CN108560072A - Antiseptic health care fiber silk and preparation method thereof - Google Patents
Antiseptic health care fiber silk and preparation method thereof Download PDFInfo
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- CN108560072A CN108560072A CN201810293996.8A CN201810293996A CN108560072A CN 108560072 A CN108560072 A CN 108560072A CN 201810293996 A CN201810293996 A CN 201810293996A CN 108560072 A CN108560072 A CN 108560072A
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- silk
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- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F1/00—General methods for the manufacture of artificial filaments or the like
- D01F1/02—Addition of substances to the spinning solution or to the melt
- D01F1/10—Other agents for modifying properties
- D01F1/103—Agents inhibiting growth of microorganisms
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F4/00—Monocomponent artificial filaments or the like of proteins; Manufacture thereof
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- Engineering & Computer Science (AREA)
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Textile Engineering (AREA)
- Manufacturing & Machinery (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
Abstract
The present invention relates to a kind of antiseptic health care fiber silks, are grouped as by each group of following parts by weight：8~14 parts of natural plant extracts, 23~36 parts of silk, 12~17 parts of bamboo charcoal fiber, 5~9 parts of granatum, 6~11 parts of chitin, 9~14 parts of acetic acid, 0.9~1.8 part of ferroso-ferric oxide, 1~3 part of aluminium chloride；The natural plant extracts include aloe, the coptis, Asian puccoon, mock-strawberry.The invention further relates to the preparation methods of the antiseptic health care fiber silk, stablize by the filament Chemical Physics performance that the formula and method are produced, it is added to natural plant extracts, there is inhibition to germs such as staphylococcus aureus, candida albicans, Escherichia coli, also have promote blood circulation, health-care efficacies such as pneumostatic with fixed attention, and effect is lasting, and low, the production suitable for textiles such as personal clothing, bedding, home decorations is influenced by washing times.
Description
Technical field
The present invention relates to chemical fibre material fields, more particularly, to a kind of antiseptic health care fiber silk and its preparation side
Method.
Background technology
With the raising of scientific and technological progress and living standards of the people, demand of the consumer to textile has no longer been simple U.S.
Element that is durable, but needing additional multifunctional and beneficial body and mind is seen, is constantly increased particular against the antibacterial textile demand of bacterium
Add.Textile can also be made to have antibiotic effect although carrying out antibiotic finish to textile, fiber is by repeatedly washing it
Afterwards, antiseptic may fall off and cause antibacterial effect can not long sustaining.If can make fiber itself that there is antibacterial and health care work(
Can, then it can make fiber that there is permanent effect, to have broader development prospect.
Invention content
The object of the present invention is to provide a kind of antiseptic health care fiber silks.
It is a further object of the present invention to provide a kind of preparation methods of the antiseptic health care fiber silk.
The object of the invention is achieved by the following technical programs：
A kind of antiseptic health care fiber silk is provided, is grouped as by each group of following parts by weight：8~14 parts of natural plant extracts,
23~36 parts of silk, 12~17 parts of bamboo charcoal fiber, 5~9 parts of granatum, 6~11 parts of chitin, 9~14 parts of acetic acid, four oxidations three
0.9~1.8 part of iron, 1~3 part of aluminium chloride.
Preferably, the antiseptic health care fiber silk is grouped as by each group of following parts by weight：Natural plant extracts 12
Part, 30 parts of silk, 15 parts of bamboo charcoal fiber, 7 parts of granatum, 8 parts of chitin, 11 parts of acetic acid, 1.2 parts of ferroso-ferric oxide, aluminium chloride 2
Part.
Preferably, the natural plant extracts include aloe, the coptis, Asian puccoon, mock-strawberry.
The present invention also provides the preparation methods of the antiseptic health care fiber silk, include the following steps：
（1）Prepare natural plant extracts：Take aloe, the coptis, Asian puccoon, the mock-strawberry of equivalent, clean dry that 3~5 times of concentration are added
95% ethyl alcohol impregnates 48~72h, ethyl alcohol is recovered by filtration, is freeze-dried after concentration, obtains natural plant extracts, spare；
（2）8~12min of hydrogen peroxide dipping of silk concentration 10% is taken, drying is taken out, it is spare；
（3）Bamboo charcoal fiber is taken, is preheated to 30~50 DEG C, then acetone soln is added in stirring at this temperature, after impregnating 3~6h,
Drying is taken out, it is spare；
（4）Granatum is taken to clean up, dries pulverizing crosses 200~300 mesh sieve, spare；
（5）It is 200~250 kPa in pressure, temperature is to carry out machine at 80~110 DEG C by processed silk and bamboo charcoal fiber
Tool is broken, and grind into powder；
（6）In step（5）Natural plant extracts, Pomegranate Rind and other remaining raw material, mixing are added in gained powder
Uniformly, 40~50 DEG C of 15~32 parts of water is added, stirs 5~8min, 2~4 parts of polyvinyl alcohol and Rosemary Oil 1~3 is added
Part, 95~100 DEG C are warming up to, 1~2h of stirring and dissolving obtains spinning solution；
（7）After spinning solution is filtered, then 20~30min of vacuum standing and defoaming at 30~60 DEG C uses conventional Wet-spinning
Silk carries out spinning and post-processing, obtains antiseptic health care fiber silk.
Compared with prior art, the invention has the advantages that：
The present invention provides a kind of antiseptic health care fiber silks, using special composition of raw materials, the fiber produced by the formula
Wire chemical stable physical property, is added to natural plant extracts, to staphylococcus aureus, candida albicans, Escherichia coli etc.
Germ has an inhibition, also have promote blood circulation, health-care efficacies such as pneumostatic with fixed attention, and effect is lasting, by washing times shadow
Sound is low, is suitable for the production of the textiles such as personal clothing, bedding, home decoration.
Specific implementation mode
With reference to specific embodiment, the present invention is further illustrated.
Embodiment 1
Present embodiment discloses a kind of antiseptic health care fiber silks, are grouped as by each group of following parts by weight：Extracted form natural plant
8 parts of object, 36 parts of silk, 12 parts of bamboo charcoal fiber, 9 parts of granatum, 6 parts of chitin, 14 parts of acetic acid, 0.9 part of ferroso-ferric oxide, chlorination
3 parts of aluminium；The natural plant extracts include aloe, the coptis, Asian puccoon, mock-strawberry.
Embodiment 2
Present embodiment discloses a kind of antiseptic health care fiber silks, are grouped as by each group of following parts by weight：Extracted form natural plant
14 parts of object, 23 parts of silk, 17 parts of bamboo charcoal fiber, 5 parts of granatum, 11 parts of chitin, 9 parts of acetic acid, 1.8 parts of ferroso-ferric oxide, chlorine
Change 1 part of aluminium；The natural plant extracts include aloe, the coptis, Asian puccoon, mock-strawberry.
Embodiment 3
Present embodiment discloses a kind of antiseptic health care fiber silks, are grouped as by each group of following parts by weight：Extracted form natural plant
10 parts of object, 25 parts of silk, 13 parts of bamboo charcoal fiber, 6 parts of granatum, 10 parts of chitin, 13 parts of acetic acid, 1.5 parts of ferroso-ferric oxide, chlorine
Change 1.5 parts of aluminium；The natural plant extracts include aloe, the coptis, Asian puccoon, mock-strawberry.
Embodiment 4
Present embodiment discloses a kind of antiseptic health care fiber silks, are grouped as by each group of following parts by weight：Extracted form natural plant
12 parts of object, 30 parts of silk, 15 parts of bamboo charcoal fiber, 7 parts of granatum, 8 parts of chitin, 11 parts of acetic acid, 1.2 parts of ferroso-ferric oxide, chlorine
Change 2 parts of aluminium；The natural plant extracts include aloe, the coptis, Asian puccoon, mock-strawberry.
Embodiment 5
The components by weight percent of 1~4 any embodiment of Example prepares antiseptic health care fiber silk, and preparation process is as follows：
（1）Prepare natural plant extracts：Take aloe, the coptis, Asian puccoon, the mock-strawberry of equivalent, clean dry that 3 times of concentration 95% are added
Ethyl alcohol, impregnate 72h, ethyl alcohol is recovered by filtration, is freeze-dried after concentration, obtains natural plant extracts, it is spare；
（2）The hydrogen peroxide dipping 8min of silk concentration 10% is taken, drying is taken out, it is spare；
（3）Bamboo charcoal fiber is taken, is preheated to 50 DEG C, then acetone soln is added in stirring at this temperature, after impregnating 3h, takes out and dries
It is dry, it is spare；
（4）Granatum is taken to clean up, dries pulverizing crosses 300 mesh sieve, spare；
（5）Be 200 kPa in pressure by processed silk and bamboo charcoal fiber, temperature be carry out Mechanical Crushing at 110 DEG C, and
Grind into powder；
（6）In step（5）Natural plant extracts, Pomegranate Rind and other remaining raw material, mixing are added in gained powder
Uniformly, 40 DEG C of 32 parts of water is added, stirs 5min, 1 part of 4 parts of polyvinyl alcohol and Rosemary Oil is added, is warming up to 100 DEG C, stirs
Dissolving 1h is mixed, spinning solution is obtained；
（7）After spinning solution is filtered, then the vacuum standing and defoaming 20min at 60 DEG C is spun with conventional wet spinning
Silk and post-processing, obtain antiseptic health care fiber silk.
Embodiment 6
The components by weight percent of 1~4 any embodiment of Example prepares antiseptic health care fiber silk, and preparation process is as follows：
（1）Prepare natural plant extracts：Take aloe, the coptis, Asian puccoon, the mock-strawberry of equivalent, clean dry that 5 times of concentration 95% are added
Ethyl alcohol, impregnate 48h, ethyl alcohol is recovered by filtration, is freeze-dried after concentration, obtains natural plant extracts, it is spare；
（2）The hydrogen peroxide dipping 12min of silk concentration 10% is taken, drying is taken out, it is spare；
（3）Bamboo charcoal fiber is taken, is preheated to 30 DEG C, then acetone soln is added in stirring at this temperature, after impregnating 6h, takes out and dries
It is dry, it is spare；
（4）Granatum is taken to clean up, dries pulverizing crosses 200 mesh sieve, spare；
（5）It is 250 kPa in pressure, temperature is to carry out Mechanical Crushing at 80 DEG C, and grind by processed silk and bamboo charcoal fiber
It clays into power；
（6）In step（5）Natural plant extracts, Pomegranate Rind and other remaining raw material, mixing are added in gained powder
Uniformly, 50 DEG C of 15 parts of water is added, stirs 8min, 3 parts of 2 parts of polyvinyl alcohol and Rosemary Oil is added, is warming up to 95 DEG C, stirring
2h is dissolved, spinning solution is obtained；
（7）After spinning solution is filtered, then the vacuum standing and defoaming 30min at 30 DEG C is spun with conventional wet spinning
Silk and post-processing, obtain antiseptic health care fiber silk.
Embodiment 7
The components by weight percent of 1~4 any embodiment of Example prepares antiseptic health care fiber silk, and preparation process is as follows：
（1）Prepare natural plant extracts：Take aloe, the coptis, Asian puccoon, the mock-strawberry of equivalent, clean dry that 4 times of concentration 95% are added
Ethyl alcohol, impregnate 60h, ethyl alcohol is recovered by filtration, is freeze-dried after concentration, obtains natural plant extracts, it is spare；
（2）The hydrogen peroxide dipping 10min of silk concentration 10% is taken, drying is taken out, it is spare；
（3）Bamboo charcoal fiber is taken, is preheated to 40 DEG C, then acetone soln is added in stirring at this temperature, after impregnating 5h, takes out and dries
It is dry, it is spare；
（4）Granatum is taken to clean up, dries pulverizing crosses 250 mesh sieve, spare；
（5）It is 220kPa in pressure, temperature is to carry out Mechanical Crushing at 100 DEG C, and grind by processed silk and bamboo charcoal fiber
It clays into power；
（6）In step（5）Natural plant extracts, Pomegranate Rind and other remaining raw material, mixing are added in gained powder
Uniformly, 45 DEG C of 25 parts of water is added, stirs 6min, 2 parts of 3 parts of polyvinyl alcohol and Rosemary Oil is added, is warming up to 98 DEG C, stirring
1.5h is dissolved, spinning solution is obtained；
（7）After spinning solution is filtered, then the vacuum standing and defoaming 25min at 50 DEG C is spun with conventional wet spinning
Silk and post-processing, obtain antiseptic health care fiber silk.
Claims (4)
1. a kind of antiseptic health care fiber silk, which is characterized in that be grouped as by each group of following weight percent：Extracted form natural plant
8~14 parts of object, 23~36 parts of silk, 12~17 parts of bamboo charcoal fiber, 5~9 parts of granatum, 6~11 parts of chitin, acetic acid 9~14
Part, 0.9~1.8 part of ferroso-ferric oxide, 1~3 part of aluminium chloride.
2. antiseptic health care fiber silk according to claim 1, which is characterized in that be grouped by each group of following weight fraction
At：12 parts of natural plant extracts, 30 parts of silk, 15 parts of bamboo charcoal fiber, 7 parts of granatum, 8 parts of chitin, 11 parts of acetic acid, four oxygen
Change 1.2 parts of three-iron, 2 parts of aluminium chloride.
3. antiseptic health care fiber silk according to claim 1 or 2, which is characterized in that the natural plant extracts include
Aloe, the coptis, Asian puccoon, mock-strawberry.
4. according to the preparation method of the antiseptic health care fiber silk of claim 1 or 3, which is characterized in that include the following steps：
（1）Prepare natural plant extracts：Take aloe, the coptis, Asian puccoon, the mock-strawberry of equivalent, clean dry that 3~5 times of concentration are added
95% ethyl alcohol impregnates 48~72h, ethyl alcohol is recovered by filtration, is freeze-dried after concentration, obtains natural plant extracts, spare；
（2）8~12min of hydrogen peroxide dipping of silk concentration 10% is taken, drying is taken out, it is spare；
（3）Bamboo charcoal fiber is taken, is preheated to 30~50 DEG C, then acetone soln is added in stirring at this temperature, after impregnating 3~6h,
Drying is taken out, it is spare；
（4）Granatum is taken to clean up, dries pulverizing crosses 200~300 mesh sieve, spare；
（5）It is 200~250 kPa in pressure, temperature is to carry out machine at 80~110 DEG C by processed silk and bamboo charcoal fiber
Tool is broken, and grind into powder；
（6）In step（5）Natural plant extracts, Pomegranate Rind and other remaining raw material, mixing are added in gained powder
Uniformly, 40~50 DEG C of 15~32 parts of water is added, stirs 5~8min, 2~4 parts of polyvinyl alcohol and Rosemary Oil 1~3 is added
Part, 95~100 DEG C are warming up to, 1~2h of stirring and dissolving obtains spinning solution；
（7）After spinning solution is filtered, then 20~30min of vacuum standing and defoaming at 30~60 DEG C uses conventional Wet-spinning
Silk carries out spinning and post-processing, obtains antiseptic health care fiber silk.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810293996.8A CN108560072A (en) | 2018-03-30 | 2018-03-30 | Antiseptic health care fiber silk and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810293996.8A CN108560072A (en) | 2018-03-30 | 2018-03-30 | Antiseptic health care fiber silk and preparation method thereof |
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| Publication Number | Publication Date |
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| CN108560072A true CN108560072A (en) | 2018-09-21 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201810293996.8A Withdrawn CN108560072A (en) | 2018-03-30 | 2018-03-30 | Antiseptic health care fiber silk and preparation method thereof |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111235684A (en) * | 2020-02-21 | 2020-06-05 | 海南女人春天美容有限公司 | Antibacterial fiber body shaping clothes |
| CN113151925A (en) * | 2021-04-07 | 2021-07-23 | 罗莱生活科技股份有限公司 | Polyquaternary ammonium salt/aloe antibacterial fiber, preparation method thereof and application thereof in antibacterial towels |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH09310235A (en) * | 1996-03-18 | 1997-12-02 | Nobuhide Maeda | Production of processed yarn by blending or twisting silk fiber with composite rayon fiber having antibacterial, deodorizing, antifungal and insectididal properties and further having far infrared light-radiating characteristic and then spinning the blend |
| CN107190358A (en) * | 2017-06-30 | 2017-09-22 | 太仓红桥服饰有限公司 | A kind of environment-friendly antibacterial anti-radiation garment fabric |
| CN107419359A (en) * | 2017-07-24 | 2017-12-01 | 湖州力行纺织有限公司 | Heat-resisting chemical fibre silk and preparation method thereof |
| CN107815773A (en) * | 2017-09-30 | 2018-03-20 | 湖州东凯纺织有限公司 | Anti-bacterial fibre cloth and preparation method thereof |
-
2018
- 2018-03-30 CN CN201810293996.8A patent/CN108560072A/en not_active Withdrawn
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH09310235A (en) * | 1996-03-18 | 1997-12-02 | Nobuhide Maeda | Production of processed yarn by blending or twisting silk fiber with composite rayon fiber having antibacterial, deodorizing, antifungal and insectididal properties and further having far infrared light-radiating characteristic and then spinning the blend |
| CN107190358A (en) * | 2017-06-30 | 2017-09-22 | 太仓红桥服饰有限公司 | A kind of environment-friendly antibacterial anti-radiation garment fabric |
| CN107419359A (en) * | 2017-07-24 | 2017-12-01 | 湖州力行纺织有限公司 | Heat-resisting chemical fibre silk and preparation method thereof |
| CN107815773A (en) * | 2017-09-30 | 2018-03-20 | 湖州东凯纺织有限公司 | Anti-bacterial fibre cloth and preparation method thereof |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111235684A (en) * | 2020-02-21 | 2020-06-05 | 海南女人春天美容有限公司 | Antibacterial fiber body shaping clothes |
| CN113151925A (en) * | 2021-04-07 | 2021-07-23 | 罗莱生活科技股份有限公司 | Polyquaternary ammonium salt/aloe antibacterial fiber, preparation method thereof and application thereof in antibacterial towels |
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Application publication date: 20180921 |