CN108676633A - A kind of preparation method of Rosa roxburghii Tratt ferment liquid detergent - Google Patents
A kind of preparation method of Rosa roxburghii Tratt ferment liquid detergent Download PDFInfo
- Publication number
- CN108676633A CN108676633A CN201810170823.7A CN201810170823A CN108676633A CN 108676633 A CN108676633 A CN 108676633A CN 201810170823 A CN201810170823 A CN 201810170823A CN 108676633 A CN108676633 A CN 108676633A
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- CN
- China
- Prior art keywords
- rosa roxburghii
- roxburghii tratt
- liquid detergent
- tratt ferment
- preparation
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/38—Products with no well-defined composition, e.g. natural products
- C11D3/382—Vegetable products, e.g. soya meal, wood flour, sawdust
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/38—Products with no well-defined composition, e.g. natural products
- C11D3/381—Microorganisms
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/48—Medical, disinfecting agents, disinfecting, antibacterial, germicidal or antimicrobial compositions
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Wood Science & Technology (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Organic Chemistry (AREA)
- Microbiology (AREA)
- Detergent Compositions (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The present invention provides a kind of preparation methods of Rosa roxburghii Tratt ferment liquid detergent, specifically first Single Roxburgh Rose Fruit is made after pulp and is fermented again using saccharomycete (Saccharomyces cerevisiae), zymotic fluid is through filtering, resin adsorption, desorption and concentration, extraction obtains Rosa roxburghii Tratt ferment extraction concentrate, Rosa roxburghii Tratt ferment is finally extracted into concentrate and liquid detergent basal liquid is mixed and stirred evenly, obtains Rosa roxburghii Tratt ferment liquid detergent.Preparation process condition of the present invention is mild, can be mixed with a variety of liquid detergent basal liquids, the antibacterial sterilization effect for preparing Rosa roxburghii Tratt ferment liquid detergent is apparent, and detergency is substantially uninfluenced.
Description
Technical field
The invention belongs to daily chemical product technical fields, and in particular to a kind of preparation method of Rosa roxburghii Tratt ferment liquid detergent.
Background technology
Liquid detergent has many advantages, such as good water solubility, easy to use, energy conservation and environmental protection, and the market share obtains explosion type in recent years
Increase.But the raising of the development and the level of consumption with society, demand of the people to articles for washing are constantly upgrading.In addition to requiring
Except good detergency, it is also required to be provided simultaneously with other functions such as submissive, easy drift, color protection or sterilization, this has also just pushed and has washed
The exploitation of clothing liquid develops to diversification, personalized direction.
Rosa roxburghii Tratt category rose family wild plant is the distinctive wild resource in the Yunnan-Guizhou Plateau, with Guizhou for the main place of production.Rosa roxburghii Tratt has
Very high medical value, rich in functional mass such as vitamin C, polyphenol, organic acid, polysaccharide, flavones, cupreols.It is carried from plant
It takes and detaches new natural active compound, be the hot spot of antibacterial bactericidal agent exploitation.Antibacterial bactericidal agent application is extracted from Single Roxburgh Rose Fruit
In liquid detergent, then it is rarely reported and studies.
Invention content
The purpose of the present invention is a kind of preparation methods of Rosa roxburghii Tratt ferment liquid detergent, by going out antibacterial in Rosa roxburghii Tratt berry extract
Bacterium ingredient is green, natural, pollution-free for liquid detergent to be made, and economic utilization rate is high.
To achieve the above object, the present invention adopts the following technical scheme that：
A kind of preparation method of Rosa roxburghii Tratt ferment liquid detergent, includes the following steps：
Step 1, Single Roxburgh Rose Fruit 0.1-10kg is added in drinking water 0.1-100kg, breaks into pulp；
Step 2, it spreads cultivation after saccharomycete (Saccharomyces cerevisiae) being activated, then the liquid that will spread cultivation is seeded to step
It is cultivated in rapid 1 obtained pulp, condition of culture is 20-28 DEG C, 5-30d, obtains zymotic fluid；
Step 3, by the zymotic fluid of step 2 successively through filtering, resin adsorption, desorption and concentration, extraction obtains Rosa roxburghii Tratt ferment
Element extraction concentrate；
Step 4,0.1-10kg Rosa roxburghii Tratt ferment is extracted into concentrate and 50kg-500kg liquid detergent basal liquids is mixed and stirred evenly, i.e.,
Rosa roxburghii Tratt ferment liquid detergent is made.
Further, described spread cultivation is that saccharomycete (Saccharomyces cerevisiae) after activating uses 8-12 °
Fructus hordei germinatus normal juice 0.1-5L is spread cultivation under the conditions of 23-28 DEG C to 2.0 × 106-1.0×108A cell/mL, is made the liquid that spreads cultivation.
Further, the filtering is to filter zymotic fluid through stainless steel filtering net and stainless steel filter successively.
Further, the resin adsorption is the filtrate that will be obtained by filtration with macroporous absorbent resin Static Adsorption 6-60h, often
It is primary every 2-12h stirrings.
Further, the desorption is will to adsorb resin to be placed in ethanol solution static desorption 1-30h, every 1-6h
Stirring is primary.
Further, the concentration is that desorption agent is concentrated under reduced pressure under the conditions of 40-50 DEG C.
The remarkable advantage of the present invention is：
1, Rosa roxburghii Tratt fallen fruits, substandard products fruit can be selected as raw material, green, natural, pollution-free, economic utilization rate is high.
2, processing conditions is mild, can be compounded with a variety of liquid detergent basal liquids.
3, by specifically fermentation, the effect of reinforcing antibacterial sterilization material, the detergency of liquid detergent basal liquid is not substantially by shadow
It rings.
Specific implementation mode
In order to make content of the present invention easily facilitate understanding, With reference to embodiment to of the present invention
Technical solution is described further, but the present invention is not limited only to this.
Embodiment 1
1, pretreatment of raw material：
Rosa roxburghii Tratt fallen fruits, substandard products fruit 1kg are taken, pulp is broken into after adding 4kg drinking water.
2, it ferments：
Saccharomycete (Saccharomyces cerevisiae) activation of separation will be collected in Rosa roxburghii Tratt orchard, with 10 ° of malt
Normal juice 0.3L spreads cultivation under the conditions of 25 DEG C to 1.5 × 107Then a cell/mL is seeded to Rosa roxburghii Tratt original pulp, in 25 DEG C of conditions
Lower culture 10d.
3, it filters：
By zymotic fluid by 160 mesh stainless steel filtering nets (self-control), obtain primary filtrate, then by primary filtrate by FT-200b not
Become rusty steel fruit wine filter, obtains refined filtration liquid.
4, resin adsorption：
0.8kg (dry weight) D101 macroporous absorbent resins are placed in above-mentioned refined filtration liquid, at normal temperatures Static Adsorption for 24 hours, often
8h stirrings are primary.
5, desorption：
Resin after above-mentioned absorption is placed in 1.5kg ethyl alcohol (volumetric concentration 65%), carries out static desorption at normal temperatures
6h, per 2h, stirring is primary.
6, it concentrates：
Above-mentioned desorption agent is concentrated into 1kg, is pierced under the conditions of 48 DEG C with RE-1002 types concentration rotary evaporator
Pears ferment extracts concentrate.
7, it compounds：
By neopelex 8.8kg, sodium sulfate of polyethenoxy ether of fatty alcohol 29.5kg, fatty alcohol polyoxyethylene ether
7kg, polyvinyl alcohol 5kg, EDTA4.5kg, Rosa roxburghii Tratt ferment extract concentrate 1kg, add deionized water to 150kg, obtain described
Rosa roxburghii Tratt ferment liquid detergent.
Effect comparison：
Antibacterial sterilization effect is measured using Odontothrips loti, detergency test is carried out simultaneously using GB/T 13174-2008 methods
Judge in conjunction with sense organ.The result shows that the liquid detergent antibacterial circle diameter of addition Rosa roxburghii Tratt ferment extraction concentrate reaches 2.5 ㎝, and not
It adds Rosa roxburghii Tratt ferment and extracts concentrate liquid detergent antibacterial circle diameter only 1.1 ㎝, illustrate to compound washing for Rosa roxburghii Tratt ferment extraction concentrate
The antibacterial sterilization effect of clothing liquid is notable.By detergency test, the synthesis of the liquid detergent of addition Rosa roxburghii Tratt ferment extraction concentrate is gone
Dirty force value is 4.8, and the synthesis decontamination force value for being not added with Rosa roxburghii Tratt ferment extraction concentrate liquid detergent is 4.7, illustrates to compound Rosa roxburghii Tratt ferment
The detergency institute of the liquid detergent of element extraction concentrate is not impacted notable.
Embodiment 2
1, pretreatment of raw material：
Rosa roxburghii Tratt fallen fruits, substandard products fruit 1kg are taken, pulp is broken into after adding 4kg drinking water.
2, it ferments：
Saccharomycete (Saccharomyces cerevisiae) activation of separation will be collected in Rosa roxburghii Tratt orchard, with 10 ° of malt
Normal juice 0.3L spreads cultivation under the conditions of 25 DEG C to 1.5 × 107Then a cell/mL is seeded to Rosa roxburghii Tratt original pulp, in 25 DEG C of conditions
Lower culture 12d.
3, it filters：
By zymotic fluid by 160 mesh stainless steel filtering nets (self-control), obtain primary filtrate, then by primary filtrate by FT-200b not
Become rusty steel fruit wine filter, obtains refined filtration liquid.
4, resin adsorption：
0.8kg (dry weight) D101 macroporous absorbent resins are placed in above-mentioned refined filtration liquid, at normal temperatures Static Adsorption for 24 hours, often
8h stirrings are primary.
5, desorption：
Resin after above-mentioned absorption is placed in 1.5kg ethyl alcohol (volumetric concentration 65%), carries out static desorption at normal temperatures
6h, per 2h, stirring is primary.
6, it concentrates：
Above-mentioned desorption agent is concentrated into 1kg, is pierced under the conditions of 45 DEG C with RE-1002 types concentration rotary evaporator
Pears ferment extracts concentrate.
7, it compounds：
Sodium sulfate of polyethenoxy ether of fatty alcohol 50kg, isomery alcohol ether 45kg, EDTA5kg, compound biological enzyme 0.05kg, a water
Citric acid 0.05kg, Rosa roxburghii Tratt ferment extract concentrate 1kg, add deionized water to 200kg, obtain the Rosa roxburghii Tratt ferment laundry
Liquid.
Effect comparison：
Antibacterial sterilization effect is measured using Odontothrips loti, detergency test is carried out simultaneously using GB/T 13174-2008 methods
Judge in conjunction with sense organ.The result shows that the liquid detergent antibacterial circle diameter of addition Rosa roxburghii Tratt ferment extraction concentrate reaches 2.8 ㎝, and not
It adds Rosa roxburghii Tratt ferment and extracts concentrate liquid detergent antibacterial circle diameter only 1.2 ㎝, illustrate to compound washing for Rosa roxburghii Tratt ferment extraction concentrate
The antibacterial sterilization effect of clothing liquid is notable.By detergency test, the synthesis of the liquid detergent of addition Rosa roxburghii Tratt ferment extraction concentrate is gone
Dirty force value is 4.3, and the synthesis decontamination force value for being not added with Rosa roxburghii Tratt ferment extraction concentrate liquid detergent is 4.1, illustrates to compound Rosa roxburghii Tratt ferment
The detergency institute of the liquid detergent of element extraction concentrate is not impacted notable.
Embodiment 3
1, pretreatment of raw material：
Rosa roxburghii Tratt fallen fruits, substandard products fruit 1kg are taken, pulp is broken into after adding 4kg drinking water.
2, it ferments：
Saccharomycete (Saccharomyces cerevisiae) activation of separation will be collected in Rosa roxburghii Tratt orchard, with 10 ° of malt
Normal juice 0.3L spreads cultivation under the conditions of 25 DEG C to 1.5 × 107Then a cell/mL is seeded to Rosa roxburghii Tratt original pulp, in 25 DEG C of conditions
Lower culture 15d.
3, it filters：
By zymotic fluid by 160 mesh stainless steel filtering nets (self-control), obtain primary filtrate, then by primary filtrate by FT-200b not
Become rusty steel fruit wine filter, obtains refined filtration liquid.
4, resin adsorption：
0.8kg (dry weight) D101 macroporous absorbent resins are placed in above-mentioned refined filtration liquid, at normal temperatures Static Adsorption for 24 hours, often
8h stirrings are primary.
5, desorption：
Resin after above-mentioned absorption is placed in 1.5kg ethyl alcohol (volumetric concentration 65%), carries out static desorption at normal temperatures
6h, per 2h, stirring is primary.
6, it concentrates：
Above-mentioned desorption agent is concentrated into 1kg, is pierced under the conditions of 45 DEG C with RE-1002 types concentration rotary evaporator
Pears ferment extracts concentrate.
7, it compounds：
Sodium sulfate of polyethenoxy ether of fatty alcohol 42kg, dodecyl benzene sulfonic acid 45kg, fatty acid methyl ester ethoxylate
27kg, fatty alcohol polyoxyethylene ether 33kg, ethyl alcohol 10kg, sodium citrate 0.2kg, protease 1kg, Kathon CG 0.3kg, Rosa roxburghii Tratt ferment
Concentrate 1kg is extracted, deionized water supplies 250kg, obtains the Rosa roxburghii Tratt ferment liquid detergent.
Effect comparison：
Antibacterial sterilization effect is measured using Odontothrips loti, detergency test is carried out simultaneously using GB/T 13174-2008 methods
Judge in conjunction with sense organ.The result shows that the liquid detergent antibacterial circle diameter of addition Rosa roxburghii Tratt ferment extraction concentrate reaches 2.5 ㎝, and not
It adds Rosa roxburghii Tratt ferment and extracts concentrate liquid detergent antibacterial circle diameter only 1.1 ㎝, illustrate to compound washing for Rosa roxburghii Tratt ferment extraction concentrate
The antibacterial sterilization effect of clothing liquid is notable.By detergency test, the synthesis of the liquid detergent of addition Rosa roxburghii Tratt ferment extraction concentrate is gone
Dirty force value is 4.6, and the synthesis decontamination force value for being not added with Rosa roxburghii Tratt ferment extraction concentrate liquid detergent is 4.6, illustrates to compound Rosa roxburghii Tratt ferment
The detergency institute of the liquid detergent of element extraction concentrate is not impacted notable.
The foregoing is merely presently preferred embodiments of the present invention, all equivalent changes done according to scope of the present invention patent with
Modification should all belong to the covering scope of the present invention.
Claims (6)
1. a kind of preparation method of Rosa roxburghii Tratt ferment liquid detergent, it is characterised in that：Include the following steps：
Step 1, Single Roxburgh Rose Fruit 0.1-10kg is added in drinking water 0.1-100kg, breaks into pulp；
Step 2, it spreads cultivation after saccharomycete (Saccharomyces cerevisiae) being activated, then the liquid that will spread cultivation is seeded to step 1
It is cultivated in obtained pulp, condition of culture is 20-28 DEG C, 5-30d, obtains zymotic fluid；
Step 3, by the zymotic fluid of step 2 successively through filtering, resin adsorption, desorption and concentration, extraction obtains Rosa roxburghii Tratt ferment and carries
Take concentrate；
Step 4,0.1-10kg Rosa roxburghii Tratt ferment is extracted into concentrate and 50kg-500kg liquid detergent basal liquids is mixed and stirred evenly, obtained
Rosa roxburghii Tratt ferment liquid detergent.
2. the preparation method of Rosa roxburghii Tratt ferment liquid detergent according to claim 1, it is characterised in that：Described spread cultivation is will to activate
Saccharomycete (Saccharomyces cerevisiae) afterwards is spread cultivation with 8-12 ° of fructus hordei germinatus normal juice 0.1-5L under the conditions of 23-28 DEG C
To 2.0 × 106-1.0×108A cell/mL, is made the liquid that spreads cultivation.
3. the preparation method of Rosa roxburghii Tratt ferment liquid detergent according to claim 1, it is characterised in that：The filtering is will to ferment
Liquid is filtered through stainless steel filtering net and stainless steel filter successively.
4. the preparation method of Rosa roxburghii Tratt ferment liquid detergent according to claim 3, it is characterised in that：The resin adsorption be by
The filtrate being obtained by filtration is primary every 2-12h stirrings with macroporous absorbent resin Static Adsorption 6-60h.
5. the preparation method of Rosa roxburghii Tratt ferment liquid detergent according to claim 4, it is characterised in that：The desorption is will to inhale
Attached resin is placed in ethanol solution static desorption 1-30h, primary every 1-6h stirrings.
6. the preparation method of Rosa roxburghii Tratt ferment liquid detergent according to claim 4, it is characterised in that：The concentration is in 40-
Desorption agent is concentrated under reduced pressure under the conditions of 50 DEG C.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810170823.7A CN108676633A (en) | 2018-03-01 | 2018-03-01 | A kind of preparation method of Rosa roxburghii Tratt ferment liquid detergent |
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| CN201810170823.7A CN108676633A (en) | 2018-03-01 | 2018-03-01 | A kind of preparation method of Rosa roxburghii Tratt ferment liquid detergent |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP3911725A4 (en) * | 2019-01-18 | 2022-10-12 | Henkel AG & Co. KGaA | Laundry detergent compositions for eliminating, reducing, and/or inhibiting malodor |
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|---|---|---|---|---|
| CN104257531A (en) * | 2014-08-29 | 2015-01-07 | 何开远 | Fresh peel ferment and preparation method thereof |
| CN105754756A (en) * | 2016-02-03 | 2016-07-13 | 云南人本生物科技有限公司 | Preparation method of gentle and non-pollution enzyme laundry detergent |
| CN106350251A (en) * | 2016-08-20 | 2017-01-25 | 石永明 | Total-effective household laundry detergent |
| CN107304391A (en) * | 2016-04-19 | 2017-10-31 | 广西芙悦堂电子商务有限公司 | A kind of blue or green bur essential oil soap and its make method by hand |
| CN107603778A (en) * | 2017-09-11 | 2018-01-19 | 郑星星 | A kind of environmental protection ferment perfumed soap and preparation method thereof |
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-
2018
- 2018-03-01 CN CN201810170823.7A patent/CN108676633A/en active Pending
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|---|---|---|---|---|
| CN104257531A (en) * | 2014-08-29 | 2015-01-07 | 何开远 | Fresh peel ferment and preparation method thereof |
| CN105754756A (en) * | 2016-02-03 | 2016-07-13 | 云南人本生物科技有限公司 | Preparation method of gentle and non-pollution enzyme laundry detergent |
| CN107304391A (en) * | 2016-04-19 | 2017-10-31 | 广西芙悦堂电子商务有限公司 | A kind of blue or green bur essential oil soap and its make method by hand |
| CN107668686A (en) * | 2016-08-02 | 2018-02-09 | 浙江妙华生物科技有限公司 | A kind of production technology of Rosa roxburghii ferment |
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| 孔令义等: "《天然药物化学》", 31 August 2008, 中国医药科技出版社 * |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP3911725A4 (en) * | 2019-01-18 | 2022-10-12 | Henkel AG & Co. KGaA | Laundry detergent compositions for eliminating, reducing, and/or inhibiting malodor |
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