CN108772037A - A kind of pulsed convection reaction kettle with double-stirring machine structure - Google Patents

A kind of pulsed convection reaction kettle with double-stirring machine structure Download PDF

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Publication number
CN108772037A
CN108772037A CN201810641294.4A CN201810641294A CN108772037A CN 108772037 A CN108772037 A CN 108772037A CN 201810641294 A CN201810641294 A CN 201810641294A CN 108772037 A CN108772037 A CN 108772037A
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CN
China
Prior art keywords
fixed plate
fixedly connected
autoclave body
pulsed
double
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Pending
Application number
CN201810641294.4A
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Chinese (zh)
Inventor
徐铭壕
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Individual
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Individual
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Priority to CN201810641294.4A priority Critical patent/CN108772037A/en
Publication of CN108772037A publication Critical patent/CN108772037A/en
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18Stationary reactors having moving elements inside
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053Details of the reactor
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053Details of the reactor
    • B01J19/0066Stirrers
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J4/00Feed or outlet devices; Feed or outlet control devices
    • B01J4/001Feed or outlet devices as such, e.g. feeding tubes
    • B01J4/002Nozzle-type elements

Abstract

The invention discloses a kind of pulsed convection reaction kettles with double-stirring machine structure,Including autoclave body,Inlet tube,Agitating shaft,Discharge gate and cushion block,The upper surface left and right ends of the autoclave body have been respectively fixedly connected with left fixed plate,Right fixed plate,The left side wall of left fixed plate is fixedly connected with first motor,Left fixed plate,Bent axle is equipped between right fixed plate,It is arranged with connecting rod at the axle journal of bent axle,The lower end of connecting rod is hinged with fixed plate,The left and right ends of fixed plate have been respectively fixedly connected with portable pillar,The lower end of portable pillar, which passes through, to be stretched at the top of autoclave body in autoclave body,The lower end of portable pillar is arranged with sleeve,The present apparatus is by being arranged two hydrojet disks,It piles up after so that two kinds of liquid reactants is sprayed,Generate pulsed convection current,Two kinds of liquid reactants are made to be sufficiently mixed,Improve reaction efficiency,Liquid reactants are stirred using stirring rod,Liquid reactants are made to be more fully mixed,Playing certain cushioning effect using leaf spring reduces the vibration generated when the present apparatus is run.

Description

A kind of pulsed convection reaction kettle with double-stirring machine structure
Technical field
The present invention relates to a kind of field of chemical equipment, specifically a kind of pulsed convection reaction with double-stirring machine structure Kettle.
Background technology
The broad understanding of reaction kettle has the container physically or chemically reacted, is matched with parameter by the structure design to container It sets, realizes the mixture function of the heating of technological requirement, evaporation, cooling and low high speed.
Reaction kettle is widely used in oil, chemical industry, rubber, pesticide, dyestuff, medicine, food, for complete vulcanization, nitrification, Pressure vessel of the technical process such as hydrogenation, hydrocarbonylation, polymerization, condensation, such as reactor, reaction pot, decomposition pot, polymeric kettle etc.;Material Matter generally has carbon manganese steel, stainless steel, zirconium, Ni-based(Kazakhstan, Monel, inconel)Alloy and other composite materials.
In chemical field, it is often necessary to inject in reaction kettle two kinds of liquid reactants and react, existing liquid is anti- Answer kettle during the reaction, it is difficult to accomplish that two kinds of liquid reactants are sufficiently mixed, reaction is not enough.
Invention content
It is above-mentioned to solve the purpose of the present invention is to provide a kind of pulsed convection reaction kettle with double-stirring machine structure The problem of being proposed in background technology.
To achieve the above object, the present invention provides the following technical solutions:
A kind of pulsed convection reaction kettle with double-stirring machine structure, including autoclave body, inlet tube, agitating shaft, discharge gate and pad The upper surface left and right ends of block, the autoclave body have been respectively fixedly connected with left fixed plate, right fixed plate, and the left side wall of left fixed plate is solid Surely be connected with first motor, be equipped with bent axle between left fixed plate, right fixed plate, the left and right ends of bent axle respectively with left fixed plate, Right fixed plate rotation connection, the axle stretch end of first motor pass through the side wall of left fixed plate to be connected with the left end of bent axle, bent axle Connecting rod is arranged at axle journal, connecting rod is connect with crank rotation, and the lower end of connecting rod is hinged with fixed plate, the left and right ends point of fixed plate It is not fixedly connected with portable pillar, the lower end of portable pillar, which passes through, to be stretched at the top of autoclave body in autoclave body, and the lower end of portable pillar is arranged with set Cylinder, portable pillar are slidably connected with sleeve, are fixedly connected at the top of the upper end of sleeve and autoclave body, the left and right sides of sleeve is installed respectively There are drain pipe, inlet tube, check valve is separately installed on drain pipe, inlet tube, two opposite sides of sleeve are respectively equipped with spray Spill disk.
As a further solution of the present invention:The sprinkling disk inner hollow, sprinkling disk are connected to drain pipe, two sprinklings Disk it is opposite nozzle is distributed on one side.
As further scheme of the invention:The lower surface of the autoclave body is fixedly connected with the second motor, the second motor Axle stretch end pass through autoclave body bottom stretch into autoclave body, the axle stretch end of the second motor is arranged with driving gear, a left side for driving gear Right both sides are respectively equipped with agitating shaft, and the lower end of agitating shaft and the lower rotation of autoclave body connect, and the lower end of agitating shaft is arranged with driven Gear, driven gear are engaged with driving gear.
As further scheme of the invention:It is fixedly connected with paddle at the top of the agitating shaft.
As further scheme of the invention:Discharge gate is installed below the right side wall of the autoclave body, is pacified on discharge gate Equipped with valve.
As further scheme of the invention:The bottom of the autoclave body is fixedly connected with fixed frame, and fixed frame shares two It is a, it is symmetrically mounted on the left and right sides of the second motor, leaf spring is fixedly connected on fixed frame, fixed frame is fixedly connected on leaf spring The both ends at middle part, leaf spring have been respectively fixedly connected with cushion block.
Compared with prior art, the beneficial effects of the invention are as follows:The present apparatus makes two kinds of liquid by the way that two hydrojet disks are arranged Reactant is piled up after spraying, and generates pulsed convection current, two kinds of liquid reactants is made to be sufficiently mixed, and improves reaction efficiency, Liquid reactants are stirred using stirring rod, so that liquid reactants is more fully mixed, certain cushioning effect is played using leaf spring Reduce the vibration generated when present apparatus operation.
Description of the drawings
Fig. 1 is the structural schematic diagram of the pulsed convection reaction kettle with double-stirring machine structure;
Fig. 2 is the left view of leaf spring in the pulsed convection reaction kettle with double-stirring machine structure;
Fig. 3 is the vertical view of the pulsed convection reaction kettle with double-stirring machine structure.
In figure:1- autoclave bodies;The left fixed plates of 2-;The right fixed plates of 3-;4- first motors;5- bent axles;6- connecting rods;7- fixed plates; 8- portable pillars;9- sleeves;10- drain pipes;11- sprays disk;12- inlet tubes;The second motors of 13-;14- agitating shafts;15- is stirred Stick;16- driven gears;17- driving gears;18- paddles;19- discharge gates;20- fixed frames;21- leaf springs;22- cushion blocks.
Specific implementation mode
Following will be combined with the drawings in the embodiments of the present invention, and technical solution in the embodiment of the present invention carries out clear, complete Site preparation describes, it is clear that described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.It is based on Embodiment in the present invention, it is obtained by those of ordinary skill in the art without making creative efforts every other Embodiment shall fall within the protection scope of the present invention.
Embodiment 1
Please refer to Fig.1-3, in the embodiment of the present invention, a kind of pulsed convection reaction kettle with double-stirring machine structure, including kettle The upper surface left and right ends of body 1, inlet tube 12, agitating shaft 14, discharge gate 19 and cushion block 22, autoclave body 1 have been respectively fixedly connected with a left side Fixed plate 2, right fixed plate 3, the left side wall of left fixed plate 2 are fixedly connected with first motor 4, left fixed plate 2, right fixed plate 3 it Between be equipped with bent axle 5, the left and right ends of bent axle 5 are rotatablely connected with left fixed plate 2, right fixed plate 3 respectively, and the axis of first motor 4 is stretched It holds the side wall across left fixed plate 2 to be connected with the left end of bent axle 5, connecting rod 6, connecting rod 6 and bent axle is arranged at the axle journal of bent axle 5 5 rotation connections, the lower end of connecting rod 6 are hinged with fixed plate 7, and the left and right ends of fixed plate 7 have been respectively fixedly connected with portable pillar 8, living The lower end of dynamic column 8 passes through the top of autoclave body 1 to stretch into autoclave body 1, and the lower end of portable pillar 8 is arranged with sleeve 9, portable pillar 8 and sleeve 9 It is slidably connected, the upper end of sleeve 9 is fixedly connected with the top of autoclave body 1, and band dynamic crankshaft 5 rotates when first motor 4 is run, Jin Ertong Crossing connecting rod 6 drives fixed plate 7 to move up and down, to drive portable pillar 8 to be moved up and down in sleeve 9, the left and right sides point of sleeve 9 Drain pipe 10, inlet tube 12 are not installed, check valve is separately installed on drain pipe 10, inlet tube 12, reaction solution can pass through Inlet tube 12 enters in sleeve 9, and the reaction solution in sleeve 9 can be discharged by drain pipe 10, the opposite side of two sleeves 9 point Disk 11 She You not be sprayed, 11 inner hollow of disk is sprayed, sprinkling disk 11 is connected to drain pipe 10, the opposite one side of two sprinkling disks 11 Nozzle is distributed with, when portable pillar 8 moves up, the pressure in sleeve 9 reduces, and liquid reactants are entered by inlet tube 12 to be covered In cylinder 9, when portable pillar 8 moves down, the pressure in sleeve 9 increases, and liquid reactants enter sprinkling disk by drain pipe 10 It in 11, is sprayed from nozzle, two kinds of liquid reactants are piled up after spraying, and are generated pulsed convection current, are made two kinds of liquid reactions Object is sufficiently mixed, and improves reaction efficiency, the lower surface of autoclave body 1 is fixedly connected with the second motor 13, the axle stretch end of the second motor 13 It is stretched into autoclave body 1 across the bottom of autoclave body 1, the axle stretch end of the second motor 13 is arranged with driving gear 17, a left side for driving gear 17 Right both sides are respectively equipped with agitating shaft 14, and the lower end of agitating shaft 14 is connect with the lower rotation of autoclave body 1, and the lower end of agitating shaft 14 is arranged There are driven gear 16, driven gear 16 to be engaged with driving gear 17, drives driving gear 17 to rotate when the second motor 13 is run, from And drive agitating shaft 14 to rotate by driven gear 16, stirring rod 15 is distributed on agitating shaft 14, liquid is stirred using stirring rod 15 Precursor reactant object, makes liquid reactants be more fully mixed, and the top of agitating shaft 14 is fixedly connected with paddle 18, the right side of autoclave body 1 Discharge gate 19 is installed below side wall, valve is installed on discharge gate 19.
The present invention operation principle be:Two kinds of liquid reactants to be reacted are injected into sleeve 9 by inlet tube 12 respectively It is interior, start first motor 4, band dynamic crankshaft 5 rotates, and then drives fixed plate 7 to move up and down by connecting rod 6, to drive activity Column 8 moves up and down in sleeve 9, and when portable pillar 8 moves up, the pressure in sleeve 9 reduces, and liquid reactants pass through feed liquor Pipe 12 enters in sleeve 9, and when portable pillar 8 moves down, the pressure in sleeve 9 increases, and liquid reactants pass through drain pipe 10 It into sprinkling disk 11, is sprayed from nozzle, two kinds of liquid reactants are piled up after spraying, and are generated pulsed convection current, are made two Kind liquid reactants are sufficiently mixed, and improve reaction efficiency, start the second motor 13, drive driving gear 17 to rotate, to pass through Driven gear 16 drives agitating shaft 14 to rotate, and stirring rod 15 is distributed on agitating shaft 14, and liquid reactions are stirred using stirring rod 15 Object makes liquid reactants be more fully mixed.
Embodiment 2
On the basis of embodiment 1, the bottom of autoclave body 1 is fixedly connected with fixed frame 20, and fixed frame 20 is symmetrically installed there are two being total to In the left and right sides of the second motor 13, leaf spring 21 is fixedly connected on fixed frame 20, fixed frame 20 is fixedly connected on leaf spring 21 The both ends at middle part, leaf spring 21 have been respectively fixedly connected with cushion block 22, and playing certain cushioning effect using leaf spring 21 reduces the present apparatus The vibration generated when operation.
It should be strongly noted that in the present invention, autoclave body 1, inlet tube 12, agitating shaft 14, discharge gate 19 and cushion block 22 are The direct application of the prior art, two pieces of hydrojet disks of setting, the innovative point that double-stirring machine structure is the present invention, so that two kinds of liquid are anti- Answer object mixing more uniform, reaction is more abundant.
It is obvious to a person skilled in the art that invention is not limited to the details of the above exemplary embodiments, Er Qie In the case of without departing substantially from spirit or essential attributes of the invention, the present invention can be realized in other specific forms.Therefore, no matter From the point of view of which point, the present embodiments are to be considered as illustrative and not restrictive, and the scope of the present invention is by appended power Profit requires rather than above description limits, it is intended that all by what is fallen within the meaning and scope of the equivalent requirements of the claims Variation is included within the present invention.Any reference signs in the claims should not be construed as limiting the involved claims.
In addition, it should be understood that although this specification is described in terms of embodiments, but not each embodiment is only wrapped Containing an independent technical solution, this description of the specification is merely for the sake of clarity, and those skilled in the art should It considers the specification as a whole, the technical solutions in the various embodiments may also be suitably combined, forms those skilled in the art The other embodiment being appreciated that.

Claims (6)

1. a kind of pulsed convection reaction kettle with double-stirring machine structure, including autoclave body(1), inlet tube(12), agitating shaft (14), discharge gate(19)And cushion block(22), which is characterized in that the autoclave body(1)Upper surface left and right ends be respectively fixedly connected with There is left fixed plate(2), right fixed plate(3), left fixed plate(2)Left side wall be fixedly connected with first motor(4), left fixed plate (2), right fixed plate(3)Between be equipped with bent axle(5), bent axle(5)Left and right ends respectively with left fixed plate(2), right fixed plate(3) Rotation connection, first motor(4)Axle stretch end pass through left fixed plate(2)Side wall and bent axle(5)Left end be connected, bent axle (5)Axle journal at be arranged with connecting rod(6), connecting rod(6)With bent axle(5)Rotation connection, connecting rod(6)Lower end be hinged with fixed plate (7), fixed plate(7)Left and right ends be respectively fixedly connected with portable pillar(8), portable pillar(8)Lower end pass through autoclave body(1)Top Portion stretches into autoclave body(1)It is interior, portable pillar(8)Lower end be arranged with sleeve(9), portable pillar(8)With sleeve(9)It is slidably connected, sleeve (9)Upper end and autoclave body(1)Top be fixedly connected, sleeve(9)The left and right sides be separately installed with drain pipe(10), inlet tube (12), drain pipe(10), inlet tube(12)On be separately installed with check valve, two sleeves(9)Opposite side is respectively equipped with spray Spill disk(11).
2. the pulsed convection reaction kettle according to claim 1 with double-stirring machine structure, which is characterized in that the spray Spill disk(11)Inner hollow sprays disk(11)With drain pipe(10)Connection, two sprinkling disks(11)Opposite is distributed with spray on one side Head.
3. the pulsed convection reaction kettle according to claim 1 with double-stirring machine structure, which is characterized in that the kettle Body(1)Lower surface be fixedly connected with the second motor(13), the second motor(13)Axle stretch end pass through autoclave body(1)Bottom stretch into Autoclave body(1)It is interior, the second motor(13)Axle stretch end be arranged with driving gear(17), driving gear(17)The left and right sides set respectively There is agitating shaft(14), agitating shaft(14)Lower end and autoclave body(1)Lower rotation connection, agitating shaft(14)Lower end be arranged with from Moving gear(16), driven gear(16)With driving gear(17)Engagement.
4. the pulsed convection reaction kettle according to claim 3 with double-stirring machine structure, which is characterized in that described to stir Mix axis(14)Top be fixedly connected with paddle(18).
5. the pulsed convection reaction kettle according to claim 1 with double-stirring machine structure, which is characterized in that the kettle Body(1)Right side wall below discharge gate is installed(19), discharge gate(19)On valve is installed.
6. the pulsed convection reaction kettle according to claim 1 with double-stirring machine structure, which is characterized in that the kettle Body(1)Bottom be fixedly connected with fixed frame(20), fixed frame(20)There are two altogether, it is symmetrically mounted on the second motor(13)A left side Right both sides, fixed frame(20)On be fixedly connected with leaf spring(21), fixed frame(20)It is fixedly connected on leaf spring(21)Middle part, leaf spring (21)Both ends be respectively fixedly connected with cushion block(22).
CN201810641294.4A 2018-06-21 2018-06-21 A kind of pulsed convection reaction kettle with double-stirring machine structure Pending CN108772037A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201810641294.4A CN108772037A (en) 2018-06-21 2018-06-21 A kind of pulsed convection reaction kettle with double-stirring machine structure

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201810641294.4A CN108772037A (en) 2018-06-21 2018-06-21 A kind of pulsed convection reaction kettle with double-stirring machine structure

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CN108772037A true CN108772037A (en) 2018-11-09

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109692642A (en) * 2019-01-16 2019-04-30 江苏新鑫隆医药科技股份有限公司 Two-in-one filter device
CN113559812A (en) * 2021-08-25 2021-10-29 福建永荣科技有限公司 Device and method for treating hydrogenation tail gas

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN206793660U (en) * 2017-05-18 2017-12-26 佛山市尚峰高分子科技有限公司 A kind of vertical response kettle
CN107739089A (en) * 2017-12-01 2018-02-27 赣州研顺飞科技有限公司 A kind of circulating sewage aeration apparatus
CN108043349A (en) * 2017-12-06 2018-05-18 郑州诚合信息技术有限公司 A kind of solid-liquid reaction kettle for increasing reaction rate
CN108079924A (en) * 2017-12-06 2018-05-29 郑州诚合信息技术有限公司 A kind of solid-liquid reaction kettle with crushing function
CN108097143A (en) * 2017-12-21 2018-06-01 张兴业 A kind of chemical liquid raw material injecting type mixing arrangement

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN206793660U (en) * 2017-05-18 2017-12-26 佛山市尚峰高分子科技有限公司 A kind of vertical response kettle
CN107739089A (en) * 2017-12-01 2018-02-27 赣州研顺飞科技有限公司 A kind of circulating sewage aeration apparatus
CN108043349A (en) * 2017-12-06 2018-05-18 郑州诚合信息技术有限公司 A kind of solid-liquid reaction kettle for increasing reaction rate
CN108079924A (en) * 2017-12-06 2018-05-29 郑州诚合信息技术有限公司 A kind of solid-liquid reaction kettle with crushing function
CN108097143A (en) * 2017-12-21 2018-06-01 张兴业 A kind of chemical liquid raw material injecting type mixing arrangement

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109692642A (en) * 2019-01-16 2019-04-30 江苏新鑫隆医药科技股份有限公司 Two-in-one filter device
CN113559812A (en) * 2021-08-25 2021-10-29 福建永荣科技有限公司 Device and method for treating hydrogenation tail gas
CN113559812B (en) * 2021-08-25 2022-09-16 福建永荣科技有限公司 Device and method for treating hydrogenation tail gas

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Application publication date: 20181109