CN108744928A - A kind of plant type space deodorant and preparation method thereof - Google Patents
A kind of plant type space deodorant and preparation method thereof Download PDFInfo
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- B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
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- B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
- B01D53/34—Chemical or biological purification of waste gases
- B01D53/46—Removing components of defined structure
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Abstract
The invention discloses a kind of plant type space deodorant and preparation method thereof, the plant type space deodorant includes the raw material of following weight parts：5-10 parts of ligustrum lucidum ait leaf extract, 2-5 parts of Flos Lonicerae extractive solution, 65-85 parts of water.Plant type space deodorant of the present invention and preparation method thereof, using natural plant extracts, it is safe and non-toxic, foreign flavor indoors can be eliminated rapidly, indoor germ can effectively be inhibited simultaneously, to provide the living environment of health, obtained plant type space deodorant stores stabilization for a long time, and active constituent discharges for a long time during use, and action time is lasting.
Description
Technical field
The present invention relates to eliminating smell agent technical fields, and in particular to a kind of plant type space deodorant and preparation method thereof.
Background technology
Eliminating smell agent is a kind of cleaning products being used for removing peculiar smell in local space.In recent years, with living standards of the people
Raising and urbanization process quickening, people's living conditions constantly improve, and have also built the high-grade office building of finishing, house ornamentation quilt
More and more people pay attention to, and thing followed finishing pollution problem is also put in face of people, the nuisance of indoor decoration pollution
Matter is mainly formaldehyde, benzene homologues, ammonia and other volatile organic matters, and wherein content of formaldehyde highest harm is maximum.
Natural timber itself has a certain amount of content of formaldehyde.Artificial board is since glue consumption is big, itself is in finishing
Dosage is also considerable, therefore the primary source polluted as indoor formaldehyde and TVOC.In addition, paint used in interior decoration,
Coating also will produce volatile organic compounds, and the closed decoration in room makes pollutant load rise, and become indoor main
Air pollutants, and contain a large amount of carcinogen in these volatile organic compounds, such as formaldehyde, benzene, toluene, diformazan
The concentration of benzene, ammonia etc. is far above international standard, this not only makes interior have unpleasant peculiar smell, and induces Several Kinds of Malignancy disease
One of an important factor for, the physical and mental health of resident is caused and is seriously threatened.In addition, carpet, furniture, fabrics etc. can also volatilize
Peculiar smell.Foreign flavor indoors not only affect the quality of house ornamentation, also bring threat to health.Someone is using activity in the prior art
Charcoal class solid adsorption material absorbs indoor volatile organic compounds, but activated carbon has the absorption limit, when its absorption
Can be discharged again again when reaching saturation, cause secondary pollution.The method that other eliminating smell agents are mostly covered with odor type in the market, cannot
Effectively absorb or remove smell.
Therefore, it is necessary to develop a kind of eliminating smell agent of environment-friendly type, foreign flavor indoors are effectively removed, and make without pair to human body is nontoxic
With.
Invention content
Technical problem to be solved by the invention is to provide a kind of plant type space deodorants and preparation method thereof, using day
Right plant extracts, it is safe and non-toxic, foreign flavor indoors are eliminated rapidly, while can effectively inhibit indoor germ, to provide health
Living environment, plant type space deodorant of the present invention stores stabilization for a long time, and active constituent discharges for a long time during use,
Action time is lasting.
Purpose of the present invention is to what is be achieved through the following technical solutions：
A kind of plant type space deodorant, includes the raw material of following weight parts：5-10 parts of ligustrum lucidum ait leaf extract, gold and silver
2-5 parts of extracting solution of flower, 65-85 parts of water.
The plant type space deodorant further includes the raw material of following weight parts：5-10 parts of balsam pear extract, Cortex Magnoliae Officinalis extraction
4-8 parts of liquid.
The plant type space deodorant further includes the raw material of following weight parts：1-2 parts of surfactant, cosolvent
0.1-1 parts.
The surfactant is that polysorbas20 and/or butynediols diethoxy compound are modified bola type organosiloxanes.
Preferably, the surfactant is that polysorbas20 and butynediols diethoxy compound are modified the organic silica of bola types
The mass ratio that the mixture of alkane, the polysorbas20 and butynediols diethoxy compound are modified bola type organosiloxanes is 1：
(1-5)
The cosolvent is one or more mixtures in carboxymethyl-beta-cyclodextrin, maltodextrin, acesulfame potassium.
Preferably, the cosolvent is carboxymethyl-beta-cyclodextrin.
The preparation method of the Cortex Magnoliae Officinalis extracting solution includes the following steps：Cortex Magnoliae Officinalis is crushed, 20-50 mesh sieve is crossed, obtains Cortex Magnoliae Officinalis
Powder, Cortex Magnoliae Officinalis powder and volume fraction are the ethanol water in mass ratio 1 of 50-70%：(4-6) is mixed, and is 10% with mass fraction
Sodium bicarbonate aqueous solution to adjust pH be 7.2-8.2, in 60-70 DEG C of refluxing extraction 100-180 minute, using the filter of 300-500 mesh
Cloth filters, and obtains first-time filtrate and a filter residue, the water of 5-10 times of Cortex Magnoliae Officinalis silty amount is added in a filter residue, is with mass fraction
It is 7.2-8.2 that 10% sodium bicarbonate aqueous solution, which adjusts pH, in 80-90 DEG C of refluxing extraction 30-50 minutes, using 300-500 mesh
Filter-cloth filtering obtains secondary filtrate and secondary filter residue, merges first-time filtrate and secondary filtrate, the density for being concentrated under reduced pressure into 60 DEG C are
1.05-1.10g/mL obtaining Cortex Magnoliae Officinalis extracting solution.
The preparation method of the balsam pear extract includes the following steps：Balsam pear drains surface moisture after cleaning, add after remove seed
Enter the water of 3-6 times of balsam pear quality, pulverizer mashing is added, obtains balsam pear slurries, balsam pear grind slurries quality is added in balsam pear slurries
The pectase of 0.1-0.3%, 60-120 minutes are kept the temperature at 45-55 DEG C, and the work of enzyme deactivation in 1-5 minutes is kept the temperature at 90-98 DEG C, is digested
Liquid, enzymolysis liquid are centrifuged 20-30 minute, supernatant use in 50-60 DEG C of ultrasonic extraction 40-80 minutes with 3000-5000 revs/min
300-500 mesh filter-cloth filterings, obtain balsam pear extract.
The preparation method of the ligustrum lucidum ait leaf extract includes the following steps：Fresh ligustrum lucidum ait leaf is taken, after cleaning
Surface moisture is drained, is dried at 40-60 DEG C to constant weight, is crushed, 20-50 mesh sieve is crossed, obtains ligustrum lucidum ait leaf powder, ligustrum lucidum ait leaf
Powder and water in mass ratio 1：(5-10) is mixed, in 85-95 DEG C of refluxing extraction 40-80 minutes, using 300-500 mesh filter-cloth filterings,
First-time filtrate and a filter residue are obtained, the water of 5-10 times of ligustrum lucidum ait leaf silty amount is added in a filter residue, flows back and carries at 85-95 DEG C
It takes 30-50 minutes, using 300-500 mesh filter-cloth filterings, obtains secondary filtrate and secondary filter residue, merge first-time filtrate and secondary filter
Liquid, the density for being concentrated under reduced pressure into 60 DEG C is 1.05-1.10g/mL, obtains ligustrum lucidum ait leaf extract.
The preparation method of the Flos Lonicerae extractive solution includes the following steps：By honeysuckle and water in mass ratio 1：(5-10) is mixed
It closes, in 85-95 DEG C of refluxing extraction 40-80 minutes, using 300-500 mesh filter-cloth filterings, obtains first-time filtrate and a filter residue, once
The water of 5-10 times of quality of Flos Lonicerae is added in filter residue, in 85-95 DEG C of refluxing extraction 30-50 minutes, using 300-500 mesh filter cloth mistakes
Filter obtains secondary filtrate and secondary filter residue, merges first-time filtrate and secondary filtrate, and the density for being concentrated under reduced pressure into 60 DEG C is 1.05-
1.10g/mL obtains Flos Lonicerae extractive solution.
The preparation method of the plant type space deodorant, includes the following steps：Water is added in surfactant, cosolvent
In, it is stirred 5-10 minutes with 100-200 revs/min, sequentially adds ligustrum lucidum ait leaf extract, balsam pear extract, honeysuckle and carry
Liquid, Cortex Magnoliae Officinalis extracting solution are taken, is stirred 10-20 minutes with 100-200 revs/min, using 300-500 mesh filter-cloth filterings, obtained filtrate
As plant type space deodorant.
The application method of plant type space deodorant of the present invention：Plant type space deodorant is contained in spray containers,
It is sprayed on body surface, or is contained in open-top receptacle, interior is statically placed in.Ensure indoor environment well-ventilated during use,
The release and volatilization that can accelerate peculiar smell, reach good using effect.
Beneficial effects of the present invention are as follows：
(1) plant type space deodorant of the present invention, it is safe and non-toxic using natural plant extracts, and natural plants carry
It takes the conjugated double bond of object to provide electronics pair to react with odor molecules, eliminates foreign flavor indoors, while natural plants rapidly
Active constituent in extract can effectively inhibit indoor germ, to provide the living environment of health；
(2) in the preparation process of plant type space deodorant of the present invention, preferably go out the day that can effectively remove foreign flavor indoors
The combination of right plant, and the preparation method of its extract is optimized, the active constituent for effectively removing peculiar smell is extracted, and
The plant origin is extensive so that plant type space deodorant it is of low cost；(3) plant type space deodorant of the present invention
Cosolvent is added in the process, so as to get plant type space deodorant long-term storage stablize, and use during activity at
Divide permanent release, action time is lasting, and surfactant makes plant type space deodorant preferably contact, ooze with body surface
Thoroughly, smell component is effectively removed.
Specific implementation mode
In the present invention, if not refering in particular to, all devices and raw material is commercially available or the industry is common are following
Method in embodiment is unless otherwise instructed this field conventional method.
Bactericidal effect is tested：By the plant type space deodorant and water in mass ratio 1 of preparation:2 dilutions, obtain dilution, take
The Escherichia coli (ATCC 25922) of activation, Candida albicans (ATCC10231), are inoculated into triangular flask, culture to logarithmic phase,
Obtain bacteria suspension.0.5ml bacteria suspensions are taken, dilution 4.5ml is added, 37 DEG C, places 10min respectively；Using distilled water as empty
White control.With the dilution detection of falling flat band method sterilizing deodoring agent to the bactericidal effects of Escherichia coli and Candida albicans, sterilizing rate=
(blank control average colony number-test sample average colony number)/blank control average colony number.
Ligustrum lucidum ait provides fresh ligustrum lucidum ait leaf by Shuyang County acute hearing swamppink grass garden spot.
Balsam pear, using commercially available fresh bitter.
Cortex Magnoliae Officinalis is Magnoliacea plant Cortex Magnoliae Officinalis Magnolia officinalis Rehd.et Wils. or Magnolia bilola
Drying dry hide, root skin and the branch of Magnolia officinalis Rehd.et Wils.var.biloba Rehd.et Wils.
Skin.Gloomy medicine company sale Co., Ltd provides in Haozhou city woods, source area：Sichuan.
Honeysuckle is caprifoliaceae plant honeysuckle Lonicera japonica Thunb., lonicera hypoglauca miq Lonicera
Hypoglauca Miq., Honeysuckle flower (hair calyx honeysuckle) Lonicera confusa DC. or hair style honeysuckle Lonicera
The dry flower of dasystyla Rehd. or with the flower just opened.Tongxiang City Haitai Ju Ye Co., Ltds provide, source area：Henan.
Polysorbas20, No. CAS：9005-64-5, Shanghai Mike's woods biochemical technology Co., Ltd provide, product identification：T6335.
Butynediols diethoxy compound is modified bola type organosiloxanes, with reference to application No. is 201710382922.7
The method of embodiment 1 is prepared in patent of invention.
Carboxymethyl-beta-cyclodextrin, No. CAS：218269-34-2, Shandong Binzhou bio tech ltd Zhi Yuan provide.
Maltodextrin, Xi'an Yue Lai Pharmaceutical Technology Co., Ltd provide.
Acesulfame potassium, the safe bio tech ltd in Tianjin provide.
Sodium bicarbonate, Shanghai Mike's woods biochemical technology Co., Ltd provide, product identification：S818079.
Pectase, one hundred emerging bio tech ltd of Wuhan provide, 30,000 U/g of enzyme activity.
Embodiment 1
Plant type space deodorant raw material (parts by weight)：8 parts of ligustrum lucidum ait leaf extract, 3 parts of Flos Lonicerae extractive solution, water 75
Part.
The preparation method of the ligustrum lucidum ait leaf extract includes the following steps：Fresh ligustrum lucidum ait leaf is taken, after cleaning
Surface moisture is drained, is dried at 50 DEG C to constant weight, is crushed, 20 mesh sieve is crossed, obtains ligustrum lucidum ait leaf powder, ligustrum lucidum ait leaf powder and water
In mass ratio 1：8 mixing, using 300 mesh filter-cloth filterings, obtained first-time filtrate and a filter residue in 90 DEG C of refluxing extractions 60 minutes,
The water of 8 times of ligustrum lucidum ait leaf silty amount is added in filter residue, in 90 DEG C of refluxing extractions 40 minutes, using 300 mesh filter-cloth filterings,
Secondary filtrate and secondary filter residue are obtained, first-time filtrate and secondary filtrate are merged, is 0.02MPa in absolute pressure, temperature is 60 DEG C and subtracts
The density that pressure is concentrated into 60 DEG C is 1.08g/mL, obtains ligustrum lucidum ait leaf extract.
The preparation method of the Flos Lonicerae extractive solution includes the following steps：By honeysuckle and water in mass ratio 1：8 mixing,
90 DEG C of refluxing extractions 60 minutes, using 300 mesh filter-cloth filterings, obtain first-time filtrate and a filter residue, gold and silver are added in a filter residue
The water of 8 times of quality of flower using 300 mesh filter-cloth filterings, obtained secondary filtrate and secondary filter residue, closes in 90 DEG C of refluxing extractions 40 minutes
And first-time filtrate and secondary filtrate, it is 0.02MPa in absolute pressure, temperature is that 60 DEG C of density for being concentrated under reduced pressure into 60 DEG C are
1.08g/mL obtains Flos Lonicerae extractive solution.
The preparation method of the plant type space deodorant, includes the following steps：By ligustrum lucidum ait leaf extract, honeysuckle
Extracting solution is added sequentially in water, is stirred 20 minutes with 150 revs/min, and using 500 mesh filter-cloth filterings, obtained filtrate is to plant
Object type space deodorant.
Embodiment 2
Plant type space deodorant raw material (parts by weight)：8 parts of ligustrum lucidum ait leaf extract, 8 parts of balsam pear extract, Cortex Magnoliae Officinalis carry
Take 6 parts of liquid, 3 parts of Flos Lonicerae extractive solution, 75 parts of water.
The preparation method of the Cortex Magnoliae Officinalis extracting solution includes the following steps：Cortex Magnoliae Officinalis is crushed, 20 mesh sieve is crossed, obtains Cortex Magnoliae Officinalis powder,
The ethanol water in mass ratio 1 that Cortex Magnoliae Officinalis powder and volume fraction are 60%：5 mixing, the sodium bicarbonate for being 10% with mass fraction
Aqueous solution adjusts 7.6, in 65 DEG C of refluxing extractions 120 minutes, using 300 mesh filter-cloth filterings, obtains first-time filtrate and a filter residue, and one
The water of 8 times of Cortex Magnoliae Officinalis silty amount is added in secondary filter residue, the sodium bicarbonate aqueous solution for being 10% with mass fraction adjusts 7.6, at 85 DEG C
Refluxing extraction 40 minutes obtains secondary filtrate and secondary filter residue using 300 mesh filter-cloth filterings, merges first-time filtrate and secondary filtrate,
It is 0.02MPa in absolute pressure, temperature is that 60 DEG C of density for being concentrated under reduced pressure into 60 DEG C are 1.08g/mL, obtains Cortex Magnoliae Officinalis extracting solution.
The preparation method of the balsam pear extract includes the following steps：Balsam pear drains surface moisture after cleaning, add after remove seed
Enter the water of 5 times of balsam pear quality, pulverizer mashing is added, obtains balsam pear slurries, balsam pear grind slurries quality 0.2% is added in balsam pear slurries
Pectase, keep the temperature 90 minutes at 50 DEG C, kept the temperature at 96 DEG C enzyme deactivation in 3 minutes work, obtain enzymolysis liquid, enzymolysis liquid is carried in 55 DEG C of ultrasounds
It takes 60 minutes, is centrifuged 20 minutes with 4000 revs/min, supernatant uses 300 mesh filter-cloth filterings, obtains balsam pear extract, described super
Sound extraction operating condition be：Supersonic frequency 30kHz, ultrasonic power 300W.
The preparation method of the ligustrum lucidum ait leaf extract includes the following steps：Fresh ligustrum lucidum ait leaf is taken, after cleaning
Surface moisture is drained, is dried at 50 DEG C to constant weight, is crushed, 20 mesh sieve is crossed, obtains ligustrum lucidum ait leaf powder, ligustrum lucidum ait leaf powder and water
In mass ratio 1：8 mixing, using 300 mesh filter-cloth filterings, obtained first-time filtrate and a filter residue in 90 DEG C of refluxing extractions 60 minutes,
The water of 8 times of ligustrum lucidum ait leaf silty amount is added in filter residue, in 90 DEG C of refluxing extractions 40 minutes, using 300 mesh filter-cloth filterings,
Secondary filtrate and secondary filter residue are obtained, first-time filtrate and secondary filtrate are merged, is 0.02MPa in absolute pressure, temperature is 60 DEG C and subtracts
The density that pressure is concentrated into 60 DEG C is 1.08g/mL, obtains ligustrum lucidum ait leaf extract.
The preparation method of the Flos Lonicerae extractive solution includes the following steps：By honeysuckle and water in mass ratio 1：8 mixing,
90 DEG C of refluxing extractions 60 minutes, using 300 mesh filter-cloth filterings, obtain first-time filtrate and a filter residue, gold and silver are added in a filter residue
The water of 8 times of quality of flower using 300 mesh filter-cloth filterings, obtained secondary filtrate and secondary filter residue, closes in 90 DEG C of refluxing extractions 40 minutes
And first-time filtrate and secondary filtrate, it is 0.02MPa in absolute pressure, temperature is that 60 DEG C of density for being concentrated under reduced pressure into 60 DEG C are
1.08g/mL obtains Flos Lonicerae extractive solution.
The preparation method of the plant type space deodorant, includes the following steps：Ligustrum lucidum ait leaf extract, balsam pear are carried
It takes liquid, Flos Lonicerae extractive solution, Cortex Magnoliae Officinalis extracting solution to be added sequentially in water, is stirred 20 minutes with 150 revs/min, using 500 mesh filter clothes
Filtering, obtained filtrate is plant type space deodorant.
Comparative example 1
Plant type space deodorant raw material (parts by weight)：8 parts of ligustrum lucidum ait leaf extract, 8 parts of balsam pear extract, honeysuckle
3 parts of extracting solution, 75 parts of water.
The preparation method of the balsam pear extract is the same as embodiment 2.
The preparation method of the ligustrum lucidum ait leaf extract is the same as embodiment 2.
The preparation method of the Flos Lonicerae extractive solution is the same as embodiment 2.
The preparation method of the plant type space deodorant, includes the following steps：Ligustrum lucidum ait leaf extract, balsam pear are carried
It takes liquid, Flos Lonicerae extractive solution to be added sequentially in water, is stirred 20 minutes with 150 revs/min, using 500 mesh filter-cloth filterings, obtained
Filtrate is plant type space deodorant.
Comparative example 2
Plant type space deodorant raw material (parts by weight)：8 parts of ligustrum lucidum ait leaf extract, 6 parts of Cortex Magnoliae Officinalis extracting solution, honeysuckle
3 parts of extracting solution, 75 parts of water.
The preparation method of the Cortex Magnoliae Officinalis extracting solution is the same as embodiment 2.
The preparation method of the ligustrum lucidum ait leaf extract is the same as embodiment 2.
The preparation method of the Flos Lonicerae extractive solution is the same as embodiment 2.
The preparation method of the plant type space deodorant, includes the following steps：By ligustrum lucidum ait leaf extract, honeysuckle
Extracting solution, Cortex Magnoliae Officinalis extracting solution are added sequentially in water, are stirred 20 minutes with 150 revs/min, using 500 mesh filter-cloth filterings, are obtained
Filtrate is plant type space deodorant.
Embodiment 3
It is substantially the same manner as Example 2, it differs only in：
The preparation method of the Cortex Magnoliae Officinalis extracting solution includes the following steps：Cortex Magnoliae Officinalis is crushed, 20 mesh sieve is crossed, obtains Cortex Magnoliae Officinalis powder,
The ethanol water in mass ratio 1 that Cortex Magnoliae Officinalis powder and volume fraction are 60%：5 mixing, the sodium bicarbonate for being 10% with mass fraction
Aqueous solution adjusts 7.6, in 65 DEG C of refluxing extractions 120 minutes, using 300 mesh filter-cloth filterings, obtains filtrate, filtrate is in absolute pressure
0.02MPa, temperature are that 60 DEG C of density for being concentrated under reduced pressure into 60 DEG C are 1.08g/mL, obtain Cortex Magnoliae Officinalis extracting solution.
Embodiment 4
It is substantially the same manner as Example 2, it differs only in：
The preparation method of the Cortex Magnoliae Officinalis extracting solution includes the following steps：Cortex Magnoliae Officinalis is crushed, 20 mesh sieve is crossed, obtains Cortex Magnoliae Officinalis powder,
The water of 8 times of Cortex Magnoliae Officinalis powder magnolia obovata silty amount mixes, and the sodium bicarbonate aqueous solution for being 10% with mass fraction adjusts 7.6, at 85 DEG C
Refluxing extraction 40 minutes, using 300 mesh filter-cloth filterings, filtrate is 0.02MPa in absolute pressure, and temperature is 60 DEG C and is concentrated under reduced pressure into
60 DEG C of density is 1.08g/mL, obtains Cortex Magnoliae Officinalis extracting solution.
Embodiment 5
It is essentially identical with embodiment 2, it differs only in：
The preparation method of the Cortex Magnoliae Officinalis extracting solution includes the following steps：Cortex Magnoliae Officinalis is crushed, 20 mesh sieve is crossed, obtains Cortex Magnoliae Officinalis powder,
The ethanol water in mass ratio 1 that Cortex Magnoliae Officinalis powder and volume fraction are 60%：5 mixing were used in 65 DEG C of refluxing extractions 120 minutes
300 mesh filter-cloth filterings obtain first-time filtrate and a filter residue, the water of 8 times of Cortex Magnoliae Officinalis silty amount are added in a filter residue, flow back at 85 DEG C
Extraction 40 minutes obtains secondary filtrate and secondary filter residue using 300 mesh filter-cloth filterings, merges first-time filtrate and secondary filtrate, exhausted
It is 0.02MPa to pressure, temperature is that 60 DEG C of density for being concentrated under reduced pressure into 60 DEG C are 1.08g/mL, obtains Cortex Magnoliae Officinalis extracting solution.
Embodiment 6
Plant type space deodorant raw material (parts by weight)：8 parts of ligustrum lucidum ait leaf extract, 8 parts of balsam pear extract, Cortex Magnoliae Officinalis carry
Take 6 parts of liquid, 3 parts of Flos Lonicerae extractive solution, 0.5 part of cosolvent, 75 parts of water.
The cosolvent is carboxymethyl-beta-cyclodextrin.
The preparation method of the balsam pear extract is the same as embodiment 2.
The preparation method of the Cortex Magnoliae Officinalis extracting solution is the same as embodiment 2.
The preparation method of the ligustrum lucidum ait leaf extract is the same as embodiment 2.
The preparation method of the Flos Lonicerae extractive solution is the same as embodiment 2.
The preparation method of the plant type space deodorant, includes the following steps：Cosolvent is added to the water, with 150 turns/
Divide stirring 5 minutes, sequentially adds ligustrum lucidum ait leaf extract, balsam pear extract, Flos Lonicerae extractive solution, Cortex Magnoliae Officinalis extracting solution, with
150 revs/min are stirred 20 minutes, and using 500 mesh filter-cloth filterings, obtained filtrate is plant type space deodorant.
Embodiment 7
It is substantially the same manner as Example 6, it differs only in：The cosolvent is maltodextrin.
Embodiment 8
It is substantially the same manner as Example 6, it differs only in：The cosolvent is acesulfame potassium.
Embodiment 9
Plant type space deodorant raw material (parts by weight)：8 parts of ligustrum lucidum ait leaf extract, 8 parts of balsam pear extract, Cortex Magnoliae Officinalis carry
Take 6 parts of liquid, 3 parts of Flos Lonicerae extractive solution, 1.5 parts of surfactant, 0.5 part of cosolvent, 75 parts of water.
The surfactant is polysorbas20.
The cosolvent is carboxymethyl-beta-cyclodextrin.
The preparation method of the balsam pear extract includes the following steps：Balsam pear drains surface moisture after cleaning, add after remove seed
Enter the water of 5 times of balsam pear quality, pulverizer mashing is added, obtains balsam pear slurries, balsam pear grind slurries quality 0.2% is added in balsam pear slurries
Pectase, keep the temperature 90 minutes at 50 DEG C, kept the temperature at 96 DEG C enzyme deactivation in 3 minutes work, obtain enzymolysis liquid, enzymolysis liquid is carried in 55 DEG C of ultrasounds
It takes 60 minutes, is centrifuged 20 minutes with 4000 revs/min, supernatant uses 300 mesh filter-cloth filterings, obtains balsam pear extract, described super
Sound extraction operating condition be：Supersonic frequency 30kHz, ultrasonic power 300W.
The preparation method of the Cortex Magnoliae Officinalis extracting solution includes the following steps：Cortex Magnoliae Officinalis is crushed, 20 mesh sieve is crossed, obtains Cortex Magnoliae Officinalis powder,
The ethanol water in mass ratio 1 that Cortex Magnoliae Officinalis powder and volume fraction are 60%：5 mixing, the sodium bicarbonate for being 10% with mass fraction
Aqueous solution adjusts 7.6, in 65 DEG C of refluxing extractions 120 minutes, using 300 mesh filter-cloth filterings, obtains first-time filtrate and a filter residue, and one
The water of 8 times of Cortex Magnoliae Officinalis silty amount is added in secondary filter residue, the sodium bicarbonate aqueous solution for being 10% with mass fraction adjusts 7.6, at 85 DEG C
Refluxing extraction 40 minutes obtains secondary filtrate and secondary filter residue using 300 mesh filter-cloth filterings, merges first-time filtrate and secondary filtrate,
It is 0.02MPa in absolute pressure, temperature is that 60 DEG C of density for being concentrated under reduced pressure into 60 DEG C are 1.08g/mL, obtains Cortex Magnoliae Officinalis extracting solution.
The preparation method of the ligustrum lucidum ait leaf extract includes the following steps：Fresh ligustrum lucidum ait leaf is taken, after cleaning
Surface moisture is drained, is dried at 50 DEG C to constant weight, is crushed, 20 mesh sieve is crossed, obtains ligustrum lucidum ait leaf powder, ligustrum lucidum ait leaf powder and water
In mass ratio 1：8 mixing, using 300 mesh filter-cloth filterings, obtained first-time filtrate and a filter residue in 90 DEG C of refluxing extractions 60 minutes,
The water of 8 times of ligustrum lucidum ait leaf silty amount is added in filter residue, in 90 DEG C of refluxing extractions 40 minutes, using 300 mesh filter-cloth filterings,
Secondary filtrate and secondary filter residue are obtained, first-time filtrate and secondary filtrate are merged, is 0.02MPa in absolute pressure, temperature is 60 DEG C and subtracts
The density that pressure is concentrated into 60 DEG C is 1.08g/mL, obtains ligustrum lucidum ait leaf extract.
The preparation method of the Flos Lonicerae extractive solution includes the following steps：By honeysuckle and water in mass ratio 1：8 mixing,
90 DEG C of refluxing extractions 60 minutes, using 300 mesh filter-cloth filterings, obtain first-time filtrate and a filter residue, gold and silver are added in a filter residue
The water of 8 times of quality of flower using 300 mesh filter-cloth filterings, obtained secondary filtrate and secondary filter residue, closes in 90 DEG C of refluxing extractions 40 minutes
And first-time filtrate and secondary filtrate, it is 0.02MPa in absolute pressure, temperature is that 60 DEG C of density for being concentrated under reduced pressure into 60 DEG C are
1.08g/mL obtains Flos Lonicerae extractive solution.
The preparation method of the plant type space deodorant, includes the following steps：Water is added in surfactant, cosolvent
In, it is stirred 5 minutes with 150 revs/min, sequentially adds ligustrum lucidum ait leaf extract, balsam pear extract, Flos Lonicerae extractive solution, thickness
Plain extracting solution is stirred 20 minutes with 150 revs/min, and using 500 mesh filter-cloth filterings, obtained filtrate is plant type indoor deodoring
Agent.
Embodiment 10
Plant type space deodorant raw material (parts by weight)：8 parts of ligustrum lucidum ait leaf extract, 8 parts of balsam pear extract, Cortex Magnoliae Officinalis carry
Take 6 parts of liquid, 3 parts of Flos Lonicerae extractive solution, 1.5 parts of surfactant, 0.5 part of cosolvent, 75 parts of water.
The surfactant is that butynediols diethoxy compound is modified bola type organosiloxanes.
The cosolvent is carboxymethyl-beta-cyclodextrin.
The preparation method of the balsam pear extract includes the following steps：Balsam pear drains surface moisture after cleaning, add after remove seed
Enter the water of 5 times of balsam pear quality, pulverizer mashing is added, obtains balsam pear slurries, balsam pear grind slurries quality 0.2% is added in balsam pear slurries
Pectase, keep the temperature 90 minutes at 50 DEG C, kept the temperature at 96 DEG C enzyme deactivation in 3 minutes work, obtain enzymolysis liquid, enzymolysis liquid is carried in 55 DEG C of ultrasounds
It takes 60 minutes, is centrifuged 20 minutes with 4000 revs/min, supernatant uses 300 mesh filter-cloth filterings, obtains balsam pear extract, described super
Sound extraction operating condition be：Supersonic frequency 30kHz, ultrasonic power 300W.
The preparation method of the Cortex Magnoliae Officinalis extracting solution includes the following steps：Cortex Magnoliae Officinalis is crushed, 20 mesh sieve is crossed, obtains Cortex Magnoliae Officinalis powder,
The ethanol water in mass ratio 1 that Cortex Magnoliae Officinalis powder and volume fraction are 60%：5 mixing, the sodium bicarbonate for being 10% with mass fraction
Aqueous solution adjusts 7.6, in 65 DEG C of refluxing extractions 120 minutes, using 300 mesh filter-cloth filterings, obtains first-time filtrate and a filter residue, and one
The water of 8 times of Cortex Magnoliae Officinalis silty amount is added in secondary filter residue, the sodium bicarbonate aqueous solution for being 10% with mass fraction adjusts 7.6, at 85 DEG C
Refluxing extraction 40 minutes obtains secondary filtrate and secondary filter residue using 300 mesh filter-cloth filterings, merges first-time filtrate and secondary filtrate,
It is 0.02MPa in absolute pressure, temperature is that 60 DEG C of density for being concentrated under reduced pressure into 60 DEG C are 1.08g/mL, obtains Cortex Magnoliae Officinalis extracting solution.
The preparation method of the ligustrum lucidum ait leaf extract includes the following steps：Fresh ligustrum lucidum ait leaf is taken, after cleaning
Surface moisture is drained, is dried at 50 DEG C to constant weight, is crushed, 20 mesh sieve is crossed, obtains ligustrum lucidum ait leaf powder, ligustrum lucidum ait leaf powder and water
In mass ratio 1：8 mixing, using 300 mesh filter-cloth filterings, obtained first-time filtrate and a filter residue in 90 DEG C of refluxing extractions 60 minutes,
The water of 8 times of ligustrum lucidum ait leaf silty amount is added in filter residue, in 90 DEG C of refluxing extractions 40 minutes, using 300 mesh filter-cloth filterings,
Secondary filtrate and secondary filter residue are obtained, first-time filtrate and secondary filtrate are merged, is 0.02MPa in absolute pressure, temperature is 60 DEG C and subtracts
The density that pressure is concentrated into 60 DEG C is 1.08g/mL, obtains ligustrum lucidum ait leaf extract.
The preparation method of the Flos Lonicerae extractive solution includes the following steps：By honeysuckle and water in mass ratio 1：8 mixing,
90 DEG C of refluxing extractions 60 minutes, using 300 mesh filter-cloth filterings, obtain first-time filtrate and a filter residue, gold and silver are added in a filter residue
The water of 8 times of quality of flower using 300 mesh filter-cloth filterings, obtained secondary filtrate and secondary filter residue, closes in 90 DEG C of refluxing extractions 40 minutes
And first-time filtrate and secondary filtrate, it is 0.02MPa in absolute pressure, temperature is that 60 DEG C of density for being concentrated under reduced pressure into 60 DEG C are
1.08g/mL obtains Flos Lonicerae extractive solution.
The preparation method of the plant type space deodorant, includes the following steps：Water is added in surfactant, cosolvent
In, it is stirred 5 minutes with 150 revs/min, sequentially adds ligustrum lucidum ait leaf extract, balsam pear extract, Flos Lonicerae extractive solution, thickness
Plain extracting solution is stirred 20 minutes with 150 revs/min, and using 500 mesh filter-cloth filterings, obtained filtrate is plant type indoor deodoring
Agent.
Embodiment 11
Plant type space deodorant raw material (parts by weight)：8 parts of ligustrum lucidum ait leaf extract, 8 parts of balsam pear extract, Cortex Magnoliae Officinalis carry
Take 6 parts of liquid, 3 parts of Flos Lonicerae extractive solution, 1.5 parts of surfactant, 0.5 part of cosolvent, 75 parts of water.
The surfactant is that polysorbas20 and butynediols diethoxy compound are modified the mixed of bola type organosiloxanes
Object is closed, the mass ratio that the polysorbas20 and butynediols diethoxy compound are modified bola type organosiloxanes is 1：2.
The cosolvent is carboxymethyl-beta-cyclodextrin.
The preparation method of the balsam pear extract includes the following steps：Balsam pear drains surface moisture after cleaning, add after remove seed
Enter the water of 5 times of balsam pear quality, pulverizer mashing is added, obtains balsam pear slurries, balsam pear grind slurries quality 0.2% is added in balsam pear slurries
Pectase, keep the temperature 90 minutes at 50 DEG C, kept the temperature at 96 DEG C enzyme deactivation in 3 minutes work, obtain enzymolysis liquid, enzymolysis liquid is carried in 55 DEG C of ultrasounds
It takes 60 minutes, is centrifuged 20 minutes with 4000 revs/min, supernatant uses 300 mesh filter-cloth filterings, obtains balsam pear extract, described super
Sound extraction operating condition be：Supersonic frequency 30kHz, ultrasonic power 300W.
The preparation method of the Cortex Magnoliae Officinalis extracting solution includes the following steps：Cortex Magnoliae Officinalis is crushed, 20 mesh sieve is crossed, obtains Cortex Magnoliae Officinalis powder,
The ethanol water in mass ratio 1 that Cortex Magnoliae Officinalis powder and volume fraction are 60%：5 mixing, the sodium bicarbonate for being 10% with mass fraction
Aqueous solution adjusts 7.6, in 65 DEG C of refluxing extractions 120 minutes, using 300 mesh filter-cloth filterings, obtains first-time filtrate and a filter residue, and one
The water of 8 times of Cortex Magnoliae Officinalis silty amount is added in secondary filter residue, the sodium bicarbonate aqueous solution for being 10% with mass fraction adjusts 7.6, at 85 DEG C
Refluxing extraction 40 minutes obtains secondary filtrate and secondary filter residue using 300 mesh filter-cloth filterings, merges first-time filtrate and secondary filtrate,
It is 0.02MPa in absolute pressure, temperature is that 60 DEG C of density for being concentrated under reduced pressure into 60 DEG C are 1.08g/mL, obtains Cortex Magnoliae Officinalis extracting solution.
The preparation method of the ligustrum lucidum ait leaf extract includes the following steps：Fresh ligustrum lucidum ait leaf is taken, after cleaning
Surface moisture is drained, is dried at 50 DEG C to constant weight, is crushed, 20 mesh sieve is crossed, obtains ligustrum lucidum ait leaf powder, ligustrum lucidum ait leaf powder and water
In mass ratio 1：8 mixing, using 300 mesh filter-cloth filterings, obtained first-time filtrate and a filter residue in 90 DEG C of refluxing extractions 60 minutes,
The water of 8 times of ligustrum lucidum ait leaf silty amount is added in filter residue, in 90 DEG C of refluxing extractions 40 minutes, using 300 mesh filter-cloth filterings,
Secondary filtrate and secondary filter residue are obtained, first-time filtrate and secondary filtrate are merged, is 0.02MPa in absolute pressure, temperature is 60 DEG C and subtracts
The density that pressure is concentrated into 60 DEG C is 1.08g/mL, obtains ligustrum lucidum ait leaf extract.
The preparation method of the Flos Lonicerae extractive solution includes the following steps：By honeysuckle and water in mass ratio 1：8 mixing,
90 DEG C of refluxing extractions 60 minutes, using 300 mesh filter-cloth filterings, obtain first-time filtrate and a filter residue, gold and silver are added in a filter residue
The water of 8 times of quality of flower using 300 mesh filter-cloth filterings, obtained secondary filtrate and secondary filter residue, closes in 90 DEG C of refluxing extractions 40 minutes
And first-time filtrate and secondary filtrate, it is 0.02MPa in absolute pressure, temperature is that 60 DEG C of density for being concentrated under reduced pressure into 60 DEG C are
1.08g/mL obtains Flos Lonicerae extractive solution.
The preparation method of the plant type space deodorant, includes the following steps：Water is added in surfactant, cosolvent
In, it is stirred 5 minutes with 150 revs/min, sequentially adds ligustrum lucidum ait leaf extract, balsam pear extract, Flos Lonicerae extractive solution, thickness
Plain extracting solution is stirred 20 minutes with 150 revs/min, and using 500 mesh filter-cloth filterings, obtained filtrate is plant type indoor deodoring
Agent.
Test case 1
The bactericidal effect of embodiment 1-11 and comparative example 1-2 the plant type space deodorant being prepared is tested,
Specific test result is shown in Table 1.
1 bactericidal effect test result table of table
| Escherichia coli sterilizing rate, % | Candida albicans sterilizing rate, % | |
| Embodiment 1 | 60.3 | 63.6 |
| Embodiment 2 | 86.5 | 88.4 |
| Comparative example 1 | 71.6 | 72.3 |
| Comparative example 2 | 76.8 | 79.6 |
| Embodiment 3 | 82.3 | 83.6 |
| Embodiment 4 | 80.7 | 82.1 |
| Embodiment 5 | 83.5 | 84.3 |
| Embodiment 6 | 89.6 | 91.3 |
| Embodiment 7 | 88.2 | 90.1 |
| Embodiment 8 | 87.9 | 89.2 |
| Embodiment 9 | 91.3 | 92.7 |
| Embodiment 10 | 92.7 | 94.1 |
| Embodiment 11 | 98.8 | 99.5 |
Test case 2
The taste removal effect of embodiment 1-11 and comparative example 1-2 the plant type space deodorant being prepared is tested.
Test method：With commercially available glued board (quality：2kg, thickness 1.5cm) as peculiar smell release source, spray embodiment
And the plant type space deodorant prepared in comparative example, every piece of glued board spray 2mL, it is 1m to be put into volume3In work chamber, work
20 DEG C of cabin temperature, relative humidity 50% seal work chamber, while preparing 2kg blank glued boards, without any processing, as
Control group, under similarity condition, sealing is placed.Work chamber is opened after 10 days, using concentration of formaldehyde in phenol reagent process determination of the environment cabin.
While opening work chamber, 140 osmatic participants are randomly divided into 14 groups, every group of 10 people, according to
Lower standard evaluates the peculiar smell of work chamber, and every group is averaged, and obtains peculiar smell evaluation result.
Evaluation criterion：Slightly weak peculiar smell, but have no irritating odor 1 point；Apparent peculiar smell, but have no irritating odor 2 points；
Slightly strong irritation peculiar smell 3 divides, strong irritation peculiar smell, it is difficult to endure 4 points.
Specific test result is shown in Table 2.
2 plant type space deodorant taste removal measure of merit result table of table
Claims (10)
1. a kind of plant type space deodorant, which is characterized in that the raw material including following weight parts：Ligustrum lucidum ait leaf extract 5-
10 parts, 2-5 parts of Flos Lonicerae extractive solution, 65-85 parts of water.
2. plant type space deodorant as described in claim 1, which is characterized in that further include the raw material of following weight parts：It is bitter
5-10 parts of melon extracting solution, 4-8 parts of Cortex Magnoliae Officinalis extracting solution.
3. plant type space deodorant as claimed in claim 2, which is characterized in that further include the raw material of following weight parts：Table
Activating agent 1-2 parts of face, 0.1-1 parts of cosolvent.
4. plant type space deodorant as claimed in claim 3, which is characterized in that the surfactant be polysorbas20 and/
Or butynediols diethoxy compound is modified bola type organosiloxanes.
5. plant type space deodorant as claimed in claim 3, which is characterized in that the cosolvent is carboxymethyl-β-ring paste
One or more mixtures in essence, maltodextrin, acesulfame potassium.
6. plant type space deodorant as claimed in claim 3, which is characterized in that the preparation method packet of the Cortex Magnoliae Officinalis extracting solution
Include following steps：Cortex Magnoliae Officinalis is crushed, 20-50 mesh sieve is crossed, obtains Cortex Magnoliae Officinalis powder, Cortex Magnoliae Officinalis powder and the ethyl alcohol that volume fraction is 50-70%
Aqueous solution in mass ratio 1：(4-6) is mixed, and it is 7.2-8.2 that the sodium bicarbonate aqueous solution for being 10% with mass fraction, which adjusts pH,
60-70 DEG C of refluxing extraction 100-180 minutes, using 300-500 mesh filter-cloth filterings, obtains first-time filtrate and a filter residue, primary to filter
The water of 5-10 times of Cortex Magnoliae Officinalis silty amount is added in slag, it is 7.2-8.2 that the sodium bicarbonate aqueous solution for being 10% with mass fraction, which adjusts pH,
In 80-90 DEG C of refluxing extraction 30-50 minutes, using 300-500 mesh filter-cloth filterings, secondary filtrate and secondary filter residue are obtained, is merged
First-time filtrate and secondary filtrate, the density for being concentrated under reduced pressure into 60 DEG C is 1.05-1.10g/mL, obtains Cortex Magnoliae Officinalis extracting solution.
7. plant type space deodorant as claimed in claim 3, which is characterized in that the preparation method packet of the balsam pear extract
Include following steps：Balsam pear drains surface moisture after cleaning, the water of 3-6 times of balsam pear quality is added after remove seed, and pulverizer mashing is added,
Balsam pear slurries are obtained, the pectase of balsam pear grind slurries quality 0.1-0.3% is added in balsam pear slurries, 60-120 is kept the temperature at 45-55 DEG C
Minute, enzyme deactivation in 1-5 minutes keep the temperature at 90-98 DEG C and is lived, obtains enzymolysis liquid, enzymolysis liquid in 50-60 DEG C of ultrasonic extraction 40-80 minutes,
It is centrifuged 20-30 minutes with 3000-5000 revs/min, supernatant uses 300-500 mesh filter-cloth filterings, obtains balsam pear extract.
8. plant type space deodorant as claimed in claim 3, which is characterized in that the preparation of the ligustrum lucidum ait leaf extract
Method includes the following steps：Fresh ligustrum lucidum ait leaf is taken, surface moisture is drained after cleaning, is dried to constant weight, powder at 40-60 DEG C
It is broken, 20-50 mesh sieve is crossed, ligustrum lucidum ait leaf powder, ligustrum lucidum ait leaf powder and water in mass ratio 1 are obtained：(5-10) is mixed, in 85-95
DEG C refluxing extraction 40-80 minutes, using 300-500 mesh filter-cloth filterings, obtains first-time filtrate and a filter residue, is added in a filter residue
The water of 5-10 times of ligustrum lucidum ait leaf silty amount, in 85-95 DEG C of refluxing extraction 30-50 minutes, using 300-500 mesh filter-cloth filterings,
Secondary filtrate and secondary filter residue are obtained, first-time filtrate and secondary filtrate are merged, the density for being concentrated under reduced pressure into 60 DEG C is 1.05-
1.10g/mL obtains ligustrum lucidum ait leaf extract.
9. plant type space deodorant as claimed in claim 3, which is characterized in that the preparation method of the Flos Lonicerae extractive solution
Include the following steps：By honeysuckle and water in mass ratio 1：(5-10) is mixed, in 85-95 DEG C of refluxing extraction 40-80 minute, use
300-500 mesh filter-cloth filterings obtain first-time filtrate and a filter residue, the water of 5-10 times of quality of Flos Lonicerae are added in a filter residue,
85-95 DEG C of refluxing extraction 30-50 minutes obtains secondary filtrate and secondary filter residue using 300-500 mesh filter-cloth filterings, merges one
Secondary filtrate and secondary filtrate, the density for being concentrated under reduced pressure into 60 DEG C is 1.05-1.10g/mL, obtains Flos Lonicerae extractive solution.
10. such as the preparation method of claim 3-9 any one of them plant type space deodorants, which is characterized in that by surface
Activating agent, cosolvent are added to the water, with 100-200 revs/min stir 5-10 minutes, sequentially add ligustrum lucidum ait leaf extract,
Balsam pear extract, Flos Lonicerae extractive solution, Cortex Magnoliae Officinalis extracting solution are stirred 10-20 minutes with 100-200 revs/min, using 300-500 mesh
Filter-cloth filtering, obtained filtrate are plant type space deodorant.
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Denomination of invention: A plant type indoor deodorant and its preparation method Effective date of registration: 20221020 Granted publication date: 20210604 Pledgee: Binkang Branch of Hangzhou United Rural Commercial Bank Co.,Ltd. Pledgor: HANGZHOU JP-TREE ENVIRONMENTAL TECHNOLOGY CO.,LTD. Registration number: Y2022330002715 |