CN108654518A - A kind of pulse spray-type solid-liquid reaction kettle with grinding function - Google Patents
A kind of pulse spray-type solid-liquid reaction kettle with grinding function Download PDFInfo
- Publication number
- CN108654518A CN108654518A CN201810578435.2A CN201810578435A CN108654518A CN 108654518 A CN108654518 A CN 108654518A CN 201810578435 A CN201810578435 A CN 201810578435A CN 108654518 A CN108654518 A CN 108654518A
- Authority
- CN
- China
- Prior art keywords
- autoclave body
- fixedly connected
- liquid
- mounting plate
- reserve tank
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J4/00—Feed or outlet devices; Feed or outlet control devices
- B01J4/001—Feed or outlet devices as such, e.g. feeding tubes
- B01J4/002—Nozzle-type elements
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F27/00—Mixers with rotary stirring devices in fixed receptacles; Kneaders
- B01F27/05—Stirrers
- B01F27/11—Stirrers characterised by the configuration of the stirrers
- B01F27/112—Stirrers characterised by the configuration of the stirrers with arms, paddles, vanes or blades
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F27/00—Mixers with rotary stirring devices in fixed receptacles; Kneaders
- B01F27/05—Stirrers
- B01F27/11—Stirrers characterised by the configuration of the stirrers
- B01F27/17—Stirrers with additional elements mounted on the stirrer, for purposes other than mixing
- B01F27/171—Stirrers with additional elements mounted on the stirrer, for purposes other than mixing for disintegrating, e.g. for milling
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F27/00—Mixers with rotary stirring devices in fixed receptacles; Kneaders
- B01F27/80—Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis
- B01F27/90—Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis with paddles or arms
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0053—Details of the reactor
- B01J19/0066—Stirrers
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/18—Stationary reactors having moving elements inside
Abstract
The invention discloses a kind of pulse spray-type solid-liquid reaction kettle with grinding function,Including autoclave body,Feeding-in solid body mouth,Grind motor,Disintegrating knife and drainage conduit,It is fixedly connected with guide rod at the top of the autoclave body,Spring is arranged on guide rod,The top of autoclave body is equipped with liquid reserve tank,Mounting plate,Guide rod runs through mounting plate,Mounting plate is slidably connected with guide rod,The upper end of spring is abutted with mounting plate,The lower end of spring is abutted with the top of autoclave body,The side wall of mounting plate is fixedly connected with vibrating motor,The bottom of liquid reserve tank is fixedly connected with piston cylinder,Piston cylinder tips upside down in liquid reserve tank,The present invention is in use,Liquid reactants pulsed may be implemented to be sprayed in autoclave body,Liquid reactants are made repeatedly to be added in autoclave body on a small quantity,Contribute to being sufficiently mixed for liquid reactants and solid reactant,Utilize Disintegrating knife comminuted solids reactant,Reaction solution is stirred using stirring blade,Solid reactant is set uniformly to be mixed with liquid reactants,Improve reaction efficiency.
Description
Technical field
The present invention relates to chemical mechanical equipment field, specifically a kind of pulse spray-type solid-liquid reaction with grinding function
Kettle.
Background technology
The broad understanding of reaction kettle has the rustless steel container physically or chemically reacted, according to different process conditions demands
The structure design and parameter configuration of container are carried out, design condition, process, inspection and manufacture, examination are needed according to Its Relevant Technology Standards,
To realize that the heating of technological requirement, evaporation, cooling and the mixture response function of low high speed, reaction kettle are widely used in oil, change
Work, rubber, pesticide, dyestuff, medicine, food, for completing the technical process such as vulcanization, nitrification, hydrogenation, hydrocarbonylation, polymerization, condensation
Pressure vessel, such as reactor, reaction pot, decomposition pot, polymeric kettle etc.；Material generally has carbon manganese steel, stainless steel, zirconium, Ni-based conjunction
Often there is material and mix non-uniform situation in golden and other composite materials, existing frequently-used solid-liquid reaction kettle, reaction is caused to be imitated
Rate is low, it is difficult to meet the daily production requirement of people.
Invention content
The purpose of the present invention is to provide a kind of pulse spray-type solid-liquid reaction kettle with grinding function, it is above-mentioned to solve
The problem of being proposed in background technology.
To achieve the above object, the present invention provides the following technical solutions：
A kind of pulse spray-type solid-liquid reaction kettle with grinding function, including autoclave body, feeding-in solid body mouth, grinding motor, crushing
Blade and drainage conduit are fixedly connected with guide rod at the top of the autoclave body, and guide rod shares two, bullet is arranged on guide rod
The top of spring, autoclave body is equipped with liquid reserve tank, is respectively fixedly connected at left and right sides of liquid reserve tank, mounting plate, and guide rod runs through mounting plate,
Mounting plate is slidably connected with guide rod, and the upper end of spring is abutted with mounting plate, and the lower end of spring is abutted with the top of autoclave body, installation
The side wall of plate is fixedly connected with vibrating motor, and the bottom of liquid reserve tank is fixedly connected with piston cylinder, and piston cylinder tips upside down in liquid reserve tank,
The upper surface of autoclave body is fixedly connected with piston rod, and piston rod passes through the bottom of liquid reserve tank to stretch into piston cylinder, the middle part of inlet tube
Check valve is installed, the right side wall of piston cylinder is equipped with drain pipe, is equipped with check valve in the middle part of drain pipe, drain pipe it is another
End extends to the lower section of liquid reserve tank across the bottom of liquid reserve tank, and the other end of drain pipe is connected with hose, and autoclave body is internally provided with
Nozzle, by being fixedly connected at the top of connecting tube and autoclave body, the top of connecting tube is connected to nozzle with hose.
As a further solution of the present invention：It is fixedly connected with feeding-in solid body mouth above the left side wall of the autoclave body.
As further scheme of the invention：The upper surface of the liquid reserve tank is fixedly connected with filler pipe, on filler pipe
Valve is installed.
As further scheme of the invention：The bottom of the autoclave body is fixedly connected with grinding motor, grinds motor
Motor shaft stretches into autoclave body, and the axle stretch end for grinding motor is fixedly connected with Disintegrating knife, stirring blade, and the bottom of autoclave body, which is equipped with, grinds
Mill, abrasive disk are set on the motor shaft of grinding motor.
As further scheme of the invention：Through-hole, the lower surface point of abrasive disk is distributed in the surface of the abrasive disk
If being furnished with dry grinding protrusion.
As further scheme of the invention：Drainage conduit is installed below the right side wall of the autoclave body, is pacified in drainage conduit
Equipped with valve.
As further scheme of the invention：The bottom of the autoclave body is fixedly connected with stabilizer blade, and the lower end of stabilizer blade is arranged
There are sleeve, the inside of sleeve that damping spring is installed.
Compared with prior art, the beneficial effects of the invention are as follows：In use, liquid reactions may be implemented in the present invention
Object pulsed is sprayed in autoclave body, so that liquid reactants is repeatedly added in autoclave body on a small quantity, is contributed to liquid reactants and solid
Reactant is sufficiently mixed, and using Disintegrating knife comminuted solids reactant, is stirred reaction solution using stirring blade, is made solid reaction
Object is uniformly mixed with liquid reactants, is improved reaction efficiency, is ground, is further increased to solid reactant using abrasive disk
The contact area of solid reactant and liquid reactants further increases reflection efficiency.
Description of the drawings
Fig. 1 is the structural schematic diagram of the pulse spray-type solid-liquid reaction kettle with grinding function；
Fig. 2 is the vertical view of the pulse spray-type solid-liquid reaction kettle with grinding function；
Fig. 3 is the structural schematic diagram of piston cylinder in the pulse spray-type solid-liquid reaction kettle with grinding function.
In figure：1- autoclave bodies；2- feeding-in solid body mouths；3- guide rods；4- liquid reserve tanks；5- mounting plates；6- vibrating motors；7- bullets
Spring；8- filler pipes；9- piston cylinders；10- piston rods；11- inlet tubes；12- drain pipes；13- hoses；14- nozzles；15- grinding electricity
Machine；16- Disintegrating knifes；17- stirring blades；18- abrasive disks；19- through-holes；20- grinding protrusions；21- stabilizer blades；22- sleeves；23-
Damping spring；24- drainage conduits.
Specific implementation mode
Following will be combined with the drawings in the embodiments of the present invention, and technical solution in the embodiment of the present invention carries out clear, complete
Site preparation describes, it is clear that described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.It is based on
Embodiment in the present invention, it is obtained by those of ordinary skill in the art without making creative efforts every other
Embodiment shall fall within the protection scope of the present invention.
Please refer to Fig.1-3, in the embodiment of the present invention, a kind of pulse spray-type solid-liquid reaction kettle with grinding function, packet
Autoclave body 1, feeding-in solid body mouth 2, grinding motor 15, Disintegrating knife 16 and drainage conduit 24 are included, is fixedly connected above the left side wall of autoclave body 1
There are feeding-in solid body mouth 2, solid reactant to enter in autoclave body 1 by feeding-in solid body mouth 2, the top of autoclave body 1 is fixedly connected with guiding
Bar 3, guide rod 3 share two, and spring 7 is arranged on guide rod 3, and the top of autoclave body 1 is equipped with liquid reserve tank 4, the left and right of liquid reserve tank 4
Both sides are respectively fixedly connected with, mounting plate 5, and guide rod 3 runs through mounting plate 5, and mounting plate 5 is slidably connected with guide rod 3, spring 7
Upper end is abutted with mounting plate 5, and the lower end of spring 7 is abutted with the top of autoclave body 1, and the side wall of mounting plate 5 is fixedly connected with vibration electricity
Machine 6, Vibration on Start-up motor 6 drive under the collective effect of vibrating motor 6 and spring 7 and do 4 up-down vibration of liquid reserve tank, liquid reserve tank 4
Upper surface be fixedly connected with filler pipe 8, valve is installed, liquid reactants pass through filler pipe 8 and inject liquid reserve tank on filler pipe 8
In 4, the bottom of liquid reserve tank 4 is fixedly connected with piston cylinder 9, and piston cylinder 9 tips upside down in liquid reserve tank 4, and the upper surface of autoclave body 1, which is fixed, to be connected
It is connected to piston rod 10, piston rod 10 passes through the bottom of liquid reserve tank 4 to stretch into piston cylinder 9, and the left side wall of piston cylinder 9 is equipped with feed liquor
The middle part of pipe 11, inlet tube 11 is equipped with check valve, and the reaction solution in liquid reserve tank 4 can enter piston cylinder 9 by inlet tube 11
Interior, the right side wall of piston cylinder 9 is equipped with drain pipe 12, and the middle part of drain pipe 12 is equipped with check valve, the other end of drain pipe 12
The lower section of liquid reserve tank 4 is extended to across the bottom of liquid reserve tank 4, the other end of drain pipe 12 is connected with hose 13, the inside of autoclave body 1
Equipped with nozzle 14, nozzle 14 is fixedly connected by connecting tube with the top of autoclave body 1, and the top of connecting tube is connected to hose 13, when
Piston cylinder 9 is driven to move up and down when 4 up-down vibration of liquid reserve tank, when piston cylinder 9 moves up, pressure reduces in piston cylinder 9, liquid
Reactant is entered by inlet tube 11 in piston cylinder 9, when piston cylinder 9 moves down, pressure rise in piston cylinder 9, and piston cylinder 9
Interior liquid reactants are discharged by drain pipe 12, are sprayed in autoclave body 1 eventually by nozzle 14, and liquid reserve tank 4 ceaselessly vibrates,
To realize that liquid reactants pulsed is sprayed in autoclave body 1, the bottom of autoclave body 1 is fixedly connected with grinding motor 15, grinding electricity
The motor shaft of machine 15 stretches into autoclave body 1, and the axle stretch end of grinding motor 15 is fixedly connected with Disintegrating knife 16, stirring blade 17, kettle
The bottom of body 1 is equipped with abrasive disk 18, and abrasive disk 18 is set on the motor shaft of grinding motor 15, and grinding motor 15 drives when running
Disintegrating knife 16, stirring blade 17 rotate, comminuted solids reactant, while stirring reaction solution, keep solid reactant anti-with liquid
It answers object uniformly to mix, improves reaction efficiency, the surface of abrasive disk 18 is distributed with through-hole, and the lower surface of abrasive disk 18 is distributed with several
Grinding protrusion 20, solid reactant pass through through-hole 19 to fall into the lower section of abrasive disk 18, grinding protrusion are utilized when abrasive disk 18 rotates
20 pairs of solid reactants are ground, and are further increased the contact area of solid reactant and liquid reactants, are further increased
Reflect that efficiency, the bottom of autoclave body 1 are fixedly connected with stabilizer blade 21, the lower end of stabilizer blade 21 is arranged with sleeve 22, the inside peace of sleeve 22
Equipped with damping spring 23, stabilizer blade 21 can slide up and down in sleeve 22, reduced when the present apparatus is run and produced using damping spring 23
The right side wall lower section of raw vibration, autoclave body 1 is equipped with drainage conduit 24, and valve is equipped in drainage conduit 24, remaining solid after reaction
Liquid mixture is discharged by drainage conduit 24.
The present invention operation principle be：Solid reactant is put by feeding-in solid body mouth 2 in autoclave body 1, Vibration on Start-up electricity
Machine 6 drives under the collective effect of vibrating motor 6 and spring 7 and does 4 up-down vibration of liquid reserve tank, piston cylinder 9 is driven to move up and down,
When piston cylinder 9 moves up, pressure reduces in piston cylinder 9, and liquid reactants are entered by inlet tube 11 in piston cylinder 9, and work is worked as
When plug cylinder 9 moves down, pressure rise in piston cylinder 9, the liquid reactants in piston cylinder 9 are discharged by drain pipe 12, finally
It is sprayed in autoclave body 1 by nozzle 14, liquid reserve tank 4 ceaselessly vibrates, to realize that liquid reactants pulsed is sprayed at autoclave body 1
It is interior, so that liquid reactants is repeatedly added in autoclave body 1 on a small quantity, contributes to being sufficiently mixed for liquid reactants and solid reactant,
Start grinding motor 15, Disintegrating knife 16, stirring blade 17 is driven to rotate, comminuted solids reactant, while reaction solution is stirred, make
Solid reactant is uniformly mixed with liquid reactants, improves reaction efficiency, and solid reactant falls into abrasive disk 18 across through-hole 19
Lower section, be ground using the raised 20 pairs of solid reactants of grinding when abrasive disk 18 rotates, further increase solid reactant
With the contact area of liquid reactants, reflection efficiency is further increased.
It is obvious to a person skilled in the art that invention is not limited to the details of the above exemplary embodiments, Er Qie
In the case of without departing substantially from spirit or essential attributes of the invention, the present invention can be realized in other specific forms.Therefore, no matter
From the point of view of which point, the present embodiments are to be considered as illustrative and not restrictive, and the scope of the present invention is by appended power
Profit requires rather than above description limits, it is intended that all by what is fallen within the meaning and scope of the equivalent requirements of the claims
Variation is included within the present invention.Any reference signs in the claims should not be construed as limiting the involved claims.
In addition, it should be understood that although this specification is described in terms of embodiments, but not each embodiment is only wrapped
Containing an independent technical solution, this description of the specification is merely for the sake of clarity, and those skilled in the art should
It considers the specification as a whole, the technical solutions in the various embodiments may also be suitably combined, forms those skilled in the art
The other embodiment being appreciated that.
Claims (7)
1. a kind of pulse spray-type solid-liquid reaction kettle with grinding function, including autoclave body（1）, feeding-in solid body mouth（2）, grinding electricity
Machine（15）, Disintegrating knife（16）And drainage conduit（24）, which is characterized in that the autoclave body（1）Top be fixedly connected with guide rod
（3）, guide rod（3）Two are shared, guide rod（3）On be arranged with spring（7）, autoclave body（1）Top be equipped with liquid reserve tank（4）, storage
Liquid case（4）The left and right sides be respectively fixedly connected with, mounting plate（5）, guide rod（3）Through mounting plate（5）, mounting plate（5）With lead
To bar（3）It is slidably connected, spring（7）Upper end and mounting plate（5）It abuts, spring（7）Lower end and autoclave body（1）Top support
It connects, mounting plate（5）Side wall be fixedly connected with vibrating motor（6）, liquid reserve tank（4）Bottom be fixedly connected with piston cylinder（9）, living
Plug cylinder（9）Tip upside down on liquid reserve tank（4）It is interior, autoclave body（1）Upper surface be fixedly connected with piston rod（10）, piston rod（10）Across storage
Liquid case（4）Bottom stretch into piston cylinder（9）It is interior, inlet tube（11）Middle part check valve, piston cylinder are installed（9）Right side wall peace
Equipped with drain pipe（12）, drain pipe（12）Middle part check valve, drain pipe are installed（12）The other end pass through liquid reserve tank（4）'s
Bottom extends to liquid reserve tank（4）Lower section, drain pipe（12）The other end be connected with hose（13）, autoclave body（1）Be internally provided with
Nozzle（14）, nozzle（14）Pass through connecting tube and autoclave body（1）Top be fixedly connected, the top of connecting tube and hose（13）Even
It is logical.
2. the pulse spray-type solid-liquid reaction kettle according to claim 1 with grinding function, which is characterized in that the kettle
Body（1）Left side wall above be fixedly connected with feeding-in solid body mouth（2）.
3. the pulse spray-type solid-liquid reaction kettle according to claim 1 with grinding function, which is characterized in that the storage
Liquid case（4）Upper surface be fixedly connected with filler pipe（8）, filler pipe（8）On valve is installed.
4. the pulse spray-type solid-liquid reaction kettle according to claim 1 with grinding function, which is characterized in that the kettle
Body（1）Bottom be fixedly connected with grinding motor（15）, grind motor（15）Motor shaft stretch into autoclave body（1）It is interior, grind motor
（15）Axle stretch end be fixedly connected with Disintegrating knife（16）, stirring blade（17）, autoclave body（1）Bottom be equipped with abrasive disk（18）,
Abrasive disk（18）It is set in grinding motor（15）Motor shaft on.
5. the pulse spray-type solid-liquid reaction kettle according to claim 4 with grinding function, which is characterized in that described to grind
Mill（18）Surface through-hole, abrasive disk is distributed with（18）If lower surface be distributed with dry grinding protrusion（20）.
6. the pulse spray-type solid-liquid reaction kettle according to claim 1 with grinding function, which is characterized in that the kettle
Body（1）Right side wall below drainage conduit is installed（24）, drainage conduit（24）On valve is installed.
7. the pulse spray-type solid-liquid reaction kettle according to claim 1 with grinding function, which is characterized in that the kettle
Body（1）Bottom be fixedly connected with stabilizer blade（21）, stabilizer blade（21）Lower end be arranged with sleeve（22）, sleeve（22）Inside installation
There is damping spring（23）.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810578435.2A CN108654518A (en) | 2018-06-07 | 2018-06-07 | A kind of pulse spray-type solid-liquid reaction kettle with grinding function |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810578435.2A CN108654518A (en) | 2018-06-07 | 2018-06-07 | A kind of pulse spray-type solid-liquid reaction kettle with grinding function |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN108654518A true CN108654518A (en) | 2018-10-16 |
Family
ID=63775541
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201810578435.2A Pending CN108654518A (en) | 2018-06-07 | 2018-06-07 | A kind of pulse spray-type solid-liquid reaction kettle with grinding function |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN108654518A (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110721623A (en) * | 2019-12-19 | 2020-01-24 | 湖南乐准智芯生物科技有限公司 | Reagent vibration mixing method |
| CN112546933A (en) * | 2020-09-21 | 2021-03-26 | 湖南嘉顺华新材料有限公司 | A agitating unit for dry powder slurrying |
| CN113583460A (en) * | 2021-06-19 | 2021-11-02 | 浙江巍翔科技集团有限公司 | Bio-based modified low-heat-generation reinforcing agent and preparation method thereof |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107999534A (en) * | 2018-01-29 | 2018-05-08 | 李子琦 | A kind of soil remediation equipment of intermittent spray |
| CN108043349A (en) * | 2017-12-06 | 2018-05-18 | 郑州诚合信息技术有限公司 | A kind of solid-liquid reaction kettle for increasing reaction rate |
-
2018
- 2018-06-07 CN CN201810578435.2A patent/CN108654518A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108043349A (en) * | 2017-12-06 | 2018-05-18 | 郑州诚合信息技术有限公司 | A kind of solid-liquid reaction kettle for increasing reaction rate |
| CN107999534A (en) * | 2018-01-29 | 2018-05-08 | 李子琦 | A kind of soil remediation equipment of intermittent spray |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110721623A (en) * | 2019-12-19 | 2020-01-24 | 湖南乐准智芯生物科技有限公司 | Reagent vibration mixing method |
| CN110721623B (en) * | 2019-12-19 | 2020-04-10 | 湖南乐准智芯生物科技有限公司 | Reagent vibration mixing method |
| CN112546933A (en) * | 2020-09-21 | 2021-03-26 | 湖南嘉顺华新材料有限公司 | A agitating unit for dry powder slurrying |
| CN113583460A (en) * | 2021-06-19 | 2021-11-02 | 浙江巍翔科技集团有限公司 | Bio-based modified low-heat-generation reinforcing agent and preparation method thereof |
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Application publication date: 20181016 |