CN1086845A

CN1086845A - A kind of tooth-brush cleaning liquid and preparation method thereof

Info

Publication number: CN1086845A
Application number: CN 92112453
Authority: CN
Inventors: 张世国; 李芳芳
Original assignee: Individual
Current assignee: Individual
Priority date: 1992-11-07
Filing date: 1992-11-07
Publication date: 1994-05-18

Abstract

The invention discloses a kind of tooth-brush cleaning liquid, it is by the A component: the distillate of elscholtiza, the root of Chinese wild ginger, peppermint, Mongollian Thyme Herb, B component: the decocting liquid of crape myrtle, the root of large-flowered skullcap, C component: the condensing crystal product of largeseed hemsleya root, giant knotweed, Glossy Privet Fruit, Han dish, the D component: the water cooking liquid of Semen Raphani, golden hop, wintergreen cooperates treated forming with certain proportion.Can make things convenient for, clean effectively or remove with this scavenging solution attached to harmful bacterium and virus on toothbrush or the artificial tooth.This product is safe in utilization, without any side effects, and is with low cost, and preparation technology is simple, easily mass-produced.

Description

A kind of tooth-brush cleaning liquid and preparation method thereof

The present invention relates to a kind of tooth-brush cleaning liquid, belong to daily life clean-out system and preparing technical field thereof.

Toothbrush is a requisite cleaning appliance in people's daily life, the method of traditional placement toothbrush is head-up or towards being placed down in the cup with it, cause and be exposed to airborne brush a large amount of bacterial reproductions are arranged, its quantity gives sb. the shiver, result of study shows that the bacterial count on the pieces of toothbrush reaches 1.5 * 10 ⁸, also there are a large amount of bacteriums in addition on the detachable dental prostheses, every square centimeter bacterial count reaches 1.1 * 10 ⁷, and these bacteriums is of a great variety, extremely harmful to human body, in addition, also has the various viruses of some amount on artificial tooth, these bacteriums and virus are because of brushing teeth once more and when wearing artificial tooth, being brought into the oral cavity, and is not only unhygienic, also may cause some disease.For this reason, press for solve toothbrush with after the bacterial contamination problem, it is essential that the scavenging solution that is exclusively used in toothbrush then becomes people's daily life institute.

Task of the present invention for a kind of tooth-brush cleaning liquid is provided, is cleaned or immersion toothbrush and artificial tooth with this scavenging solution exactly, can kill up hill and dale or remove attached to each bacterioid and virus on toothbrush or the artificial tooth, and bacterium is brought into when having avoided brushing teeth once more.

Another task of the present invention provides a kind of preparation method of tooth-brush cleaning liquid.

Task of the present invention is finished like this.The alleged selected raw material of tooth-brush cleaning liquid is based on the pharmacology analysis of these raw materials and definite among the present invention.

Tooth-brush cleaning liquid of the present invention is made of with the certain proportion cooperation following several components:

The A component: the distillate of elscholtiza, the root of Chinese wild ginger, peppermint, Mongollian Thyme Herb, surplus liquid filtered liquid and residue filtrate,

The B component: the decocting liquid of crape myrtle, the root of large-flowered skullcap and the crude product behind the suction filtration,

The C component: the crystallization product after the concentrated solution of largeseed hemsleya root, giant knotweed, Glossy Privet Fruit, Han dish and the filtration,

D component: dish clothes, golden hop, wintergreen water cooking liquid.

Above-mentioned each component is promptly got tooth-brush cleaning liquid of the present invention after the combination treatment in certain proportion.

The ratio (weight ratio) of generally getting A: B: C: D is 1: 4-5: 4-6: 1-3.

Best proportioning A: B: C: D selects 1: 4: 5: 2 is best.

Proportioning raw materials in the each component is (weight):

A component: elscholtiza: the root of Chinese wild ginger: peppermint: Mongollian Thyme Herb selects 1: 1-2: 1-3: 1-2,

Preferably select 1: 1: 1: 1

B component: crape myrtle: the root of large-flowered skullcap=1: 1-3

Preferably select crape myrtle: the root of large-flowered skullcap=1: 1

C component: largeseed hemsleya root: giant knotweed: Glossy Privet Fruit ∶ Han dish=1: 1-2: 1-2: 1-3

Preferably select 1: 1: 1: 1

D component: dish clothes: golden hop: wintergreen=1: 1-2: 1-2

Preferably select 1: 1: 1

The preparation method of tooth-brush cleaning liquid of the present invention is as follows:

At first prepare A, B, C, D divide component:

Preparation A component: after mixing by listed proportioning material cleaned up and add hydrodistillation extractive distillation liquid, surplus liquid filters, and residue adds ethanol and soaks certain hour and get filtrate, and heating uses activated carbon decolorizing, suction filtration to get filtrate and distillate promptly gets the A component.

Used ethanol liquid is generally 40-70% ethanol in the aforesaid method, soaks about 30 minutes of activated carbon decolorizing, bleaching temperature 60-80 ℃ 30-60 minute.

Preparation B component: mix back employing hot water extraction method by described material proportion and extract for several times, collecting decoction is adjusted PH=1-3,60-85 ℃ of insulation, places and filters, and collecting precipitation is used the alcohol flushing suction filtration, and getting crude product after the drying is the B component.

Extracting temperature in the aforesaid method is advisable for 60-100 ℃.

Preparation C component: with mixing of materials, use ethyl acetate backflow by described proportioning, phegma is condensed into medicinal extract, adds water and stirs evenly, and leaves standstill, cross the leaching precipitation, be dried again, use dissolve with ethanol, activated carbon decolorizing, alkalization then, with its filtration, filtrate is adjusted PH=1-3, separates out crystallization, i.e. the C component.

Among the preparation method of C component, the liquid temperature control is at 70-90 ℃, and return time 0.5-2 hour,

Alkalize to PH=8-10 and be advisable.

Preparation D component:, boil for several times mixing of materials by described proportioning with hot water, merging filtrate, activated carbon decolorizing 1 hour filters, and filtrate is the D component.

At last above-mentioned each component is pressed described mixed, adjust PH=5-6, add ethanol liquid, and then be heated to 80-100 ℃, add sanitas and solubilizing agent again, add the distillate in the A component at last, suction filtration promptly gets finished product while hot.

Used ethanol is advisable with 20-50% in the aforesaid method.

What used solubilizing agent was commonly used is tween 80.

The following examples can further specify the present invention.

Embodiment:

(1) preparation A component

Get elscholtiza, the root of Chinese wild ginger, peppermint, each 10g of Mongollian Thyme Herb, mix afterwash and add the water distillation, 100 ℃ of extractive distillation liquid, liquid temperature, surplus liquid filters, residue adds 50% ethanol and soaked 40 minutes, gets filtrate, and filtrate is merged, and is heated to 60-80 ℃, with activated carbon decolorizing 30 minutes, suction filtration was got the about 800ml of filtrate

(2) preparation B component:

Get crape myrtle, each 40g of the root of large-flowered skullcap, mixing the back extracts with the hot water extraction method, amount of water is 8-10 a times of inventory, be heated to 60-80 ℃ and boil 30 minutes 2 times, merge 2 times decocting liquid, transfer PH=1-2 with hydrochloric acid, be incubated 30 minutes down at 80 ℃, placement, filtration, collecting precipitation, with 95% alcohol flushing suction filtration, the dry about 0.5g of crude product that gets in the time of 60 ℃.

(3) preparation C component:

Get largeseed hemsleya root, giant knotweed, Glossy Privet Fruit, each 5g of Han dish, after the mixing, refluxed 1 hour down at 80 ℃ with ethyl acetate, phegma is condensed into medicinal extract, adds water and stirs evenly, and leaves standstill, crossing 80 ℃ of dryings of leaching precipitation is raw product, further use dissolve with ethanol again, use activated carbon decolorizing, alkalization makes PH=8-9 then, filter, again filtrate PH is transferred to 1-2, separate out crystallization, about 3-5g.

(4) preparation D component:

Get dish clothes, golden hop, each 20g of wintergreen, add the water heated and boiled 2 times, merging filtrate is used activated carbon decolorizing, filters filtrate for later use.

(5) with the gained each component with 1: 4: 5: 2 mixed (weight), transfer PH=5, add 20% ethanol, be heated to 100 ℃ then to certain volume, after 30 minutes, add Sodium Benzoate to concentration 0.1%, add the distillate in the A component at last, add the solubilizing agent tween 80 again, suction filtration while hot, filtrate is faint yellow, and mouthfeel and smell are all good, and the gained the finished product are the about 600ml of tooth-brush cleaning liquid of the present invention.

Tooth-brush cleaning liquid of the present invention can be used for the cleaning to the artificial tooth of wearing equally, and it is safe in utilization and convenient, can reach the purpose of health, sterilization, and without any side effects.

Claims

1, a kind of tooth-brush cleaning liquid is formed with the certain proportion cooperation by following several minutes components:

A component: elscholtiza: the root of Chinese wild ginger: peppermint: Mongollian Thyme Herb=1: 1-2: 1-3: 1-2, their mixed distillates, surplus liquid filtered liquid and residue filtrate,

B component: crape myrtle: the root of large-flowered skullcap=1: 1-3, the crude product that their mixed decocting liquid and suction filtration get,

C component: largeseed hemsleya root: giant knotweed: Glossy Privet Fruit ∶ Han dish=1: 1-2: 1-2: 1-3, the crystallization product that get after mixed concentrated solution and the filtration,

D component: Semen Raphani: golden hop: brave hoof grass=1: 1-2: the water cooking liquid of 1-2 mixture, each component cooperation ratio are A: B: C: D=1: 4-5: 4-6: 1-3 (weight).

2, tooth-brush cleaning liquid according to claim 1, it is characterized in that: each raw material blending ratio is (weight) 1: 1: 1 in the A component: 1, the blending ratio of each material (weight) is 1: 1 in the B component, the blending ratio of each material is (weight) 1: 1: 1 in the C component: 1, the blending ratio of each material (weight) is 1: 1: 1 in the D component, A: B: C: D=1: 4: 5: 2.

3, a kind of preparation method of tooth-brush cleaning liquid, it is characterized in that preparation A, B, C, D each minute component earlier, wherein the preparation method of A component is: get elscholtiza, the root of Chinese wild ginger, peppermint, Mongollian Thyme Herb with 1: after the weight ratio of 1-2: 1-3: 1-2 is mixed, add hydrodistillation extractive distillation liquid, surplus liquid filters, residue leaches filtrate with ethanol, and heating is got filtrate with activated carbon decolorizing, suction filtration then;

The preparation method of B component is: get crape myrtle, the root of large-flowered skullcap with 1: 1-3(weight) adopt the hot water extraction method to extract for several times than mixing the back, collecting decoction is adjusted PH=1-3,60-85 ℃ of insulation down, place and filter, collecting precipitation, use the alcohol flushing suction filtration, get crude product after the drying

The preparation of C component: get largeseed hemsleya root, giant knotweed, Glossy Privet Fruit, Han dish with 1: 1-2: 1-2: the 1-3(weight ratio) mix, use ethyl acetate backflow, phegma is condensed into medicinal extract, adding water stirs evenly, leave standstill, get precipitation after the filtration, be dried again, use dissolve with ethanol, activated carbon decolorizing, alkalinisation treatment is filtered again then, filtrate is adjusted PH=1-3 must separate out the crystallization product

The preparation of D component: get dish clothes, golden hop, brave hoof grass with 1: 1-2: the mixing 1-2(weight ratio), boil for several times with hot water, merging filtrate, activated carbon decolorizing filters to get filtrate.

With A, the B of above-mentioned gained, C, D each component with 1: the ratio of 4-5: 4-6: 1-3 (weight) is mixed.Method be the filtrate of A component with after B, C, D component mix, adjust PH=5-6, add ethanol liquid, be heated to 80-100 ℃ then, add sanitas and solubilizing agent again, add the distillate in the A component at last, suction filtration promptly gets finished product while hot.

4, by the described method of claim 3, it is characterized in that ethanol used among the preparation method of A component is 40-70%(concentration), soaked about 30 minutes of activated carbon decolorizing, bleaching temperature 60-80 ℃ 30-60 minute.

5, by the described method of claim 3, it is characterized in that among the preparation method of B component, extract 60-100 ℃ of temperature.

6, by the described method of claim 3, it is characterized in that among the preparation method of C component that the liquid temperature control return time 0.5-2 hour, is alkalized to PH=8-10 at 70-90 ℃.

7,, it is characterized in that among the preparation method of D component activated carbon decolorizing 1 hour by the described method of claim 3.

8, by the described method of claim 3, it is characterized in that A, B, C, D component mix after, used ethanol liquid is 20-50%(concentration).

9, by the described method of claim 3, it is characterized in that used sanitas is a Sodium Benzoate, add-on is the 0.1%(weight of the finished product).

10, by the described method of claim 3, it is characterized in that used solubilizing agent is tween 80.