CN108567583A - A kind of amino acid is from thickener composition, system and application - Google Patents
A kind of amino acid is from thickener composition, system and application Download PDFInfo
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- CN108567583A CN108567583A CN201810800265.8A CN201810800265A CN108567583A CN 108567583 A CN108567583 A CN 108567583A CN 201810800265 A CN201810800265 A CN 201810800265A CN 108567583 A CN108567583 A CN 108567583A
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- amino acid
- alkyl glycosides
- lauroyl sarcosine
- sodium lauroyl
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/60—Sugars; Derivatives thereof
- A61K8/604—Alkylpolyglycosides; Derivatives thereof, e.g. esters
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
- A61K8/442—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof substituted by amido group(s)
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/02—Preparations for cleaning the hair
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/20—Chemical, physico-chemical or functional or structural properties of the composition as a whole
- A61K2800/26—Optical properties
- A61K2800/262—Transparent; Translucent
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/20—Chemical, physico-chemical or functional or structural properties of the composition as a whole
- A61K2800/30—Characterized by the absence of a particular group of ingredients
- A61K2800/34—Free of silicones
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/48—Thickener, Thickening system
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- Animal Behavior & Ethology (AREA)
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Abstract
The invention belongs to daily chemicals fields, more particularly to a kind of amino acid from thickener composition, it is characterized in that, it is made of sodium lauroyl sarcosine, alkyl glycosides and compound surfactant, the compound surfactant is one kind in Cocoamidopropyl betaine, cocoamido sodium propionate, cocounut oil acyl both sexes base diethyl acid disodium;The weight ratio of the sodium lauroyl sarcosine, compound surfactant is 1:1‑1:4;The sum of weight of sodium lauroyl sarcosine, compound surfactant and the ratio of alkyl glycosides are:12‑16:1‑3.It is strong from thickening capabilities that the purpose of the present invention is to provide one kind, and the amino acid of low temperature not jelly also discloses the particular use comprising the system of the composition and the system from thickener composition.
Description
Technical field
The present invention relates to daily chemicals fields, and in particular to a kind of amino acid is from thickener composition, system and application.
Background technology
Amino acid surfactant has the function from thickening, so in many daily use chemicals formula, it is more and more to use
Amino acid not only has from thickening function from thickener, also has mild surface-active.
CN201310127769.5 discloses a kind of amino acid type surfactant from thickener composition, and it includes cocounut oil acyls
Amine propyl hydroxyl sulphur glycine betaine and sodium N-lauroyl sarcosinate are as thickener.
CN201310153564.4 discloses a kind of agricultural thickening builder, and it includes fatty alcohol polyoxyethylene ether sulfuric acid
Salt, alkyl glycosides, sodium N-lauroyl sarcosinate, neopelex are recorded in specification:Contain aliphatic alcohol polyethenoxy
Ether sulfate so that auxiliary agent itself has wetting synergy more preferably, the more stable feature of performance, and it is more preferable to thicken synergistic effect.
CN201711263120.0 discloses a kind of nourishing of camellia seed oil containing high oil content foam bath breast, and it includes hydroxypropyls
Phosphate ester starch, C8-C10 alkyl glycosides, cocounut oil acyl propyl betaine, cocounut oil acyl glycine potassium, sldium lauryl sulfate, laruyl alcohol
Phosphate potassium, 30 epigallocatechin glucogallic acids of JC are modified thickener, and record washing for amino acid system in the description
What shield formula was most difficult to is exactly to thicken problem.Amidates anionic surfactant has head base larger, is not easy to form close-packed arrays
Rod-shaped micelle the characteristics of.Micella factor cannot be satisfied thickening, can be slowed down by compounding the surfactant of other types
The trend of hardly possible thickening.The another way of thickening is liquid crystal accumulation.It is assisted with the surfactant of amino acid sylvite and phosphate potassium
With thickening capabilities epigallocatechin glucogallic acid thickener very outstanding as main thickening means, it is only necessary to sufficient amount
Propylhomoserin sylvite be that can reach consistency close to lotion.It can be seen that the program using amino acid sylvite, phosphate potassium,
Epigallocatechin glucogallic acid thickener synergistic thickening.
CN201510206608.4 discloses a kind of no silicon shampoo, includes the component of following weight percent meter:Inulin
0.5~5%, vegetable fat 0.2~5%, solubilizer 0.2~2%, thickener 0.2~2%, laureth sodium sulfovinate 3~
8%, Cocoamidopropyl betaine 3~8%, alkyl glycosides 1~5%, sodium cocoyl glycinate 1~5%, ethylenediamine tetra-acetic acid
Four sodium 0.05~0.5%, citric acid 0.05~0.5%, preservative 0.2~1%, essence 0.2~1% and water 58~90%.
Above-mentioned technical proposal or need additional thickener auxiliary or the case where not increasing additional thickener
Lower thickening capabilities are limited.
Also, a prodigious problem existing for amino acid surfactant is:Jelly is easily become under low temperature condition
Shape.
Invention content
It is strong from thickening capabilities that the object of the present invention is to provide one kind, and the amino acid of low temperature not jelly is from thickener composition, together
When also disclose the system comprising the composition.
The concrete scheme of the present invention is as follows:A kind of amino acid is from thickener composition, by sodium lauroyl sarcosine, alkyl glycosides
And compound surfactant composition, the compound surfactant are Cocoamidopropyl betaine, cocoamido third
One kind in sour sodium, cocounut oil acyl both sexes base diethyl acid disodium;
The weight ratio of the sodium lauroyl sarcosine, compound surfactant is 1:1-1:4;Sodium lauroyl sarcosine,
The sum of weight of compound surfactant and the ratio of alkyl glycosides are:12-16:1-3.
In above-mentioned amino acid from thickener composition, the alkyl glycosides is C12-C14 alkyl glycosides, C12-C16
Alkyl glycosides, C8-C14 alkyl glycosides.
In practical applications, C12-C14 alkyl glycosides, C12-C16 alkyl glycosides, C8-C14 alkyl glycosides are applied to interworking
In system, system viscosity will produce faint variation, and this variation will not generate conclusive influence to the final performance of product,
In general, average carbon chain is longer, and the viscosity of system can be slightly higher, and average carbon chain is shorter, and the viscosity of system can be slightly lower.
In above-mentioned amino acid from thickener composition, by sodium lauroyl sarcosine, Cocoamidopropyl betaine, alkyl
Glucosides form, wherein sodium lauroyl sarcosine, Cocoamidopropyl betaine, alkyl glycosides weight ratio be 4:12:1-3.
In above-mentioned amino acid from thickener composition, by sodium lauroyl sarcosine, cocoamido sodium propionate, alkyl sugar
Glycosides form, wherein sodium lauroyl sarcosine, cocoamido sodium propionate, alkyl glycosides weight ratio be 4-8:4-8:1-3.
Meanwhile the invention also discloses a kind of amino acid from thickened systems, including amino acid as described above is from thickening group
Close object, water and pH adjusting agent, the sodium lauroyl sarcosine, compound surfactant the sum of weight be equivalent to system gross weight
12-16%;1-3% of the alkyl glycosides quite with system gross weight.
In above-mentioned amino acid from thickened systems, the pH adjusting agent is citric acid, and the pH value of system is 5.2-
5.8。
The invention also discloses amino acid as described above from the application of thickened systems, is applied to daily use chemicals and thickens field.
Amino acid as described above is from thickened systems applied to no silicone oil without in the transparent shampoo of sulfate amino acid.
The present invention has the following advantages and effects with respect to the prior art:
The composition of the present invention is less than compound surfactant dosage in the dosage of sodium lauroyl sarcosine, and adds certain
Excellent thickening properties can be shown after the alkyl glycosides of amount, with mild surface-active, do not using thickening completely
In the case of agent, such compound system viscosity is easy to reach 6000-10000mPas.The composition is also shown excellent simultaneously
Low temperature not jelly performance.
In the aqueous solution of surfactant, surfactant molecule can form various micella knots by way of self assembly
Structure.When concentration is close to critical micelle concentration (CMC), it may appear that spherical micelle;With the increase of surfactant concentration, gradually
There is rod-shaped micelle, rod-shaped micelle, which further assembles winding, so that solution viscosity is had a distinct increment;When surfactant concentration increases
When being added to a certain degree, lameller micelles is formed, solution viscosity is very big at this time, hardly flows.Surfactant is in the solution
The micelle state of formation can use critical Packing parameter CpPrediction, expression formula Cp=V/LcAc, wherein V indicates hydrophobic last-of-chain
Volume, LcIndicate the maximum development length of hydrophobic chain, AcIndicate sectional area of the head base on interface.CpBy the shadow of self assembly condition
It rings and changes, CpWhen≤1/3, spherical micelle is generally formed;1/3 < CpWhen < 1/2, rod-shaped micelle is formed;1/2≤CpWhen≤1,
Form lameller micelles;It follows that surfactant C in a certain rangepBigger, the rodlike and lameller micelles of easier formation is molten
Liquid system viscosity is bigger.Amino acid surfactant is due to the larger i.e. A of head basecBeing worth larger leads to its CpIt is smaller to be difficult to realize thicken.
After a certain amount of APG is added in the solution, due to the Interaction enhanced between hydrophobic alkyl chain, compression amino acid surface is lived
Property agent head base space and hydrophobic group range increase, to improve solution viscosity.
Description of the drawings
Fig. 1 is the test result of the embodiment of the present invention 1;
Fig. 2 is the test result of the embodiment of the present invention 2;
Fig. 3 is the test result of the embodiment of the present invention 3;
Fig. 4 is the test result of the application test of the present invention.
Specific implementation mode
With reference to embodiment, the invention will be further described, but does not constitute any limitation of the invention, any
In the modification for the limited number of time that scope of the invention as claimed is made, still in scope of the presently claimed invention.
Embodiment 1
The present embodiment investigates sodium lauroyl sarcosine (LS), cocoamido sodium propionate (CA), alkyl glycosides (C12-
C14APG compound property).
The accurate sodium lauroyl sarcosine for weighing certain mass, cocoamido sodium propionate, alkyl glycosides, deionized water,
Citric acid, 45 DEG C of heating water baths, sealing, which is put into 25 DEG C of insulating boxs, after stirring evenly stands for 24 hours, and pH5.2-5.8 is measured after taking-up
And viscosity and observe system appearance.
Sodium lauroyl sarcosine, cocoamido sodium propionate, alkyl glycosides additive amount (weight percent) be respectively:
8%:4%:0%;8%:4%:1%;8%:4%:3%;6%:6%:0%;6%:6%:1%;6%:6%:
3%;4%:8%:0%;4%:8%:1%;4%:8%:3%;
Its performance data is shown in attached drawing 1.
Embodiment 2
The present embodiment investigates sodium lauroyl sarcosine (LS), Cocoamidopropyl betaine (CAB), alkyl glycosides (C12-
C14APG compound property).
Accurate sodium lauroyl sarcosine, Cocoamidopropyl betaine, alkyl glycosides, the deionization for weighing certain mass
Water, citric acid, 45 DEG C of heating water baths, sealing, which is put into 25 DEG C of insulating boxs, after stirring evenly stands for 24 hours, and pH5.2- is measured after taking-up
5.8 and viscosity and observe system appearance.
Sodium lauroyl sarcosine, Cocoamidopropyl betaine, alkyl glycosides additive amount (weight percent) be respectively:
8%:4%:0%;8%:4%:1%;8%:4%:3%;6%:6%:0%;6%:6%:1%;6%:6%:3%;4%:
8%:0%;4%:8%:1%;4%:8%:3%;12%:4%:0%;12%:4%:1%;12%:4%:3%;8%:
8%:0%;8%:8%:1%;8%:8%:3%;4%:12%:0%;4%:12%:1%;4%:12%:3%;
Its performance data is shown in attached drawing 2.
Embodiment 3
The present embodiment investigates sodium lauroyl sarcosine (LS), cocounut oil acyl both sexes base diethyl acid disodium (MAB), alkyl glycosides
(C12-C14APG) compound property.
The accurate sodium lauroyl sarcosine for weighing certain mass, cocounut oil acyl both sexes base diethyl acid disodium, alkyl glycosides, go from
Sub- water, citric acid, 45 DEG C of heating water baths, sealing, which is put into 25 DEG C of insulating boxs, after stirring evenly stands for 24 hours, is measured after taking-up
PH5.2-5.8 and viscosity simultaneously observe system appearance.
The additive amount (weight percent) point of sodium lauroyl sarcosine, cocounut oil acyl both sexes base diethyl acid disodium, alkyl glycosides
It is not:8%:4%:0%;8%:4%:1%;8%:4%:3%;6%:6%:0%;6%:6%:1%;6%:6%:3%;
4%:8%:0%;4%:8%:1%;4%:8%:3%;12%:4%:0%;12%:4%:1%;12%:4%:3%;
8%:8%:0%;8%:8%:1%;8%:8%:3%;4%:12%:0%;4%:12%:1%;4%:12%:3%;
Its performance data is shown in attached drawing 3.
By the experiment of embodiment 1-3, we can obtain as drawn a conclusion:
In the case where not using thickener completely, system is in the alkyl glycosides for being added to 1%-3%, and lauroyl flesh
The dosage of propylhomoserin sodium shows excellent from thickening properties less than system in the case of compound surfactant dosage.
Low-temperature antifreeze performance such as the following table 1 of above-described embodiment 2:
1 system Low-temperature antifreeze performance of table
System in table 1 is not in jelly phenomenon at low temperatures.
Meanwhile the Cocoamidopropyl betaine in embodiment 2 is also replaced with into cocamidopropyl propyl amide amine oxide
(CAO), then find that the Low-temperature antifreeze performance of system is obviously deteriorated.
2 system Low-temperature antifreeze performance of table
At low temperatures, there is jelly phenomenon in each test example in table 2.
Using test
The problems such as considering market trend in practical application, cost, stability, use feeling, develop no silicone oil without
The transparent shampoo of sulfate amino acid, it is desirable to support can be provided for the practical application of sodium lauroyl sarcosine.It is formulated with reference to table 3
Shampoo is prepared, final products pH value is 5.40, and viscosity 5000mPas, appearance is colourless transparent liquid.And to the product
Consumer rating is carried out, consumer's shampoo used in everyday is assessed as 3 points, it is transparent without sulfate amino acid to no silanol terminated polydimethylsiloxane
Shampoo makes subjective evaluation with regard to 7 evaluation items in Fig. 4.Assessment result shows that no silicone oil is washed without sulfate amino acid is transparent
Foam, flush performance, wet hair and the dry hair conditioning performance of shampoo are superior to routine use shampoo.
Specific formula such as the following table 3.
Table 3 is without silicone oil without the transparent shampoo formula of sulfate amino acid
The above embodiment is a preferred embodiment of the present invention, but embodiments of the present invention are not by above-described embodiment
Limitation, it is other it is any without departing from the spirit and principles of the present invention made by changes, modifications, substitutions, combinations, simplifications,
Equivalent substitute mode is should be, is included within the scope of the present invention.
Claims (8)
1. a kind of amino acid is from thickener composition, which is characterized in that by sodium lauroyl sarcosine, alkyl glycosides and compounding surface
Activating agent forms, and the compound surfactant is Cocoamidopropyl betaine, cocoamido sodium propionate, cocounut oil acyl two
One kind in property base diethyl acid disodium;
The weight ratio of the sodium lauroyl sarcosine, compound surfactant is 1:1-1:4;Sodium lauroyl sarcosine, compounding
The sum of weight of surfactant and the ratio of alkyl glycosides are:12-16:1-3.
2. amino acid according to claim 1 is from thickener composition, which is characterized in that the alkyl glycosides is C12-
C14 alkyl glycosides, C12-C16 alkyl glycosides, C8-C14 alkyl glycosides.
3. amino acid according to claim 2 is from thickener composition, which is characterized in that by sodium lauroyl sarcosine, cocounut oil
Amido propyl betaine, alkyl glycosides composition, wherein sodium lauroyl sarcosine, Cocoamidopropyl betaine, alkyl glycosides
Weight ratio is 4:12:1-3.
4. amino acid according to claim 2 is from thickener composition, which is characterized in that by sodium lauroyl sarcosine, cocounut oil
Acylamino- sodium propionate, alkyl glycosides composition, wherein sodium lauroyl sarcosine, cocoamido sodium propionate, alkyl glycosides weight
Than for 4-8:4-8:1-3.
5. a kind of amino acid is from thickened systems, it is characterised in that:It include the amino acid thickening certainly as described in claim 1-4 is any
Composition, water and pH adjusting agent, the sodium lauroyl sarcosine, compound surfactant the sum of weight to be equivalent to system total
The 12-16% of weight;1-3% of the alkyl glycosides quite with system gross weight.
6. amino acid according to claim 5 is from thickened systems, it is characterised in that:The pH adjusting agent is citric acid,
The pH value of system is 5.2-5.8.
7. a kind of application of such as amino acid described in claim 5 or 6 from thickened systems, which is characterized in that be applied to daily use chemicals and increase
Thick field.
8. amino acid according to claim 7 is from the application of thickened systems, which is characterized in that applied to no silicone oil without sulfuric acid
In the transparent shampoo of salt amino acid.
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Cited By (2)
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CN110840773A (en) * | 2019-11-04 | 2020-02-28 | 广东丽臣奥威实业有限公司 | High-viscosity high-foam surfactant composition |
CN113018207A (en) * | 2019-12-24 | 2021-06-25 | 上海家化联合股份有限公司 | Self-thickening composition of amino acid surfactants |
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