter, in S1, and the moisture for controlling textile raw material is less than 15%, S4, ultrasound Wave cleans the water temperature in pond and controls at 90 DEG C, and in S7, the desizing liquid and the PVA slurry mixed proportions that are adjusted by acid-base property are 1 to 1
The foregoing is only a preferred embodiment of the present invention, but scope of protection of the present invention is not limited thereto, and it is any Those familiar with the art in the technical scope disclosed by the present invention, according to the technique and scheme of the present invention and its invents Design is subject to equivalent substitution or change, should be covered by the protection scope of the present invention.

Claims (6)

1. a kind of method of spinning sizing agent recycling, which is characterized in that include the following steps:
S1:Textile processing, the surface floating dust of textile raw material is cleared up, and is dried to textile raw material;
S2:Textile raw material is immersed in PVA slurries by PVA slurry sizings, carries out starching processing, is then completed dry and is spun It knits to obtain fabric A;
S3:Ultrasonic cleaning puts into fabric A in ultrasonic cleaning pond, and is added into ultrasonic cleaning pond suitable pure Water, control supersonic cleaning pond carry out low frequency cleaning;
S4:Desizing carries out desizing processing to the fabric A Jing Guo ultrasonic cleaning, obtains desizing liquid and fabric B;
S5:Desizing liquid filter, desizing liquid is put into pumping and filtering device and is filtered, and injects suitable pure water, to waste residue into Row rinses;
S6:Acid-base property is adjusted, and carries out pH value detection to the desizing liquid by filtering, and put into reagent and pH value is adjusted;
S7:Desizing liquid recycles, and the desizing liquid adjusted by acid-base property is mixed with PVA slurries, serves as sizing material use.
2. a kind of method of spinning sizing agent recycling according to claim 1, which is characterized in that will be knitted in the S4 Object A is put into ultrasonic cleaning pond, by strong illumination, is carried out photocatalytic, is used in combination flow to be rinsed, controls certain water Then position controls the work of ultrasonic cleaning pond, carries out ultrasonication, accelerates desizing.
3. a kind of method of spinning sizing agent recycling according to claim 1, which is characterized in that in the S3, note The temperature for entering pure water is controlled at 15 DEG C or less.
4. a kind of method of spinning sizing agent recycling according to claim 1, which is characterized in that in the S1, control The moisture of textile raw material processed is less than 15%.
5. a kind of method of spinning sizing agent recycling according to claim 1, which is characterized in that the S4, ultrasound Wave cleans the water temperature in pond and controls between 70 to 90 DEG C.
6. a kind of method of spinning sizing agent recycling according to claim 1, which is characterized in that in the S7, warp It is 1 to 1 to cross the desizing liquid of acid-base property adjusting and PVA slurry mixed proportions.
CN201810688867.9A 2018-06-28 2018-06-28 A kind of method of spinning sizing agent recycling Pending CN108797125A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201810688867.9A CN108797125A (en) 2018-06-28 2018-06-28 A kind of method of spinning sizing agent recycling

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Application Number Priority Date Filing Date Title
CN201810688867.9A CN108797125A (en) 2018-06-28 2018-06-28 A kind of method of spinning sizing agent recycling

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Publication Number Publication Date
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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN114292437A (en) * 2021-12-31 2022-04-08 石狮市中纺学服装及配饰产业研究院 Method for extracting PVA (polyvinyl alcohol) in slurry by supercritical carbon dioxide

Citations (7)

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Publication number Priority date Publication date Assignee Title
CN2649617Y (en) * 2003-11-08 2004-10-20 江阴市科达机械电子有限公司 Double-side supersonic wave device
CN101629368A (en) * 2009-08-14 2010-01-20 李建华 Ultrasonic wave desizing device
CN101643998A (en) * 2009-08-25 2010-02-10 苏州大学 Treatment method of textile
CN102978894A (en) * 2012-12-11 2013-03-20 愉悦家纺有限公司 Printing and dyeing pretreatment process
CN205617084U (en) * 2016-05-09 2016-10-05 南通职业大学 Detachable ultrasonic wave destarch economizer
CN107724082A (en) * 2017-11-28 2018-02-23 翁书豪 A kind of destarch fabric production technology
CN107815850A (en) * 2017-11-14 2018-03-20 江阴市海特网络科技有限公司 A kind of method for material secondary use of weaving

Patent Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN2649617Y (en) * 2003-11-08 2004-10-20 江阴市科达机械电子有限公司 Double-side supersonic wave device
CN101629368A (en) * 2009-08-14 2010-01-20 李建华 Ultrasonic wave desizing device
CN101643998A (en) * 2009-08-25 2010-02-10 苏州大学 Treatment method of textile
CN102978894A (en) * 2012-12-11 2013-03-20 愉悦家纺有限公司 Printing and dyeing pretreatment process
CN205617084U (en) * 2016-05-09 2016-10-05 南通职业大学 Detachable ultrasonic wave destarch economizer
CN107815850A (en) * 2017-11-14 2018-03-20 江阴市海特网络科技有限公司 A kind of method for material secondary use of weaving
CN107724082A (en) * 2017-11-28 2018-02-23 翁书豪 A kind of destarch fabric production technology

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Title
但卫华等: "《轻化工清洁生产技术》", 30 November 2016, 中国纺织出版社 *
姜兆华等: "《应用表面化学与技术》", 28 February 2009, 哈尔滨工业大学出版社 *
张世源: "《生态纺织工程》", 31 May 2004, 中国纺织出版社 *

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN114292437A (en) * 2021-12-31 2022-04-08 石狮市中纺学服装及配饰产业研究院 Method for extracting PVA (polyvinyl alcohol) in slurry by supercritical carbon dioxide

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Address after: 210000 industrial project concentration area of Huangma Township, Qingpu District, Huai'an City, Jiangsu Province

Applicant after: Huaian Shengwei Weaving Co., Ltd

Address before: 210000 industrial project concentration area of Huangma Township, Qingpu District, Huai'an City, Jiangsu Province

Applicant before: HUAI'AN SHENGWEI WEAVING Co.,Ltd.

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Application publication date: 20181113

RJ01 Rejection of invention patent application after publication