CN108559244A - The preparation method of rare-earth-based precision equipment cable material - Google Patents
The preparation method of rare-earth-based precision equipment cable material Download PDFInfo
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- CN108559244A CN108559244A CN201810325682.1A CN201810325682A CN108559244A CN 108559244 A CN108559244 A CN 108559244A CN 201810325682 A CN201810325682 A CN 201810325682A CN 108559244 A CN108559244 A CN 108559244A
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L69/00—Compositions of polycarbonates; Compositions of derivatives of polycarbonates
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- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01B—CABLES; CONDUCTORS; INSULATORS; SELECTION OF MATERIALS FOR THEIR CONDUCTIVE, INSULATING OR DIELECTRIC PROPERTIES
- H01B3/00—Insulators or insulating bodies characterised by the insulating materials; Selection of materials for their insulating or dielectric properties
- H01B3/18—Insulators or insulating bodies characterised by the insulating materials; Selection of materials for their insulating or dielectric properties mainly consisting of organic substances
- H01B3/30—Insulators or insulating bodies characterised by the insulating materials; Selection of materials for their insulating or dielectric properties mainly consisting of organic substances plastics; resins; waxes
- H01B3/42—Insulators or insulating bodies characterised by the insulating materials; Selection of materials for their insulating or dielectric properties mainly consisting of organic substances plastics; resins; waxes polyesters; polyethers; polyacetals
- H01B3/421—Polyesters
- H01B3/426—Polycarbonates
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2203/00—Applications
- C08L2203/20—Applications use in electrical or conductive gadgets
- C08L2203/202—Applications use in electrical or conductive gadgets use in electrical wires or wirecoating
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
- C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
Abstract
The invention discloses the preparation methods of rare-earth-based precision equipment cable material, the technique is by vinyltriethoxysilane, polymethylphenyl siloxane fluid, sodium pyrosulfite, cyclosiloxane fatty ester, repefral, manganese acetate, sodium chromate, the raw materials such as hexa be prepared into activation adhesive after with rare earth, ethyl methacrylate, makrolon, polysulfones, polymethyl methacrylate, polyalkylene glycol, rosin resin, barium ferrite, azo-bis-isobutyl cyanide, 6 methoxyl group, 2 naphthaldehyde, hexadienoic acid, diethylene triamine pentaacetic acid, the raw materials such as triethyl phosphate pass through high temperature mixing respectively, magnetic agitation, casting die, stand cooling, water cooling drawing, solid solution aging and etc. rare-earth-based precision equipment cable material is prepared.The rare-earth-based precision equipment cable material being prepared, chemical property is good, material settling out, can be adapted for the use of a variety of precision equipments.
Description
Technical field
The present invention relates to cable material technical fields, and in particular to arrives the preparation side of rare-earth-based precision equipment cable material
Method.
Background technology
Electric wire includes mainly bare wire, electromagnetic wire and electrical equipment and electrical insulated electric conductor, power cable, communication cable and light
Cable.Electric wire refers to the material for electric power, communication and associated transport purposes." electric wire " and " cable " there is no stringent boundaries
Limit.The product that core number is few, product diameter is small, simple in structure is usually known as electric wire, what is do not insulated is known as bare wire, others
Referred to as cable；Conductor cross sectional area larger (being more than 6 square millimeters) is known as big electric wire, and smaller (is less than or equal to 6 squares of millis
Rice) it is known as small electric wire, insulated electric conductor is also known as cotton covered wire.
Cable can be divided into power cable, communication cable and control cable etc. by its purposes.Compared with overhead line, cable it is excellent
Point is that insulation distance is small between line, and space is small, and underground laying is without the above space in occupation of land face, not by ambient contamination shadow
It rings, power transmission reliability is high, small to personal safety and ambient enviroment interference.But cost is high, and construction, maintenance are cumbersome, manufacture
It is more complex.Therefore, cable is applied to the dense area of densely populated and power grid and congested in traffic busy place more；It crossing river, crossing the river, seabed
Laying then can avoid using large span overhead line.It is needing to avoid overhead line to the place of Communication Jamming and is needing to consider beautiful
Or avoid the occasion to give away one's position that cable can also be used.
Invention content
In order to solve the above-mentioned technical problem, the invention discloses the preparation method of rare-earth-based precision equipment cable material,
The technique is by vinyltriethoxysilane, polymethylphenyl siloxane fluid, sodium pyrosulfite, cyclosiloxane fatty ester, phthalic acid two
The raw materials such as methyl esters, manganese acetate, sodium chromate, hexa be prepared into activation adhesive after with rare earth, ethyl methacrylate,
Makrolon, polysulfones, polymethyl methacrylate, polyalkylene glycol, rosin resin, barium ferrite, azo-bis-isobutyl cyanide, 6-
The raw materials such as methoxy-2-naphthaldehyde, hexadienoic acid, diethylene triamine pentaacetic acid, triethyl phosphate pass through high temperature mixing, magnetic respectively
Power stirring, casting die, stand cooling, water cooling drawing, solid solution aging and etc. rare-earth-based precision equipment cable is prepared
Material.The rare-earth-based precision equipment cable material being prepared, chemical property is good, material settling out, can be adapted for more
The use of kind precision equipment.
Technical solution：To solve the above-mentioned problems, the present invention provides the preparations of rare-earth-based precision equipment cable material
Method includes the following steps：
（1）By 5-10 parts of rare earth, 15-20 parts of ethyl methacrylate, 10-20 parts of makrolon, 5-10 parts of polysulfones, poly- methyl-prop
7-15 parts of e pioic acid methyl ester, 4-9 parts of polyalkylene glycol, 5-9 parts of rosin resin, 3-7 parts of barium ferrite, azo-bis-isobutyl cyanide 4-8
Part, 2-6 parts of 6- methoxy-2-naphthaldehydes, 3-5 parts of hexadienoic acid, 1-4 parts of diethylene triamine pentaacetic acid, 2-3 parts of triethyl phosphate
Mixing, is added to and is preheated in 65 DEG C of glycerite in advance, inject mixer after stirring evenly together, temperature is increased to 550-
620 DEG C, pyroreaction 60-75 minutes, be cooled to 230 DEG C it is spare；
（2）By 3 parts of vinyltriethoxysilane, 1 part of polymethylphenyl siloxane fluid, 4 parts of sodium pyrosulfite, 2 parts of cyclosiloxane fatty ester,
5 parts of repefral, 1 part of manganese acetate, 2 parts of sodium chromate, 4 parts of hexa carry out ultrasound point after mixing
It dissipates, prepares activation adhesive；
（3）By step（2）Activation adhesive be added to step（1）Mixture in, be uniformly mixed, then by mixture
It is cast to standing cooling in mold and obtains ingot casting；
（4）By step（3）Ingot casting extruding be drawn into linear or sheet, then carry out solid solution and at the beginning of timeliness obtains cable material
Product；
（5）By step（4）Cable material first product cut, plastotype, packaging are got product.
Preferably, the step（1）In heating rate be 60 DEG C/min.
Preferably, the step（2）In supersound process frequency be 50-60KHz, power 500-800W, when ultrasonic
Between be 20-45 minutes.
Preferably, the step（3）In stirring use bilateral flow electromagnetic agitation, frequency 20-35Hz.
Preferably, the step（4）In drawing process use Water Cooling Technology, temperature be 0-4 DEG C.
Preferably, the step（4）In solid solubility temperature be 500-520 DEG C, time 12-15h.
Preferably, the step（4）In heat treatment timeliness be 170-175 DEG C, time 4-8h.
Compared with prior art, the present invention advantage is：
（1）The preparation method of the rare-earth-based precision equipment cable material of the present invention is by vinyltriethoxysilane, benzyl
Silicone oil, sodium pyrosulfite, cyclosiloxane fatty ester, repefral, manganese acetate, sodium chromate, hexa etc.
Raw material is prepared into after activation adhesive and rare earth, ethyl methacrylate, makrolon, polysulfones, polymethyl methacrylate, poly-
Aklylene glycol, rosin resin, barium ferrite, azo-bis-isobutyl cyanide, 6- methoxy-2-naphthaldehydes, hexadienoic acid, divinyl three
The raw materials such as five acetic acid of amine, triethyl phosphate pass through high temperature mixing, magnetic agitation, casting die, stand cooling, water cooling drawing respectively
Pull out, solid solution aging and etc. rare-earth-based precision equipment cable material is prepared.The rare-earth-based precision equipment being prepared is used
Cable material, chemical property is good, material settling out, can be adapted for the use of a variety of precision equipments.
（2）The rare-earth-based precision equipment of the present invention is easy to get with cable material feedstock, is simple for process, is suitable for heavy industrialization
With highly practical.
Specific implementation mode
Embodiment 1
（1）By 5 parts of rare earth, 15 parts of ethyl methacrylate, 10 parts of makrolon, 5 parts of polysulfones, 7 parts of polymethyl methacrylate,
4 parts of polyalkylene glycol, 5 parts of rosin resin, 3 parts of barium ferrite, 4 parts of azo-bis-isobutyl cyanide, 2 parts of 6- methoxy-2-naphthaldehydes,
2 parts of 3 parts of hexadienoic acid, 1 part of diethylene triamine pentaacetic acid, triethyl phosphate mixing, it is molten to be added to the advance glycerine for being preheated to 65 DEG C
In liquid, mixer is injected after stirring evenly together, temperature is increased to 550 DEG C, and heating rate is 60 DEG C/min, and pyroreaction 60 is divided
Clock, be cooled to 230 DEG C it is spare；
（2）By 3 parts of vinyltriethoxysilane, 1 part of polymethylphenyl siloxane fluid, 4 parts of sodium pyrosulfite, 2 parts of cyclosiloxane fatty ester,
5 parts of repefral, 1 part of manganese acetate, 2 parts of sodium chromate, 4 parts of hexa carry out ultrasound point after mixing
It dissipates, the frequency of supersound process is 50KHz, and power 500W, ultrasonic time is 20 minutes, prepares activation adhesive；
（3）By step（2）Activation adhesive be added to step（1）Mixture in, be uniformly mixed, stirring is using two-way
Then mixture is cast to standing cooling in mold and obtains ingot casting by convection current electromagnetic agitation, frequency 20Hz；
（4）By step（3）Ingot casting extruding be drawn into linear or sheet, it is 0-4 DEG C that drawing process, which uses Water Cooling Technology, temperature,
Then it carries out solid solution and timeliness obtains cable material first product, solid solubility temperature is 500 DEG C, time 12h, and heat treatment timeliness is 170
DEG C, time 4h；
（5）By step（4）Cable material first product cut, plastotype, packaging are got product.
The performance test results of rare-earth-based precision equipment cable material obtained are as shown in table 1.
Embodiment 2
（1）By 7 parts of rare earth, 16 parts of ethyl methacrylate, 14 parts of makrolon, 7 parts of polysulfones, 9 parts of polymethyl methacrylate,
5 parts of polyalkylene glycol, 6 parts of rosin resin, 5 parts of barium ferrite, 6 parts of azo-bis-isobutyl cyanide, 3 parts of 6- methoxy-2-naphthaldehydes,
2 parts of 4 parts of hexadienoic acid, 2 parts of diethylene triamine pentaacetic acid, triethyl phosphate mixing, it is molten to be added to the advance glycerine for being preheated to 65 DEG C
In liquid, mixer is injected after stirring evenly together, temperature is increased to 560 DEG C, and heating rate is 60 DEG C/min, and pyroreaction 65 is divided
Clock, be cooled to 230 DEG C it is spare；
（2）By 3 parts of vinyltriethoxysilane, 1 part of polymethylphenyl siloxane fluid, 4 parts of sodium pyrosulfite, 2 parts of cyclosiloxane fatty ester,
5 parts of repefral, 1 part of manganese acetate, 2 parts of sodium chromate, 4 parts of hexa carry out ultrasound point after mixing
It dissipates, the frequency of supersound process is 52KHz, and power 600W, ultrasonic time is 25 minutes, prepares activation adhesive；
（3）By step（2）Activation adhesive be added to step（1）Mixture in, be uniformly mixed, stirring is using two-way
Then mixture is cast to standing cooling in mold and obtains ingot casting by convection current electromagnetic agitation, frequency 25Hz；
（4）By step（3）Ingot casting extruding be drawn into linear or sheet, it is 0-4 DEG C that drawing process, which uses Water Cooling Technology, temperature,
Then it carries out solid solution and timeliness obtains cable material first product, solid solubility temperature is 505 DEG C, time 13h, and heat treatment timeliness is 172
DEG C, time 5h；
（5）By step（4）Cable material first product cut, plastotype, packaging are got product.
The performance test results of rare-earth-based precision equipment cable material obtained are as shown in table 1.
Embodiment 3
（1）By 9 parts of rare earth, 18 parts of ethyl methacrylate, 19 parts of makrolon, 8 parts of polysulfones, polymethyl methacrylate 14
Part, 8 parts of polyalkylene glycol, 8 parts of rosin resin, 6 parts of barium ferrite, 7 parts of azo-bis-isobutyl cyanide, 6- methoxy-2-naphthaldehydes 5
3 parts of part, 4 parts of hexadienoic acid, 3 parts of diethylene triamine pentaacetic acid, triethyl phosphate mixing, are added to the advance glycerine for being preheated to 65 DEG C
In solution, mixer is injected after stirring evenly together, temperature is increased to 590 DEG C, and heating rate is 60 DEG C/min, pyroreaction 70
Minute, be cooled to 230 DEG C it is spare；
（2）By 3 parts of vinyltriethoxysilane, 1 part of polymethylphenyl siloxane fluid, 4 parts of sodium pyrosulfite, 2 parts of cyclosiloxane fatty ester,
5 parts of repefral, 1 part of manganese acetate, 2 parts of sodium chromate, 4 parts of hexa carry out ultrasound point after mixing
It dissipates, the frequency of supersound process is 55KHz, and power 700W, ultrasonic time is 35 minutes, prepares activation adhesive；
（3）By step（2）Activation adhesive be added to step（1）Mixture in, be uniformly mixed, stirring is using two-way
Then mixture is cast to standing cooling in mold and obtains ingot casting by convection current electromagnetic agitation, frequency 30Hz；
（4）By step（3）Ingot casting extruding be drawn into linear or sheet, it is 0-4 DEG C that drawing process, which uses Water Cooling Technology, temperature,
Then it carries out solid solution and timeliness obtains cable material first product, solid solubility temperature is 515 DEG C, time 14h, and heat treatment timeliness is 174
DEG C, time 7h；
（5）By step（4）Cable material first product cut, plastotype, packaging are got product.
The performance test results of rare-earth-based precision equipment cable material obtained are as shown in table 1.
Embodiment 4
（1）By 10 parts of rare earth, 20 parts of ethyl methacrylate, 20 parts of makrolon, 10 parts of polysulfones, polymethyl methacrylate 15
Part, 9 parts of polyalkylene glycol, 9 parts of rosin resin, 7 parts of barium ferrite, 8 parts of azo-bis-isobutyl cyanide, 6- methoxy-2-naphthaldehydes 6
3 parts of part, 5 parts of hexadienoic acid, 4 parts of diethylene triamine pentaacetic acid, triethyl phosphate mixing, are added to the advance glycerine for being preheated to 65 DEG C
In solution, mixer is injected after stirring evenly together, temperature is increased to 620 DEG C, and heating rate is 60 DEG C/min, pyroreaction 75
Minute, be cooled to 230 DEG C it is spare；
（2）By 3 parts of vinyltriethoxysilane, 1 part of polymethylphenyl siloxane fluid, 4 parts of sodium pyrosulfite, 2 parts of cyclosiloxane fatty ester,
5 parts of repefral, 1 part of manganese acetate, 2 parts of sodium chromate, 4 parts of hexa carry out ultrasound point after mixing
It dissipates, the frequency of supersound process is 60KHz, and power 800W, ultrasonic time is 45 minutes, prepares activation adhesive；
（3）By step（2）Activation adhesive be added to step（1）Mixture in, be uniformly mixed, stirring is using two-way
Then mixture is cast to standing cooling in mold and obtains ingot casting by convection current electromagnetic agitation, frequency 35Hz；
（4）By step（3）Ingot casting extruding be drawn into linear or sheet, it is 0-4 DEG C that drawing process, which uses Water Cooling Technology, temperature,
Then it carries out solid solution and timeliness obtains cable material first product, solid solubility temperature is 520 DEG C, time 15h, and heat treatment timeliness is 175
DEG C, time 8h；
（5）By step（4）Cable material first product cut, plastotype, packaging are got product.
The performance test results of rare-earth-based precision equipment cable material obtained are as shown in table 1.
Comparative example 1
（1）By 15 parts of ethyl methacrylate, 10 parts of makrolon, 5 parts of polysulfones, 7 parts of polymethyl methacrylate, polyalkylene
4 parts of glycol, 5 parts of rosin resin, 3 parts of barium ferrite, 4 parts of azo-bis-isobutyl cyanide, 2 parts of 6- methoxy-2-naphthaldehydes, hexadienoic acid
3 parts, 1 part of diethylene triamine pentaacetic acid, the mixing of 2 parts of triethyl phosphate, be added to and be preheated in 65 DEG C of glycerite in advance, stirring
Mixer is injected after uniformly together, temperature is increased to 550 DEG C, and heating rate is 60 DEG C/min, and pyroreaction 60 minutes is cooled to
230 DEG C spare；
（2）By 3 parts of vinyltriethoxysilane, 1 part of polymethylphenyl siloxane fluid, 4 parts of sodium pyrosulfite, 2 parts of cyclosiloxane fatty ester,
5 parts of repefral, 1 part of manganese acetate, 2 parts of sodium chromate, 4 parts of hexa carry out ultrasound point after mixing
It dissipates, the frequency of supersound process is 50KHz, and power 500W, ultrasonic time is 20 minutes, prepares activation adhesive；
（3）By step（2）Activation adhesive be added to step（1）Mixture in, be uniformly mixed, stirring is using two-way
Then mixture is cast to standing cooling in mold and obtains ingot casting by convection current electromagnetic agitation, frequency 20Hz；
（4）By step（3）Ingot casting extruding be drawn into linear or sheet, it is 0-4 DEG C that drawing process, which uses Water Cooling Technology, temperature,
Then it carries out solid solution and timeliness obtains cable material first product, solid solubility temperature is 500 DEG C, time 12h, and heat treatment timeliness is 170
DEG C, time 4h；
（5）By step（4）Cable material first product cut, plastotype, packaging are got product.
The performance test results of rare-earth-based precision equipment cable material obtained are as shown in table 1.
Comparative example 2
（1）By 10 parts of rare earth, 20 parts of ethyl methacrylate, 20 parts of makrolon, 10 parts of polysulfones, polymethyl methacrylate 15
Part, 9 parts of polyalkylene glycol, 9 parts of rosin resin, 8 parts of azo-bis-isobutyl cyanide, 6 parts of 6- methoxy-2-naphthaldehydes, hexadienoic acid 5
4 parts of part, diethylene triamine pentaacetic acid mixing, are added to and are preheated in 65 DEG C of glycerite in advance, injected together after stirring evenly
Mixer, temperature are increased to 620 DEG C, and heating rate is 60 DEG C/min, pyroreaction 75 minutes, be cooled to 230 DEG C it is spare；
（2）By 3 parts of vinyltriethoxysilane, 1 part of polymethylphenyl siloxane fluid, 4 parts of sodium pyrosulfite, 2 parts of cyclosiloxane fatty ester,
5 parts of repefral, 1 part of manganese acetate, 2 parts of sodium chromate, 4 parts of hexa carry out ultrasound point after mixing
It dissipates, the frequency of supersound process is 60KHz, and power 800W, ultrasonic time is 45 minutes, prepares activation adhesive；
（3）By step（2）Activation adhesive be added to step（1）Mixture in, be uniformly mixed, stirring is using two-way
Then mixture is cast to standing cooling in mold and obtains ingot casting by convection current electromagnetic agitation, frequency 35Hz；
（4）By step（3）Ingot casting extruding be drawn into linear or sheet, it is 0-4 DEG C that drawing process, which uses Water Cooling Technology, temperature,
Then it carries out solid solution and timeliness obtains cable material first product, solid solubility temperature is 520 DEG C, time 15h, and heat treatment timeliness is 175
DEG C, time 8h；
（5）By step（4）Cable material first product cut, plastotype, packaging are got product.
The performance test results of rare-earth-based precision equipment cable material obtained are as shown in table 1.
The rare-earth-based precision equipment obtained of embodiment 1-4 and comparative example 1-2 is carried out surface respectively with cable material to split
This several line rate, elongation at break, creep-resistant property performance tests.
Table 1
| Face crack rate（%） | Elongation at break（%） | Creep-resistant property % | |
| Embodiment 1 | 10.70 | 450 | 350 |
| Embodiment 2 | 11.03 | 470 | 365 |
| Embodiment 3 | 10.90 | 480 | 355 |
| Embodiment 4 | 11.14 | 440 | 360 |
| Comparative example 1 | 20.60 | 210 | 270 |
| Comparative example 2 | 29.27 | 260 | 220 |
The preparation method of the rare-earth-based precision equipment cable material of the present invention is by vinyltriethoxysilane, benzyl silicon
The originals such as oil, sodium pyrosulfite, cyclosiloxane fatty ester, repefral, manganese acetate, sodium chromate, hexa
Material is prepared into after activation adhesive and rare earth, ethyl methacrylate, makrolon, polysulfones, polymethyl methacrylate, poly- Asia
Alkyl diol, rosin resin, barium ferrite, azo-bis-isobutyl cyanide, 6- methoxy-2-naphthaldehydes, hexadienoic acid, diethylenetriamine
The raw materials such as five acetic acid, triethyl phosphate respectively pass through high temperature mixing, magnetic agitation, casting die, stand cooling, water cooling drawing,
Solid solution aging and etc. rare-earth-based precision equipment cable material is prepared.The rare-earth-based precision equipment cable being prepared
Material, chemical property is good, material settling out, can be adapted for the use of a variety of precision equipments.The rare-earth-based of the present invention is accurate
If cable in stock material feedstock is easy to get, is simple for process, it is suitable for heavy industrialization and uses, it is highly practical.
Example the above is only the implementation of the present invention is not intended to limit the scope of the invention, every to utilize this hair
Equivalent structure or equivalent flow shift made by bright description is applied directly or indirectly in other relevant technology necks
Domain is included within the scope of the present invention.
Claims (7)
1. the preparation method of rare-earth-based precision equipment cable material, which is characterized in that include the following steps：
（1）By 5-10 parts of rare earth, 15-20 parts of ethyl methacrylate, 10-20 parts of makrolon, 5-10 parts of polysulfones, poly- methyl-prop
7-15 parts of e pioic acid methyl ester, 4-9 parts of polyalkylene glycol, 5-9 parts of rosin resin, 3-7 parts of barium ferrite, azo-bis-isobutyl cyanide 4-8
Part, 2-6 parts of 6- methoxy-2-naphthaldehydes, 3-5 parts of hexadienoic acid, 1-4 parts of diethylene triamine pentaacetic acid, 2-3 parts of triethyl phosphate
Mixing, is added to and is preheated in 65 DEG C of glycerite in advance, inject mixer after stirring evenly together, temperature is increased to 550-
620 DEG C, pyroreaction 60-75 minutes, be cooled to 230 DEG C it is spare；
（2）By 3 parts of vinyltriethoxysilane, 1 part of polymethylphenyl siloxane fluid, 4 parts of sodium pyrosulfite, 2 parts of cyclosiloxane fatty ester,
5 parts of repefral, 1 part of manganese acetate, 2 parts of sodium chromate, 4 parts of hexa carry out ultrasound point after mixing
It dissipates, prepares activation adhesive；
（3）By step（2）Activation adhesive be added to step（1）Mixture in, be uniformly mixed, then by mixture
It is cast to standing cooling in mold and obtains ingot casting；
（4）By step（3）Ingot casting extruding be drawn into linear or sheet, then carry out solid solution and at the beginning of timeliness obtains cable material
Product；
（5）By step（4）Cable material first product cut, plastotype, packaging are got product.
2. the preparation method of rare-earth-based precision equipment cable material according to claim 1, which is characterized in that the step
Suddenly（1）In heating rate be 60 DEG C/min.
3. the preparation method of rare-earth-based precision equipment cable material according to claim 1, which is characterized in that the step
Suddenly（2）In supersound process frequency be 50-60KHz, power 500-800W, ultrasonic time be 20-45 minutes.
4. the preparation method of rare-earth-based precision equipment cable material according to claim 1, which is characterized in that the step
Suddenly（3）In stirring use bilateral flow electromagnetic agitation, frequency 20-35Hz.
5. the preparation method of rare-earth-based precision equipment cable material according to claim 1, which is characterized in that the step
Suddenly（4）In drawing process use Water Cooling Technology, temperature be 0-4 DEG C.
6. the preparation method of rare-earth-based precision equipment cable material according to claim 1, which is characterized in that the step
Suddenly（4）In solid solubility temperature be 500-520 DEG C, time 12-15h.
7. the preparation method of rare-earth-based precision equipment cable material according to claim 1, which is characterized in that the step
Suddenly（4）In heat treatment timeliness be 170-175 DEG C, time 4-8h.
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN110433757A (en) * | 2019-08-22 | 2019-11-12 | 安徽比特海新材料股份有限公司 | A kind of polymeric kettle of polymethylphenyl siloxane fluid automatic charging |
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