CN108741408A - Insole and preparation method thereof with health-care efficacy - Google Patents
Insole and preparation method thereof with health-care efficacy Download PDFInfo
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- CN108741408A CN108741408A CN201810352973.XA CN201810352973A CN108741408A CN 108741408 A CN108741408 A CN 108741408A CN 201810352973 A CN201810352973 A CN 201810352973A CN 108741408 A CN108741408 A CN 108741408A
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- A—HUMAN NECESSITIES
- A43—FOOTWEAR
- A43B—CHARACTERISTIC FEATURES OF FOOTWEAR; PARTS OF FOOTWEAR
- A43B17/00—Insoles for insertion, e.g. footbeds or inlays, for attachment to the shoe after the upper has been joined
- A43B17/003—Insoles for insertion, e.g. footbeds or inlays, for attachment to the shoe after the upper has been joined characterised by the material
- A43B17/006—Insoles for insertion, e.g. footbeds or inlays, for attachment to the shoe after the upper has been joined characterised by the material multilayered
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- Footwear And Its Accessory, Manufacturing Method And Apparatuses (AREA)
Abstract
The invention discloses the insole and preparation method thereof with health-care efficacy, which includes three layers of nonwoven layer, two layers of cotton layer, one layer of polyurethane foaming layer, three layers of spandex fibre layer of cloth.Preparation method is：The aromatic micro-capsule prepared is organized on the cotton fabric of silicone Quaternary Ammonium Salt Antimicrobial Agent；Selection makes the cloth of insole, and layers of material is cut into the shape of insole；Insole is followed successively by spandex fibre layer of cloth, cotton layer, three layers of nonwoven layer, cotton layer, bamboo charcoal fiber layer of cloth, spandex fibre layer of cloth from lower to upper；Each layer is added glue in mold to be combined into one, forms insole.It has the beneficial effect that：Insole of the present invention can effectively inhibit bacteria breed on foot, cover foot odour, and performance is good, and health care can be carried out during shoes to sole by making to wear；Preparation method simple possible of the present invention, can make insole wrinkle resistant, keep original smooth appearance.
Description
Technical field
The present invention relates to insole technical fields, more particularly to the insole and preparation method thereof with health-care efficacy.
Background technology
With increasingly sharpening for today's society environmental problem, more and more bacteriums, microorganism, harmful fungoid invade
Our life causes the generation of many diseases and some puzzlements in life.In daily life, especially a large amount of movements
Afterwards, the sweat being discharged in vivo provides good growing environment to the growth of microorganism.Therefore, imparting dress materials are certain resists
Bacterium performance, which seems, to be even more important.For take and shoes textile for, be all added antiseptic mostly and have antibacterial
Function.Inorganic antiseptic is applied relatively broad in the fabric.Foot is one of human body significant points, because daily obtain wear shoes, foot quilt
Seal influences eubolism in shoes, can cause many step diseases, such as rheumatism, rheumatoid arthritis, tinea pedis, foot
Cold, foot odour etc..Existing insole has certain pliability as just a part for the support of shoes.But due to very much
The permeability of shoes is poor, causes to make the bacteria breed on foot, the skin for influencing foot normal during dress.So thoroughly controlling
More tinea pedis has become a great problem that people are badly in need of solution.
Invention content
One of the objects of the present invention is to provide a kind of bacteria breed that can effectively inhibit on foot, foot odour is covered, is used
Excellent performance makes to wear the insole with health-care efficacy that can carry out health care during shoes to sole.
The second object of the present invention is to provide a kind of preparation method simple possible, insole can be made wrinkle resistant, keep original flat
The preparation method of the insole with health-care efficacy of whole appearance.
The present invention in view of the above technology in the problem of mentioning, the technical solution taken is：
Insole with health-care efficacy contains essential oil microcapsules on insole cotton layer, and the preparation method of essential oil microcapsules is：It will
Saturation beta-cyclodextrin aqueous solution is slowly poured into the ethyl alcohol dissolving of lemon, and glyceraldehyde, the micro- glue that will be prepared after stirring is added
Capsule lotion stands 20-30h under conditions of 2-6 DEG C, after vacuum filtration low temperature drying to constant weight to get essential oil microcapsules.The system
Preparation Method embedding rate is high, yield is high, and essential oil microcapsules particle diameter distribution obtained is uniform, and microcapsules of the grain size between 10 μm account for
90% or more, microcapsules obtained can effectively kill a large amount of bacteriums, achieve the purpose that treat foot odour, while also having contraction micro-
Blood vessel, the effect of itching, slowing down inflammation and burn of releiving, can also exclude vivotoxin, be played to eczema, addiction caused by skin
Good improvement result, and foot odour can be covered so that insole has preferable healthcare function.
Preferably, the ratio of R types and S types is 55-60 in glyceraldehyde:1.The addition of the glyceraldehyde can reduce lemon extract
Van der Waals between oil molecule so that the grain size of lemon reduces rapidly under stirring conditions, can be easier
It obtains and enters in cyclodextrin cavity, while the group on glyceraldehyde and beta-cyclodextrin is mutually handed over by molecular force or electrostatic interaction
Connection gets up, and forms the macromolecule of reticular structure, and lemon is wrapped up wherein during being cross-linked with each other to form microballoon,
Improve the stability of follow-up essential oil microcapsules, and the addition of glyceraldehyde can improve lemon molecule and beta-cyclodextrin water with
Dispersibility in the continuous phase that ethyl alcohol is blended, and then coated well by cyclodextrin, improve embedding rate and the production of essential oil microcapsules
Rate, and then the bactericidal effect of essential oil microcapsules is improved, the final antibiotic health function of improving insole.
Preferably, the volume ratio of lemon and ethyl alcohol is 1:The weight ratio of 8-12, lemon and beta-cyclodextrin is
1:7-9。
Preferably, whipping temp is 45-55 DEG C, mixing speed 800-1000r/min, time 2-3h.
Preferably, insole includes three layers of nonwoven layer, two layers of cotton layer, one layer of polyurethane foaming layer, three layers of spandex fibre
Tie up layer of cloth.The insole can ensure that essential oil microcapsules cotton layer exists by the design of essential oil microcapsules cotton layer and each bed of cloth
It is firm inside sole to retain, it can effectively inhibit the bacteria breed on foot, sole can be protected during shoes by making to wear
It is strong, it is with obvious effects.
The preparation method of insole with health-care efficacy, it is characterised in that：Include the following steps：
Cotton Fabric：The aromatic micro-capsule prepared is organized on the cotton fabric of silicone Quaternary Ammonium Salt Antimicrobial Agent；
Sorting：Selection make insole cloth, including three layers of nonwoven layer, two layers of cotton layer, two layers of spandex fibre layer of cloth, one layer
Bamboo charcoal fiber layer of cloth, and layers of material is cut into the shape of insole；
Prepare insole：It is fine that insole is followed successively by spandex fibre layer of cloth, cotton layer, three layers of nonwoven layer, cotton layer, bamboo charcoal from lower to upper
Tie up layer of cloth, spandex fibre layer of cloth；
Composite molding：Each layer is added glue in mold to be combined into one, forms insole.The preparation method of the insole is simple,
Can mass produce, preparation so that insole has both function that is antimycotic, covering foot odour, making to wear can be right during shoes
Sole carries out health care, and insole can be made wrinkle resistant, keeps original smooth appearance, improves the performance of insole.
Preferably, Cotton Fabric the specific steps are：Crosslinking agent is added to 45-55（g/L）Essential oil microcapsules
In lotion, the weight ratio of crosslinking agent and essential oil microcapsules is 1:0.4-0.6, the method rolled using two leachings two, pick-up 65-
75%, prebaking temperature is 65-75 DEG C, time 2-3min, and baking temperature is 100-120 DEG C, time 3-5min, will there is essence
Oil microcapsule is organized on the cotton fabric layer of silicone Quaternary Ammonium Salt Antimicrobial Agent, bath raio 1:38-43 is dried after washing, you can.
Active group in silicone Quaternary Ammonium Salt Antimicrobial Agent contains more alkyl again, by crosslinking agent first and in antibacterial cotton fabric
OH-Or beta-cyclodextrin reaction, then with the OH on beta-cyclodextrin or antibacterial cotton fabric footwear material-Reaction, makes essential oil microcapsules anchor at anti-
The film surface of bacterium cotton fabric so that insole has both function that is antimycotic, covering foot odour.
Further preferably, it is 1 that crosslinking agent, which is weight ratio,:The citric acid of 0.23-0.29 and the mixture of malic acid, malic acid
The weight ratio of middle D-malic acid and L MALIC ACID is 0.35-0.43:1.The rational proportion of citric acid and malic acid in the crosslinking agent,
The stress distribution that crosslinking generates can be made uniform, and then distribution and combination of the essential oil microcapsules on cotton fabric are evenly, to
Slow down cotton fabric strength retention variation, and in the malic acid D-malic acid and L MALIC ACID special proportioning, may make
Crosslinking agent occurs covalent cross-linking with the cellulosic molecule on cotton fabric and reacts, and crosslinking agent is connected to cotton fabric with covalent bond effect
On, to strengthen the lateral force between cellulosic molecule, the opposite sliding between cellulosic molecule is hindered, cotton fabric can be made
Original smooth appearance is kept, it is wrinkle resistant to achieve the purpose that even if deformation, is also easy to restore, improve the performance of insole.
Compared with the prior art, the advantages of the present invention are as follows：1）Insole of the present invention is by essential oil microcapsules cotton layer and respectively
The design of a bed of cloth can ensure that essential oil microcapsules cotton layer consolidates inside sole and retain, can effectively inhibit thin on foot
Bacterium grows, and sole can be carried out health care during shoes by making to wear, with obvious effects；2）The preparation method letter of insole of the present invention
It is single, can mass produce, essential oil microcapsules is made to anchor at the film surface of antibacterial cotton fabric so that insole have both it is antimycotic,
Cover the function of foot odour；3）The present invention keeps original smooth appearance with cotton fabric, even if deformation, is also easy to restore, to make
Insole achievees the purpose that wrinkle resistant, improves the performance of insole.
Specific implementation mode
The present invention program is described further below by embodiment：
Embodiment 1：
Insole with health-care efficacy contains essential oil microcapsules on insole cotton layer, and the preparation method of essential oil microcapsules is：It will
Saturation beta-cyclodextrin aqueous solution is slowly poured into the ethyl alcohol dissolving of lemon, and glyceraldehyde, the micro- glue that will be prepared after stirring is added
Capsule lotion stands 30h under conditions of 2 DEG C, after vacuum filtration low temperature drying to constant weight to get essential oil microcapsules.The preparation method
Embedding rate is high, yield is high, and essential oil microcapsules particle diameter distribution obtained is uniform, and microcapsules of the grain size between 10 μm account for 90% or more,
Microcapsules obtained can effectively kill a large amount of bacteriums, achieve the purpose that treat foot odour, while also having and shrinking capilary, releiving
The effect of itching, slowing down inflammation and burn, can also exclude vivotoxin, play to eczema, addiction caused by skin and change well
Kind effect, and foot odour can be covered so that insole has preferable healthcare function.
The ratio of R types and S types is 55 in above-mentioned glyceraldehyde:1.The addition of the glyceraldehyde can reduce lemon molecule it
Between Van der Waals for so that the grain size of lemon reduces rapidly under stirring conditions, can be easier enter ring
Group in dextrin cavity, while on glyceraldehyde and beta-cyclodextrin is cross-linked with each other by molecular force or electrostatic interaction,
The macromolecule of reticular structure is formed, and lemon is wrapped up wherein, after raising during being cross-linked with each other to form microballoon
The stability of continuous essential oil microcapsules, and the addition of glyceraldehyde can improve lemon molecule and beta-cyclodextrin and is total in water and ethyl alcohol
Dispersibility in mixed continuous phase, and then coated well by cyclodextrin, the embedding rate and yield of essential oil microcapsules are improved, in turn
Improve the bactericidal effect of essential oil microcapsules, the final antibiotic health function of improving insole.
The volume ratio of above-mentioned lemon and ethyl alcohol is 1:12, the weight ratio of lemon and beta-cyclodextrin is 1:7.
Above-mentioned whipping temp is 45 DEG C, mixing speed 1000r/min, time 2h.
Above-mentioned insole includes three layers of nonwoven layer, two layers of cotton layer, one layer of polyurethane foaming layer, three layers of spandex fibre cloth
Layer.The insole can ensure that essential oil microcapsules cotton layer in sole by the design of essential oil microcapsules cotton layer and each bed of cloth
Inside is firm to retain, and can effectively inhibit the bacteria breed on foot, and sole can be carried out health care, effect during shoes by making to wear
Fruit is apparent.
The preparation method of insole with health-care efficacy, it is characterised in that：Include the following steps：
1）Cotton Fabric：The aromatic micro-capsule prepared is organized on the cotton fabric of silicone Quaternary Ammonium Salt Antimicrobial Agent；
2）Sorting：Selection makes the cloth of insole, including three layers of nonwoven layer, two layers of cotton layer, two layers spandex fibre layer of cloth, one
Layer bamboo charcoal fiber layer of cloth, and layers of material is cut into the shape of insole；
3）Prepare insole：Insole is followed successively by spandex fibre layer of cloth, cotton layer, three layers of nonwoven layer, cotton layer, bamboo charcoal from lower to upper
Scrim cloth, spandex fibre layer of cloth；
4）Composite molding：Each layer is added glue in mold to be combined into one, forms insole.The preparation method letter of the insole
It is single, it can mass produce, preparation makes insole have both function that is antimycotic, covering foot odour, makes to wear shoes in the process i.e.
Health care can be carried out to sole, and insole can be made wrinkle resistant, kept original smooth appearance, improve the performance of insole.
Above-mentioned Cotton Fabric the specific steps are：Crosslinking agent is added to 55（g/L）Essential oil microcapsules lotion in, hand over
The weight ratio for joining agent and essential oil microcapsules is 1:0.4, the method rolled using two leachings two, pick-up 75%, prebaking temperature is 65
DEG C, time 3min, baking temperature is 100 DEG C, time 5min, will have essential oil microcapsules to be organized in and resists in organosilicon quaternary ammonium salt
On the cotton fabric layer of microbial inoculum, bath raio 1:38, it is dried after washing, you can.Active group weight in silicone Quaternary Ammonium Salt Antimicrobial Agent
Containing more alkyl, pass through OH of the crosslinking agent first and in antibacterial cotton fabric-Or beta-cyclodextrin reaction, then with beta-cyclodextrin or anti-
OH in bacterium cotton fabric footwear material-Reaction, makes essential oil microcapsules anchor at the film surface of antibacterial cotton fabric so that insole has both anti-
Fungi, the function of covering foot odour.
Above-mentioned crosslinking agent is that weight ratio is 1:0.29 citric acid and the mixture of malic acid, in malic acid D-malic acid and
The weight ratio of L MALIC ACID is 0.35:1.The rational proportion of citric acid and malic acid in the crosslinking agent can be such that crosslinking generates
Stress distribution is uniform, and then distribution and combination of the essential oil microcapsules on cotton fabric are evenly, to slow down the strong of cotton fabric
Power retention rate changes, and in the malic acid D-malic acid and L MALIC ACID special proportioning, may make on crosslinking agent and cotton fabric
Cellulosic molecule occur covalent cross-linking reaction, crosslinking agent is connected on cotton fabric with covalent bond effect, to strengthen fibre
The intermolecular lateral force of dimension element hinders the opposite sliding between cellulosic molecule, cotton fabric can be made to keep original smooth
Appearance, it is wrinkle resistant to achieve the purpose that even if deformation, is also easy to restore, improve the performance of insole.
Embodiment 2：
Insole with health-care efficacy contains essential oil microcapsules on insole cotton layer, and the preparation method of essential oil microcapsules is：It will
Saturation beta-cyclodextrin aqueous solution is slowly poured into the ethyl alcohol dissolving of lemon, and glyceraldehyde, the micro- glue that will be prepared after stirring is added
Capsule lotion is stood for 24 hours under conditions of 4 DEG C, after vacuum filtration low temperature drying to constant weight to get essential oil microcapsules.Above-mentioned glyceraldehyde
The ratio of middle R types and S types is 58:1；The volume ratio of lemon and ethyl alcohol is 1:10, the weight of lemon and beta-cyclodextrin
Than being 1:8；Whipping temp is 50 DEG C, mixing speed 900r/min, time 2.5h.
Above-mentioned insole includes three layers of nonwoven layer, two layers of cotton layer, one layer of polyurethane foaming layer, three layers of spandex fibre cloth
Layer.
The preparation method of insole with health-care efficacy, it is characterised in that：Include the following steps：
1）Cotton Fabric：Crosslinking agent is added to 50（g/L）Essential oil microcapsules lotion in, crosslinking agent and essential oil microcapsules
Weight ratio is 1:0.5, using two leachings, two methods rolled, pick-up 70%, prebaking temperature is 70 DEG C, time 2.5min, roasting
Dry temperature be 110 DEG C, time 4min, will there are essential oil microcapsules to be organized in the cotton fabric layer in silicone Quaternary Ammonium Salt Antimicrobial Agent
On, bath raio 1:40, it is dried after washing, you can, above-mentioned crosslinking agent is that weight ratio is 1:0.26 citric acid and malic acid it is mixed
Object is closed, the weight ratio of D-malic acid and L MALIC ACID is 0.4 in malic acid:1；
2）Sorting：Selection makes the cloth of insole, including three layers of nonwoven layer, two layers of cotton layer, two layers spandex fibre layer of cloth, one
Layer bamboo charcoal fiber layer of cloth, and layers of material is cut into the shape of insole；
3）Prepare insole：Insole is followed successively by spandex fibre layer of cloth, cotton layer, three layers of nonwoven layer, cotton layer, bamboo charcoal from lower to upper
Scrim cloth, spandex fibre layer of cloth；
4）Composite molding：Each layer is added glue in mold to be combined into one, forms insole.
Embodiment 3：
The preparation method of essential oil microcapsules is：Saturation beta-cyclodextrin aqueous solution is slowly poured into the ethyl alcohol dissolving of lemon, is stirred
The microcapsule emulsion prepared is stood for 24 hours under conditions of 4 DEG C after mixing, after vacuum filtration low temperature drying to constant weight to get essence
Oil microcapsule.The volume ratio of above-mentioned lemon and ethyl alcohol is 1:10, the weight ratio of lemon and beta-cyclodextrin is 1:8；It stirs
Mix temperature be 50 DEG C, mixing speed 900r/min, time 2.5h.
Embodiment 4：
The embedding rate and yield of essential oil microcapsules
The essential oil microcapsules prepared are weighed into 0.5g, are dissolved in 20mL ethyl alcohol, ultrasonication 15min makes essential oil microcapsules
Wall material fully ruptures, and releases lemon, then the essential oil microcapsules that ultrasound is crossed filter, and obtain lemon ethanol solution,
It takes out 5mL solution and measures its concentration.
Essential oil microcapsules drugloading rate and the governing equation of its concentration are：
α=(w×5×5)/(0.5×106)×100%
In formula：α is essential oil microcapsules drugloading rate（%）；W is the concentration of lemon ethanol solution（mg/mL）.
The governing equation of the embedding rate of the micro- glue of essential oil is：
λ=(α×M)/m1×100%
In formula：λ is the embedding rate of the micro- glue of essential oil（%）, M is the quality of obtained essential oil microcapsules（g）；m1For lemon
Quality（g）.
The governing equation of the micro- glue yield of essential oil is：
b=M/(m1+ m2)×100%
In formula：B is the micro- glue yield of essential oil（%）, m2For the quality of beta-cyclodextrin（g）.
The embedding rate and yield of essential oil microcapsules in embodiment 2 and embodiment 3 are calculated, the results are shown in Table 1.
The embedding rate and yield of 1 essential oil microcapsules of table
| Sample | Embedding rate（%） | Yield（%） |
| Embodiment 2 | 79.98 | 70.24 |
| Embodiment 3 | 67.56 | 61.32 |
As shown in Table 1, implement the embedding rate of 2 essential oil microcapsules and yield is above embodiment 3, illustrate the addition energy of glyceraldehyde
Enough improve the embedding rate and yield of essential oil microcapsules.
Routine operation in the operating procedure of the present invention is well known to those skilled in the art, herein without repeating.
Technical scheme of the present invention is described in detail in embodiment described above, it should be understood that the above is only
For specific embodiments of the present invention, it is not intended to restrict the invention, all any modifications made in the spirit of the present invention,
Supplement or similar fashion replacement etc., should all be included in the protection scope of the present invention.
Claims (8)
1. the insole with health-care efficacy, it is characterised in that：Contain essential oil microcapsules, the essential oil on the insole cotton layer
The preparation method of microcapsules is：Saturation beta-cyclodextrin aqueous solution is slowly poured into the ethyl alcohol dissolving of lemon, glyceraldehyde is added,
The microcapsule emulsion prepared is stood into 20-30h under conditions of 2-6 DEG C after stirring, after vacuum filtration low temperature drying to constant weight,
Up to essential oil microcapsules.
2. the insole according to claim 1 with health-care efficacy, it is characterised in that：R types and S types in the glyceraldehyde
Ratio is 55-60:1.
3. the insole according to claim 1 with health-care efficacy, it is characterised in that：The body of the lemon and ethyl alcohol
Product is than being 1:The weight ratio of 8-12, lemon and beta-cyclodextrin is 1:7-9.
4. the insole according to claim 1 with health-care efficacy, it is characterised in that：The whipping temp be 45-55 DEG C,
Mixing speed is 800-1000r/min, time 2-3h.
5. the insole according to claim 1 with health-care efficacy, it is characterised in that：The insole includes three layers of non-woven fabrics
Layer, two layers of cotton layer, one layer of polyurethane foaming layer, three layers of spandex fibre layer of cloth.
6. the preparation method of the insole with health-care efficacy, it is characterised in that：Include the following steps：
1）Cotton Fabric：The aromatic micro-capsule prepared is organized on the cotton fabric of silicone Quaternary Ammonium Salt Antimicrobial Agent；
2）Sorting：Selection makes the cloth of insole, including three layers of nonwoven layer, two layers of cotton layer, two layers spandex fibre layer of cloth, one
Layer bamboo charcoal fiber layer of cloth, and layers of material is cut into the shape of insole；
3）Prepare insole：Insole is followed successively by spandex fibre layer of cloth, cotton layer, three layers of nonwoven layer, cotton layer, bamboo charcoal from lower to upper
Scrim cloth, spandex fibre layer of cloth；
4）Composite molding：Each layer is added glue in mold to be combined into one, forms insole.
7. the preparation method of the insole according to claim 6 with health-care efficacy, it is characterised in that：The cotton fabric is whole
Reason the specific steps are：Crosslinking agent is added to 45-55（g/L）Essential oil microcapsules lotion in, crosslinking agent and essential oil microcapsules
Weight ratio be 1:0.4-0.6, using two leachings, two methods rolled, pick-up 65-75%, prebaking temperature is 65-75 DEG C, when
Between be 2-3min, baking temperature is 100-120 DEG C, time 3-5min, will have essential oil microcapsules to be organized in organosilicone quaternary ammonium
On the cotton fabric layer of salt antiseptic, bath raio 1:38-43 is dried after washing, you can.
8. the preparation method of the insole according to claim 6 with health-care efficacy, it is characterised in that：The crosslinking agent is
Weight ratio is 1:The citric acid of 0.23-0.29 and the mixture of malic acid, D-malic acid and L MALIC ACID in the malic acid
Weight ratio is 0.35-0.43:1.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810352973.XA CN108741408B (en) | 2018-04-19 | 2018-04-19 | Insole with health care effect and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810352973.XA CN108741408B (en) | 2018-04-19 | 2018-04-19 | Insole with health care effect and preparation method thereof |
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| Publication Number | Publication Date |
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| CN108741408A true CN108741408A (en) | 2018-11-06 |
| CN108741408B CN108741408B (en) | 2021-03-02 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201810352973.XA Active CN108741408B (en) | 2018-04-19 | 2018-04-19 | Insole with health care effect and preparation method thereof |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110564515A (en) * | 2019-08-20 | 2019-12-13 | 广东工业大学 | Essence microcapsule grafted with organic silicon quaternary ammonium salt and preparation method and application thereof |
| USD903268S1 (en) | 2019-02-06 | 2020-12-01 | S. C. Johnson & Son, Inc. | Insole |
| USD906658S1 (en) | 2019-02-19 | 2021-01-05 | S. C. Johnson & Son, Inc. | Insole |
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| CN103170286A (en) * | 2013-01-30 | 2013-06-26 | 天津商业大学 | Method for preparing melissa officinalis L. essential oil and beta-cyclodextrin molecule microcapsule |
| CN104921406A (en) * | 2015-07-06 | 2015-09-23 | 陕西科技大学 | Preparation method for antifungal and deodorized insole |
| CN105544230A (en) * | 2016-01-15 | 2016-05-04 | 中山大学惠州研究院 | Method for perfuming textile by applying tea tree essential oil microcapsules |
| CN106263263A (en) * | 2016-08-12 | 2017-01-04 | 张太平 | A kind of shoe pad with bacteriostatic deodorizing effect |
| CN107772647A (en) * | 2017-10-17 | 2018-03-09 | 李海明 | A kind of preparation method of health insoles |
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2018
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Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103170286A (en) * | 2013-01-30 | 2013-06-26 | 天津商业大学 | Method for preparing melissa officinalis L. essential oil and beta-cyclodextrin molecule microcapsule |
| CN104921406A (en) * | 2015-07-06 | 2015-09-23 | 陕西科技大学 | Preparation method for antifungal and deodorized insole |
| CN105544230A (en) * | 2016-01-15 | 2016-05-04 | 中山大学惠州研究院 | Method for perfuming textile by applying tea tree essential oil microcapsules |
| CN106263263A (en) * | 2016-08-12 | 2017-01-04 | 张太平 | A kind of shoe pad with bacteriostatic deodorizing effect |
| CN107772647A (en) * | 2017-10-17 | 2018-03-09 | 李海明 | A kind of preparation method of health insoles |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| USD903268S1 (en) | 2019-02-06 | 2020-12-01 | S. C. Johnson & Son, Inc. | Insole |
| USD906658S1 (en) | 2019-02-19 | 2021-01-05 | S. C. Johnson & Son, Inc. | Insole |
| USD935758S1 (en) | 2019-02-19 | 2021-11-16 | S. C. Johnson & Son, Inc. | Insole |
| CN110564515A (en) * | 2019-08-20 | 2019-12-13 | 广东工业大学 | Essence microcapsule grafted with organic silicon quaternary ammonium salt and preparation method and application thereof |
Also Published As
| Publication number | Publication date |
|---|---|
| CN108741408B (en) | 2021-03-02 |
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