CN108641279A - A kind of thermal insulation board that flame retardant property is good - Google Patents
A kind of thermal insulation board that flame retardant property is good Download PDFInfo
- Publication number
- CN108641279A CN108641279A CN201810539584.8A CN201810539584A CN108641279A CN 108641279 A CN108641279 A CN 108641279A CN 201810539584 A CN201810539584 A CN 201810539584A CN 108641279 A CN108641279 A CN 108641279A
- Authority
- CN
- China
- Prior art keywords
- parts
- thermal insulation
- insulation board
- flame retardant
- phenolic resin
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J9/00—Working-up of macromolecular substances to porous or cellular articles or materials; After-treatment thereof
- C08J9/04—Working-up of macromolecular substances to porous or cellular articles or materials; After-treatment thereof using blowing gases generated by a previously added blowing agent
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J9/00—Working-up of macromolecular substances to porous or cellular articles or materials; After-treatment thereof
- C08J9/0061—Working-up of macromolecular substances to porous or cellular articles or materials; After-treatment thereof characterized by the use of several polymeric components
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J9/00—Working-up of macromolecular substances to porous or cellular articles or materials; After-treatment thereof
- C08J9/0066—Use of inorganic compounding ingredients
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J2361/00—Characterised by the use of condensation polymers of aldehydes or ketones; Derivatives of such polymers
- C08J2361/04—Condensation polymers of aldehydes or ketones with phenols only
- C08J2361/06—Condensation polymers of aldehydes or ketones with phenols only of aldehydes with phenols
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J2423/00—Characterised by the use of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Derivatives of such polymers
- C08J2423/26—Characterised by the use of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Derivatives of such polymers modified by chemical after-treatment
- C08J2423/30—Characterised by the use of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Derivatives of such polymers modified by chemical after-treatment by oxidation
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J2433/00—Characterised by the use of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and only one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Derivatives of such polymers
- C08J2433/04—Characterised by the use of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and only one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Derivatives of such polymers esters
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J2475/00—Characterised by the use of polyureas or polyurethanes; Derivatives of such polymers
- C08J2475/04—Polyurethanes
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J2491/00—Characterised by the use of oils, fats or waxes; Derivatives thereof
- C08J2491/06—Waxes
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K13/00—Use of mixtures of ingredients not covered by one single of the preceding main groups, each of these compounds being essential
- C08K13/04—Ingredients characterised by their shape and organic or inorganic ingredients
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/34—Silicon-containing compounds
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K7/00—Use of ingredients characterised by shape
- C08K7/02—Fibres or whiskers
- C08K7/04—Fibres or whiskers inorganic
- C08K7/14—Glass
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K7/00—Use of ingredients characterised by shape
- C08K7/22—Expanded, porous or hollow particles
- C08K7/24—Expanded, porous or hollow particles inorganic
- C08K7/26—Silicon- containing compounds
Abstract
The invention discloses a kind of good thermal insulation boards of flame retardant property, including below according to the raw material of parts by weight：50 80 parts of polyacrylate dispersion, 80 100 parts of phenolic resin, 30 50 parts of expanded perlite, 20 30 parts of porous ceramic grain, 80 100 parts of deionized water, 20 30 parts of hydrophobicity aluminium-magnesium silicate, 8 10 parts of oxidized polyethylene wax, 13 parts of divinylbenzene, 12 parts of foaming agent, 15 20 parts of alumina silicate, 10 15 parts of polyurethane, 13 parts of fire retardant, 35 parts of glass fibre, 25 parts of paraffin.The invention also discloses the preparation methods of the good thermal insulation board of the flame retardant property.Thermal insulation board prepared by the present invention can effectively completely cut off heat under the common mating reaction of various raw materials, and thermal insulation board prepared by the present invention also has good flame retardant property.
Description
Technical field
The present invention relates to environment-friendly materials technical field, the good thermal insulation board of specifically a kind of flame retardant property.
Background technology
With the fast development of China's urban construction, mega structure energy consumption has become China's economy and social development
Great burden, therefore, green energy conservation have become the theme of current architectural development.External-wall heat-insulation material is in building energy conservation process
In play very important role, be external walls heating insulation implement a key link.Unquestionably, excellent heat preservation
Performance is the critical index of external-wall heat-insulation material production and preparation.
Thermal insulation board is isolation indoor environment and a kind of common used material of external environment, at present the thermal insulation board heat preservation in construction market
Effect is general, and part thermal insulation board is made of plastic foam, and anti-flammability is poor, when fire occurs, external wall insulation burning,
Threat is brought to resident's life and property.
Invention content
It is mentioned above in the background art to solve the purpose of the present invention is to provide a kind of good thermal insulation board of flame retardant property
Problem.
To achieve the above object, the present invention provides the following technical solutions：
A kind of thermal insulation board that flame retardant property is good, including below according to the raw material of parts by weight：Polyacrylate dispersion 50-80
It is part, 80-100 parts of phenolic resin, 30-50 parts of expanded perlite, 20-30 parts of porous ceramic grain, 80-100 parts of deionized water, hydrophobic
20-30 parts of aluminium-magnesium silicate of property, 8-10 parts of oxidized polyethylene wax, 1-3 parts of divinylbenzene, 1-2 parts of foaming agent, alumina silicate 15-20
Part, 10-15 parts of polyurethane, 1-3 parts of fire retardant, 3-5 parts of glass fibre, 2-5 parts of paraffin.
As a further solution of the present invention：Including below according to the raw material of parts by weight：Polyacrylate dispersion 60-70
Part, 85-95 parts of phenolic resin, 35-45 parts of expanded perlite, 22-27 parts of porous ceramic grain, 85-95 parts of deionized water, hydrophobicity
23-27 parts of aluminium-magnesium silicate, 8-9 parts of oxidized polyethylene wax, 2-3 parts of divinylbenzene, 1.2-1.7 parts of foaming agent, alumina silicate 16-
18 parts, 12-14 parts of polyurethane, 1-2 parts of fire retardant, 3.5-4.5 parts of glass fibre, 3-4 parts of paraffin.
As further scheme of the invention：Including below according to the raw material of parts by weight：65 parts of polyacrylate dispersion,
90 parts of phenolic resin, 40 parts of expanded perlite, 25 parts of porous ceramic grain, 90 parts of deionized water, 25 parts of hydrophobicity aluminium-magnesium silicate, oxygen
Change 9 parts of polyethylene wax, 2 parts of divinylbenzene, 1.5 parts of foaming agent, 17 parts of alumina silicate, 12 parts of polyurethane, 2 parts of fire retardant, glass
4 parts of fiber, 3 parts of paraffin.
As further scheme of the invention：The fire retardant is made of magnesium hydroxide and aluminium hydroxide mixing.
As further scheme of the invention：The composition weight ratio of magnesium hydroxide and aluminium hydroxide is in the fire retardant
3:1。
The preparation method of the good thermal insulation board of the flame retardant property, steps are as follows：
1) phenolic resin, expanded perlite, porous ceramic grain and glass fibre are smashed it through into 150-200 mesh sieve respectively, obtained
Obtain glass bead, phenolic resin, alumina silicate and glass fibre powder；
2) polyacrylate dispersion, phenolic resin, expanded perlite, porous ceramic grain and deionized water are mixed, in 200-
It under 300r/min speed conditions, stirs 20-35 minutes, obtains mixture I；
3) by hydrophobicity aluminium-magnesium silicate, oxidized polyethylene wax, divinylbenzene, alumina silicate, polyurethane, glass fibre and
Paraffin is added in the mixture that step 2) obtains, and mixing is warming up to 120-150 DEG C, under the rotating speed of 400-600r/min, stirs
It mixes 30-50 minutes, stands 10-15min, obtain mixture II；
4) foaming agent and fire retardant are added in the mixture II that step 3) obtains, 50-60 DEG C are cooled to, in 300-
It under the rotating speed of 500r/min, stirs 10-15 minutes, obtains mixture III.
5) mixture III that step 4) obtains is poured into mold, is cooled to room temperature, is press-formed, then will be after extrusion forming
Obtained module, which is sent into baking oven, dries, cooling.
The application of above-mentioned thermal insulation board in the field of construction.
Compared with prior art, the beneficial effects of the invention are as follows：
Thermal insulation board prepared by the present invention can effectively completely cut off heat under the common mating reaction of various raw materials, play guarantor
The effect of temperature avoids Summer Indoor high temperature from conducting to heat loss in indoor or winter room, reduces the use of air-conditioning or heating,
It is energy saving；Thermal insulation board prepared by the present invention also has good flame retardant property, prevents from burning, and when fire occurs, effectively protects
Hinder resident's safety of life and property.
Specific implementation mode
The technical scheme in the embodiments of the invention will be clearly and completely described below, it is clear that described implementation
Example is only a part of the embodiment of the present invention, instead of all the embodiments.Based on the embodiments of the present invention, this field is general
The every other embodiment that logical technical staff is obtained without making creative work, belongs to protection of the present invention
Range.
Embodiment 1
A kind of thermal insulation board that flame retardant property is good, including below according to the raw material of parts by weight：50 parts of polyacrylate dispersion, phenol
80 parts of urea formaldehyde, 30 parts of expanded perlite, 20 parts of porous ceramic grain, 80 parts of deionized water, 20 parts of hydrophobicity aluminium-magnesium silicate, oxidation
8 parts of polyethylene wax, 1 part of divinylbenzene, 1 part of foaming agent, 15 parts of alumina silicate, 10 parts of polyurethane, 1 part of fire retardant, glass fibre
3 parts, 2 parts of paraffin.
Wherein, the fire retardant is made of magnesium hydroxide and aluminium hydroxide mixing.
Wherein, the composition weight ratio of magnesium hydroxide and aluminium hydroxide is 3 in the fire retardant:1.
In the present embodiment, the preparation method of the good thermal insulation board of the flame retardant property, steps are as follows：
1) phenolic resin, expanded perlite, porous ceramic grain and glass fibre are smashed it through into 150 mesh sieve respectively, obtains glass
Change microballon, phenolic resin, alumina silicate and glass fibre powder；
2) polyacrylate dispersion, phenolic resin, expanded perlite, porous ceramic grain and deionized water are mixed, in 200r/
It under min speed conditions, stirs 20 minutes, obtains mixture I；
3) by hydrophobicity aluminium-magnesium silicate, oxidized polyethylene wax, divinylbenzene, alumina silicate, polyurethane, glass fibre and
Paraffin is added in the mixture that step 2) obtains, and mixing is warming up to 120 DEG C, under the rotating speed of 400r/min, stirs 30 minutes,
10min is stood, mixture II is obtained；
4) foaming agent and fire retardant are added in the mixture II that step 3) obtains, 50 DEG C are cooled to, 300r/min's
It under rotating speed, stirs 10 minutes, obtains mixture III.
5) mixture III that step 4) obtains is poured into mold, is cooled to room temperature, is press-formed, then will be after extrusion forming
Obtained module, which is sent into baking oven, dries, cooling.
Embodiment 2
A kind of thermal insulation board that flame retardant property is good, including below according to the raw material of parts by weight：70 parts of polyacrylate dispersion, phenol
95 parts of urea formaldehyde, 45 parts of expanded perlite, 27 parts of porous ceramic grain, 95 parts of deionized water, 23 parts of hydrophobicity aluminium-magnesium silicate, oxidation
8 parts of polyethylene wax, 2 parts of divinylbenzene, 1.2 parts of foaming agent, 16 parts of alumina silicate, 12 parts of polyurethane, 1 part of fire retardant, glass fibers
Tie up 3.5 parts, 3 parts of paraffin.
Wherein, the fire retardant is made of magnesium hydroxide and aluminium hydroxide mixing.
Wherein, the composition weight ratio of magnesium hydroxide and aluminium hydroxide is 3 in the fire retardant:1.
In the present embodiment, the preparation method of the good thermal insulation board of the flame retardant property, steps are as follows：
1) phenolic resin, expanded perlite, porous ceramic grain and glass fibre are smashed it through into 180 mesh sieve respectively, obtains glass
Change microballon, phenolic resin, alumina silicate and glass fibre powder；
2) polyacrylate dispersion, phenolic resin, expanded perlite, porous ceramic grain and deionized water are mixed, in 250r/
It under min speed conditions, stirs 28 minutes, obtains mixture I；
3) by hydrophobicity aluminium-magnesium silicate, oxidized polyethylene wax, divinylbenzene, alumina silicate, polyurethane, glass fibre and
Paraffin is added in the mixture that step 2) obtains, and mixing is warming up to 135 DEG C, under the rotating speed of 500r/min, stirs 40 minutes,
12min is stood, mixture II is obtained；
4) foaming agent and fire retardant are added in the mixture II that step 3) obtains, 55 DEG C are cooled to, 400r/min's
It under rotating speed, stirs 12 minutes, obtains mixture III.
5) mixture III that step 4) obtains is poured into mold, is cooled to room temperature, is press-formed, then will be after extrusion forming
Obtained module, which is sent into baking oven, dries, cooling.
Embodiment 3
A kind of thermal insulation board that flame retardant property is good, including below according to the raw material of parts by weight：65 parts of polyacrylate dispersion, phenol
90 parts of urea formaldehyde, 40 parts of expanded perlite, 25 parts of porous ceramic grain, 90 parts of deionized water, 25 parts of hydrophobicity aluminium-magnesium silicate, oxidation
9 parts of polyethylene wax, 2 parts of divinylbenzene, 1.5 parts of foaming agent, 17 parts of alumina silicate, 12 parts of polyurethane, 2 parts of fire retardant, glass fibers
Tie up 4 parts, 3 parts of paraffin.
Wherein, the fire retardant is made of magnesium hydroxide and aluminium hydroxide mixing.
Wherein, the composition weight ratio of magnesium hydroxide and aluminium hydroxide is 3 in the fire retardant:1.
In the present embodiment, the preparation method of the good thermal insulation board of the flame retardant property, steps are as follows：
1) phenolic resin, expanded perlite, porous ceramic grain and glass fibre are smashed it through into 180 mesh sieve respectively, obtains glass
Change microballon, phenolic resin, alumina silicate and glass fibre powder；
2) polyacrylate dispersion, phenolic resin, expanded perlite, porous ceramic grain and deionized water are mixed, in 250r/
It under min speed conditions, stirs 28 minutes, obtains mixture I；
3) by hydrophobicity aluminium-magnesium silicate, oxidized polyethylene wax, divinylbenzene, alumina silicate, polyurethane, glass fibre and
Paraffin is added in the mixture that step 2) obtains, and mixing is warming up to 135 DEG C, under the rotating speed of 500r/min, stirs 40 minutes,
12min is stood, mixture II is obtained；
4) foaming agent and fire retardant are added in the mixture II that step 3) obtains, 55 DEG C are cooled to, 400r/min's
It under rotating speed, stirs 12 minutes, obtains mixture III.
5) mixture III that step 4) obtains is poured into mold, is cooled to room temperature, is press-formed, then will be after extrusion forming
Obtained module, which is sent into baking oven, dries, cooling.
Embodiment 4
A kind of thermal insulation board that flame retardant property is good, including below according to the raw material of parts by weight：60 parts of polyacrylate dispersion, phenol
85 parts of urea formaldehyde, 35 parts of expanded perlite, 22 parts of porous ceramic grain, 85 parts of deionized water, 27 parts of hydrophobicity aluminium-magnesium silicate, oxidation
9 parts of polyethylene wax, 3 parts of divinylbenzene, 1.7 parts of foaming agent, 18 parts of alumina silicate, 14 parts of polyurethane, 2 parts of fire retardant, glass fibers
Tie up 4.5 parts, 4 parts of paraffin.
Wherein, the fire retardant is made of magnesium hydroxide and aluminium hydroxide mixing.
Wherein, the composition weight ratio of magnesium hydroxide and aluminium hydroxide is 3 in the fire retardant:1.
In the present embodiment, the preparation method of the good thermal insulation board of the flame retardant property, steps are as follows：
1) phenolic resin, expanded perlite, porous ceramic grain and glass fibre are smashed it through into 180 mesh sieve respectively, obtains glass
Change microballon, phenolic resin, alumina silicate and glass fibre powder；
2) polyacrylate dispersion, phenolic resin, expanded perlite, porous ceramic grain and deionized water are mixed, in 250r/
It under min speed conditions, stirs 28 minutes, obtains mixture I；
3) by hydrophobicity aluminium-magnesium silicate, oxidized polyethylene wax, divinylbenzene, alumina silicate, polyurethane, glass fibre and
Paraffin is added in the mixture that step 2) obtains, and mixing is warming up to 135 DEG C, under the rotating speed of 500r/min, stirs 40 minutes,
12min is stood, mixture II is obtained；
4) foaming agent and fire retardant are added in the mixture II that step 3) obtains, 55 DEG C are cooled to, 400r/min's
It under rotating speed, stirs 12 minutes, obtains mixture III.
5) mixture III that step 4) obtains is poured into mold, is cooled to room temperature, is press-formed, then will be after extrusion forming
Obtained module, which is sent into baking oven, dries, cooling.
Embodiment 5
A kind of thermal insulation board that flame retardant property is good, including below according to the raw material of parts by weight：80 parts of polyacrylate dispersion, phenol
100 parts of urea formaldehyde, 50 parts of expanded perlite, 30 parts of porous ceramic grain, 100 parts of deionized water, 30 parts of hydrophobicity aluminium-magnesium silicate, oxygen
Change 10 parts of polyethylene wax, 3 parts of divinylbenzene, 2 parts of foaming agent, 20 parts of alumina silicate, 15 parts of polyurethane, 3 parts of fire retardant, glass
5 parts of fiber, 5 parts of paraffin.
Wherein, the fire retardant is made of magnesium hydroxide and aluminium hydroxide mixing.
Wherein, the composition weight ratio of magnesium hydroxide and aluminium hydroxide is 3 in the fire retardant:1.
In the present embodiment, the preparation method of the good thermal insulation board of the flame retardant property, steps are as follows：
1) phenolic resin, expanded perlite, porous ceramic grain and glass fibre are smashed it through into 200 mesh sieve respectively, obtains glass
Change microballon, phenolic resin, alumina silicate and glass fibre powder；
2) polyacrylate dispersion, phenolic resin, expanded perlite, porous ceramic grain and deionized water are mixed, in 300r/
It under min speed conditions, stirs 35 minutes, obtains mixture I；
3) by hydrophobicity aluminium-magnesium silicate, oxidized polyethylene wax, divinylbenzene, alumina silicate, polyurethane, glass fibre and
Paraffin is added in the mixture that step 2) obtains, and mixing is warming up to 150 DEG C, under the rotating speed of 600r/min, stirs 50 minutes,
15min is stood, mixture II is obtained；
4) foaming agent and fire retardant are added in the mixture II that step 3) obtains, 60 DEG C are cooled to, 500r/min's
It under rotating speed, stirs 15 minutes, obtains mixture III.
5) mixture III that step 4) obtains is poured into mold, is cooled to room temperature, is press-formed, then will be after extrusion forming
Obtained module, which is sent into baking oven, dries, cooling.
Comparative example 1
Compared with Example 3, glass fibre is free of, other are same as Example 3.
Comparative example 2
Compared with Example 3, paraffin is free of, other are same as Example 3.
Comparative example 3
Compared with Example 3, glass fibre and paraffin are free of, other are same as Example 3.
Thermal insulation board prepared by embodiment 1-5 and comparative example 1-3 is tested for the property, test result is as shown in table 1.
Table 1
From in result above as can be seen that the thermal insulation board for preparing of the present invention is under the common mating reaction of various raw materials, energy
Enough effectively isolation heats, play the role of heat preservation, and Summer Indoor high temperature is avoided to conduct to heat loss in indoor or winter room,
The use of air-conditioning or heating is reduced, it is energy saving；Thermal insulation board prepared by the present invention also has good flame retardant property, prevents from firing
It burns, when fire occurs, effective guarantee resident's safety of life and property.
It is obvious to a person skilled in the art that invention is not limited to the details of the above exemplary embodiments, Er Qie
In the case of without departing substantially from spirit or essential attributes of the invention, the present invention can be realized in other specific forms.Therefore, nothing
By from the point of view of which point, the present embodiments are to be considered as illustrative and not restrictive, and the scope of the present invention is by institute
Attached claim rather than above description limit, it is intended that will fall within the meaning and scope of the equivalent requirements of the claims
All changes be included within the present invention.
In addition, it should be understood that although this specification is described in terms of embodiments, but not each embodiment is only wrapped
Containing an independent technical solution, this description of the specification is merely for the sake of clarity, and those skilled in the art should
It considers the specification as a whole, the technical solutions in the various embodiments may also be suitably combined, forms those skilled in the art
The other embodiment being appreciated that.
Claims (7)
1. a kind of good thermal insulation board of flame retardant property, which is characterized in that including below according to the raw material of parts by weight：Polyacrylate breast
50-80 parts of liquid, 80-100 parts of phenolic resin, 30-50 parts of expanded perlite, 20-30 parts of porous ceramic grain, deionized water 80-100
Part, 20-30 parts of hydrophobicity aluminium-magnesium silicate, 8-10 parts of oxidized polyethylene wax, 1-3 parts of divinylbenzene, 1-2 parts of foaming agent, silicic acid
15-20 parts of aluminium, 10-15 parts of polyurethane, 1-3 parts of fire retardant, 3-5 parts of glass fibre, 2-5 parts of paraffin.
2. the good thermal insulation board of flame retardant property according to claim 1, which is characterized in that including below according to the original of parts by weight
Material：60-70 parts of polyacrylate dispersion, 35-45 parts of expanded perlite, 22-27 parts of porous ceramic grain, is gone 85-95 parts of phenolic resin
85-95 parts of ionized water, 23-27 parts of hydrophobicity aluminium-magnesium silicate, 8-9 parts of oxidized polyethylene wax, 2-3 parts of divinylbenzene, foaming agent
1.2-1.7 parts, 16-18 parts of alumina silicate, 12-14 parts of polyurethane, 1-2 parts of fire retardant, 3.5-4.5 parts of glass fibre, paraffin 3-4
Part.
3. the good thermal insulation board of flame retardant property according to claim 2, which is characterized in that including below according to the original of parts by weight
Material：65 parts of polyacrylate dispersion, 90 parts of phenolic resin, 40 parts of expanded perlite, 25 parts of porous ceramic grain, 90 parts of deionized water,
25 parts of hydrophobicity aluminium-magnesium silicate, 9 parts of oxidized polyethylene wax, 2 parts of divinylbenzene, 1.5 parts of foaming agent, 17 parts of alumina silicate, poly- ammonia
12 parts of ester, 2 parts of fire retardant, 4 parts of glass fibre, 3 parts of paraffin.
4. the good thermal insulation board of flame retardant property according to claim 1, which is characterized in that the fire retardant by magnesium hydroxide and
Aluminium hydroxide mixing composition.
5. the good thermal insulation board of flame retardant property according to claim 1, which is characterized in that in the fire retardant magnesium hydroxide and
The composition weight ratio of aluminium hydroxide is 3:1.
6. a kind of preparation method of the good thermal insulation board of flame retardant property according to any one of claims 1 to 5, which is characterized in that step
It is as follows：
1) phenolic resin, expanded perlite, porous ceramic grain and glass fibre are smashed it through into 150-200 mesh sieve respectively, obtains glass
Change microballon, phenolic resin, alumina silicate and glass fibre powder；
2) polyacrylate dispersion, phenolic resin, expanded perlite, porous ceramic grain and deionized water are mixed, in 200-300r/
It under min speed conditions, stirs 20-35 minutes, obtains mixture I；
3) hydrophobicity aluminium-magnesium silicate, oxidized polyethylene wax, divinylbenzene, alumina silicate, polyurethane, glass fibre and paraffin are added
In the mixture for entering step 2) acquisition, mixing is warming up to 120-150 DEG C, under the rotating speed of 400-600r/min, stirs 30-50
Minute, 10-15min is stood, mixture II is obtained；
4) foaming agent and fire retardant are added in the mixture II that step 3) obtains, 50-60 DEG C are cooled to, in 300-500r/min
Rotating speed under, stir 10-15 minute, acquisition mixture III.
5) mixture III that step 4) obtains is poured into mold, is cooled to room temperature, is press-formed, then will be obtained after extrusion forming
Module be sent into baking oven and dry, it is cooling.
7. a kind of application of thermal insulation board according to any one of claims 1 to 5 in the field of construction.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810539584.8A CN108641279A (en) | 2018-05-30 | 2018-05-30 | A kind of thermal insulation board that flame retardant property is good |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810539584.8A CN108641279A (en) | 2018-05-30 | 2018-05-30 | A kind of thermal insulation board that flame retardant property is good |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN108641279A true CN108641279A (en) | 2018-10-12 |
Family
ID=63758609
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201810539584.8A Pending CN108641279A (en) | 2018-05-30 | 2018-05-30 | A kind of thermal insulation board that flame retardant property is good |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN108641279A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110981408A (en) * | 2019-12-13 | 2020-04-10 | 陕西速源节能科技有限公司 | Heat-preserving and heat-insulating energy-saving material |
| CN111647264A (en) * | 2020-07-04 | 2020-09-11 | 上海方之德新材料有限公司 | High-flame-retardant low-smoke halogen-free TPU cable material and preparation method thereof |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105089233A (en) * | 2015-08-06 | 2015-11-25 | 安徽铭源新型建材科技有限公司 | High-performance heat insulation wallboard and method for preparing fireproof material thereof |
| US20150345132A1 (en) * | 2014-05-30 | 2015-12-03 | Guang Zhou Zong Bao Xian Wei Zhi Pin Co., Ltd. | Fiber reinforcement fire-proof thermal insulation plate and preparation process thereof |
| CN105585814A (en) * | 2015-12-29 | 2016-05-18 | 青岛宏宇环保空调设备有限公司 | Fireproof and flame-retardant thermal insulation board |
| CN106554598A (en) * | 2016-11-09 | 2017-04-05 | 郑州圣莱特空心微珠新材料有限公司 | A kind of phenolic resin warming plate and preparation method thereof |
| CN107163355A (en) * | 2017-07-12 | 2017-09-15 | 合肥梵腾环保科技有限公司 | A kind of construction material of energy-conserving and environment-protective and preparation method thereof |
-
2018
- 2018-05-30 CN CN201810539584.8A patent/CN108641279A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20150345132A1 (en) * | 2014-05-30 | 2015-12-03 | Guang Zhou Zong Bao Xian Wei Zhi Pin Co., Ltd. | Fiber reinforcement fire-proof thermal insulation plate and preparation process thereof |
| CN105089233A (en) * | 2015-08-06 | 2015-11-25 | 安徽铭源新型建材科技有限公司 | High-performance heat insulation wallboard and method for preparing fireproof material thereof |
| CN105585814A (en) * | 2015-12-29 | 2016-05-18 | 青岛宏宇环保空调设备有限公司 | Fireproof and flame-retardant thermal insulation board |
| CN106554598A (en) * | 2016-11-09 | 2017-04-05 | 郑州圣莱特空心微珠新材料有限公司 | A kind of phenolic resin warming plate and preparation method thereof |
| CN107163355A (en) * | 2017-07-12 | 2017-09-15 | 合肥梵腾环保科技有限公司 | A kind of construction material of energy-conserving and environment-protective and preparation method thereof |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110981408A (en) * | 2019-12-13 | 2020-04-10 | 陕西速源节能科技有限公司 | Heat-preserving and heat-insulating energy-saving material |
| CN111647264A (en) * | 2020-07-04 | 2020-09-11 | 上海方之德新材料有限公司 | High-flame-retardant low-smoke halogen-free TPU cable material and preparation method thereof |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN103275459B (en) | Urea resin foam thermal-insulation composite material and preparation method thereof | |
| CN103553502A (en) | Lightweight inorganic insulation board containing silica aerogel and preparation method thereof | |
| CN102924037B (en) | Fire protection insulation board for building outer wall and method for producing fire protection insulation board | |
| CN107619224B (en) | Anti-cracking heat-preserving recycled aggregate mortar and preparation method thereof | |
| CN104556954A (en) | Magnesium phosphate cement-base porous material and preparation method thereof | |
| CN106478077A (en) | A kind of porous thermal insulating ceramic material for building and preparation method thereof | |
| CN106117856A (en) | A kind of fire prevention polystyrene thermal insulation plate and preparation method thereof | |
| CN104016706A (en) | Environment-friendly building board and preparation method thereof | |
| CN102503495B (en) | Fireproof thermal insulation plate base material and preparation method thereof | |
| CN104804368A (en) | Phenolic resin and polyurethane prepolymer composite foam material and preparation method | |
| CN108641279A (en) | A kind of thermal insulation board that flame retardant property is good | |
| CN104086210A (en) | Improved environment-friendly building board and preparation method thereof | |
| CN108976666A (en) | A kind of high-strength waterproofness and thermal insulation plate and preparation method thereof | |
| CN105733173A (en) | Preparation method of high efficient and energy saving phenolic foam board | |
| CN102745953B (en) | Steam-cured high-performance foam concrete block, production method and application thereof | |
| CN102219450B (en) | Waterproof crack-resistant fireproof internal and external wall heat-preserving heat-insulating coating and preparation method thereof | |
| CN101781919A (en) | Low heat conduction light heat insulating silica brick | |
| CN103408283A (en) | Light burning-avoiding heat-insulating material and preparation method thereof | |
| CN109305793A (en) | A kind of pitchstone thermal insulation material and preparation method thereof | |
| CN110563423B (en) | Preparation method of paper-surface gypsum board and paper-surface gypsum board | |
| CN105948721A (en) | Light foamed thermal insulation material and preparation method thereof | |
| CN104058785B (en) | A kind of foaming cement thermal insulation plate | |
| CN112521123B (en) | Preparation method of basic magnesium sulfate cement foam concrete thermal insulation material | |
| CN108821710A (en) | A kind of expansion type energy-saving heat preserving fire proofing material and its preparation process | |
| CN105864578A (en) | Antibacterial and energy-saving glass fiber and magnesium composite air duct and manufacturing method thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20181012 |