CN108585069A - Aquaculture purifying water process compound formulation and preparation method thereof - Google Patents
Aquaculture purifying water process compound formulation and preparation method thereof Download PDFInfo
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- CN108585069A CN108585069A CN201810254879.0A CN201810254879A CN108585069A CN 108585069 A CN108585069 A CN 108585069A CN 201810254879 A CN201810254879 A CN 201810254879A CN 108585069 A CN108585069 A CN 108585069A
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/52—Treatment of water, waste water, or sewage by flocculation or precipitation of suspended impurities
- C02F1/54—Treatment of water, waste water, or sewage by flocculation or precipitation of suspended impurities using organic material
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/52—Treatment of water, waste water, or sewage by flocculation or precipitation of suspended impurities
- C02F1/54—Treatment of water, waste water, or sewage by flocculation or precipitation of suspended impurities using organic material
- C02F1/56—Macromolecular compounds
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F2101/00—Nature of the contaminant
- C02F2101/10—Inorganic compounds
- C02F2101/16—Nitrogen compounds, e.g. ammonia
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F2101/00—Nature of the contaminant
- C02F2101/30—Organic compounds
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F2101/00—Nature of the contaminant
- C02F2101/30—Organic compounds
- C02F2101/38—Organic compounds containing nitrogen
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- Hydrology & Water Resources (AREA)
- Engineering & Computer Science (AREA)
- Environmental & Geological Engineering (AREA)
- Water Supply & Treatment (AREA)
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Feed For Specific Animals (AREA)
- Fodder In General (AREA)
Abstract
The present invention relates to a kind of aquaculture purifying water process compound formulations and preparation method thereof, and the compound formulation is formed by the Raw material processing of following parts by weight：80 90 parts of multicomponent organic acid, 5 10 parts of B family vitamin, 38 parts of compound amino acid, 35 parts of oxidized form of glutathione, 13 parts of polylysine, 26 parts of oat beta glucan, 140 160 parts of deionized water；The beneficial effects of the invention are as follows：The compound formulation can look for the toxin such as quaternary ammonium salt and the organophosphor of that enrichment with the poisonous and harmful substances such as fast degradation and the ammonia nitrogen being complexed in water body, efficient catalytic degrading cultivation process, alleviate aquatic livestock emergency reaction, keep water stabilization.The compound formulation of the present invention can quickly be complexed the various noxious materials of water body into innocuous substance and be degraded, while adjust water body Carbon balance, repair the various degradation modes of cultivation water environment.
Description
Technical field
The present invention relates to a kind of aquaculture purifying water process compound formulations and preparation method thereof, belong to aquaculture system
Purification treatment technology field.
Background technology
With the development of aquaculture, inter-industry competition is growing more intense, and scale, the intensivization development of culture fishery have become
For an inexorable trend, there is higher cultural technique, unified management to reduce cost for scale aquaculture, improve through
Ji benefit, but requirement of the large-scale cultivation to water body is extremely important comprising following aspects：
1. batch production, feed coefficient and pond culture put seedling before water quality need to handle, with ammonia nitrogen in fast degradation and complexing water body,
The poisonous and harmful substances such as nitrite, heavy metal.The survival rate of seed is improved, the laundering period is shortened.
2. the quaternary amine being enriched with during large-scale cultivation, heavy metal (such as copper sulphate, potassium permanganate), organophosphor are (as opposed
Hundred worms), pyrethroids class, the toxin after the uses such as antibiotics；It needs timely processing to degrade, avoids toxin persistent accumulation；
3. rainstorm weather, fall suddenly algae, water quality bleach, redden, blackening when, need to be added water scavengine agent alleviate aquatic livestock stress
Reaction keeps water stabilization.
4. being used when the water body " dirty " of large-scale cultivation or " muddiness ", need addition water scavengine agent to enhance the transparency,
Water quality is allowed to become salubrious；It is periodically used in aging pond, to avoid water stratification and substrate fever phenomenon.
Invention content
It is an object of the present invention to solving the deficiencies in the prior art, it is compound to provide a kind of aquaculture purifying water process
Preparation, the compound formulation can be with the poisonous and harmful substances such as fast degradation and the ammonia nitrogen being complexed in water body, efficient catalytic degrading cultivations
Process looks for the toxin such as quaternary ammonium salt and the organophosphor of that enrichment, alleviates aquatic livestock emergency reaction, keeps water stabilization.
The second object of the present invention is to provide a kind of preparation method of aquaculture purifying water process compound formulation.
The technical solution adopted by the present invention to solve the technical problems is：
A kind of aquaculture purifying water process compound formulation, the compound formulation are formed by the Raw material processing of following parts by weight：
80-90 parts of organic acid, 5-10 parts of B family vitamin, 3-8 parts of compound amino acid, 3-5 parts of oxidized form of glutathione gather bad ammonia
It is 1-3 parts sour, oat -2-6 parts of beta glucan, 140-160 parts of deionized water；
The preparation method of the oxidized form of glutathione is as follows：Reduced glutathione is taken, in 40-45 DEG C of dissolving, obtains 50-
The reduced glutathione solution of 100g/L, it is A1 to survey its pH value；With barium hydroxide tune pH to 7.0-7.2；It is added a certain amount of double
Oxygen water, it is stirring while adding, continue to be stirred to react 0.2-0.5h after adding；After reaction, a certain amount of manganese dioxide is added, stirs
Then 5-10min fully filters off manganese dioxide；With sulphur acid for adjusting pH to A3, A1-0.1≤A3≤A1；It is heavy fully to filter off barium sulfate
It forms sediment, spray drying obtains oxidized form of glutathione.
Preferably, the compound formulation is formed by the Raw material processing of following parts by weight：
85 parts of organic acid, 8 parts of B family vitamin, 5 parts of compound amino acid, 4 parts of oxidized form of glutathione, 2 parts of polylysine, oat-
4 parts of beta glucan, 150 parts of deionized water；
The preparation method of the oxidized form of glutathione is as follows：Reduced glutathione is taken, in 40-45 DEG C of dissolving, obtains 80g/L
Reduced glutathione solution, survey its pH value be A1；With barium hydroxide tune pH to 7.1；A certain amount of hydrogen peroxide, side edged is added
Stirring, continues to be stirred to react 25min after adding；After reaction, a certain amount of manganese dioxide is added, stirs 6min, then fully
Filter off manganese dioxide；With sulphur acid for adjusting pH to A3=A1-0.05；Barium sulfate precipitate is fully filtered off, spray drying obtains oxidized form
Glutathione.Oxidized form of glutathione acts synergistically with reduced glutathione complementation intrinsic in histocyte, realizes efficient
Anti-oxidation function, aquatic animal tissue cell health, activity is high, efficient to the removing toxic substances of poisonous and harmful substance；
Preferably, any one or the combination of several of them object in malic acid, citric acid and tartaric acid.
Preferably, the compound amino acid is glycine, alanine, leucine, isoleucine, valine, cystine, half
Cystine, methionine, threonine, serine, phenylalanine, tyrosine, tryptophan, proline, hydroxyproline, glutamic acid and
The combination at least 5 in asparatate.
Preferably, a concentration of the 30% of hydrogen peroxide, additive amount are 0.3-0.5ml/g reduced glutathiones.
Preferably, filtering twice is all made of the miillpore filter essence filtering of 0.2-0.45 μm of precision.
The preparation method of aquaculture purifying water process compound formulation, steps are as follows for the preparation method：
S1:20-30 parts of B family vitamin of formula ratio, compound amino acid, polylysine and deionized water deionizations are mixed, are filled
Divide stirring 1-2h；
S2:The oxidized form of glutathione of formula ratio, oat-beta glucan are added in step S1,0.5-1h is futher stirred；
S3：The organic acid of formula ratio is added in S2, the deionized water of surplus is added, stirs 30-40min, filters off impurity, is obtained
Compound formulation finished product.
The beneficial effects of the invention are as follows：The compound formulation can be poisonous and harmful with fast degradation and the ammonia nitrogen being complexed in water body etc.
Substance, efficient catalytic degrading cultivation process look for the toxin such as quaternary ammonium salt and the organophosphor of that enrichment, and it is emergent anti-to alleviate aquatic livestock
It answers, keeps water stabilization.
The compound formulation of the present invention can quickly be complexed the various noxious materials of water body into innocuous substance and be degraded, and adjust simultaneously
Water-saving body Carbon balance repairs the various degradation modes of cultivation water environment.
Specific implementation mode
Below by specific embodiment, technical scheme of the present invention will be further explained in detail.
Embodiment 1：
A kind of aquaculture purifying water process compound formulation, the compound formulation are formed by the Raw material processing of following parts by weight：
80 parts of organic acid, 5 parts of B family vitamin, 3 parts of compound amino acid, 3 parts of oxidized form of glutathione, 1 part of polylysine, oat-
2 parts of beta glucan, 140 parts of deionized water；
The preparation method of the oxidized form of glutathione is as follows：Reduced glutathione is taken, in 40 DEG C of dissolvings, obtains 50g/L's
Reduced glutathione solution, it is A1 to survey its pH value；With barium hydroxide tune pH to 7.0；A certain amount of hydrogen peroxide is added, side edged stirs
It mixes, continues to be stirred to react 0.2-h after adding；After reaction, a certain amount of manganese dioxide is added, stirs 5-min, then fully filter
Remove manganese dioxide；With sulphur acid for adjusting pH to A3=A1；Barium sulfate precipitate is fully filtered off, spray drying obtains oxidized form gluathione
Peptide.
The organic acid is selected from malic acid；The compound amino acid is glycine, alanine, leucine, isoleucine, figured silk fabrics
The equal proportion combination of propylhomoserin, cystine, a concentration of the 30% of hydrogen peroxide, additive amount is 0.3ml/g reduced glutathiones, twice
Filtering is all made of the miillpore filter essence filtering of 0.2-0.45 μm of precision.
The preparation method of aquaculture purifying water process compound formulation is as follows：
S1:20 parts of B family vitamin of formula ratio, compound amino acid, polylysine and deionized water deionizations are mixed, fully
Stir 2h；
S2:The oxidized form of glutathione of formula ratio, oat-beta glucan are added in step S1,0.5h is futher stirred；
S3：The organic acid of formula ratio is added in S2, the deionized water of surplus is added, stirs 30min, impurity is filtered off, is answered
Close finished dosage form.
Embodiment 2：
A kind of aquaculture purifying water process compound formulation, the compound formulation are formed by the Raw material processing of following parts by weight：
90 parts of organic acid, 10 parts of B family vitamin, 8 parts of compound amino acid, 5 parts of oxidized form of glutathione, 3 parts of polylysine, swallow
6 parts of wheat-beta glucan, 160 parts of deionized water；
The preparation method of the oxidized form of glutathione is as follows：Reduced glutathione is taken, in 45 DEG C of dissolvings, obtains 100g/L's
Reduced glutathione solution, it is A1 to survey its pH value；With barium hydroxide tune pH to 7.2；A certain amount of hydrogen peroxide is added, side edged stirs
It mixes, continues to be stirred to react 0.5h after adding；After reaction, a certain amount of manganese dioxide is added, stirs 10min, then fully filter
Remove manganese dioxide；With sulphur acid for adjusting pH to A3=A1-0.1；Barium sulfate precipitate is fully filtered off, spray drying obtains oxidized form paddy Guang
Sweet peptide.
The organic acid is selected from tartaric acid；The compound amino acid be glycine, alanine, cysteine, methionine,
The equal proportion combination of threonine, serine, phenylalanine, a concentration of the 30% of hydrogen peroxide, additive amount is 0.5ml/g reduced form paddy
The sweet peptide of Guang, twice filtering are all made of the miillpore filter essence filtering of 0.2-0.45 μm of precision.
The preparation method of aquaculture purifying water process compound formulation, steps are as follows for the preparation method：
S1:30 parts of B family vitamin of formula ratio, compound amino acid, polylysine and deionized water deionizations are mixed, fully
Stir 2h；
S2:The oxidized form of glutathione of formula ratio, oat-beta glucan are added in step S1,1h is futher stirred；
S3：The organic acid of formula ratio is added in S2, the deionized water of surplus is added, stirs 40min, impurity is filtered off, is answered
Close finished dosage form.
Embodiment 3：
A kind of aquaculture purifying water process compound formulation, the compound formulation are formed by the Raw material processing of following parts by weight：Have
85 parts of machine acid, 8 parts of B family vitamin, 5 parts of compound amino acid, 4 parts of oxidized form of glutathione, 2 parts of polylysine, oat-β-Portugal are poly-
4 parts of sugar, 150 parts of deionized water；
The preparation method of the oxidized form of glutathione is as follows：Reduced glutathione is taken, in 40-45 DEG C of dissolving, obtains 80g/L
Reduced glutathione solution, survey its pH value be A1；With barium hydroxide tune pH to 7.1；A certain amount of hydrogen peroxide, side edged is added
Stirring, continues to be stirred to react 25min after adding；After reaction, a certain amount of manganese dioxide is added, stirs 6min, then fully
Filter off manganese dioxide；With sulphur acid for adjusting pH to A3=A1-0.05；Barium sulfate precipitate is fully filtered off, spray drying obtains oxidized form
Glutathione.
The organic acid is selected from the equal proportion mixture of citric acid and tartaric acid；The compound amino acid is glycine, third
Propylhomoserin, leucine, isoleucine, valine, cystine, cysteine, methionine, threonine, serine, phenylalanine,
The equal proportion combination of tyrosine, tryptophan, proline, hydroxyproline, glutamic acid and asparatate, hydrogen peroxide it is a concentration of
30%, additive amount is 0.4ml/g reduced glutathiones, and filtering twice is all made of the miillpore filter essence mistake of 0.2-0.45 μm of precision
Filter.
The preparation method of aquaculture purifying water process compound formulation is as follows：
S1:25 parts of B family vitamin of formula ratio, compound amino acid, polylysine and deionized water deionizations are mixed, fully
Stir 1.5h；
S2:The oxidized form of glutathione of formula ratio, oat-beta glucan are added in step S1,0.5h is futher stirred；
S3：The organic acid of formula ratio is added in S2, the deionized water of surplus is added, stirs 35min, impurity is filtered off, is answered
Close finished dosage form.
The compound formulation of the present invention is suitable for the aquatic products such as river crab, white shrimp, Macrobrachium rosenbergii, sea cucumber, jellyfish, various fish and supports
Grow animal.
1. for the water treatment before putting seedling of batch production, feed coefficient and pond culture, ammonia in fast degradation and complexing water body
The poisonous and harmful substances such as nitrogen, nitrite, heavy metal.
2. as quaternary amine, heavy metal (such as copper sulphate, potassium permanganate), organophosphor (such as metrifonate), pyrethroids class, antibiotic
Toxin degradation after the uses such as class.
3. rich water product, biological agent and oxygenation agent is coordinated to use, notable synergistic can be played.
4. rainstorm weather, fall suddenly algae, water quality bleach, redden, blackening when use, stress response of aquatic animals can be alleviated,
Keep water stabilization.
5. being used when water body " dirty " or " muddiness ", it can enhance the transparency, water quality becomes salubrious；Periodically make in aging pond
With being avoided that water stratification and substrate fever phenomenon.
6. adjusting excessively high pH value, stabilizing water quality acid-base value reduces the turbidity of aging water body, keeps water quality salubrious.
The compound formulation usage and dosage of the present invention：Full pond is uniformly splashed after being diluted with water.
Seedling rearing room, industrial aquaculture：1m3Water body this product 3-5ml, i.e. 3-5ppm.
Above-mentioned embodiment is only a preferred solution of the present invention, not the present invention is made in any form
Limitation, on the premise of not exceeding the technical scheme recorded in the claims also other variations and modifications.
Claims (7)
1. a kind of aquaculture purifying water process compound formulation, it is characterised in that：The compound formulation by following parts by weight original
Material is process：
80-90 parts of organic acid, 5-10 parts of B family vitamin, 3-8 parts of compound amino acid, 3-5 parts of oxidized form of glutathione gather bad ammonia
It is 1-3 parts sour, oat -2-6 parts of beta glucan, 140-160 parts of deionized water；
The preparation method of the oxidized form of glutathione is as follows：Reduced glutathione is taken, in 40-45 DEG C of dissolving, obtains 50-
The reduced glutathione solution of 100g/L, it is A1 to survey its pH value；With barium hydroxide tune pH to 7.0-7.2；It is added a certain amount of double
Oxygen water, it is stirring while adding, continue to be stirred to react 0.2-0.5h after adding；After reaction, a certain amount of manganese dioxide is added, stirs
Then 5-10min fully filters off manganese dioxide；With sulphur acid for adjusting pH to A3, A1-0.1≤A3≤A1；It is heavy fully to filter off barium sulfate
It forms sediment, spray drying obtains oxidized form of glutathione.
2. aquaculture purifying water process compound formulation according to claim 1, it is characterised in that：The compound formulation by
The Raw material processing of following parts by weight forms：
85 parts of organic acid, 8 parts of B family vitamin, 5 parts of compound amino acid, 4 parts of oxidized form of glutathione, 2 parts of polylysine, oat-
4 parts of beta glucan, 150 parts of deionized water；
The preparation method of the oxidized form of glutathione is as follows：Reduced glutathione is taken, in 40-45 DEG C of dissolving, obtains 80g/L
Reduced glutathione solution, survey its pH value be A1；With barium hydroxide tune pH to 7.1；A certain amount of hydrogen peroxide, side edged is added
Stirring, continues to be stirred to react 25min after adding；After reaction, a certain amount of manganese dioxide is added, stirs 6min, then fully
Filter off manganese dioxide；With sulphur acid for adjusting pH to A3=A1-0.05；Barium sulfate precipitate is fully filtered off, spray drying obtains oxidized form
Glutathione.
3. aquaculture purifying water process compound formulation according to claim 1 or 2, it is characterised in that：The organic acid
Any one or the combination of several of them object in malic acid, citric acid and tartaric acid.
4. aquaculture purifying water process compound formulation according to claim 1 or 2, it is characterised in that：The compound ammonia
Base acid is glycine, alanine, leucine, isoleucine, valine, cystine, cysteine, methionine, threonine, silk
The group at least 5 in propylhomoserin, phenylalanine, tyrosine, tryptophan, proline, hydroxyproline, glutamic acid and asparatate
It closes.
5. aquaculture purifying water process compound formulation according to claim 1 or 2, it is characterised in that：Hydrogen peroxide it is dense
Degree is 30%, and additive amount is 0.3-0.5ml/g reduced glutathiones.
6. aquaculture purifying water process compound formulation according to claim 1 or 2, it is characterised in that：Filtering is equal twice
Using 0.2-0.45 μm of miillpore filter essence filtering of precision.
7. the preparation method of aquaculture purifying water process compound formulation described in claim 1-6 any one, which is characterized in that
Steps are as follows for the preparation method：
S1:20-30 parts of B family vitamin of formula ratio, compound amino acid, polylysine and deionized water deionizations are mixed, are filled
Divide stirring 1-2h；
S2:The oxidized form of glutathione of formula ratio, oat-beta glucan are added in step S1,0.5-1h is futher stirred；
S3：The organic acid of formula ratio is added in S2, the deionized water of surplus is added, stirs 30-40min, filters off impurity, is obtained
Compound formulation finished product.
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| CN201810254879.0A CN108585069A (en) | 2018-03-27 | 2018-03-27 | Aquaculture purifying water process compound formulation and preparation method thereof |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109607640A (en) * | 2019-01-21 | 2019-04-12 | 湖北紫荆生物技术有限公司 | A kind of water body removing toxic substances, water transfer, steady water reclamation agent and its preparation and application |
| CN110980907A (en) * | 2019-12-12 | 2020-04-10 | 湖南中车环境工程有限公司 | High-efficiency coagulant special for strong-acid antimony-containing wastewater |
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| CN105523594A (en) * | 2016-01-15 | 2016-04-27 | 绵阳金欧生物科技有限公司 | Wastewater treatment agent for aquaculture |
| CN106830358A (en) * | 2017-02-21 | 2017-06-13 | 佛山市碧沃丰生物科技股份有限公司 | A kind of sewage disposal biological growth promoter and preparation method thereof, applying method |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101898830A (en) * | 2010-05-05 | 2010-12-01 | 麦广鸿 | Complex enzyme preparation for sewage treatment and application method thereof |
| CN105523594A (en) * | 2016-01-15 | 2016-04-27 | 绵阳金欧生物科技有限公司 | Wastewater treatment agent for aquaculture |
| CN106830358A (en) * | 2017-02-21 | 2017-06-13 | 佛山市碧沃丰生物科技股份有限公司 | A kind of sewage disposal biological growth promoter and preparation method thereof, applying method |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN109607640A (en) * | 2019-01-21 | 2019-04-12 | 湖北紫荆生物技术有限公司 | A kind of water body removing toxic substances, water transfer, steady water reclamation agent and its preparation and application |
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