CN1087148A - Huang, bluish dogbane bast softening agent and production method thereof - Google Patents
Huang, bluish dogbane bast softening agent and production method thereof Download PDFInfo
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- CN1087148A CN1087148A CN 93109719 CN93109719A CN1087148A CN 1087148 A CN1087148 A CN 1087148A CN 93109719 CN93109719 CN 93109719 CN 93109719 A CN93109719 A CN 93109719A CN 1087148 A CN1087148 A CN 1087148A
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Abstract
The present invention relates to a kind of composition of mixture.By mineral oil, vegetable oil, lipophilic surfactant, organic aliphatic acid, organic amine, hydrophilic surfactant active, water and prepare by a certain percentage, stir and form.This bast softening agent outward appearance is the oyster white glop, pH value 7.0, solid content (105 ℃) % is 76.82, the aqueous solution is " all energy is miscible with cold water, hot water arbitrary proportion ", stability is " 1% aqueous solution put 72 hours not stratified ", and smell is " having no irritating odor ".Reach soft before adopting this bast softening agent can make Huang, bluish dogbane combing spinning, also can be used as the softener of all kinds of bast fibre spinning products, have stronger permeability, the fermentation calefaction performance of coming unstuck is also better.Characteristics be the processing time short, the finished product whiteness is good, method of operating simple, save time, laborsaving.
Description
The present invention relates to a kind of composition of mixture, especially bast softening agent and the production method of using for a kind of bast fibre spinning processing industry thereof.
At present, bast fibre spinning producer adopts traditional linen softening oil system emulsifying process on the softening engineering, this linen softening oil system breast technology: exist heavy operation work, and emulsion quality instability, very easily separate, thereby reduced its permeability, lubricity effect; Exist also that the technological process of production is long, the many easily plugging roads of foam, cost height, poor product quality, whiteness are poor; Also exist: the bast fibre spinning goods with linen softening oil production have been subjected to clients' restriction abroad such as the U.S., West Germany in the export trade, require to use linen softening oil less than 3%, propose again now to stop to use linen softening oil, and this has just limited the foreign trade activity of jute mill's product.
The object of the invention is to avoid the weak point in the above prior art, and provide a kind of water-soluble, good stability, that have no irritating odor, good penetrability, when making labour intensity little, the oyster white glop.
Composition of the present invention, proportioning (percentage by weight) are: mineral oil 30-50, vegetable oil 1-10, lipophilic surfactant 0.2-3.0, organic aliphatic acid 0.5-10, organic amine 0.3-6.0, hydrophilic surfactant active 0.1-3.0, the water yield is the surplus in the percentage.Said vegetable oil can be peanut oil, can be rapeseed oil, can be soya-bean oil, can be the cottonseed wet goods.
Preparation method of the present invention (referring to: technological process of production figure):
A certain amount of mineral oil, vegetable oil, hydrophilic surfactant active are added in the I reactor, adding a certain amount of cold water again stirs, in addition, with a certain amount of hot water, organic aliphatic acid, organic amine insert in another container mix after, slowly join in the I reactor, stirred 30 minutes emulsion; Add a certain amount of water, hydrophilic surfactant active again in the II reactor, under agitation slowly join the emulsion in the I reactor in the II reactor this moment, and stirred 30 minutes milky glop, i.e. the bast softening agent of paste body shape.
Embodiment 1, as stated above, in the I reactor, add mineral oil 400kg, vegetable oil 100kg, lipophilic surfactant 2kg, start stirring, add cold water 80kg, in addition with organic aliphatic acid 10kg, organic amine 5kg, after 70 ℃ of hot water 80kg mix, slowly join in the I reactor, continue to stir 30 minutes; In the II reactor, add hydrophilic surfactant active 1kg, cold water 322kg starts stirring, and the emulsion in the I reactor slowly is added in the II reactor, adds the back and continues to stir 30 minutes, gets product-bast softening agent 1000kg.
Embodiment 2, as stated above, in the I reactor, add mineral oil 450kg, vegetable oil 50kg, lipophilic surfactant 3kg, start stirring, add cold water 80kg, after in addition organic aliphatic acid 5kg, organic amine 3kg, 70 ℃ of hot water 80kg being mixed, slowly join in the I reactor, continue to stir 30 minutes; In the II reactor, add hydrophilic surfactant active 2kg, cold water 327kg, start stirring, and, slowly join in the II reactor the emulsion in the I reactor, add the back and continue to stir 30 minutes, get product-bast softening agent 1000kg.
Embodiment 3, as stated above adds mineral oil 500kg, vegetable oil 30kg, lipophilic surfactant 5kg, start stirring, add cold water 80kg, in addition, with organic aliphatic acid 5kg, organic amine 10kg, 70 ℃ of hot water 80kg, after the mixing, slowly join in the I reactor, continue to stir 30 minutes; In the II reactor, add hydrophilic surfactant active 5kg, cold water 285kg starts stirring, and with the emulsion in the I reactor, slowly is added in the II reactor, after adding, continues to stir 30 minutes, gets product-bast softening agent 1000kg.
The main performance index of this bast softening agent: outward appearance is the oyster white glop, pH value 7.0, solid content (105 ℃) % is 76.82, the aqueous solution is " all energy is miscible with cold water, hot water arbitrary proportion ", stability is " 1% aqueous solution put 72 hours not stratified ", and smell is " having no irritating odor ".
When this bast softening agent dispatches from the factory, adopt iron sheet barrel with cover or Plastic Drum packing, can store six months under the normal temperature.
Good effect of the present invention:
This bast softening agent is easy to use, need not heat and make, and can dilute with normal temperature running water or well water, and have certain stability, and 1% aqueous solution is put 72 hours no multi_layer extraction phenomenons; In the use, each operation semi-finished product regain keeps better having stronger permeability, and the fermentation calefaction performance of coming unstuck is also better; The characteristics of this Huang, bluish dogbane bast softening agent be the processing time short, the finished product whiteness is good, method of operating is simple, time saving and energy saving; Reach soft before making Huang, bluish dogbane combing spinning, the softening agent that also can be used as all kinds of flax products uses.
Claims (2)
1, a kind of Huang, bluish dogbane bast softening agent is characterized in that:
A, this bast softening agent are a kind of compositions of mixture, and outward appearance is milky glop-paste body shape,
The composition of b, this bast softening agent and percentage by weight are: mineral oil 30-50, and vegetable oil 1-10, lipophilic surfactant 0.2-3.0, organic aliphatic acid 0.5-10, organic amine 0.3-6.0, hydrophilic surfactant active 0.1-3.0, the water yield is the surplus in the percentage.
2,, it is characterized in that the production method of this bast softening agent is according to the production method of the described Huang of claim 1, bluish dogbane bast softening agent:
A certain amount of mineral oil, vegetable oil, hydrophilic surfactant active are added in the I reactor, adding a certain amount of cold water again stirs, in addition a certain amount of hot water, organic aliphatic acid, organic amine are inserted in another container mix after, slowly join in the I reactor, stirred 30 minutes; Add a certain amount of water, hydrophilic surfactant active again in the II reactor, under agitation slowly join the material in the I reactor (emulsion) in the II reactor this moment, stirred 30 minutes.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 93109719 CN1087148A (en) | 1993-08-14 | 1993-08-14 | Huang, bluish dogbane bast softening agent and production method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 93109719 CN1087148A (en) | 1993-08-14 | 1993-08-14 | Huang, bluish dogbane bast softening agent and production method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN1087148A true CN1087148A (en) | 1994-05-25 |
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ID=4987758
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 93109719 Pending CN1087148A (en) | 1993-08-14 | 1993-08-14 | Huang, bluish dogbane bast softening agent and production method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN1087148A (en) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN100427666C (en) * | 2005-12-20 | 2008-10-22 | 东华大学 | Carding refining method for jute |
| CN106676886A (en) * | 2015-11-05 | 2017-05-17 | 南通恒成化工有限公司 | Linen softening oil |
| CN106676896A (en) * | 2015-11-05 | 2017-05-17 | 南通恒成化工有限公司 | Linen softening agent |
| CN110230192A (en) * | 2019-06-27 | 2019-09-13 | 重庆市晶苎纺织品有限公司 | A kind of preparation method for expecting high-quality softening liquid for softening fiber crops |
-
1993
- 1993-08-14 CN CN 93109719 patent/CN1087148A/en active Pending
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN100427666C (en) * | 2005-12-20 | 2008-10-22 | 东华大学 | Carding refining method for jute |
| CN106676886A (en) * | 2015-11-05 | 2017-05-17 | 南通恒成化工有限公司 | Linen softening oil |
| CN106676896A (en) * | 2015-11-05 | 2017-05-17 | 南通恒成化工有限公司 | Linen softening agent |
| CN110230192A (en) * | 2019-06-27 | 2019-09-13 | 重庆市晶苎纺织品有限公司 | A kind of preparation method for expecting high-quality softening liquid for softening fiber crops |
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| C01 | Deemed withdrawal of patent application (patent law 1993) | ||
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