CN108559672A - It smears the processing method of tea handmade soap and what is obtained smears tea handmade soap - Google Patents
It smears the processing method of tea handmade soap and what is obtained smears tea handmade soap Download PDFInfo
- Publication number
- CN108559672A CN108559672A CN201810522277.9A CN201810522277A CN108559672A CN 108559672 A CN108559672 A CN 108559672A CN 201810522277 A CN201810522277 A CN 201810522277A CN 108559672 A CN108559672 A CN 108559672A
- Authority
- CN
- China
- Prior art keywords
- handmade soap
- tea
- processing method
- smearing
- water
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/005—Synthetic soaps
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/04—Topical preparations for affording protection against sunlight or other radiation; Topical sun tanning preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D13/00—Making of soap or soap solutions in general; Apparatus therefor
- C11D13/14—Shaping
- C11D13/16—Shaping in moulds
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/48—Medical, disinfecting agents, disinfecting, antibacterial, germicidal or antimicrobial compositions
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/02—Compositions of detergents based essentially on soap on alkali or ammonium soaps
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/38—Products in which the composition is not well defined
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Organic Chemistry (AREA)
- Wood Science & Technology (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Animal Behavior & Ethology (AREA)
- Veterinary Medicine (AREA)
- Public Health (AREA)
- General Health & Medical Sciences (AREA)
- Dermatology (AREA)
- Detergent Compositions (AREA)
Abstract
The invention discloses a kind of processing method for smearing tea handmade soap and what is obtained smear tea handmade soap, and wherein processing method includes：Dispensing：Quantitatively weigh grease, alkali and water；Saponification：Alkali is dissolved in water, is mixed afterwards with grease, is added thereto and is smeared tea and reacted；Curing molding：Reaction solution obtained by the reaction is poured into mold, is dried, obtains smearing tea handmade soap.Smearing in the application adds in tea handmade soap smears tea so that the handmade soap also has the function of resisting and even eliminate computer radiation hazradial bundle other than with basic cleaning action.
Description
Technical field
The present invention relates to handmade soap fields, and in particular to smears the processing method of tea handmade soap and what is obtained smears tea handmade soap.
Background technology
As people are continuously increased cleaning supplies demand, different cleaning supplies are also produced therewith in the market, but
It is such as facial cleanser, hand cleanser and various perfumed soaps etc., but more additive may be added in its process, with
Requirement of the people to health environment-friendly constantly improves, and handmade soap is increasingly liked by people.Along with people opponent's electromechanics
The dependence of the electronic products such as brain leads to the time radiated and slight constantly increase, skin aging fixture, therefore one kind can subtract
The handmade soap gently radiated can be liked by consumers in general.
Invention content
The purpose of the present invention is to provide a kind of processing method for smearing tea handmade soap and what is obtained smear tea handmade soap, solves existing
The problem of having a large amount of additives that refuel in the cleaning supplies such as perfumed soap, cannot be satisfied the requirement of consumer health's environmental protection concept.
In order to solve the above technical problems, the present invention uses following technical scheme：
A kind of processing method for smearing tea handmade soap, including：
Dispensing：Quantitatively weigh grease, alkali and water；
Saponification：Alkali is dissolved in water, is mixed afterwards with grease, is added thereto and is smeared tea and reacted；
Curing molding：Reaction solution obtained by the reaction is poured into mold, is dried, obtains smearing tea handmade soap.
Preferably, the alkali is sodium hydroxide and/or potassium hydroxide, the molar ratio of the grease and alkali is 1:3-
3.5。
Preferably, the mass ratio of the alkali and water is 1:2.4-2.8.
Preferably, in the saponification step, reaction temperature is 70-80 degrees Celsius, and stir speed (S.S.) is 8-15 revolutions per minute
Clock, reaction time are 4-6 hours.
Preferably, the 2-5% for smearing tea and accounting for raw material gross weight.
Preferably, the tea of smearing is to take the intraday tealeaves of picking, steam beating is carried out to it, then dry, mill
Powder；
Wherein, steam beating temperature is 160-180 degrees Celsius, humidity 80-83%, time are 6-8 minutes.
Preferably, before the drying, microwave de-enzyming, the microwave de-enzyming also are carried out to the tealeaves after steam beating
Time is 3~4 minutes.
Preferably, squeezing the tea cake after the steam beating and/or microwave de-enzyming, isolate wherein
Liquid phase, used as the water in batching step；The solid phase isolated is dried.
Preferably, the step of drying is carried out according to following operation successively：
It is 10-20 hours dry at 18-25 degrees Celsius；
60-70 degrees Celsius and surely temperature 10-20 hours are raised the temperature to the rate of 1-2 centigrade per minutes；
It is cooled to 18-25 degrees Celsius with the rate of 1-2 centigrade per minutes, ventilation is subsequently placed in and dries 10 days or more.
One kind smearing tea handmade soap, processes to obtain according to the above-mentioned processing method for smearing tea handmade soap.
Compared with prior art, beneficial effects of the present invention are at least one of following：
Smearing in tea handmade soap process in the application, defines the ratio of raw material and the temperature of reaction, stir speed (S.S.), to
Accelerate the completeness of the rate and reaction of reflection, improves efficiency and quality.
It adds thereto and smears tea so that the handmade soap also has and resists even other than with basic cleaning action
It is the effect for eliminating computer radiation hazradial bundle.
Collect water-removing during tealeaves be lost in moisture, for dissolving alkali, and will smear tea in good fortune step just and raw material
Mixing, the multiple beneficial ingredient smeared in tea can adequately be reacted with raw material, be uniformly dispersed in system as possible.
In curing molding step, handmade soap is dried using gradient increased temperature and gradient cooling, rate of drying is fast, and energy
Enough make internal moisture quickly to external diffusion, so as to get handmade soap inside and outside degree of drying it is consistent, prevent dry tack free internal moisture
The excessive situation of content.
Specific implementation mode
In order to make the purpose , technical scheme and advantage of the present invention be clearer, with reference to embodiments, to the present invention
It is further elaborated.It should be appreciated that the specific embodiments described herein are merely illustrative of the present invention, it is not used to
Limit the present invention.
Embodiment 1：
It present embodiments provides a kind of processing method that smearing tea handmade soap and what this method obtained smears tea handmade soap, wherein processing
Method includes：
Dispensing：Quantitatively weigh grease, sodium hydroxide, water, wherein the molar ratio of grease and sodium hydroxide is 1:3, sodium hydroxide with
The mass ratio of water is 1:2.4；
Saponification：Sodium hydroxide is dissolved in water, is mixed afterwards with grease, is added thereto and is accounted for the tea of smearing of raw material gross weight 2% and go forward side by side
Row reaction, reaction temperature are 70 degrees Celsius, and stir speed (S.S.) is 15 rpms, and the reaction time is 4 hours；Wherein, described to smear tea
It is to take the intraday tealeaves of picking, steam beating and microwave de-enzyming is carried out to it, steam beating temperature is 160 degrees Celsius, humidity
It it is 8 minutes for 80%, time, the microwave de-enzyming time is 3 minutes；Then to after the steam beating and microwave de-enzyming
Tea cake squeezed, isolate liquid phase therein, used as the water in batching step；The solid phase isolated is dried
Milling；
Curing molding：Reaction solution obtained by the reaction is poured into mold, is dried, obtains smearing tea handmade soap, wherein described to dry step
Suddenly it is carried out successively according to following operation：
It is 20 hours dry at 18 degrees Celsius；
60 degrees Celsius and surely temperature 20 hours are raised the temperature to the rate of 1 centigrade per minute；
18 degrees Celsius are cooled to the rate of 1 centigrade per minute, ventilation is subsequently placed in and dries 10 days.
Embodiment 2：
It present embodiments provides a kind of processing method that smearing tea handmade soap and what this method obtained smears tea handmade soap, wherein processing
Method includes：
Dispensing：Quantitatively weigh grease, potassium hydroxide, water, wherein the molar ratio of grease and potassium hydroxide is 1:3.5, hydroxide
The mass ratio of potassium and water is 1: 2.8；
Saponification：Potassium hydroxide is dissolved in water, is mixed afterwards with grease, is added thereto and is accounted for the tea of smearing of raw material gross weight 5% and go forward side by side
Row reaction, reaction temperature are 80 degrees Celsius, and stir speed (S.S.) is 8 rpms, and the reaction time, wherein for 6 hours the tea of smearing was
The intraday tealeaves of picking is taken, steam beating and microwave de-enzyming are carried out to it, steam beating temperature is 180 degrees Celsius, humidity is
83%, the time is 6 minutes, and the microwave de-enzyming time is 4 minutes；Then to after the steam beating and microwave de-enzyming
Tea cake is squeezed, and liquid phase therein is isolated, and is used as the water in batching step；Mill is dried to the solid phase isolated
Powder；
Curing molding：Reaction solution obtained by the reaction is poured into mold, is dried, obtains smearing tea handmade soap, wherein described to dry step
Suddenly it is carried out successively according to following operation：
It is 10 hours dry at 25 degrees Celsius；
70 degrees Celsius and surely temperature 10 hours are raised the temperature to the rate of 2 centigrade per minutes；
25 degrees Celsius are cooled to the rate of 2 centigrade per minutes, ventilation is subsequently placed in and dries 10 days.
Embodiment 3：
It present embodiments provides a kind of processing method that smearing tea handmade soap and what this method obtained smears tea handmade soap, wherein processing
Method includes：
Dispensing：Quantitatively weigh grease, sodium hydroxide and potassium hydroxide, water, wherein grease and sodium hydroxide and potassium hydroxide total amount
Molar ratio be 1:The mass ratio of 3-3.5, sodium hydroxide and potassium hydroxide and water is 1:2.6；
Saponification：Sodium hydroxide and potassium hydroxide are dissolved in water, mixed afterwards with grease, is added accounts for raw material gross weight thereto
3.5% smears tea and is reacted, and reaction temperature is 75 degrees Celsius, and stir speed (S.S.) is 11 rpms, and the reaction time is 5 hours；
Wherein, the tea of smearing is to take the intraday tealeaves of picking, steam beating and microwave de-enzyming is carried out to it, steam beating temperature is
170 degrees Celsius, humidity 81%, time be 7 minutes, the microwave de-enzyming time is 3.5 minutes；Then to passing through the steam
Tea cake after water-removing and microwave de-enzyming is squeezed, and is isolated liquid phase therein, is used as the water in batching step；To separation
Milling is dried in the solid phase gone out；
Curing molding：Reaction solution obtained by the reaction is poured into mold, is dried, obtains smearing tea handmade soap, wherein described to dry step
Suddenly it is carried out successively according to following operation：
It is 15 hours dry at 21 degrees Celsius；
65 degrees Celsius and surely temperature 15 hours are raised the temperature to the rate of 1.5 centigrade per minutes；
21 degrees Celsius are cooled to the rate of 1.5 centigrade per minutes, ventilation is subsequently placed in and dries 10 days.
The properties such as the appearance for smearing tea handmade soap obtained to tri- kinds of methods of embodiment 1-3 are identified, outside obtained soap body
It sees：Writing clear patterns, soap type rectify, uniform color, it is smooth it is fine and smooth, without apparent impurity and stain；And there are stable tea perfume, object
Bad smell.It is emphasized that the time of normal handmade soap drying is very long, and it is most short also to take one month, if increasing temperature
Degree is wanted to shorten the dry time, then very likely results in the non-uniform situation of moisture distribution inside and outside soap body.The application is using ladder
Degree heating and cooling are ensureing that moisture distribution is uniform inside and outside soap body, shortens drying time, and surfacing is without splitting
Line.
Although reference be made herein to invention has been described for multiple explanatory embodiments of the invention, however, it is to be understood that ability
Field technique personnel can be designed that a lot of other modification and implementations, these modifications and implementations will be fallen in the application public affairs
Within the scope and spirit opened.It more specifically, within the scope of the present disclosure and claims, can be to theme group
The building block and/or layout for closing layout carry out a variety of variations and modifications.In addition to the deformation carried out to building block and/or layout
Outer with improving, to those skilled in the art, other purposes also will be apparent.
Claims (10)
1. a kind of processing method for smearing tea handmade soap, it is characterised in that：Including：
Dispensing：Quantitatively weigh grease, alkali and water；
Saponification：Alkali is dissolved in water, is mixed afterwards with grease, is added thereto and is smeared tea and reacted；
Curing molding：Reaction solution obtained by the reaction is poured into mold, is dried, obtains smearing tea handmade soap.
2. the processing method according to claim 1 for smearing tea handmade soap, which is characterized in that the alkali be sodium hydroxide and/
Or potassium hydroxide, the molar ratio of the grease and alkali is 1:3-3.5.
3. the processing method according to claim 1 for smearing tea handmade soap, which is characterized in that the mass ratio of the alkali and water is
1:2.4-2.8。
4. the processing method according to claim 1 for smearing tea handmade soap, which is characterized in that in the saponification step, reaction
Temperature is 70-80 degrees Celsius, and stir speed (S.S.) is 8-15 rpms, and the reaction time is 4-6 hours.
5. the processing method according to claim 1 for smearing tea handmade soap, which is characterized in that the tea of smearing accounts for raw material gross weight
2-5%.
6. the processing method according to claim 1 for smearing tea handmade soap, which is characterized in that the tea of smearing is to take picking one day
Interior tealeaves carries out steam beating to it, then dry, milling；
Wherein, steam beating temperature is 160-180 degrees Celsius, humidity 80-83%, time are 6-8 minutes.
7. the processing method according to claim 6 for smearing tea handmade soap, which is characterized in that before the drying, also to steaming
Tealeaves after vapour water-removing carries out microwave de-enzyming, and the microwave de-enzyming time is 3~4 minutes.
8. the processing method according to claim 7 for smearing tea handmade soap, which is characterized in that passing through the steam beating
And/or the tea cake after microwave de-enzyming is squeezed, and liquid phase therein is isolated, and is used as the water in batching step；To separation
The solid phase gone out is dried.
9. the processing method according to claim 1 for smearing tea handmade soap, which is characterized in that it is described dry step successively according to
Following operation carries out：
It is 10-20 hours dry at 18-25 degrees Celsius；
60-70 degrees Celsius and surely temperature 10-20 hours are raised the temperature to the rate of 1-2 centigrade per minutes；
It is cooled to 18-25 degrees Celsius with the rate of 1-2 centigrade per minutes, ventilation is subsequently placed in and dries 10 days or more.
10. one kind smearing tea handmade soap, which is characterized in that obtained according to claim 1-9 any one the methods.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810522277.9A CN108559672B (en) | 2018-05-28 | 2018-05-28 | Processing method of matcha handmade soap and matcha handmade soap obtained by processing method |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810522277.9A CN108559672B (en) | 2018-05-28 | 2018-05-28 | Processing method of matcha handmade soap and matcha handmade soap obtained by processing method |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN108559672A true CN108559672A (en) | 2018-09-21 |
| CN108559672B CN108559672B (en) | 2020-08-04 |
Family
ID=63540287
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201810522277.9A Active CN108559672B (en) | 2018-05-28 | 2018-05-28 | Processing method of matcha handmade soap and matcha handmade soap obtained by processing method |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN108559672B (en) |
Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103834505A (en) * | 2014-03-26 | 2014-06-04 | 唐李晨 | Matcha handmade soap |
| CN105400617A (en) * | 2015-12-17 | 2016-03-16 | 宁波工程学院 | Preparation method of cold-formed soap |
| CN106350312A (en) * | 2016-08-18 | 2017-01-25 | 河南中医学院 | Traditional Chinese medicine anti-wrinkle handmade soap |
| CN107418792A (en) * | 2017-06-14 | 2017-12-01 | 崔志强 | Natural handmade soap and preparation method thereof |
| CN107629900A (en) * | 2017-09-27 | 2018-01-26 | 中国林业科学研究院林产化学工业研究所 | A kind of preparation method of cape jasmine whitening anti-acne type craft cold process soap |
| CN107868735A (en) * | 2016-09-28 | 2018-04-03 | 夏安娜 | A kind of retaining whitening handmade soap and preparation method thereof |
| CN107868736A (en) * | 2016-09-28 | 2018-04-03 | 夏安娜 | A kind of antipruritic handmade soap and preparation method thereof |
-
2018
- 2018-05-28 CN CN201810522277.9A patent/CN108559672B/en active Active
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103834505A (en) * | 2014-03-26 | 2014-06-04 | 唐李晨 | Matcha handmade soap |
| CN105400617A (en) * | 2015-12-17 | 2016-03-16 | 宁波工程学院 | Preparation method of cold-formed soap |
| CN106350312A (en) * | 2016-08-18 | 2017-01-25 | 河南中医学院 | Traditional Chinese medicine anti-wrinkle handmade soap |
| CN107868735A (en) * | 2016-09-28 | 2018-04-03 | 夏安娜 | A kind of retaining whitening handmade soap and preparation method thereof |
| CN107868736A (en) * | 2016-09-28 | 2018-04-03 | 夏安娜 | A kind of antipruritic handmade soap and preparation method thereof |
| CN107418792A (en) * | 2017-06-14 | 2017-12-01 | 崔志强 | Natural handmade soap and preparation method thereof |
| CN107629900A (en) * | 2017-09-27 | 2018-01-26 | 中国林业科学研究院林产化学工业研究所 | A kind of preparation method of cape jasmine whitening anti-acne type craft cold process soap |
Also Published As
| Publication number | Publication date |
|---|---|
| CN108559672B (en) | 2020-08-04 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN102125508A (en) | Hair-treating and anti-dandruff shampoo and preparation method thereof | |
| CN103409233A (en) | Processing method for rice bran oil | |
| CN106035598A (en) | Edible casings prepared from collagen and other edible proteins | |
| CN104372611B (en) | A kind of preparation technology who simulates classical Chinese painting on silk historical relic in ancient times | |
| CN103783279A (en) | Food or feed additive produced by debitterizing orange peel, flavedo and shaddock peel, and preparation method of food or feed additive | |
| CN108559672A (en) | It smears the processing method of tea handmade soap and what is obtained smears tea handmade soap | |
| CN107304391A (en) | A kind of blue or green bur essential oil soap and its make method by hand | |
| CN104739717A (en) | Shampoo with linseed extract and preparation method of shampoo with linseed extract | |
| CN102524844A (en) | Preparation method for sugar-free water melon seeds containing prebiotics | |
| CN103911236A (en) | Manufacturing method for camellia dreg perfumed soap | |
| CN109648670A (en) | A kind of moistureproof and mildewproof additive and preparation method and applications are in the manufacture of moistureproof and mildewproof fiberboard | |
| CN105380173A (en) | Ultramicro whole purple sweet potato powder and preparation method thereof | |
| CN106281012A (en) | A kind of damp-proof paint mortar and preparation method thereof | |
| CN105411876B (en) | A kind of Haircare composition and its application | |
| CN103783580A (en) | Method for processing tea-peanut fruits | |
| EP1928257A1 (en) | Process for obtaining a soft white milk-based coating and coating so obtained | |
| CN104357604B (en) | Sheep skin fleece is fabricated to the method for uniform pearl particles frizzle | |
| CN107365643A (en) | A kind of sea-buckthorn renders ancient method cold process soap and preparation method thereof | |
| CN102561046A (en) | Method for manufacturing fragrance down | |
| US2663645A (en) | Method of treating popcorn | |
| CN103230352A (en) | Method for preparing plant extract and hydrolyzed pearl-containing toner composition | |
| CN103549094B (en) | Green tea and wheat seedling chocolates and preparation method thereof | |
| CN108524363A (en) | A kind of shampoo and preparation method thereof improving hair quality | |
| CN107535664A (en) | A kind of tart flavour fruit jelly and preparation method thereof | |
| CN102113989A (en) | Egg cream shampoo and preparation method thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| GR01 | Patent grant | ||
| GR01 | Patent grant |