CN108611007A - A kind of polyvinyl fluoride weather-resistant glue band - Google Patents
A kind of polyvinyl fluoride weather-resistant glue band Download PDFInfo
- Publication number
- CN108611007A CN108611007A CN201611244574.9A CN201611244574A CN108611007A CN 108611007 A CN108611007 A CN 108611007A CN 201611244574 A CN201611244574 A CN 201611244574A CN 108611007 A CN108611007 A CN 108611007A
- Authority
- CN
- China
- Prior art keywords
- polyvinyl fluoride
- weather
- release film
- film layer
- layer
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J153/00—Adhesives based on block copolymers containing at least one sequence of a polymer obtained by reactions only involving carbon-to-carbon unsaturated bonds; Adhesives based on derivatives of such polymers
- C09J153/02—Vinyl aromatic monomers and conjugated dienes
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J11/00—Features of adhesives not provided for in group C09J9/00, e.g. additives
- C09J11/02—Non-macromolecular additives
- C09J11/06—Non-macromolecular additives organic
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J11/00—Features of adhesives not provided for in group C09J9/00, e.g. additives
- C09J11/08—Macromolecular additives
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J145/00—Adhesives based on homopolymers or copolymers of compounds having no unsaturated aliphatic radicals in a side chain, and having one or more carbon-to-carbon double bonds in a carbocyclic or in a heterocyclic system; Adhesives based on derivatives of such polymers
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2201/00—Properties
- C08L2201/08—Stabilised against heat, light or radiation or oxydation
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J2301/00—Additional features of adhesives in the form of films or foils
- C09J2301/10—Additional features of adhesives in the form of films or foils characterized by the structural features of the adhesive tape or sheet
- C09J2301/12—Additional features of adhesives in the form of films or foils characterized by the structural features of the adhesive tape or sheet by the arrangement of layers
- C09J2301/122—Additional features of adhesives in the form of films or foils characterized by the structural features of the adhesive tape or sheet by the arrangement of layers the adhesive layer being present only on one side of the carrier, e.g. single-sided adhesive tape
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J2301/00—Additional features of adhesives in the form of films or foils
- C09J2301/10—Additional features of adhesives in the form of films or foils characterized by the structural features of the adhesive tape or sheet
- C09J2301/12—Additional features of adhesives in the form of films or foils characterized by the structural features of the adhesive tape or sheet by the arrangement of layers
- C09J2301/124—Additional features of adhesives in the form of films or foils characterized by the structural features of the adhesive tape or sheet by the arrangement of layers the adhesive layer being present on both sides of the carrier, e.g. double-sided adhesive tape
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J2453/00—Presence of block copolymer
Abstract
The invention discloses a kind of weather-proof polyvinyl fluoride tapes, are combined by polyvinyl fluoride thin film layer, adhesive layer and release film layer, or are combined by release film layer, adhesive layer, polyvinyl fluoride thin film layer, adhesive layer and release film layer.Polyvinyl fluoride tape provided by the invention is suitable for the weather-proof field required, the protection particularly suitable for insulating sheath, air charge configuration and bridge cable casing.
Description
Technical field
The invention belongs to Process Technology of Polymer field, more particularly to a kind of polyvinyl fluoride weather-resistant glue band.
Background technology
Polyvinyl fluoride (PVF) film have excellent weatherability, when by as protective layer be applied to house wallboards, roof and
Whens building board etc., the service life of house wallboards, roof and building board can be extended, or even can ensure that service life exists
25 years or more.Just because of excellent performance, polyvinyl fluoride thin film is by widely applied to base material under adverse circumstances in recent years
Durability protection, as house and business wooden partition, decoration and reinforcement material, wall covering, ceiling, sound panel, insulating sheath,
Heat-insulated or sound insulation material material bag packaging film, fitting building board and noise barrier etc..
When by polyvinyl fluoride thin film for building aspect protection, the prior art is generally by it in such a way that dry type is compound
It is compounded in protected surface.General way is to release base material by unreeling machine, glue, and being then passed through hot drying tunnel makes rapidly
Solvent volatilization in glue, is then finally placed the base material for being coated with glue-line by pressure roller and polyvinyl fluoride thin film composite molding
In an oven after curing a period of time to obtain the final product.
The method that composite material is prepared disclosed in the prior art can be used in large-scale building, sound panel, house roof etc.
Field, but in certain special dimensions such as insulating sheath, air charge configuration and bridge cable casing protection etc., due to base material or
Limitation in terms of construction technology limits the application of polyvinyl fluoride thin film.
Therefore, it is necessary to be further improved to the preparation of the composite material containing polyvinyl fluoride thin film.
Invention content
The purpose of the present invention is to provide a kind of weather-proof polyvinyl fluoride tapes, suitable for the weather-proof neck required
Domain.
The present invention provides the following technical solutions：
A kind of weather-proof polyvinyl fluoride tape, the adhesive tape are compound by polyvinyl fluoride thin film layer, adhesive layer and release film layer
It forms,
Or it is combined by release film layer, adhesive layer, polyvinyl fluoride thin film layer, adhesive layer and release film layer；
It is compound by adhesive layer between the polyvinyl fluoride thin film layer and release film layer；
The adhesive layer contains in mass：Styrene-isoprene-styrene block copolymer and/or styrene-fourth
100 parts of styrene block copolymer, 30~150 parts of tackifying resin, 10~50 parts of softening agent, 0.5~2 part of anti-aging agent.
Polyvinyl fluoride tape provided by the invention can be bonded through adhesive layer by polyvinyl fluoride thin film layer and release film layer
Made of three-decker, can also be bonded through two layers of adhesive layer by release film layer, polyvinyl fluoride thin film layer and release film layer and
At five-layer structure.Additionally can be as needed, polyvinyl fluoride thin film layer and release film layer are bonded into five by adhesive layer
Layer or more structure.
Polyvinyl fluoride tape provided by the invention, the adhesive layer used contain in mass：Styrene-isoprene-benzene
100 parts of ethylene block copolymer (referred to as " SIS ") and/or Styrene-Butadiene-Styrene Block Copolymer (referred to as " SBS "),
30~150 parts of tackifying resin, 10~50 parts of softening agent, 0.5~2 part of anti-aging agent.
The tackifying resin used in adhesive layer, it is preferred that the tackifying resin is in terpene resin and C9 resins
It is at least one.
The softening agent used in adhesive layer, it is preferred that the softening agent is in epoxidized soybean oil and chlorinated paraffin
It is at least one.
The anti-aging agent used in adhesive layer, it is preferred that the anti-aging agent is selected from N, and N- dibutyl vulcanizes Aminobenzoic Acid zinc
At least one of with two thio Aminobenzoic Acid zinc of ethylphenyl.
Polyvinyl fluoride tape provided by the invention, the release film layer used, it is preferred that the release film is selected from polyethylene
At least one of release film, polypropylene release film, polyimides release film and polyethylene terephthalate release film.
The release film layer, it is preferred that its off-type force is 1~60gf/in.
Polyvinyl fluoride tape provided by the invention, the polyvinyl fluoride thin film used, it is preferred that the polyvinyl fluoride thin film
Surface tension be 40~55dyne/cm.
The thickness of polyvinyl fluoride tape provided by the invention, polyvinyl fluoride thin film layer is preferably 15~60 μm.
Polyvinyl fluoride tape provided by the invention, gluing layer thickness are preferably 5~25 μm.
Polyvinyl fluoride tape provided by the invention, has weatherability, suitable for the weather-proof field required.
Preferably, the polyvinyl fluoride tape is particularly suitable for insulating sheath, air charge configuration and bridge cable
The protection of casing.
Specific implementation mode
With reference to specific embodiment, invention is further explained, but does not limit the invention to these tools
Body embodiment.One skilled in the art would recognize that present invention encompasses may include in Claims scope
All alternatives, improvement project and equivalent scheme.
In following embodiment, each indication test method is as follows：
(1) cohesive force：It is tested according to GB/T8808 methods；
(2) tensile strength:It is tested according to ASTM D882 methods；
(3) moisture-vapor transmission：It is tested according to 1037 methods of GB/T.
Embodiment 1
In mass, gluing layer formula is as follows：
100 parts of SIS resins, 120 parts of terpene resin, 20 parts of epoxidized soybean oil, N, N- dibutyl vulcanize Aminobenzoic Acid zinc 0.5
Part.
The release film used is polyethylene release film, off-type force 6gf/in.
Three layers of polyvinyl fluoride thin film, adhesive layer and release film be combined with each other successively, wherein polyvinyl fluoride thin film layer
Thickness is 50 μm, the thickness of adhesive layer is 15 μm, the thickness of release film is 20 μm.
Embodiment 2
In mass, gluing layer formula is as follows：
100 parts of SIS resins, 120 parts of terpene resin, 20 parts of epoxidized soybean oil, N, N- dibutyl vulcanize Aminobenzoic Acid zinc 0.5
Part.
The release film used is polyethylene release film, off-type force 6gf/in.
Five layers of release film layer, adhesive layer, polyvinyl fluoride thin film layer, adhesive layer and release film layer are combined with each other successively,
Wherein each layer thickness is followed successively by：It is 15 μm of release film layer, 15 μm of adhesive layer, 50 μm of polyvinyl fluoride thin film layer, 15 μm of adhesive layer, release
15 μm of film layer.
Embodiment 3
In mass, gluing layer formula is as follows：
100 parts of SBS resins, 120 parts of terpene resin, 30 parts of chlorinated paraffin, N, N- dibutyl vulcanize Aminobenzoic Acid zinc 0.5
Part.
The release film used is polyethylene terephthalate release film, off-type force 12gf/in.
Three layers of polyvinyl fluoride thin film, adhesive layer and release film be combined with each other successively, wherein polyvinyl fluoride thin film layer
Thickness is 45 μm, the thickness of adhesive layer is 25 μm, the thickness of release film is 25 μm.
Embodiment 4
In mass, gluing layer formula is as follows：
100 parts of SBS resins, 120 parts of terpene resin, 30 parts of chlorinated paraffin, N, N- dibutyl vulcanize Aminobenzoic Acid zinc 0.5
Part.
The release film used is polyethylene terephthalate release film, off-type force 12gf/in.
Five layers of polyvinyl fluoride thin film layer, adhesive layer, polyvinyl fluoride thin film layer, adhesive layer and release film layer are compounded in successively
Together, wherein each layer thickness is followed successively by：25 μm of polyvinyl fluoride thin film layer, 15 μm of adhesive layer, 25 μm of polyvinyl fluoride thin film layer, gluing
Layer 15 μm, 20 μm of release film layer.
Polyvinyl fluoride tape prepared by embodiment 1 to 4 is tested for the property, as a result such as the following table 1.
Table 1, different polyvinyl fluoride tape the performance test results
| Performance indicator | Embodiment 1 | Embodiment 2 | Embodiment 3 | Embodiment 4 |
| PVF and adhesive bonds power (N/cm) | 7.2 | 7.1 | 8.1 | 7.3 |
| With PE cohesive forces (N/cm) | 5.1 | 4.9 | 5.2 | 5.0 |
| Tensile strength (MPa) | 60.3 | 58.3 | 61.5 | 69.2 |
| Moisture-vapor transmission (g/m2, for 24 hours) | 3.2 | 2.6 | 3.9 | 0.8 |
| Ultraviolet ageingaPost-tensioning intensity (MPa) | 48.4 | 46.1 | 49.3 | 52.3 |
| Ultraviolet ageingaCohesive force (N/cm) afterwards | 4.4 | 4.2 | 4.6 | 4.5 |
| Hydrothermal agingbPost-tensioning intensity (MPa) | 42.3 | 40.9 | 42.5 | 45.1 |
| Hydrothermal agingbCohesive force (N/cm) afterwards | 4.1 | 3.9 | 4.3 | 4.2 |
Note：A is ultraviolet accelerated ageing GB/T19394 (2000h) in table 1, and b is 120 DEG C of hydrothermal aging, 100%RH, 96h.
Claims (9)
1. a kind of weather-proof polyvinyl fluoride tape, it is characterised in that：The adhesive tape is by polyvinyl fluoride thin film layer, adhesive layer and release
Film layer is combined,
Or it is combined by release film layer, adhesive layer, polyvinyl fluoride thin film layer, adhesive layer and release film layer；
It is compound by adhesive layer between the polyvinyl fluoride thin film layer and release film layer；
The adhesive layer contains in mass：Styrene-isoprene-styrene block copolymer and/or styrene-fourth two
100 parts of alkene-styrene block copolymer, 30~150 parts of tackifying resin, 10~50 parts of softening agent, 0.5~2 part of anti-aging agent.
2. weather-proof polyvinyl fluoride tape described in accordance with the claim 1, it is characterised in that：The tackifying resin is selected from terpenes tree
At least one of fat and C9 resins.
3. weather-proof polyvinyl fluoride tape described in accordance with the claim 1, it is characterised in that：The softening agent is selected from epoxy soybean
At least one of oil and chlorinated paraffin.
4. weather-proof polyvinyl fluoride tape described in accordance with the claim 1, it is characterised in that：The anti-aging agent is selected from N, bis- fourths of N-
Base vulcanizes at least one of Aminobenzoic Acid zinc and two thio Aminobenzoic Acid zinc of ethylphenyl.
5. weather-proof polyvinyl fluoride tape described in accordance with the claim 1, it is characterised in that：The release film be selected from polyethylene from
At least one of type film, polypropylene release film, polyimides release film and polyethylene terephthalate release film.
6. weather-proof polyvinyl fluoride tape described in accordance with the claim 1, it is characterised in that：The release film, off-type force 1
~60gf/in.
7. weather-proof polyvinyl fluoride tape described in accordance with the claim 1, it is characterised in that：The thickness of the polyvinyl fluoride thin film layer
Degree is 15~60 μm, and the gluing layer thickness is 5~25 μm.
8. weather-proof polyvinyl fluoride tape described in accordance with the claim 1, it is characterised in that：The polyvinyl fluoride thin film, table
Face tension is 40~55dyne/cm.
9. a kind of application of weather-proof polyvinyl fluoride tape, it is characterised in that the adhesive tape is for insulating sheath, air inflation knot
The protection of structure and bridge cable casing.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611244574.9A CN108611007A (en) | 2016-12-29 | 2016-12-29 | A kind of polyvinyl fluoride weather-resistant glue band |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611244574.9A CN108611007A (en) | 2016-12-29 | 2016-12-29 | A kind of polyvinyl fluoride weather-resistant glue band |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN108611007A true CN108611007A (en) | 2018-10-02 |
Family
ID=63658402
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201611244574.9A Pending CN108611007A (en) | 2016-12-29 | 2016-12-29 | A kind of polyvinyl fluoride weather-resistant glue band |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN108611007A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114196341A (en) * | 2020-09-02 | 2022-03-18 | 乔成辉 | Colored polyvinyl fluoride bridge cable protection adhesive tape and manufacturing method thereof |
| CN117126615A (en) * | 2023-07-14 | 2023-11-28 | 广东省公路建设有限公司湾区特大桥养护技术中心 | Fluorocarbon polymer composite wrapping tape and preparation method and application thereof |
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| CN1436203A (en) * | 2000-06-09 | 2003-08-13 | 3M创新有限公司 | Adherable fluorine-contg. sheet and adhering method and adhesion structure using same |
| CN1782009A (en) * | 2004-11-30 | 2006-06-07 | 日东电工株式会社 | Pressure-sensitive adhesive sheet |
| CN101818035A (en) * | 2010-03-25 | 2010-09-01 | 同济大学 | Hot melt adhesive for quick joint coating of metallic pipeline and preparation method thereof |
| JP2011032451A (en) * | 2009-08-05 | 2011-02-17 | Dengiken:Kk | Composite adhesive tape and solar cell module using the same |
| CN102017177A (en) * | 2008-04-24 | 2011-04-13 | 日东电工株式会社 | Adhesive sheet for solar cell panel, solar cell panel using the adhesive sheet, and method for manufacturing a solar cell panel using the adhesive sheet |
| CN102020943A (en) * | 2009-09-18 | 2011-04-20 | 日东电工株式会社 | Insulating tape |
| CN103540281A (en) * | 2013-10-21 | 2014-01-29 | 广东东方树脂有限公司 | Quickly-cured rubber-type hot melt adhesive |
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-
2016
- 2016-12-29 CN CN201611244574.9A patent/CN108611007A/en active Pending
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| CN102017177A (en) * | 2008-04-24 | 2011-04-13 | 日东电工株式会社 | Adhesive sheet for solar cell panel, solar cell panel using the adhesive sheet, and method for manufacturing a solar cell panel using the adhesive sheet |
| JP2011032451A (en) * | 2009-08-05 | 2011-02-17 | Dengiken:Kk | Composite adhesive tape and solar cell module using the same |
| CN102020943A (en) * | 2009-09-18 | 2011-04-20 | 日东电工株式会社 | Insulating tape |
| CN101818035A (en) * | 2010-03-25 | 2010-09-01 | 同济大学 | Hot melt adhesive for quick joint coating of metallic pipeline and preparation method thereof |
| CN103540281A (en) * | 2013-10-21 | 2014-01-29 | 广东东方树脂有限公司 | Quickly-cured rubber-type hot melt adhesive |
| CN105602518A (en) * | 2015-12-31 | 2016-05-25 | 光山县博正树脂有限公司 | Colorless and transparent environment-friendly handbag spray glue and preparation method thereof |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114196341A (en) * | 2020-09-02 | 2022-03-18 | 乔成辉 | Colored polyvinyl fluoride bridge cable protection adhesive tape and manufacturing method thereof |
| CN117126615A (en) * | 2023-07-14 | 2023-11-28 | 广东省公路建设有限公司湾区特大桥养护技术中心 | Fluorocarbon polymer composite wrapping tape and preparation method and application thereof |
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Application publication date: 20181002 |