CN108751310A - A kind of integrated processing system of heavy metal-containing waste water - Google Patents
A kind of integrated processing system of heavy metal-containing waste water Download PDFInfo
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- CN108751310A CN108751310A CN201810577123.XA CN201810577123A CN108751310A CN 108751310 A CN108751310 A CN 108751310A CN 201810577123 A CN201810577123 A CN 201810577123A CN 108751310 A CN108751310 A CN 108751310A
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- water
- condensing crystallizing
- condenser
- crystallizing device
- processing system
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/02—Treatment of water, waste water, or sewage by heating
- C02F1/04—Treatment of water, waste water, or sewage by heating by distillation or evaporation
- C02F1/16—Treatment of water, waste water, or sewage by heating by distillation or evaporation using waste heat from other processes
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F2101/00—Nature of the contaminant
- C02F2101/10—Inorganic compounds
- C02F2101/20—Heavy metals or heavy metal compounds
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- Life Sciences & Earth Sciences (AREA)
- Hydrology & Water Resources (AREA)
- Engineering & Computer Science (AREA)
- Environmental & Geological Engineering (AREA)
- Water Supply & Treatment (AREA)
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Heat Treatment Of Water, Waste Water Or Sewage (AREA)
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Abstract
The invention discloses a kind of integrated processing systems of heavy metal-containing waste water, including heat pump of high-temp water source unit, condensing crystallizing device, solid-liquid separator, vacuum unit and condenser, heat pump of high-temp water source unit is equipped with hot water delivery pipe, hot water input pipe, cold water efferent duct and cold water inlet pipe, hot water delivery pipe is connected to the first inlet of condensing crystallizing device, hot water input pipe is connected to the first liquid outlet of condensing crystallizing device, the discharge of materials mouth of condensing crystallizing device is connected to the inlet of solid-liquid separator, the liquid outlet of solid-liquid separator is connected to the material inlet of condensing crystallizing device, cold water efferent duct and cold water inlet pipe are connected to condenser respectively, vacuum unit is connected to condensing crystallizing device and condenser.The present invention uses heat pump of high-temp water source unit to provide the required heat of evaporation for waste water treatment system simultaneously and condense required cold, energy-efficient;The useless zero-emission of solid waste liquid, energy conservation and environmental protection can be achieved in the present invention.
Description
Technical field
The present invention relates to technical field of waste water processing, especially a kind of integrated processing system of heavy metal-containing waste water.
Background technology
Wastewater flow rate is quite big caused by heavy metal-containing waste water, especially PCB industries, electroplating industry, main succession
Based on COD and heavy metal.Past generally use heavy metal chemical coagulation-sedimentation method, makes metal ion in waste water be formed with alkaline agent
After hydroxide flco, then to precipitate separate mode removal, waste water is again into biochemical treatment after heavy-metal ion removal.But this place
Reason method, consumption of chemicals is big, and processing cost is high, and heavy workload, treatment effect is unstable, is unable to qualified discharge.
The treatment process technology of current relatively conventional high concentration heavy metal-containing waste water have chemical reduction method, electrolysis, from
Sub- exchange process and membrane separation method.
Chemical reduction method:It is chemically reacted by putting into relevant medicament in heavy metal-containing waste water, each metal ion
Generation synthetic is reacted with medicament and carries out precipitation separation removal, and this method is uncontrollable etc. by influent concentration and Adding medicine control variation
Factor can not accomplish that stably reaching standard discharges, and treated, and waste water also cannot achieve reuse to procedure for producing.
Electrolysis:The method of electrolysis is moved to the metal ion in heavy metal-containing waste water by electric field, charge potential
Move the treatment technology of attachment.This treatment technology is generally only applicable to that water is less, highly concentrated without other foreign metal ions
Waste water is spent, the ion in waste water is finally recycled with sheet metal.But to general low concentration, concentration only have tens or
Hundreds of ppm, water is big, and low concentration and concentration change greatly heavy metal-containing waste water, and the method for electrolysis is difficult to realize in waste water
Metal ion carries out effective mobility.Moreover, waste water its salinity after electrolysis has larger increase, it is difficult to accomplish stable emissions and
Reuse.
Ion-exchange:Ion-exchange inhales the metal ion in waste water generally by ion exchange resin
It is attached.By resin adsorption, resin saturation failure after a period of time needs to expend a large amount of acid or alkali carries out metal ion in waste water
Elution and regeneration.Regenerative process needs a large amount of tap water to be eluted and cleaned, this large amount of ejected wash water also contains residue gold
Belong to ion, it is also desirable to could be discharged after being handled.Ion exchange resin will fail for a period of time after Reusability,
Whole all replacements are needed after failure, cause high processing cost.
And film process is used, waste water can be handled well, and film produces water also can stably reaching standard discharge.But the concentration of film has centainly
The limit, i.e., when Waste water concentrating to a certain extent after, with the raising of concentration, conductivity rises, concentration of metal ions rises,
The solutes such as COD accordingly rise, so that film permeant flux declines, cycles of concentration is obstructed.Pass through membranous system treated concentrate
It is difficult to handle, Crystallization Separation effect has not only been not achieved but also reuse concentration is not achieved;In addition some heavy metal wastewater therebies are not suitable for into membrane system
System, has damage to film, influences membrane lifetime;And some conductivity of waste water are excessively high, are also not suitable for into membranous system, can cause membranous system without
Produce water.
Processing is seen through using counter, to low concentration, in the waste water of≤500mg/L, processing water outlet can continue metal ion content
It is used in plating piece rinsing, does not influence wash effect, but for the higher dope of metal ion 500mg/L concentrations above containing a huge sum of money
Belong to waste water, water is produced after processing and is unable to stably reaching standard, is more than discharge standard value range.Coating bath cannot be directly returned simultaneously, can be influenced
Plating quality.
Invention content
Based on the above issues, it is provided a kind of containing weight it is an object of the invention to overcome above-mentioned the deficiencies in the prior art place
The integrated processing system of metallic wastewater, the system medicament consumption is small, processing cost is low, treatment effect is stablized, and meets waste water
Discharge standard.
To achieve the above object, the technical solution that the present invention takes is:A kind of integrated treatment system of heavy metal-containing waste water
System, including heat pump of high-temp water source unit, condensing crystallizing device, solid-liquid separator, vacuum unit and condenser, the high-temp water source heat
Pump assembly be equipped with hot water delivery pipe, hot water input pipe, cold water efferent duct and cold water inlet pipe, the hot water delivery pipe with it is described
First inlet of condensing crystallizing device is connected to, and the hot water input pipe is connected to the first liquid outlet of the condensing crystallizing device, institute
The discharge of materials mouth for stating condensing crystallizing device is connected to the inlet of the solid-liquid separator, the liquid outlet of the solid-liquid separator with
The material inlet of the condensing crystallizing device is connected to, and the cold water efferent duct and cold water inlet pipe are connected to the condenser respectively,
The vacuum unit is connected to the condensing crystallizing device and condenser.
Wherein, the main function of condensing crystallizing device is constantly to be added the material (heavy metal-containing waste water) of required evaporation
Heat simultaneously constantly carries out gas-liquid separation, and evaporative crystallization is done step-by-step;The main function of condenser is that will flash steam condenses
Cheng Shui;The main function of solid-liquid separator is the material after crystallization being separated by solid-liquid separation;Vacuum unit acts predominantly on
In maintaining whole system negative-pressure vacuum, negative pressure low-temperature evaporation is realized;The solid-liquid separator is preferably centrifuge.
Preferably, the cold water efferent duct is connected to the condenser bottom, the cold water inlet pipe and the condenser
Top connection, the vacuum unit is connected to the condenser, and the top of the condensing crystallizing device is upper with the condenser
Portion is connected to;Vacuum unit can be realized simultaneously the negative pressure of vacuum environment of condensing crystallizing device and condenser as a result,.Preferably, described
Condensing crystallizing device is crystallizing pan.
Preferably, the system also includes horizontal speed-reducer, the horizontal speed-reducer is set to the top of the crystallizing pan, institute
It states and is equipped with blender in condensing crystallizing device, the top of the blender is connect with the horizontal speed-reducer;Pass through speed reducer as a result,
The rotating speed that blender can be adjusted at any time, to adjust the efficiency being concentrated by evaporation.
Preferably, the system also includes water collect tank, the water outlet of the condenser is connected to the water collect tank, described true
Dummy cell is connected to the top of the water collect tank.
Preferably, the system also includes mother liquor pond, accumulator tank and Matter Transfer pump, the liquid outlet of the centrifuge and institutes
State the connection of mother liquor pond, the mother liquor pond also be connected to Matter Transfer pump, the liquid outlet that the Matter Transfer pumps also with it is described
The material inlet of condensing crystallizing device is connected to, and the centrifuge is additionally provided with crystal floss hole, the crystal floss hole and the storage
Slot is connected to.
Preferably, liquid level detector and material concentration detector are additionally provided in the condensing crystallizing device.Level sensing as a result,
Device can monitor the liquid level of material in condensing crystallizing device, when system just starts, can open quick feeding pattern, work as level sensing
When device monitors that material reaches a certain amount of, normal feed mode can be changed into, to save feed time;Material concentration detector
The concentration of the material after evaporation and concentration can be monitored in real time, according to demand, discharge may be selected and be concentrated by evaporation to certain density
Material can also select the material crystal after discharge condensing crystallizing, realize the discharge method of zero-emission.
In conclusion beneficial effects of the present invention are:
1, the present invention uses heat pump to provide the heat needed for evaporating and the cold needed for condensation simultaneously for waste water treatment system,
Without mating pre-heating system, simple system, system support is few, cold and heat combined supply, and Energy Efficiency Ratio is high;Compared to the side such as former boiler or electrical heating
Formula, energy consumption significantly reduce, and take full advantage of the energy that the cold and hot both ends of heat pump generate, energy-efficient;
2, the final evaporative crystallization of the achievable waste water of the present invention, the solid crystals of formation can carry out packaging outward transport, can also
It is utilized again, the mother liquor after separation of solid and liquid can reenter condensing crystallizing device and carry out continuous evaporating, concentrating and crystallizing, realize
The useless zero-emission of solid waste liquid, realizes the abundant recycling of the energy, energy conservation and environmental protection;
3, whole system of the invention is easy to operate, it can be achieved that start & shutdown through one key, automation control, service life is long, failure
Rate is few.
Description of the drawings
Fig. 1 is the principle schematic of the integrated processing system of the present invention;
Fig. 2 is the structural schematic diagram of the integrated processing system of the present invention;
Wherein, 1, heat pump of high-temp water source unit, 2, crystallizing pan, 3, solid-liquid separator, 4, vacuum unit, 5, condenser, 6,
Horizontal speed-reducer, 7, water collect tank, 8, mother liquor pond, 9, accumulator tank, 10, Matter Transfer pump, 11, hot water delivery pipe, 12, hot water input
Pipe, 13, cold water efferent duct, 14, cold water inlet pipe, the 15, first inlet, the 16, first liquid outlet, 17, discharge of materials mouth, 18,
Blender, 19, material inlet, 20, crystal floss hole, 21, draining pump, 22, condensing crystallizing device.
Specific implementation mode
The present invention is suitable for PCB (plating, circuit board, wiring board) industry, food-processing industry, chemical industry, medical row
The concentration of evaporation decrement and zero-emission of the industries waste water such as industry, mechanical processing manufacturing and waste liquid;The present invention is by using high temperature
Water source heat pump units provide the heat needed for high-concentration heavy metal waste water evaporative crystallization and the cold needed for gas-liquid separation, realization pair
Solid, air-liquid separation and recovery processing in high-concentration heavy metal waste water.
To better illustrate the object, technical solutions and advantages of the present invention, below in conjunction with the drawings and specific embodiments pair
The present invention is described further.
Embodiment 1
As illustrated in fig. 1 and 2, a kind of embodiment of the integrated processing system of heavy metal-containing waste water of the invention, including height
Warm water source heat pump unit 1, crystallizing pan 2, solid-liquid separator 3, vacuum unit, 4, condenser 5, horizontal speed-reducer 6, water collect tank 7, female
Liquid pool 8, accumulator tank 9 and Matter Transfer pump 10, solid-liquid separator 3 uses centrifuge;
Wherein, heat pump of high-temp water source unit 1 is equipped with hot water delivery pipe 11, hot water input pipe 12,13 and of cold water efferent duct
Cold water inlet pipe 14, hot water delivery pipe 11 are connected to the first inlet 15 of crystallizing pan 2, hot water input pipe 12 and crystallizing pan 2
First liquid outlet 16 is connected to, and the discharge of materials mouth 17 of crystallizing pan 2 is connected to the inlet of solid-liquid separator 3, cold water efferent duct 13
It is connected to 5 bottom of condenser, cold water inlet pipe 14 is connected to the top of condenser 5, and vacuum unit 4 is connected to condenser 5, crystallization
The top of pot 2 is connected to the top of condenser 5, and negative-pressure vacuum environment can be achieved at the same time (close to very in crystallizing pan and condenser as a result,
Sky, opposite outer environment are negative pressure);The water outlet of condenser 5 is connected to water collect tank 7, the top of vacuum unit 4 and water collect tank 7
Connection;
Horizontal speed-reducer 6 is set to the top of crystallizing pan 2, is equipped with blender 18 in crystallizing pan 2, the top of blender 18 with it is sleeping
Formula speed reducer 6 connects;It is additionally provided with liquid level detector (not shown) in crystallizing pan 2 and material concentration detector (does not show in figure
Go out);The liquid outlet of solid-liquid separator 3 is connected to mother liquor pond 8, and mother liquor pond 8 is also connected to Matter Transfer pump 10, Matter Transfer pump 10
Liquid outlet be also connected to the material inlet of crystallizing pan 2 19, solid-liquid separator 3 is additionally provided with crystal floss hole 20, crystal floss hole
20 are connected to accumulator tank 9.
The present invention can also include auxiliary unit, such as draining pump 21, flowmeter, various valve (not shown)s etc..
The integrated processing system of the present invention is in use, have the characteristics that:
1) heat pump of high-temp water source unit generates the hot water of T1~T2 DEG C of high temperature, into the shell side of integrated condensing crystallizing device
And tube side, indirect heat exchange is carried out with the material (heavy metal-containing waste water) of required heating evaporation, so that material is reached evaporating temperature, so
After be back to hot water circuit water pot (not shown), enter heat pump unit finally by heat-exchanger pump (not shown), realize
High-temperature-hot-water sustainable supply;
2) material after heat exchange heating realizes its gas-liquid separation, separation in integrated condensing crystallizing device bottom by stirring
Saturated steam afterwards enters the shell side of condenser;
3) T3~T4 DEG C of the cooling water that heat pump of high-temp water source unit generates simultaneously enters the tube side of condenser, will be outside shell side
Saturated vapor be condensed into water, condensed water passes through water collect tank and collects discharge (distillate);
4) it is back to circulating chilled water tank (not shown) after the condensed device heat exchange of cooling water, then passes through water supply pump
(not shown) enters heat pump unit, realizes consecutive low temperature cooling water supply;
5) material after gas-liquid separation by the stirring of integrated condensing crystallizing device bottom constantly carry out heating evaporation and
Gas-liquid separation forms crystal after material evaporation to a certain concentration, and the material after crystallization passes through integrated condensing crystallizing device bottom
Discharge port discharge, into solid-liquid separator;
6) material after crystallization is separated by solid-liquid separation by solid-liquid separator, forms crystal and mother liquor, crystal are discharged to storage tank,
It realizes that its recycling, mother liquor return to mother liquor pond, integrated condensing crystallizing device can be again introduced into material and is evaporated concentration knot
Crystalline substance processing;
7) vacuum unit:Vacuum pump unicom condenser, integrated condensing crystallizing device, separation of solid and liquid in vacuum unit
Device realizes stable negative-pressure vacuum, it is ensured that material maintains boiling at low temperature to steam for the entire integrated processing system that is concentrated by evaporation
Hair;
8) unpowered charging:Vacuum unit has realized the entire negative-pressure vacuum for being concentrated by evaporation integrated processing system and stablizing,
Material is not necessarily to feed pump, can be realized by vacuum and be inhaled into integrated condensing crystallizing device;When system just starts charging, system
Start quick feeding pattern, open quick feeding valve (not shown), material is directly entered integration by quick feeding valve
Condensing crystallizing device middle and lower part, when the liquid level detector in integrated condensing crystallizing device detects that material reaches a certain amount of,
System starts normal feed mode, and machine automatization inlet valve (not shown) is opened, by machine automatization inlet valve and instantaneous steaming
Hair control valve (not shown) automatically controls inlet amount;
9) integrated condensing crystallizing device bottom is equipped with material concentration detector, and detection is after evaporating, concentrating and crystallizing in real time
The concentration of material can control discharge method according to actual demand, and discharge may be selected and be concentrated by evaporation to certain density material,
The material crystal after discharge condensing crystallizing may be selected, realize the discharge method of zero-emission;
10) pipeline and each device of evaporation and concentration integrated processing system can be different according to actual demand and region, use
The anti-corrosion resistant material such as stainless steel, dual phase steel, titanium, modified graphite.
Finally, it should be noted that the above embodiments are merely illustrative of the technical solutions of the present invention rather than is protected to the present invention
The limitation of range is protected, although being explained in detail to the present invention with reference to preferred embodiment, those skilled in the art should
Understand, technical scheme of the present invention can be modified or replaced equivalently, without departing from the essence of technical solution of the present invention
And range.
Claims (7)
1. a kind of integrated processing system of heavy metal-containing waste water, which is characterized in that including heat pump of high-temp water source unit, concentration knot
Brilliant device, solid-liquid separator, vacuum unit and condenser, the heat pump of high-temp water source unit are defeated equipped with hot water delivery pipe, hot water
Enter pipe, cold water efferent duct and cold water inlet pipe, the hot water delivery pipe is connected to the first inlet of the condensing crystallizing device, institute
Hot water input pipe is stated to be connected to the first liquid outlet of the condensing crystallizing device, the discharge of materials mouth of the condensing crystallizing device with it is described
The inlet of solid-liquid separator is connected to, and the liquid outlet of the solid-liquid separator is connected to the material inlet of the condensing crystallizing device,
The cold water efferent duct and cold water inlet pipe are connected to the condenser respectively, the vacuum unit and the condensing crystallizing device and
Condenser is connected to.
2. integrated processing system according to claim 1, which is characterized in that the cold water efferent duct and the condenser
Bottom is connected to, and the cold water inlet pipe is connected to the top of the condenser, and the vacuum unit is connected to the condenser, institute
The top for stating condensing crystallizing device is connected to the top of the condenser.
3. integrated processing system according to claim 1, which is characterized in that the condensing crystallizing device is crystallizing pan.
4. integrated processing system according to claim 3, which is characterized in that the system also includes horizontal speed-reducer,
The horizontal speed-reducer is set to the top of the crystallizing pan, and blender, the top of the blender are equipped in the condensing crystallizing device
End is connect with the horizontal speed-reducer.
5. integrated processing system according to claim 1, which is characterized in that the system also includes water collect tanks, described
The water outlet of condenser is connected to the water collect tank, and the vacuum unit is connected to the top of the water collect tank.
6. integrated processing system according to claim 2, which is characterized in that the system also includes mother liquor pond, storages
Slot and Matter Transfer pump, the liquid outlet of the centrifuge is connected to the mother liquor pond, the mother liquor pond also with the Matter Transfer
The liquid outlet of pump connection, the Matter Transfer pump is also connected to the material inlet of the condensing crystallizing device, and the centrifuge is also set
There are crystal floss hole, the crystal floss hole to be connected to the accumulator tank.
7. integrated processing system according to claim 1, which is characterized in that be additionally provided with liquid level in the condensing crystallizing device
Detector and material concentration detector.
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
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CN111544908A (en) * | 2019-02-12 | 2020-08-18 | 义铠科技股份有限公司 | Energy-saving concentration system |
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