CN108658578A - A kind of preparation method of the colorful ceramic material of dicoration - Google Patents
A kind of preparation method of the colorful ceramic material of dicoration Download PDFInfo
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- C04B33/02—Preparing or treating the raw materials individually or as batches
- C04B33/13—Compounding ingredients
- C04B33/132—Waste materials; Refuse; Residues
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- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
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- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/34—Non-metal oxides, non-metal mixed oxides, or salts thereof that form the non-metal oxides upon heating, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
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- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
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Abstract
The invention discloses a kind of preparation methods of the colorful ceramic material of dicoration, by oyster shell whiting, metal oxide, aggregate mill it is even after, with ester and absolute ethyl alcohol mixing and ball milling, drying, sieving, the calcining of ceramic particle, positive silicic acid, silicate, colorant, after chromium mixing, the ultrasonic disperses such as dispersant are added, grinding heating, pour into mold solidification drying pre-burning, sand paper is polished, and is cleaned by ultrasonic, dry glaze spraying after being drawn, microwave radiation technology sintering after be freeze-dried, both the colorful ceramic material of dicoration.The advantages that present invention is molded by carrying out under the condition of high temperature, carries out microwave sintering with after freeze-drying, and the ceramic color of preparation interweaves, decorative strong, specific lightweight, high-strength tenacity.
Description
Technical field
The invention belongs to ceramic processing technique fields, and in particular to a kind of preparation method of the colorful ceramic material of dicoration.
Background technology
In the historical floods of ceramic art, Chinese ceramic art occupies very important status, bright at thousands of years
In rotten culture, six big porcelain systems have been pregnant with, the Ceramics Cultures such as five big kilns and countless civil kiln systems, history inside information is deep,
A large amount of Ceramics Culture precious deposits are left to descendant, Ceramics Culture is most characteristic one of the traditional culture of China, even to this day,
With the expansion of the change and technology diversification of Design ideological trend, Ceramics Culture is in the development in a nearly century, before having risen to
The height not having, before scientific and technological progress pushes the great development of productivity, technology with rapid changepl. never-ending changes and improvements to be brought to Ceramics Culture
The facility not having.
Invention content
The present invention provides a kind of preparation method of the colorful ceramic material of dicoration, the present invention by carry out under the condition of high temperature at
Type carries out microwave sintering with after freeze-drying, and the ceramic color of preparation interweaves, and decorative strong, specific lightweight, high-strength tenacity etc. are excellent
Point.
The present invention is achieved by the following technical solutions:
A kind of preparation method of the colorful ceramic material of dicoration, which is characterized in that include the following steps:
(1)Wet ball grinding
Oyster shell whiting, metal oxide, aggregate are respectively put into ball grinder after ball milling, after mixing in proportion, with ceramics
High purity aluminium oxide ball grinder is poured into after grain mixing, positive silicic acid ester and absolute ethyl alcohol is added, it is oxidation that ball milling, which is mixed evenly abrading-ball,
Aluminium, slurry drying, sieving, calcining;
(2)Hybrid Heating
By step(1)With silicate, colorant, after chromium mixing, dispersant, solvent and antifoaming agent mixing is added in proportion in gains
After be stirred, carry out ultrasonic disperse, after the completion with stainless steel ball be mill be situated between, be ground and added using planetary ball mill
Then uniformly mixed raw material is heated 0.5-1 hours, for use by heat under 200-500 DEG C of high temperature after the completion;
(3)Molding and colouring
Layout retouches original text, after mold is made, by step(2)The uniformly mixed liquid of gained is quickly poured into mold, and it is fixed to stand
To after solidification, solidifying body is obtained, drying pre-burning is carried out at a temperature of 50-80 DEG C, after sand paper is polished, after ultrasonic cleaning, in green body
On drawn a design with mineral pigment or writing words, the excessively dry kiln drying of green body is dry, be sent into glaze spraying machine glaze spraying, for use;
(4)Microwave sintering and freezing
By step(3)Gained green body is positioned in attemperator, and attemperator is integrally positioned over to microwave high-temperature vacuum burning later
In freezing of a furnace, inert gas is passed through as protective gas, sets the sintering temperature of microwave high-temperature vacuum sintering furnace, control heating speed
Rate is sintered, and cools to room temperature with the furnace, be placed on and be freeze-dried 24-48 hours in vacuum freezing drying oven after, both institute
State decorative colorful ceramic material.
The colorful ceramic material of dicoration is made of following raw material:5-8 parts of oyster shell whiting, metal oxide 5-7
Part, 5-10 parts of aggregate, 5-10 parts of ceramic particle, 0.01-0.3 parts of dispersant, 40-100 parts of solvent, 0.01-0.2 parts of antifoaming agent,
Positive silicic acid ester 1-2 parts by weight, absolute ethyl alcohol 20-30 parts by weight, silicate 1-5 parts by weight, 0.1-1 parts of colorant, chromium 0.5-
1。
The ratio of grinding media to material of the ball milling is 8-10:1, Ball-milling Time is 24-48 hours.
The solvent is selected from polyethylene glycol, alcohol, deionized water, N-Methyl pyrrolidone and ten disulfo Sodium Benzoates
It is at least one.
The antifoaming agent in mineral oil defoaming agent, silicone oil antifoaming agent, dimethyl-silicon oils antifoaming agent at least
It is a kind of
The microwave sintering temperature is set as 1700-2000 DEG C, and speed control is 30-40 DEG C/min.
It is an advantage of the invention that:
The present invention by oyster shell whiting, metal oxide, aggregate mill it is even after, ester and absolute ethyl alcohol mix with ceramic particle, positive silicic acid
After chromium mixing, the ultrasonic disperses such as dispersant are added in ball milling, drying, sieving, calcining, silicate, colorant, and grinding heating is poured into
Mold solidification dries pre-burning, and sand paper polishing is cleaned by ultrasonic, and dry glaze spraying after being drawn is freezed after microwave radiation technology sintering
It is dry, both the colorful ceramic material of dicoration.The invention enables oyster shell whiting, metal oxide, aggregate, ceramic particles in machine
Under tool force effect, powder granule size is refined, improve its dispersibility and improves powder sintering activity, it will be between powder particle after calcining
Organic matter and moisture, compound to prepare a kind of material of light-weight environment-friendly, the use of the materials such as metal oxide later is further dropped
Low ceramic sintering temperature, crystallite dimension reduce, and more multichannel, dispersant, antifoaming agent, the solvent of addition etc. are provided for stomata exclusion
Reduce the generation of lamination blistering so that ceramic clay powder and evenly dispersed ceramic slurry is being obtained with preferable dispersibility,
To obtain the good ceramic body of appearance, the condition of high temperature is to rapid shaping is conducive to, with non-fading mineral raw material so that
The color portrayed enters pottery body surface with pattern, and product is as smooth as jade, and pattern is combined together with pottery body, and color interweaves, decoration
Property it is strong, using microwave sintering method prepare ceramics, sintering time is short, efficient, can to avoid dephasign occur have efficiently, green
It with energy saving feature, then is placed in low temperature environment and freezes, deionized water ice crystal is made to distil so that is the specific lightweight of ceramics, high tough
The advantages that property.The present invention is molded by carrying out under the condition of high temperature, after carrying out microwave sintering and being freeze-dried, the ceramic color of preparation
The advantages that intertexture, dicoration is strong, specific lightweight, high-strength tenacity.
Specific implementation mode
A kind of preparation method of the colorful ceramic material of dicoration, which is characterized in that include the following steps:
(1)Wet ball grinding
Oyster shell whiting, metal oxide, aggregate are respectively put into ball grinder after ball milling, after mixing in proportion, with ceramics
High purity aluminium oxide ball grinder is poured into after grain mixing, positive silicic acid ester and absolute ethyl alcohol is added, it is oxidation that ball milling, which is mixed evenly abrading-ball,
Aluminium, slurry drying, sieving, calcining;
(2)Hybrid Heating
By step(1)With silicate, colorant, after chromium mixing, dispersant, solvent and antifoaming agent mixing is added in proportion in gains
After be stirred, carry out ultrasonic disperse, after the completion with stainless steel ball be mill be situated between, be ground and added using planetary ball mill
Then uniformly mixed raw material is heated 0.5-1 hours, for use by heat under 200-500 DEG C of high temperature after the completion;
(3)Molding and colouring
Layout retouches original text, after mold is made, by step(2)The uniformly mixed liquid of gained is quickly poured into mold, and it is fixed to stand
To after solidification, solidifying body is obtained, drying pre-burning is carried out at a temperature of 50-80 DEG C, after sand paper is polished, after ultrasonic cleaning, in green body
On drawn a design with mineral pigment or writing words, the excessively dry kiln drying of green body is dry, be sent into glaze spraying machine glaze spraying, for use;
(4)Microwave sintering and freezing
By step(3)Gained green body is positioned in attemperator, and attemperator is integrally positioned over to microwave high-temperature vacuum burning later
In freezing of a furnace, inert gas is passed through as protective gas, sets the sintering temperature of microwave high-temperature vacuum sintering furnace, control heating speed
Rate is sintered, and cools to room temperature with the furnace, be placed on and be freeze-dried 24-48 hours in vacuum freezing drying oven after, both institute
State decorative colorful ceramic material.
The colorful ceramic material of dicoration is made of following raw material:7 parts of oyster shell whiting, 6 parts of metal oxide, bone
8 parts of material, 7 parts of ceramic particle, 0.05 part of dispersant, 60 parts of solvent, 0.05 part of antifoaming agent, positive silicic acid 2 parts by weight of ester, anhydrous second
25 parts by weight of alcohol, 4 parts by weight of silicate, 0.5 part of colorant, chromium 0.5.
The ratio of grinding media to material of the ball milling is 8:1, Ball-milling Time is 24-48 hours.
The solvent is selected from polyethylene glycol, alcohol, deionized water, N-Methyl pyrrolidone and ten disulfo Sodium Benzoates
It is at least one.
The antifoaming agent in mineral oil defoaming agent, silicone oil antifoaming agent, dimethyl-silicon oils antifoaming agent at least
It is a kind of
The microwave sintering temperature is set as 1700-2000 DEG C, and speed control is 30-40 DEG C/min.
Claims (6)
1. a kind of preparation method of the colorful ceramic material of dicoration, which is characterized in that include the following steps:
(1)Wet ball grinding
Oyster shell whiting, metal oxide, aggregate are respectively put into ball grinder after ball milling, after mixing in proportion, with ceramics
High purity aluminium oxide ball grinder is poured into after grain mixing, positive silicic acid ester and absolute ethyl alcohol is added, it is oxidation that ball milling, which is mixed evenly abrading-ball,
Aluminium, slurry drying, sieving, calcining;
(2)Hybrid Heating
By step(1)With silicate, colorant, after chromium mixing, dispersant, solvent and antifoaming agent mixing is added in proportion in gains
After be stirred, carry out ultrasonic disperse, after the completion with stainless steel ball be mill be situated between, be ground and added using planetary ball mill
Then uniformly mixed raw material is heated 0.5-1 hours, for use by heat under 200-500 DEG C of high temperature after the completion;
(3)Molding and colouring
Layout retouches original text, after mold is made, by step(2)The uniformly mixed liquid of gained is quickly poured into mold, and it is fixed to stand
To after solidification, solidifying body is obtained, drying pre-burning is carried out at a temperature of 50-80 DEG C, after sand paper is polished, after ultrasonic cleaning, in green body
On drawn a design with mineral pigment or writing words, the excessively dry kiln drying of green body is dry, be sent into glaze spraying machine glaze spraying, for use;
(4)Microwave sintering and freezing
By step(3)Gained green body is positioned in attemperator, and attemperator is integrally positioned over to microwave high-temperature vacuum burning later
In freezing of a furnace, inert gas is passed through as protective gas, sets the sintering temperature of microwave high-temperature vacuum sintering furnace, control heating speed
Rate is sintered, and cools to room temperature with the furnace, be placed on and be freeze-dried 24-48 hours in vacuum freezing drying oven after, both institute
State decorative colorful ceramic material.
2. a kind of preparation method of the colorful ceramic material of dicoration as described in claim 1, which is characterized in that the dicoration
Colorful ceramic material is made of following raw material:5-8 parts of oyster shell whiting, 5-7 parts of metal oxide, 5-10 parts of aggregate, ceramics
5-10 parts of particle, 0.01-0.3 parts of dispersant, 40-100 parts of solvent, 0.01-0.2 parts of antifoaming agent, positive silicic acid ester 1-2 weight
Part, absolute ethyl alcohol 20-30 parts by weight, silicate 1-5 parts by weight, 0.1-1 parts of colorant, chromium 0.5-1.
3. a kind of preparation method of the colorful ceramic material of dicoration as described in claim 1, which is characterized in that the ball milling
Ratio of grinding media to material be 8-10:1, Ball-milling Time is 24-48 hours.
4. a kind of preparation method of the colorful ceramic material of dicoration as described in claim 1, which is characterized in that the solvent choosing
From at least one of polyethylene glycol, alcohol, deionized water, N-Methyl pyrrolidone and ten disulfo Sodium Benzoates.
5. a kind of preparation method of the colorful ceramic material of dicoration as described in claim 1, which is characterized in that the antifoaming agent
Selected from least one of mineral oil defoaming agent, silicone oil antifoaming agent, dimethyl-silicon oils antifoaming agent.
6. a kind of preparation method of the colorful ceramic material of dicoration as described in claim 1, which is characterized in that the microwave
Sintering temperature is set as 1700-2000 DEG C, and speed control is 30-40 DEG C/min.
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Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN109849244A (en) * | 2019-03-11 | 2019-06-07 | 广东四会互感器厂有限公司 | A kind of method of pressure gel mold scale removal |
CN113548875A (en) * | 2021-07-13 | 2021-10-26 | 烟台大学 | Oyster shell ceramic separator and preparation process and application thereof |
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CN103467041A (en) * | 2013-09-11 | 2013-12-25 | 杨益 | Ceramic tile and manufacturing method thereof |
CN103497008A (en) * | 2013-09-18 | 2014-01-08 | 海瓷艺术研究院 | Underglaze hand painting production technique of calcium porcelain |
CN104944912A (en) * | 2015-06-19 | 2015-09-30 | 揭阳市揭东易成陶瓷实业有限公司 | Formula for environment-friendly energy-saving low-temperature white semi-porcelain and method for preparing the same |
CN106082988A (en) * | 2016-06-12 | 2016-11-09 | 安徽省亚欧陶瓷有限责任公司 | A kind of mould proof ceramic tile and preparation method thereof |
CN106278149A (en) * | 2016-08-11 | 2017-01-04 | 桐城市福润包装材料有限公司 | A kind of manufacture method of vase |
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Patent Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
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CN103467041A (en) * | 2013-09-11 | 2013-12-25 | 杨益 | Ceramic tile and manufacturing method thereof |
CN103497008A (en) * | 2013-09-18 | 2014-01-08 | 海瓷艺术研究院 | Underglaze hand painting production technique of calcium porcelain |
CN104944912A (en) * | 2015-06-19 | 2015-09-30 | 揭阳市揭东易成陶瓷实业有限公司 | Formula for environment-friendly energy-saving low-temperature white semi-porcelain and method for preparing the same |
CN106082988A (en) * | 2016-06-12 | 2016-11-09 | 安徽省亚欧陶瓷有限责任公司 | A kind of mould proof ceramic tile and preparation method thereof |
CN106278149A (en) * | 2016-08-11 | 2017-01-04 | 桐城市福润包装材料有限公司 | A kind of manufacture method of vase |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN109849244A (en) * | 2019-03-11 | 2019-06-07 | 广东四会互感器厂有限公司 | A kind of method of pressure gel mold scale removal |
CN113548875A (en) * | 2021-07-13 | 2021-10-26 | 烟台大学 | Oyster shell ceramic separator and preparation process and application thereof |
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