CN108751848A - A kind of high-strength water-resistance tile adhesives and preparation method thereof - Google Patents
A kind of high-strength water-resistance tile adhesives and preparation method thereof Download PDFInfo
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- CN108751848A CN108751848A CN201810657902.0A CN201810657902A CN108751848A CN 108751848 A CN108751848 A CN 108751848A CN 201810657902 A CN201810657902 A CN 201810657902A CN 108751848 A CN108751848 A CN 108751848A
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- parts
- powder
- resistance
- tile adhesives
- strength water
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Classifications
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B28/00—Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements
- C04B28/02—Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements containing hydraulic cements other than calcium sulfates
- C04B28/04—Portland cements
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2111/00—Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
- C04B2111/00474—Uses not provided for elsewhere in C04B2111/00
- C04B2111/00637—Uses not provided for elsewhere in C04B2111/00 as glue or binder for uniting building or structural materials
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2201/00—Mortars, concrete or artificial stone characterised by specific physical values
- C04B2201/50—Mortars, concrete or artificial stone characterised by specific physical values for the mechanical strength
Abstract
The invention discloses a kind of high-strength water-resistance tile adhesives and preparation method thereof, are made of the raw material of following parts by weight：50-60 parts of Portland cement, 20-30 parts of bunt gypsum, 28-34 parts of slate, 22-28 parts of beidellite, 15-20 parts of diabase, magnesium is powder 10-15 parts strong, 5-10 parts of torispherical glass powder, 8-16 parts of lithium magnesium silicate, vinyl acetate-tertiary ethylene carbonate -4-8 parts of butyl acrylate ternary polymerization latex powder, 3-6 parts of edible seaweed powder, 2-5 parts of ghatti gum, 1-2 parts of the chloro- N- of 4- (stearmide methyl) pyridine, 0.5-1.5 parts of rosin acid calcium soap, 0.5-1.5 parts of zirconium stearate.Adhesive produced by the present invention not only has higher adhesive strength, also has excellent water resistance, heat resistance, acid-alkali-corrosive-resisting, resistance to ag(e)ing, freeze-thaw resistance and weatherability, safety and environmental protection is easy for construction, is a kind of ideal tile bonding material.
Description
Invention field
The present invention relates to a kind of flocculation deposited formulations and preparation method thereof, and in particular to a kind of high-strength water-resistance ceramic tile bonding
Agent and preparation method thereof.
Background technology
Tile adhesives, also known as glue for tile, ceramic tile bond or ceramic tile viscose glue mud, be mainly used for paste ceramic tile, face brick,
The ornament materials such as brick are widely used in the facing decoration places of the buildings such as inside and outside metope, ground, bathroom, kitchen.Ceramic tile is viscous at present
Knot agent mostly uses cement mortar, this ceramic tile bond the shortcomings that there is also adhesion strength is low and poor water resistance, influences ceramic tile
Durability, ceramic tile be easy peel off.
Invention content
The purpose of the present invention is to provide a kind of high-strength water-resistance tile adhesives and preparation method thereof.It is produced by the present invention
Adhesive not only have higher adhesive strength, also have excellent water resistance, heat resistance, acid-alkali-corrosive-resisting, resistance to ag(e)ing,
Freeze-thaw resistance and weatherability.
To achieve the above object, the technical solution used in the present invention is：
The invention discloses a kind of high-strength water-resistance tile adhesives, are made of the raw material of following parts by weight：
50-60 parts of Portland cement, 20-30 parts of bunt gypsum, 28-34 parts of slate, 22-28 parts of beidellite, diabase
15-20 parts, magnesium is powder 10-15 parts strong, 5-10 parts of torispherical glass powder, 8-16 parts of lithium magnesium silicate, vinyl acetate-versatic acid ethylene
Ester -4-8 parts of butyl acrylate ternary polymerization latex powder, 3-6 parts of edible seaweed powder, 2-5 parts of ghatti gum, 4- chloro- N- (stearmide first
Base) 1-2 parts of pyridine, 0.5-1.5 parts of rosin acid calcium soap, 0.5-1.5 parts of zirconium stearate.
Preferably, a kind of high-strength water-resistance tile adhesives, are made of the raw material of following parts by weight：Normal silicate water
54-56 parts of mud, 23-27 parts of bunt gypsum, 30-32 parts of slate, 24-26 parts of beidellite, 17-19 parts of diabase, the strong powder 12-14 of magnesium
Part, 6-8 parts of torispherical glass powder, 10-14 parts of lithium magnesium silicate, vinyl acetate-tertiary ethylene carbonate-butyl acrylate ternary polymerization
5-7 parts of latex powder, 4-5 parts of edible seaweed powder, 3-4 parts of ghatti gum, 1.2-1.8 parts of the chloro- N- of 4- (stearmide methyl) pyridine, rosin
Sour calcium soap 0.8-1.2 parts, 0.9-1.1 parts of zirconium stearate.
Preferably, a kind of high-strength water-resistance tile adhesives, are made of the raw material of following parts by weight：Normal silicate water
55 parts of mud, 25 parts of bunt gypsum, 31 parts of slate, 25 parts of beidellite, 18 parts of diabase, 13 parts of the strong powder of magnesium, 7 parts of torispherical glass powder,
12 parts of lithium magnesium silicate, vinyl acetate-tertiary ethylene carbonate -6 parts of butyl acrylate ternary polymerization latex powder, 4.5 parts of edible seaweed powder, print
3.5 parts of degree natural gum, 1.5 parts of the chloro- N- of 4- (stearmide methyl) pyridine, 1 part of rosin acid calcium soap, 1 part of zirconium stearate.
The invention also discloses a kind of preparation methods of high-strength water-resistance tile adhesives, include the following steps：
(1) bunt gypsum, slate, beidellite, diabase are mixed, is crushed, sieving, for use；
(2) edible seaweed powder, the strong powder of magnesium, torispherical glass powder are added to together in crushed material made from step (1), stirring is mixed
15-25min is closed, mixture A is obtained；
(3) lithium magnesium silicate, ghatti gum, ethylene-tertiary ethylene carbonate-butyl acrylate ternary polymerization latex powder are added
Into Portland cement, it is stirred 5-10min, obtains mixture B；
(4) by the chloro- N- of mixture A and 4- (stearmide methyl) pyridine made from step (1), rosin acid calcium soap, hard
Resin acid zirconium is added to together in mixture B, is stirred 10-20min, discharging packing.
Preferably, it is 300-500 mesh that grit number is crossed described in step (1).
Preferably, speed of agitator described in step (2) is 50-100r/min.
Preferably, speed of agitator described in step (3) is 100-150r/min.
Preferably, speed of agitator described in step (4) is 80-120r/min.
Beneficial effects of the present invention：
Bunt gypsum, slate, beidellite, diabase and the Portland cement that the present invention adds are used cooperatively, and not only may be used
To significantly improve the adhesive property of adhesive, mechanical strength, moisture resistance and the water resistance of adhesive can also be improved；The vinegar of addition
Sour ethylene-tertiary ethylene carbonate-butyl acrylate ternary polymerization latex powder is used cooperatively with edible seaweed powder, ghatti gum, and collaboration is mutual
Synergy is mended, adhesion strength, water-resistance, antiacid caustic corrosion and the weatherability of adhesive, the strong powder of magnesium of addition can be significantly improved
With torispherical glass powder, the mechanical property of adhesive, chemical stability, thermal stability, water resistance and resistance to old can be significantly improved
The property changed, three kinds of chloro- N- of 4- (stearmide methyl) pyridine of addition, rosin acid calcium soap, zirconium stearate raw material mutual cooperation conducts
Waterproofing agent significantly improves the water resistance of adhesive.Adhesive produced by the present invention not only has higher adhesive strength, also has
Excellent water resistance, heat resistance, acid-alkali-corrosive-resisting, resistance to ag(e)ing, freeze-thaw resistance and weatherability, safety and environmental protection is easy for construction,
It is a kind of ideal tile bonding material.
Specific implementation mode
Technical solution of the present invention is further described with reference to specific embodiment.
Embodiment 1：
A kind of high-strength water-resistance tile adhesives, are made of the raw material of following parts by weight：50 parts of Portland cement,
20 parts of bunt gypsum, 28 parts of slate, 22 parts of beidellite, 15 parts of diabase, 10 parts of the strong powder of magnesium, 5 parts of torispherical glass powder, lithium magnesium silicate
8 parts, vinyl acetate-tertiary ethylene carbonate -4 parts of butyl acrylate ternary polymerization latex powder, 3 parts of edible seaweed powder, 2 parts of ghatti gum,
1 part of the chloro- N- of 4- (stearmide methyl) pyridine, 0.5 part of rosin acid calcium soap, 0.5 part of zirconium stearate.
A kind of preparation method of high-strength water-resistance tile adhesives, includes the following steps：
(1) bunt gypsum, slate, beidellite, diabase are mixed, is crushed, cross 300 mesh sieve, for use；
(2) edible seaweed powder, the strong powder of magnesium, torispherical glass powder are added to together in crushed material made from step (1), are being stirred
Rotating speed is stirred 25min under conditions of being 50r/min, obtains mixture A；
(3) lithium magnesium silicate, ghatti gum, ethylene-tertiary ethylene carbonate-butyl acrylate ternary polymerization latex powder are added
Into Portland cement, it is stirred 10min under conditions of speed of agitator is 100r/min, obtains mixture B；
(4) by the chloro- N- of mixture A and 4- (stearmide methyl) pyridine made from step (1), rosin acid calcium soap, hard
Resin acid zirconium is added to together in mixture B, and 20min is stirred under conditions of speed of agitator is 80r/min, and discharging packing is
It can.
Embodiment 2：
A kind of high-strength water-resistance tile adhesives, are made of the raw material of following parts by weight：55 parts of Portland cement,
25 parts of bunt gypsum, 31 parts of slate, 25 parts of beidellite, 18 parts of diabase, 13 parts of the strong powder of magnesium, 7 parts of torispherical glass powder, lithium magnesium silicate
12 parts, vinyl acetate-tertiary ethylene carbonate -6 parts of butyl acrylate ternary polymerization latex powder, 4.5 parts of edible seaweed powder, ghatti gum
3.5 parts, 1.5 parts of the chloro- N- of 4- (stearmide methyl) pyridine, 1 part of rosin acid calcium soap, 1 part of zirconium stearate.
The invention also discloses a kind of preparation methods of high-strength water-resistance tile adhesives, include the following steps：
(1) bunt gypsum, slate, beidellite, diabase are mixed, is crushed, cross 400 mesh sieve, for use；
(2) edible seaweed powder, the strong powder of magnesium, torispherical glass powder are added to together in crushed material made from step (1), are being stirred
Rotating speed is stirred 20min under conditions of being 80r/min, obtains mixture A；
(3) lithium magnesium silicate, ghatti gum, ethylene-tertiary ethylene carbonate-butyl acrylate ternary polymerization latex powder are added
Into Portland cement, it is stirred 8min under conditions of speed of agitator is 120r/min, obtains mixture B；
(4) by the chloro- N- of mixture A and 4- (stearmide methyl) pyridine made from step (1), rosin acid calcium soap, hard
Resin acid zirconium is added to together in mixture B, and 15min, discharging packing are stirred under conditions of speed of agitator is 100r/min
?.
Embodiment 3：
A kind of high-strength water-resistance tile adhesives, are made of the raw material of following parts by weight：60 parts of Portland cement,
30 parts of bunt gypsum, 34 parts of slate, 28 parts of beidellite, 20 parts of diabase, 15 parts of the strong powder of magnesium, 10 parts of torispherical glass powder, magnesium silicate
16 parts of lithium, vinyl acetate-tertiary ethylene carbonate -8 parts of butyl acrylate ternary polymerization latex powder, 6 parts of edible seaweed powder, ghatti gum 5
Part, 2 parts of the chloro- N- of 4- (stearmide methyl) pyridine, 1.5 parts of rosin acid calcium soap, 1.5 parts of zirconium stearate.
A kind of preparation method of high-strength water-resistance tile adhesives, includes the following steps：
(1) bunt gypsum, slate, beidellite, diabase are mixed, is crushed, cross 500 mesh sieve, for use；
(2) edible seaweed powder, the strong powder of magnesium, torispherical glass powder are added to together in crushed material made from step (1), are being stirred
Rotating speed is stirred 15min under conditions of being 100r/min, obtains mixture A；
(3) lithium magnesium silicate, ghatti gum, ethylene-tertiary ethylene carbonate-butyl acrylate ternary polymerization latex powder are added
Into Portland cement, it is stirred 5min under conditions of speed of agitator is 150r/min, obtains mixture B；
(4) by the chloro- N- of mixture A and 4- (stearmide methyl) pyridine made from step (1), rosin acid calcium soap, hard
Resin acid zirconium is added to together in mixture B, and 10min, discharging packing are stirred under conditions of speed of agitator is 120r/min
?.
Comparative example 1
A kind of tile adhesives are made of the raw material of following parts by weight：50 parts of Portland cement, bunt gypsum 85
Part, 15 parts of the strong powder of magnesium, 8 parts of lithium magnesium silicate, 9 parts of edible seaweed powder, 2 parts of rosin acid calcium soap.
A kind of preparation method of high-strength water-resistance tile adhesives, includes the following steps：
(1) bunt gypsum is crushed, crosses 300 mesh sieve, for use；
(2) edible seaweed powder and the strong powder of magnesium are added in crushed material made from step (1), are 50r/min's in speed of agitator
Under the conditions of be stirred 25min, obtain mixture A；
(3) lithium magnesium silicate is added in Portland cement, is stirred under conditions of speed of agitator is 100r/min
10min is mixed, mixture B is obtained；
(4) mixture A and rosin acid calcium soap made from step (1) are added to together in mixture B, in speed of agitator
To be stirred 20min, discharging packing under conditions of 80r/min.
The performance test of tile adhesives
P is used as tentative standard ceramic tile, Portland cement is surveyed using national standard 48mm × 48mm Tai-Tao ceramic tiles
042.5 grade products.
The processing mode of ceramic tile follows the requirement of national standard, and first experiment Ceramic Tiles are soaked for 24 hours, boiling water boiling 2h, 105 DEG C
4h is dried, is at least placed for 24 hours under standard test conditions.Experimental data is the average value after 5 pieces of ceramic tile tests.
Test method according to《Ceramic wall and floor bricks adhesive》JCT 547-2005 standards require test experiments.
The main performance of tile adhesives made from above-described embodiment 1-3 and comparative example 1 and existing tile adhesives is examined
It surveys as shown in the table：
Table 1
| Detection project | Embodiment 1 | Embodiment 2 | Embodiment 3 | Comparative example 1 |
| Shear strength (MPa) | 2.35 | 2.49 | 2.41 | 1.57 |
| Linear shrinkage (%) | 0.4 | 0.2 | 0.3 | 0.9 |
| Normal temperature state adhesion strength (MPa) | 2.76 | 2.87 | 2.81 | 1.96 |
| Adhesion strength (MPa) after immersion | 2.01 | 2.12 | 2.07 | 1.32 |
| Adhesion strength (MPa) after heat ageing | 2.14 | 2.26 | 2.19 | 1.38 |
| Adhesion strength (MPa) after Frozen-thawed cycled | 2.23 | 2.31 | 2.25 | 1.51 |
| Water permeability | Nothing | Nothing | Nothing | Have |
As can be seen from the above table, compared with the tile adhesives of comparative example 1, ceramic tile made from 1-3 of the embodiment of the present invention
Adhesive is acted on the basis of identical additive amount using various ingredients coordinated, with higher adhesion strength and preferably
Water resistance, and adhesive layer is waterproof, can greatly improve the durability of ceramic tile, ceramic tile is unlikely to be peel off, and extends the use of ceramic tile
Service life.
The foregoing is only a preferred embodiment of the present invention, is not intended to restrict the invention, for the skill of this field
For art personnel, the invention may be variously modified and varied.All within the spirits and principles of the present invention, any made by repair
Change, equivalent replacement, improvement etc., should all be included in the protection scope of the present invention.
Claims (8)
1. a kind of high-strength water-resistance tile adhesives, which is characterized in that it is made of the raw material of following parts by weight：Normal silicate
50-60 parts of cement, 20-30 parts of bunt gypsum, 28-34 parts of slate, 22-28 parts of beidellite, 15-20 parts of diabase, the strong powder 10-15 of magnesium
Part, 5-10 parts of torispherical glass powder, 8-16 parts of lithium magnesium silicate, vinyl acetate-tertiary ethylene carbonate-butyl acrylate ternary polymerization
4-8 parts of latex powder, 3-6 parts of edible seaweed powder, 2-5 parts of ghatti gum, 1-2 parts of the chloro- N- of 4- (stearmide methyl) pyridine, rosin acid calcium
0.5-1.5 parts of soap, 0.5-1.5 parts of zirconium stearate.
2. high-strength water-resistance tile adhesives according to claim 1, which is characterized in that its by following parts by weight raw material
It is made：54-56 parts of Portland cement, 23-27 parts of bunt gypsum, 30-32 parts of slate, 24-26 parts of beidellite, diabase 17-
19 parts, magnesium is powder 12-14 parts strong, 6-8 parts of torispherical glass powder, 10-14 parts of lithium magnesium silicate, vinyl acetate-tertiary ethylene carbonate-the third
5-7 parts of olefin(e) acid butyl ester ternary polymerization latex powder, 4-5 parts of edible seaweed powder, 3-4 parts of ghatti gum, the chloro- N- of 4- (stearmide methyl) pyrrole
1.2-1.8 parts of pyridine, 0.8-1.2 parts of rosin acid calcium soap, 0.9-1.1 parts of zirconium stearate.
3. high-strength water-resistance tile adhesives according to claim 1, which is characterized in that its by following parts by weight raw material
It is made：55 parts of Portland cement, 25 parts of bunt gypsum, 31 parts of slate, 25 parts of beidellite, 18 parts of diabase, 13 parts of the strong powder of magnesium,
7 parts of torispherical glass powder, 12 parts of lithium magnesium silicate, vinyl acetate-tertiary ethylene carbonate-butyl acrylate ternary polymerization latex powder 6
It is part, 4.5 parts of edible seaweed powder, 3.5 parts of ghatti gum, 1.5 parts of the chloro- N- of 4- (stearmide methyl) pyridine, 1 part of rosin acid calcium soap, hard
1 part of resin acid zirconium.
4. a kind of preparation method of high-strength water-resistance tile adhesives as described in any one of claims 1-3, which is characterized in that
Include the following steps：
(1) bunt gypsum, slate, beidellite, diabase are mixed, is crushed, sieving, for use；
(2) edible seaweed powder, the strong powder of magnesium, torispherical glass powder are added to together in crushed material made from step (1), are stirred
15-25min obtains mixture A；
(3) lithium magnesium silicate, ghatti gum, ethylene-tertiary ethylene carbonate-butyl acrylate ternary polymerization latex powder are added to general
In logical portland cement, it is stirred 5-10min, obtains mixture B；
(4) by the chloro- N- of mixture A and 4- (stearmide methyl) pyridine, rosin acid calcium soap, stearic acid made from step (1)
Zirconium is added to together in mixture B, is stirred 10-20min, discharging packing.
5. the preparation method of high-strength water-resistance tile adhesives according to claim 4, which is characterized in that in step (1)
The grit number of crossing is 300-500 mesh.
6. the preparation method of high-strength water-resistance tile adhesives according to claim 4, which is characterized in that in step (2)
The speed of agitator is 50-100r/min.
7. the preparation method of high-strength water-resistance tile adhesives according to claim 4, which is characterized in that in step (3)
The speed of agitator is 100-150r/min.
8. the preparation method of high-strength water-resistance tile adhesives according to claim 4, which is characterized in that in step (4)
The speed of agitator is 80-120r/min.
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| CN201810657902.0A CN108751848B (en) | 2018-06-22 | 2018-06-22 | High-strength water-resistant ceramic tile adhesive and preparation method thereof |
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| CN201810657902.0A CN108751848B (en) | 2018-06-22 | 2018-06-22 | High-strength water-resistant ceramic tile adhesive and preparation method thereof |
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| CN108751848B CN108751848B (en) | 2021-09-24 |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109626929A (en) * | 2019-01-07 | 2019-04-16 | 浙江建工创生建材科技有限公司 | A kind of thin layer gravity flowing levelling mortar of water proof anti-seepage |
| CN114591702A (en) * | 2021-12-30 | 2022-06-07 | 湖北碱克新材料有限公司 | Tile back glue |
| CN114907067A (en) * | 2022-05-05 | 2022-08-16 | 安徽盛城新型材料有限公司 | Strong heavy brick adhesive and construction process |
| TWI783367B (en) * | 2021-02-04 | 2022-11-11 | 毅馨國際有限公司 | Pipe filling material and method of filling pipe without wall drilling |
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| KR20100083669A (en) * | 2009-01-14 | 2010-07-22 | 태양산업개발 주식회사 | Manufacture method of coat contained seven preciousstone |
| CN104860601A (en) * | 2014-02-25 | 2015-08-26 | 如皋市滨江城建投资有限公司 | Ceramic brick adhesive |
| CN107512892A (en) * | 2017-09-30 | 2017-12-26 | 潍坊骏兴防水材料有限公司 | A kind of ceramic tile adhesive and preparation method thereof |
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| KR20100083669A (en) * | 2009-01-14 | 2010-07-22 | 태양산업개발 주식회사 | Manufacture method of coat contained seven preciousstone |
| CN104860601A (en) * | 2014-02-25 | 2015-08-26 | 如皋市滨江城建投资有限公司 | Ceramic brick adhesive |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109626929A (en) * | 2019-01-07 | 2019-04-16 | 浙江建工创生建材科技有限公司 | A kind of thin layer gravity flowing levelling mortar of water proof anti-seepage |
| TWI783367B (en) * | 2021-02-04 | 2022-11-11 | 毅馨國際有限公司 | Pipe filling material and method of filling pipe without wall drilling |
| CN114591702A (en) * | 2021-12-30 | 2022-06-07 | 湖北碱克新材料有限公司 | Tile back glue |
| CN114907067A (en) * | 2022-05-05 | 2022-08-16 | 安徽盛城新型材料有限公司 | Strong heavy brick adhesive and construction process |
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| CN108751848B (en) | 2021-09-24 |
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