CN108579587A - A kind of high-efficiency stirring method and device of no volume gas nickel-graphite semi solid slurry - Google Patents

A kind of high-efficiency stirring method and device of no volume gas nickel-graphite semi solid slurry Download PDF

Info

Publication number
CN108579587A
CN108579587A CN201810010417.4A CN201810010417A CN108579587A CN 108579587 A CN108579587 A CN 108579587A CN 201810010417 A CN201810010417 A CN 201810010417A CN 108579587 A CN108579587 A CN 108579587A
Authority
CN
China
Prior art keywords
graphite
nickel
volume
solid slurry
semi solid
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Withdrawn
Application number
CN201810010417.4A
Other languages
Chinese (zh)
Inventor
杜云慧
张伟
张伟一
张鹏
王玉洁
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Beijing Jiaotong University
Original Assignee
Beijing Jiaotong University
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Beijing Jiaotong University filed Critical Beijing Jiaotong University
Priority to CN201810010417.4A priority Critical patent/CN108579587A/en
Publication of CN108579587A publication Critical patent/CN108579587A/en
Withdrawn legal-status Critical Current

Links

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F33/00Other mixers; Mixing plants; Combinations of mixers
    • B01F33/45Magnetic mixers; Mixers with magnetically driven stirrers
    • B01F33/451Magnetic mixers; Mixers with magnetically driven stirrers wherein the mixture is directly exposed to an electromagnetic field without use of a stirrer, e.g. for material comprising ferromagnetic particles or for molten metal
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22CALLOYS
    • C22C1/00Making non-ferrous alloys
    • C22C1/10Alloys containing non-metals
    • C22C1/1036Alloys containing non-metals starting from a melt
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22CALLOYS
    • C22C19/00Alloys based on nickel or cobalt
    • C22C19/03Alloys based on nickel or cobalt based on nickel
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F27FURNACES; KILNS; OVENS; RETORTS
    • F27DDETAILS OR ACCESSORIES OF FURNACES, KILNS, OVENS, OR RETORTS, IN SO FAR AS THEY ARE OF KINDS OCCURRING IN MORE THAN ONE KIND OF FURNACE
    • F27D27/00Stirring devices for molten material
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F2101/00Mixing characterised by the nature of the mixed materials or by the application field
    • B01F2101/26Mixing ingredients for casting metals

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Mechanical Engineering (AREA)
  • Materials Engineering (AREA)
  • Metallurgy (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Engineering & Computer Science (AREA)
  • Manufacture And Refinement Of Metals (AREA)

Abstract

The invention discloses a kind of high-efficiency stirring method and devices of no volume gas nickel graphite semi-solid slurry, belong to the materials working research field such as metallurgical, casting, the present invention, which using inner wall is furnished with the variable volume graphite crucible of prismatic blade and stirs with high speed electromagnetic, to be combined mode and be stirred to nickel graphite semi-solid slurry;It is stirred using high speed electromagnetic, in the case where no volume gas fetters, nickel graphite semi-solid slurry is set to generate circumferential high-speed stirred movement, utilize the prismatic blade on graphite crucible inner wall, internal nickel graphite semi-solid slurry is constantly moved on into surrounding, the nickel graphite semi-solid slurry on top is moved on into lower part, and then the floating of graphite particle and central segregation is prevented to move, the equally distributed nickel graphite semi-solid slurry of graphite particle to efficiently obtain no volume gas, mixing time can shorten to 2 minutes, solve the problems, such as volume gas and stirring efficiency low technical present in the stirring of nickel graphite semi-solid slurry.

Description

A kind of high-efficiency stirring method and device of no volume gas nickel-graphite semi solid slurry
Technical field
The invention belongs to the materials working research fields such as metallurgical, casting, more particularly to a kind of no volume gas nickel-graphite semisolids The high-efficiency stirring method and device of slurry.
Background technology
In the materials working research fields such as metallurgical, casting, it is often necessary to be stirred to various melts, such as metal half Solid size, the stirring etc. for adding particle melt, it is therefore an objective to make the homogenization such as temperature, ingredient, the tissue of melt.Stirring efficiency Stirring intensity is generally depended on, stirring intensity is bigger, and the shearing of formation and turbulent flow are stronger, and melt realizes temperature, ingredient, tissue etc. The mixing time of homogenization is shorter, and stirring efficiency is higher.However, strong stirring can lead to the volume gas problem of melt, easily High-temperature fusant oxidation, formation is caused to be mingled with tissue etc., even with protective atmosphere, volume gas can also make to spread stomata in melt, Material property is caused to deteriorate, it is seen then that volume gas problem has fettered the stirring intensity of melt, reduces stirring efficiency.Nickel-graphite is compound Material contains the zirconium of 3wt% or so and the graphite particle of 3wt% or so, and the extension ability for having Ni substrate concurrently is strong, plasticity is good, corrosion resistant Erosion and the greasy property of graphite particle the advantages that well especially high temperature lubrication property is good, arc ablation resistance ability is strong, be to prepare height The ideal material of warm friction parts, electric contact part, machine components.Due to 3652 DEG C of fusing points 1453 for being higher than nickel of fusing point of graphite DEG C, thus graphite be in nickel liquid in the form of solid granulates existing for, in addition, due to 8.5~8.9g/cm of density of nickel3 More than 1.9~2.2g/cm of density of graphite3, so, during the routine casting of nickel-graphite melt, graphite particle is easy hair It is raw to float.If semi solid slurry is made in nickel-graphite melt, the high viscosity of semi solid slurry and nascent solid phase particles have Effect prevents graphite particle from floating, and still, the high viscosity of semi solid slurry and nascent solid phase particles equally can also hinder graphite particle Dispersion therefore the equally distributed nickel-graphite semi solid slurry of graphite particle and then obtain high-performance to expeditiously prepare Nickel-graphite composite material, must just increase the stirring intensity to semi solid slurry, such volume gas problem just more highlights. The patents of invention such as Authorization Notice No. CN105436436B, Authorization Notice No. CN 103307900B are by " narrowing molten in stir chamber The methods of body fluid face ", " setting melt disturbance isolator " transmit obstructing agitation to melt liquid level, avoid melt volume gas.This hair The bright angle completely cut off completely from melt and gas, carries out the creativity and innovation in terms of semi solid slurry stirring, has broken away from volume gas Constraint to stirring intensity and stirring efficiency can expeditiously prepare the equally distributed nickel-graphite of graphite particle half of no volume gas Solid size.
Invention content
The technical problem to be solved by the present invention is to volume gas present in the stirring of nickel-graphite semi solid slurry and stirring are imitated The low problem of rate provides a kind of high-efficiency stirring method and device of no volume gas nickel-graphite semi solid slurry.
The technical solution adopted by the present invention to solve the technical problems is:
The variable volume graphite crucible that prismatic blade is furnished with using inner wall is combined mode to nickel-graphite half with high speed electromagnetic stirring Solid size is stirred;It is emptied partly solid in graphite crucible using variable volume graphite crucible by reducing the volume of graphite crucible The all gas on state slurry top, and under conditions of semi solid slurry and ambient atmos completely cut off completely, i.e., no gas source Under conditions of, the stirring of semi solid slurry is carried out, and then avoid semi solid slurry volume gas from the root cause;It is stirred using high speed electromagnetic It mixes, in the case where no volume gas fetters, so that nickel-graphite semi solid slurry is generated circumferential high-speed stirred movement, utilize graphite crucible Prismatic blade on inner wall, constantly by internal nickel-graphite semi solid slurry move on to around, by the nickel-graphite semisolid on top Slurry moves on to lower part, and then the floating of graphite particle and central segregation is prevented to move, to efficiently obtain the stone of no volume gas The black equally distributed nickel-graphite semi solid slurry of particle.
The beneficial effects of the invention are as follows:Using the present invention, nickel-graphite semi solid slurry is stirred, can directly be made For the nickel-graphite semi solid slurry for going out no volume gas, graphite particle is evenly distributed, mixing time can shorten to 2 minutes, stirring efficiency It improves 310% within 20 seconds 8 minutes than CN102181703A patent disclosure, solves and deposited in the stirring of nickel-graphite semi solid slurry Volume gas and stirring efficiency low technical problem.
Description of the drawings
Fig. 1 is the front view that the method for the present invention stirs nickel-graphite production device for semisolid slurry.
In figure, graphite crucible 2, prismatic blade 3, heating tube 4, cooling tube 5, nickel-graphite semi solid slurry 6, blocking 7, outer cover 8, chassis 9, volume adjustment head 10, thermocouple 11, conical gas vent 12, blocking 13, trip bolt 14, spring 15, bearing shell 16, Thrust bearing 17, motor 18, transmission mechanism 19, guide plate 20 connect slide plate 21, buffer spring 22, connecting screw 23, guide groove 24, rack 25, motor 26, transmission mechanism 27, holder 28.
Fig. 2 is the A-A views that the method for the present invention stirs nickel-graphite production device for semisolid slurry.
In figure, electromagnetic pole pair 1.
Fig. 3 is the B-B views that the method for the present invention stirs nickel-graphite production device for semisolid slurry.
Fig. 4 is the C-C views that the method for the present invention stirs nickel-graphite production device for semisolid slurry.
Fig. 5 is the D-D partial views that the method for the present invention stirs nickel-graphite production device for semisolid slurry.
Fig. 6 is the E-E partial views that the method for the present invention stirs nickel-graphite production device for semisolid slurry.
Fig. 7 is the water quenching microstructure of the nickel-graphite semi solid slurry of the method for the present invention stirring.
Specific implementation mode
The method of the present invention stirring nickel-graphite production device for semisolid slurry is described as follows in conjunction with attached drawing:
As Figure 1-Figure 4, the Efficient Agitator of no volume gas nickel-graphite semi solid slurry is mainly stirred by high speed electromagnetic Device, graphite crucible 2 and its volume adjustment device are constituted with device, thermocouple 11, blocking 7 and chassis 9 is moved up and down.
As shown in Figure 1, Figure 2, Figure 4 shows, three pairs of electromagnetic poles pair 1 of high speed electromagnetic agitating device are distributed on around graphite crucible 2, The distance between 2 outer wall of graphite crucible is 5mm, 1 outside of electromagnetic pole pair plus outer cover 8.
As shown in Figure 1, Figure 2, Figure 3 shows, graphite crucible 2 is fixed on using mechanical connection manner on chassis 9, graphite crucible 2 Heating tube 4 and cooling tube 5 uniformly at intervals in wall are connect with external power supply with cooling liquid supply system respectively;In graphite crucible 2 Upper inside wall is machined with internal thread, cooperates with the external screw thread of 10 lower end of volume adjustment head;Graphite crucible 2 internal thread with Under inner wall on prismatic blade 3 is distributed with, connect with the inner wall of graphite crucible 2 using mechanical connection manner.Prismatic blade 3 is in graphite earthenware It is distributed in horizontal layer on 2 different height of crucible, the interval a of the lower edge of undermost prismatic blade 3 and the inner bottom surface of graphite crucible 2 For 0~20mm, the interval b between adjacent prismatic blade layer is 0~20mm makes the upper of the prismatic blade 3 of top layer by adjusting a and b The lowermost interval c at edge and 2 internal thread of graphite crucible is maintained at 0~10mm, the upper surface of nickel-graphite semi solid slurry 6 The lowermost distance d for being higher by 2 internal thread of graphite crucible upwards is 5~10mm.In same prismatic blade layer, three prismatic blades 3 Root position be distributed on the inner wall of graphite crucible 2 i.e. interval α angle be 120 °, the length e of prismatic blade 3 is graphite crucible 2 Radius, width is the one third of the radius of graphite crucible 2.On the length direction of each prismatic blade 3, prismatic blade 3 Head tilts on the basis of being directed toward 2 horizontal circle center of graphite crucible against the flow direction of nickel-graphite semi solid slurry 6, The angle β of prismatic blade 3 and the 2 horizontal circumference line of centres of its root and graphite crucible is 20 °, so as to constantly by internal nickel- Around graphite semi-solid slurry 6 moves on to;In the width direction of each prismatic blade 3, the upper blade of prismatic blade 3 descends blade inverse relatively The flow direction for nickel-graphite semi solid slurry 6 tilts, and the width direction of prismatic blade 3 and the angle γ of horizontal plane are 45 °, with Just the nickel-graphite semi solid slurry 6 on top is constantly moved on into lower part.The root position of prismatic blade 3 in adjacent prismatic blade layer The interval angles δ on same level perspective plane are 60 °.
As shown in Figure 1, Figure 4, Figure 5, the volume adjustment device of graphite crucible 2 is by volume adjustment head 10, blocking 13, fastening spiral shell Nail 14, spring 15 and driving device are constituted, and are adjusted for realizing the volume of graphite crucible 2.Volume adjusts head 10, and material is stone Ink, upper part are round bar, and lower part is disk, are machined with external screw thread in disk side, the internal thread with 2 upper inside wall of graphite crucible It cooperates;Infundibulate gas vent 12 is equipped on disk.The rectangular tablet lower left quarter of blocking 13 is carried adjusts head 10 with volume Disk uniform thickness round platform, rectangular tablet right part is equipped with circular hole, and blocking 13 is limited in leakage by right part circular hole by trip bolt 14 In bucket shape gas vent 12, there is the gap of 1mm between the round platform and infundibulate gas vent 12 of blocking 13;Spring 15 is sleeved on trip bolt On 14 screw rod, effect is to jack up blocking 13, when screw-in makes 2 volume of graphite crucible reduce to volume adjustment head 10 downwards, just In the air discharge in graphite crucible 2;Rotate clockwise the rectangular handle at 14 top of trip bolt, the disk below handle The rectangular flat-plate compressed of blocking 13 is attached to the upper surface that volume adjusts 10 lower disk of head, infundibulate gas vent 12 is made to seal.It drives Dynamic device is made of motor 18, transmission mechanism 19 and detent mechanism, for driving volume adjustment head 10 to screw in downwards and rotation upwards Go out graphite crucible 2, is the key device for realizing the adjustment of 2 volume of graphite crucible;Transmission mechanism 19 is by turbine and worm screw, gear and tooth Wheel transmission is constituted;Detent mechanism is located at the round bar top of volume adjustment head 10, and located lateral is carried out by upper and lower two bearing shells 16, by Upper and lower two thrust bearings 17 carry out longitudinal register;Motor 18, transmission mechanism 19 and the detent mechanism of driving device are respectively adopted Mechanical connection manner is fixed on guide plate 20, carries out moving down in the guide groove 24 that guide plate 20 can be on being fixed on holder 28 It is dynamic.
As shown in Fig. 1, Fig. 6, move up and down device by motor 26, transmission mechanism 27, connection slide plate 21, buffer spring 22, Connecting screw 23 is constituted.Transmission mechanism 27 is made of rack 25 and gear, turbine and worm-drive, the lower end of rack 25 and connection Slide plate 21 is connected using mechanical connection manner.In the guide groove 24 that connection slide plate 21 can be on being fixed on holder 28 move down It is dynamic, and connect with guide plate 20 by buffer spring 22 and connecting screw 23, make volume adjustment head 10 and its driving device or more It is mobile.In bearer connection screw rod 23, guide plate 20, volume adjustment head 10 and its driving device, thermocouple 11, blocking 13, fastening After the related components such as screw 14, spring 15, the decrement of buffer spring 22 is also greater than the maximum of 2 internal thread of graphite crucible Screw-in depth.Move up and down the motor 26 of device, transmission mechanism 27 is fixed on using mechanical connection manner on holder 28.
As Figure 1 and Figure 4, thermocouple 11 is fixed on volume adjustment head 10, lower end and nickel-graphite semi solid slurry 6 contact of material, stretches into 4mm in nickel-graphite semi solid slurry 6, blocks 7 bottoms for being located at graphite crucible 2.
A kind of high-efficiency stirring method of no volume gas nickel-graphite semi solid slurry, the change of prismatic blade is furnished with using above-mentioned inner wall Volume graphite crucible is combined mode with high speed electromagnetic stirring and is stirred to nickel-graphite semi solid slurry;Utilize variable volume stone Black crucible empties all gas on semi solid slurry top in graphite crucible, and half by reducing the volume of graphite crucible Solid size under conditions of that is, no gas source, carries out the stirring of semi solid slurry under conditions of ambient atmos completely isolation, And then semi solid slurry volume gas is avoided from the root cause;It is stirred using high speed electromagnetic, in the case where no volume gas fetters, makes nickel-stone Black semi solid slurry generates circumferential high-speed stirred movement, using the prismatic blade on graphite crucible inner wall, constantly by internal nickel- Graphite semi-solid slurry moves on to surrounding, the nickel-graphite semi solid slurry on top is moved on to lower part, and then prevents the upper of graphite particle Floating and central segregation moves, the equally distributed nickel-graphite semi solid slurry of graphite particle to efficiently obtain no volume gas. Include the following steps:
Step 1, nickel-graphite melt is prepared, temperature is controlled at 1500 DEG C;
Step 2, above-mentioned nickel-graphite melt to be poured into graphite crucible 2, the preheating temperature of graphite crucible 2 is 1300 DEG C, by Heating tube 4 in its wall realizes preheating;
Step 3, start and move up and down device, the external screw thread of 10 lower end of volume adjustment head is dropped into edge on graphite crucible 2 Internal thread at, closing move up and down device;Volume, is adjusted the external screw thread of head 10 by the driving device for starting volume adjustment head 10 It screws in the internal thread of graphite crucible 2, when nickel-graphite melt starts along between the round platform and infundibulate gas vent 12 of blocking 13 Gap, when being overflowed from the lower part of the rectangular tablet of blocking 13, close the driving device of volume adjustment head 10;It tightens clockwise tight Gu screw 14 seals infundibulate gas vent 12, melt is made to completely cut off completely with ambient atmos;
Step 4, thermocouple 11 is connected, using thermocouple 11 to external power supply and cooling liquid supply system input information, is adjusted Heating tube 4 and cooling tube 5 are saved, the temperature of nickel-graphite melt is made to stablize a certain temperature in 1320~1358 DEG C of solid-liquid two-phase region Degree starts high speed electromagnetic agitating device, carries out Isothermal stirring to nickel-graphite melt, stablizes stirring 2 minutes;
Step 5, closing high-speed electromagnetic mixing apparatus unscrews trip bolt 14 counterclockwise, makes blocking 13 in the work of spring 15 It is bounced under, nickel-graphite semi solid slurry 6 can be released by opening blocking 7, for using.
Fig. 7 is the water quenching microstructure of the nickel-graphite semi solid slurry of the method for the present invention stirring, and light areas is nickel in figure Matrix, wherein spherical in shape or elliposoidal part is nascent nickel solid phase particles, darker regions are graphite particle, it is seen then that Ni substrate Upper no stomata, graphite particle are evenly distributed in Ni substrate.
Embodiment one, the power of high speed electromagnetic agitating device is 20kW, rotating speed is 900 revs/min, nickel-graphite melt Whipping temp be 1320 DEG C, under conditions of a 0mm, b 0mm, c 0mm, d are 5mm, after stablizing stirring 2 minutes, can be obtained The nickel-graphite semi solid slurry 6 that no volume gas, graphite particle are evenly distributed, solid rate is 25%.
Embodiment two, the power of high speed electromagnetic agitating device is 20kW, rotating speed is 1200 revs/min, nickel-graphite melt Whipping temp be 1358 DEG C, under conditions of a 20mm, b 20mm, c 10mm, d are 10mm, can after stablizing stirring 2 minutes Obtain no volume gas, the nickel-graphite semi solid slurry 6 that graphite particle is evenly distributed, solid rate is 15%.
As it can be seen that under the premise of the contact being emptied using variable volume graphite crucible and completely cutting off gas with semi solid slurry, in turn Under high-power, high speed electromagnetic stirring condition, the method for the present invention can expeditiously prepare no volume gas, graphite particle is evenly distributed Nickel-graphite semi solid slurry.

Claims (4)

1. a kind of high-efficiency stirring method of no volume gas nickel-graphite semi solid slurry, which is characterized in that be furnished with prismatic blade using inner wall Variable volume graphite crucible be combined mode with high speed electromagnetic stirring nickel-graphite semi solid slurry be stirred;Utilize variant Product graphite crucible empties all gas on semi solid slurry top in graphite crucible by the volume of reduction graphite crucible, and Under conditions of semi solid slurry and ambient atmos completely cut off completely, i.e., under conditions of no gas source, carry out semi solid slurry Stirring, and then semi solid slurry volume gas is avoided from the root cause;It is stirred using high speed electromagnetic, in the case where no volume gas fetters, is made Nickel-graphite semi solid slurry generates circumferential high-speed stirred movement, constantly will be internal using the prismatic blade on graphite crucible inner wall Nickel-graphite semi solid slurry move on to around, the nickel-graphite semi solid slurry on top moves on to lower part, and then prevent graphite The floating of grain and central segregation move, and the equally distributed nickel-graphite of graphite particle to efficiently obtain no volume gas half is solid State slurry, includes the following steps:
Step 1, nickel-graphite melt is prepared, temperature is controlled at 1500 DEG C;
Step 2, above-mentioned nickel-graphite melt is poured into graphite crucible, the preheating temperature of graphite crucible is 1300 DEG C, by its wall Heating tube realize preheating;
Step 3, start and move up and down device, the external screw thread of volume adjustment head lower end is dropped to the internal thread on edge on graphite crucible Place, closing move up and down device;Volume adjustment head is screwed into graphite crucible by the driving device for starting volume adjustment head Internal thread in, when nickel-graphite melt start along between the round platform and infundibulate gas vent of blocking gap, from the length of blocking When the lower part of square tablet is overflowed, the driving device of volume adjustment head is closed;Trip bolt is tightened clockwise, by infundibulate gas vent It seals, melt is made to completely cut off completely with ambient atmos;
Step 4, thermocouple is connected, using thermocouple to external power supply and cooling liquid supply system input information, adjusts heating tube And cooling tube, so that the temperature of nickel-graphite melt is stablized a certain temperature in 1320~1358 DEG C of solid-liquid two-phase region, starts high speed Electromagnetic mixing apparatus carries out Isothermal stirring to nickel-graphite melt, stablizes stirring 2 minutes;
Step 5, closing high-speed electromagnetic mixing apparatus unscrews trip bolt counterclockwise, and blocking is made to bounce under the action of the spring, beats Nickel-graphite semi solid slurry can be released by opening blocking, for using.
2. a kind of high-efficiency stirring method of no volume gas nickel-graphite semi solid slurry according to claim 1, feature exist In the rotating speed of high speed electromagnetic agitating device is 900~1200 revs/min.
3. a kind of Efficient Agitator of no volume gas nickel-graphite semi solid slurry, the device include:High speed electromagnetic agitating device, It graphite crucible 2 and its volume adjustment device and moves up and down device, thermocouple 11, block 7 and chassis 9;It is characterized in that:
It is machined with internal thread in the upper inside wall of graphite crucible 2, is cooperated with the external screw thread of 10 lower end of volume adjustment head;Graphite The volume adjustment device of crucible 2 is made of volume adjustment head 10, blocking 13, trip bolt 14, spring 15 and driving device, is used for Realize the volume adjustment of graphite crucible 2;Volume adjusts head 10, and material is graphite, and upper part is round bar, and lower part is disk, in circle Disc side is machined with external screw thread, cooperates with the internal thread of 2 upper inside wall of graphite crucible;Infundibulate is equipped on disk to deflate Mouth 12;The rectangular tablet lower left quarter of blocking 13 carries the round platform for the disk uniform thickness that head 10 is adjusted with volume, and rectangular tablet right part is set There are circular hole, blocking 13 to be limited in infundibulate gas vent 12 by trip bolt 14 by right part circular hole, the round platform of blocking 13 and leakage There is the gap of 1mm between bucket shape gas vent 12;Spring 15 is sleeved on the screw rod of trip bolt 14, and effect is to jack up blocking 13, When screw-in makes 2 volume of graphite crucible reduce to volume adjustment head 10 downwards, convenient for the air discharge in graphite crucible 2;Clockwise The rectangular flat-plate compressed of blocking 13 can be attached to volume tune by the rectangular handle at the top of rotational fastener screw 14, the disk below handle The upper surface of 10 lower disk of whole head, makes infundibulate gas vent 12 seal;Driving device is by motor 18, transmission mechanism 19 and positioning Mechanism is constituted, and is to realize 2 volume of graphite crucible for driving volume adjustment head 10 to screw in downwards and screwing out graphite crucible 2 upwards The key device of adjustment;Transmission mechanism 19 is made of turbine and worm screw, gear and gear drive;Detent mechanism is located at volume adjustment First 10 round bar top, located lateral is carried out by upper and lower two bearing shells 16, and longitudinal register is carried out by upper and lower two thrust bearings 17; Motor 18, transmission mechanism 19 and the detent mechanism of driving device are respectively adopted mechanical connection manner and are fixed on guide plate 20, lead To plate 20 can be on being fixed on holder 28 guide groove 24 in move up and down;Device is moved up and down by motor 26, driver Structure 27, connection slide plate 21, buffer spring 22, connecting screw 23 are constituted;Transmission mechanism 27 is by rack 25 and gear, turbine and worm screw Transmission is constituted, and the lower end of rack 25 is connected with slide plate 21 is connect using mechanical connection manner;Connection slide plate 21 can be fixed on branch It moves up and down in guide groove 24 on frame 28, and is connect with guide plate 20 by buffer spring 22 and connecting screw 23, made Volume adjusts head 10 and its driving device moves up and down;In bearer connection screw rod 23, guide plate 20, volume adjustment head 10 and its drive After the related components such as dynamic device, thermocouple 11, blocking 13, trip bolt 14, spring 15, the decrement of buffer spring 22 is also It is greater than the maximum screw-in depth of 2 internal thread of graphite crucible;Move up and down the motor 26 of device, transmission mechanism 27 is connected using machinery The mode of connecing is fixed on holder 28;
4. a kind of Efficient Agitator of no volume gas nickel-graphite semi solid slurry according to claim 3, feature exist In it is 5~10mm that the upper table of nickel-graphite semi solid slurry 6, which faces upward and is higher by the lowermost distance d of 2 internal thread of graphite crucible,.
CN201810010417.4A 2018-01-05 2018-01-05 A kind of high-efficiency stirring method and device of no volume gas nickel-graphite semi solid slurry Withdrawn CN108579587A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201810010417.4A CN108579587A (en) 2018-01-05 2018-01-05 A kind of high-efficiency stirring method and device of no volume gas nickel-graphite semi solid slurry

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201810010417.4A CN108579587A (en) 2018-01-05 2018-01-05 A kind of high-efficiency stirring method and device of no volume gas nickel-graphite semi solid slurry

Publications (1)

Publication Number Publication Date
CN108579587A true CN108579587A (en) 2018-09-28

Family

ID=63599844

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201810010417.4A Withdrawn CN108579587A (en) 2018-01-05 2018-01-05 A kind of high-efficiency stirring method and device of no volume gas nickel-graphite semi solid slurry

Country Status (1)

Country Link
CN (1) CN108579587A (en)

Similar Documents

Publication Publication Date Title
CN108187560A (en) A kind of high-efficiency stirring method and device of no volume gas aluminium-graphite semi-solid slurry
CN108225039A (en) A kind of high-efficiency stirring method and device of no volume gas nickel-silicon nitride semi solid slurry
CN108579587A (en) A kind of high-efficiency stirring method and device of no volume gas nickel-graphite semi solid slurry
CN108559862A (en) A kind of high-efficiency stirring method and device of no volume gas magnesium-carbonization silicon melt
CN108220653A (en) A kind of high-efficiency stirring method and device of no volume gas aluminum-boron nitride semi solid slurry
CN108165806A (en) A kind of high-efficiency stirring method and device of no volume gas zinc-carbonization silicon melt
CN108144518A (en) A kind of high-efficiency stirring method and device of 28 lead melt of no volume gas aluminium
CN107983245A (en) A kind of high-efficiency stirring method and device of no volume gas iron-graphite melt
CN108144512A (en) A kind of high-efficiency stirring method and device of no volume gas iron-graphite semi solid slurry
CN108579586A (en) A kind of high-efficiency stirring method and device of no volume gas iron-aluminium oxide semi solid slurry
CN108579588A (en) A kind of high-efficiency stirring method and device of no volume gas nickel-boron nitride semi-solid slurry
CN108187563A (en) A kind of high-efficiency stirring method and device of no volume gas copper-graphite semi solid slurry
CN108579585A (en) A kind of high-efficiency stirring method and device of no volume gas titanium-boron nitride semi-solid slurry
CN108144513A (en) A kind of high-efficiency stirring method and device of no volume gas titanium-graphite semi-solid slurry
CN108554292A (en) A kind of high-efficiency stirring method and device of no volume gas nickel-graphite melt
CN108144515A (en) A kind of high-efficiency stirring method and device of no volume gas zinc-aluminium oxide semi solid slurry
CN108220654A (en) A kind of high-efficiency stirring method and device of no volume gas copper-boron nitride semi-solid slurry
CN108144516A (en) A kind of high-efficiency stirring method and device of no volume gas copper-Ni-coated graphite semi solid slurry
CN108144514A (en) A kind of high-efficiency stirring method and device of no volume gas copper-aluminium oxide semi solid slurry
CN108220658A (en) A kind of high-efficiency stirring method and device of no volume gas zinc-silicon carbide semi solid slurry
CN108165802A (en) A kind of high-efficiency stirring method and device of no volume gas copper-graphite melt
CN108187564A (en) A kind of high-efficiency stirring method and device of no volume gas magnesium-aluminium oxide semi solid slurry
CN108144523A (en) A kind of high-efficiency stirring method and device of no volume gas aluminium-aluminium oxide semi solid slurry
CN108144519A (en) A kind of high-efficiency stirring method and device of no volume gas zinc-silicon nitride semi solid slurry
CN108187561A (en) A kind of high-efficiency stirring method and device of no volume gas iron-boron nitride semi-solid slurry

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
WW01 Invention patent application withdrawn after publication

Application publication date: 20180928

WW01 Invention patent application withdrawn after publication