CN108550692A - A kind of adjustable magneto-electric coupled composite material and preparation method of resonance mode - Google Patents
A kind of adjustable magneto-electric coupled composite material and preparation method of resonance mode Download PDFInfo
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- CN108550692A CN108550692A CN201810276137.8A CN201810276137A CN108550692A CN 108550692 A CN108550692 A CN 108550692A CN 201810276137 A CN201810276137 A CN 201810276137A CN 108550692 A CN108550692 A CN 108550692A
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- H10N35/00—Magnetostrictive devices
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Abstract
The present invention proposes a kind of with the adjustable magneto-electric coupled composite material and preparation method of resonance mode.It is a kind of a kind of compound magnetoelectric material for the cantilever beam structure for being fixed on T-type structure glass substrate and being formed after being formed by stacking by direct magnetostriction material, piezoelectric material and negative magnetostriction material layer, and the thickness ratio of positive and negative magnetostriction materials is 1:0.4~2.Under high or low bias magnetic field effect, with positive and negative magnetostriction layer thickness than difference, resonance mode can also change.In the preparation, positive and negative magnetostrictive layer different-thickness ratio is adjusted, different resonance modes can be obtained.The present invention magneto-electric coupled material single compared to other resonance modes, by changing positive and negative magnetostriction layer thickness ratio, the resonance mode of magnetoelectric effect is effectively regulated and controled, the enhancing of multifrequency magnetoelectric effect can be realized under more resonance modes, to contribute for the development of multifrequency device.
Description
Technical field
The present invention relates to a kind of composite material and its technology of preparing with magnetoelectric effect, more particularly to one kind have
The adjustable magneto-electric coupled composite material and preparation method of resonance mode.
Background technology
Compound magnetoelectric material is the material for having magnetoelectric effect, with good magnetic energy and electric transformation of energy work(
Can, electric polarization or magnetization are generated respectively under the action of externally-applied magnetic field either extra electric field.Magnetoelectric material is prepared into magnetic
Electricity Functional device can be applied to the technologies neck such as magnetic field and electric field sensing, magnetoelectronics information storage, current detecting, microwave leakage detection
Domain has many advantages, such as that small, magnetic energy and energy conversion efficiency are high, is easily integrated, being easy to multifunction design, therefore, exploitation
Magnetoelectric material and device with big magnetoelectric effect are valued by people all the time.
Compound magnetoelectric material is mutually compounded to form with ferromagnetic by ferroelectric phase, and ferroelectric phase therein and ferromagnetic phase itself do not have
Magnetoelectric effect, but after the two is compound, ferroelectricity-iron can be made by " product interaction " that two-phase interface stress is medium
Magnetic coexisting body ties up to generates apparent magnetoelectric effect at room temperature.The power of magnetoelectric effect is carried out by magneto-electric coupled coefficient
Characterization, is defined as αE=dE/dH, wherein E is that the electric field of material exports, and H is the external magnetic field that is applied.All the time, it passes through
The unremitting effort of people is crossed, the compound magnetoelectric material of a variety of communicate-type structures and coupled modes nowadays has been developed.Such as 2-2
The CoFe of type lamellar composite magnetoelectric material Terfenol-D/PZT, 0-3 type2O4/ PZT composite materials, etc..But it is most multiple
The order of magnitude of the magneto-electric coupled coefficient of condensation material in mV/cmOe.Later it is found that under the pattern of resonance coupling, compound magnetic
The magneto-electric coupled coefficient of electric material can have apparent increase.Such as M.I.Bichurin [M.I.Bichurin,
D.A.Filippov, et.al.Resonance magnetoelectric effects in layered
Magnetostrictive-piezoelectric composites.PHYSICAL REVIEW B 2003,68:132408-1-
132408-4.] report NiFe2O4Magnetic of/PZT cofiring magnetic electric compound material the disks in single order transverse resonance frequency 320kHz
Piezoelectric voltage coefficient is up to 23V/cmOe.Magnetic electric compound material square under the longitudinal coupled mode of patent ZL03132167.4 reports
Magnetoelectric voltage coefficient of the shape piece in single order longitudinal resonance frequencies about 60kHz has also reached 8.7V/cmOe, etc..Although people
Realize the enhancing of magnetoelectric effect under resonance mode, but its resonance mode is single, can not effectively be regulated and controled, no
Conducive to the development of multifrequency device.
Invention content
The purpose of the present invention is the single deficiencies of the resonance mode for above-mentioned compound magnetoelectric material, provide a kind of with altogether
The adjustable magneto-electric coupled composite material and preparation method of pattern of shaking, structure novel, preparation process are simple, it is intended to by altogether
The regulation and control for pattern of shaking contribute for the theory of multifrequency device and development.
The invention is realized in this way.It is mainly by negative magnetostriction material nickel sheet, piezoelectric material PZT, direct magnetostriction
Material Terfenol-D (Tb1-xDyxFe2) and basal plane composition, it is bonded with direct magnetostriction material in the front of piezoelectric material PZT
Terfenol-D is bonded with negative magnetostriction material nickel sheet in its reverse side, then the either end of piezoelectric material PZT is vertically fixed on
On basal plane, a kind of cantilever beam structure is formed;The thickness ratio of positive and negative magnetostriction materials is 1:0.4~2, wherein Terfenol-D
Along its length, the polarization through-thickness of PZT, nickel magnetostriction is along its length for magnetostriction.
The thickness ratio of the positive and negative magnetostriction materials is 1:0.4, or be 1:1, or be 1:2.
The basal plane material is metal either glass or plastics.
The bonding is epoxy resin with adhesive.
Preparation method specifically includes following steps:
Step 1:With one holder with T-type structure of glass preparation.
Step 2:Choose the identical direct magnetostriction material Terfenol-D of size and negative magnetostriction material nickel sheet each one
Piece, then the PZT pieces of the big 2.5~5mm of both ends size are chosen, first use adhesive by direct magnetostriction material Terfenol-D and pressure
Electric material PZT is bonded together, and both ends leave some space, and then again glues negative magnetostriction material nickel sheet with epobond epoxyn
In the reverse side of PZT, and corresponding with positive Terfenol-D, wherein direct magnetostriction material Terfenol-D and negative magnetostriction
The thickness ratio of material nickel sheet is 1:0.4~2.
Step 3:By the sample in step 2, adhere on a basal plane of T-type structure made from step 1 or other
On basal plane, after being placed to dry, a kind of adjustable magneto-electric coupled composite material of the resonance mode of cantilever beam structure is formed.
When bonding, wherein along its length, the polarization through-thickness of PZT, nickel mangneto is stretched for Terfenol-D magnetostriction
Contracting is along its length.
Following technique effect can be reached using the present invention:
(1) cheap magneto-electric coupled composite material is obtained:Nickel sheet of the present invention, piezoelectric material PZT, rare earth
Alloy Terfenol-D, the industrialization of adhesive epoxy resin, and preparation process is simple.
(2) the adjustable magneto-electric coupled composite material of performance is obtained:Under conditions of quasi-static bias magnetic field, with positive and negative
Magnetostriction materials rare earth alloy Terfenol-D and the thickness of nickel sheet than difference, realize the regulation and control of its magneto-electric coupled performance.
(3) the adjustable magneto-electric coupled composite material of resonance mode is obtained:With positive and negative magnetostriction materials rare earth alloy
The thickness of Terfenol-D and nickel than difference, can further regulate and control its resonance mode.
Description of the drawings
Fig. 1 is the structural schematic diagram of the present invention.
Fig. 2 is the pictorial diagram of the magneto-electric coupled composite material of cantilever beam structure of the present invention.
Fig. 3 is at high bias magnetic field 400Oe, and magneto-electric coupled composite material Terfenol-D/PZT/Ni is in cantilever beam knot
Magneto-electric coupled coefficient relational graph with frequency change under structure.Wherein f1 b,f2 b,f3 bRespectively single order, second order, three rank bending vibrations
The corresponding frequency of pattern peak value, f1 l,f2 l,f3 lRespectively single order, second order, the corresponding frequency of three rank beam mode peak values.
Fig. 4 is at low bias magnetic field -50Oe, and compound magnetoelectric material Terfenol-D/PZT/Ni is under cantilever beam structure
Magneto-electric coupled coefficient relational graph with frequency change.
Specific implementation mode
Embodiment
It is that 0.5mm is constant that the magneto-electric coupled composite material, which keeps the thickness of Terfenol-D, Ni thickness be respectively 0.2mm,
0.5mm, 1mm prepare positive and negative magnetostrictive layer (Terfenol-D and Ni) thickness ratio and do not remain 1:0.4、1:1、1:2
Three kinds of samples.
Step 1:Two pieces of glass slides are taken, it is one of to be cut to long 15mm, wide 5mm, thickness 1mm, i.e. size with glass cutter
For the strip of 15mm × 5mm × 1mm, then the strip sheet glass cut vertically is sticked to separately by using epoxy resin
On one piece of glass slide, a T-type structure is formed, places 48 hours and dries, do 3 altogether.
Step 2:The Terfenol- for being 15mm × 5mm × 0.5mm with size by the PZT that size is 20mm × 5mm × 1mm
D is bonded in the front of PZT with epobond epoxyn, and wherein the two of PZT ends are respectively kept with the part of vacating of 2.5mm, so
The nickel sheet that size is 15mm × 5mm × 0.2mm, 15mm × 5mm × 0.5mm, 15mm × 5mm × 1mm is used into asphalt mixtures modified by epoxy resin respectively afterwards
Fat adhesive is sticked to the reverse side of PZT, and corresponding with positive Terfenol-D, and thickness ratio is made Wei 1:0.4、1:1、1:2
Three samples, place and dry for 48 hours.
Step 3:The sample that step 2 is prepared is adhered to epoxy resin on the T-type glass structure of step 1,
Then it is placed to dry, beam type Terfenol-D/PZT/Ni layered electromagnetics coupling composite material shown in FIG. 1 is finally made
Sample.
The high bias magnetic field for applying 400Oe to the sample obtained by the above method, obtains Terfenol-D/ shown in Fig. 3
PZT/Ni magneto-electric coupled coefficient relational graphs with frequency change under cantilever beam structure.Wherein direct magnetostriction layer Terfenol-D
Thickness is 0.5mm, and negative magnetostriction layer Ni thickness is 0.2mm, 0.5mm, 1mm so that positive and negative magnetostrictive layer thickness ratio is other
It is 1:0.4、1:1、1:2.Under cantilever beam structure, there are six formants in lamellar composite magnetoelectricity structure, including three
Flexural vibrations peak, three length vibration peaks.It is 1 when Ni thickness is the i.e. positive and negative magnetostriction layer thickness ratios of 0.5mm:When 1, second order is curved
Bent vibration peak reaches maximum value, and magneto-electric coupled coefficient is 1.38V/cmOe, and first-order bending vibration peak is greatly lowered, when Ni thickness
It is 1 that degree, which is 1mm, that is, positive and negative magnetostriction layer thickness ratio,:When 2, first-order bending vibration peak reaches maximum value, and magneto-electric coupled coefficient is
1.34V/cmOe, and second order bending vibration intensity is greatly lowered.Under high bias magnetic field, direct magnetostriction layer
The magnetostrictive effect of Terfenol-D is much larger than the magnetostrictive effect of negative magnetostriction layer Ni, thus in PZT and magnetosphere
Layer coupling occur mainly in the interfaces Terfenol-D/PZT, magnetoelectricity voltage signal is dominated by the interface coupling, and lower surface
Ni layers to the contribution very little of magneto-electric coupled signal, and because itself and PZT layers bond together, the Ni layers of negative magnetic shown
It causes flex effect that can compress PZT layers, forms certain clamping action, weaken length vibration coupling;With the increase of Ni thickness, folder
Holding effect should enhance therewith, and clamping effect helps to enhance the especially bending vibration of low-frequency resonance intensity, and it is strong to reduce high-frequency resonance
Degree.So under high bias magnetic field, there is multifrequency resonance in the magnetic electric compound material with cantilever beam structure, and by changing just
Oscillation intensity of the negative magnetostriction layer thickness than different vibration modes can be regulated and controled, with the increasing of negative magnetostriction layer Ni thickness
Add, low frequency bending vibration enhancing.
Unlike expressed above, Fig. 4 is the magneto-electric coupled composite material Terfenol- at low bias magnetic field -50Oe
D/PZT/Ni magneto-electric coupled coefficient relational graphs with frequency change under cantilever beam structure.Wherein direct magnetostriction layer
Terfenol-D thickness is 0.5mm, and negative magnetostriction layer Ni thickness is 0.2mm, 0.5mm, 1mm, positive and negative magnetostriction layer thickness
Than being respectively 1:0.4、1:1、1:2.Under low bias magnetic field, equally there are six formants in layered electromagnetic composite construction,
Include three flexural vibrations peaks, three length vibration peaks, peak position with measured under high bias magnetic field it is consistent.With negative magnetic
The increase of stretchable layer Ni thickness is caused, formant is all to high-frequency mobile.When Ni thickness is 0.2mm, that is, positive and negative magnetostriction layer thickness ratio
It is 1:When 0.4, first-order bending vibration intensity and single order length oscillation intensity are all bigger;When Ni thickness is 0.5mm, that is, positive and negative magnetic
It is 1 to cause flexible layer thickness ratio:When 1, second order bending vibration intensity reaches maximum, and magneto-electric coupled coefficient is 0.75V/cmOe;When
Ni thickness is that the i.e. positive and negative magnetostriction layer thickness ratios of 1mm are 1:When 2, resonance peak intensity is all greatly lowered.In low bias magnetic field
Under, Terfenol-D is suitable with the magnetostrictive effect intensity of Ni, and the magnetostrictive effect of the two is vied each other at this time.Positive and negative magnetic
It is 1 to cause flexible layer thickness ratio:When 0.4, the magnetostrictive effect of Terfenol-D is better than Ni, is mainly risen to PZT for Ni layers at this time
Clamping action;Positive and negative magnetostriction layer thickness ratio is 1:When 1, Terfenol-D is suitable with the magnetostrictive effect of Ni, causes to grow
The stretching vibration in degree direction is greatly lowered, but second order bending vibration intensity improves;Positive and negative magnetostriction layer thickness ratio is 1:2
When, the magnetostrictive effect of Terfenol-D is weaker than the magnetostrictive effect of Ni, and the negative magnetostriction characteristic of Ni is to PZT layers at this time
Play compression, it is suppressed that all high-frequency resonance patterns, only first-order flexure formant have larger intensity.
From among the above it is recognised that lamellar composite magnetoelectricity structure Terfenol-D/PZT/Ni under cantilever beam structure
Six resonant frequencies, including three flexural resonance frequencies, three length resonant frequencies.Under the action of bias magnetic field, with
Positive and negative magnetostriction layer thickness than difference, resonance mode can also change:Under high bias magnetic field 400Oe, positive and negative magnetic
It is 1 to cause flexible layer thickness ratio:When 1, second order bending vibration intensity reaches maximum, and first-order bending vibration intensity is greatly lowered;Just
Negative magnetostriction layer thickness ratio is 1:When 2, first-order bending vibration intensity reaches maximum, and other resonance peak intensities are all significantly
It reduces;Under low bias magnetic field -50Oe, positive and negative magnetostriction layer thickness ratio is 1:When 0.4, first-order bending vibration shakes with single order length
The Oscillation Amplitude of dynamic model formula is all bigger;Positive and negative magnetostriction layer thickness ratio is 1:When 1, second order bending vibration intensity reaches most
Greatly;Positive and negative magnetostriction layer thickness ratio is 1:When 2, first-order bending vibration has maximum intensity value, others resonance peak intensity all big
Amplitude reduction.
Therefore, we can with it is concluded that:In the layered electromagnetic coupling composite material with cantilever beam structure, by changing
Become the thickness ratio of positive and negative magnetostriction materials, effective regulation and control can be realized to the resonance mode of compound magnetoelectric material.
The preferred embodiment of the present invention above described embodiment only expresses, the description thereof is more specific and detailed, but simultaneously
Cannot the limitation to the scope of the claims of the present invention therefore be interpreted as.It should be pointed out that for those of ordinary skill in the art
For, without departing from the inventive concept of the premise, several improvement and replacement can also be made, these belong to the guarantor of the present invention
Protect range.Therefore, the protection domain of patent of the present invention should be determined by the appended claims.Such as direct magnetostriction material with
And negative magnetostriction material, Terfenol-D and Ni are only illustrated as an example, can be changed other direct magnetostrictions into and be born
Magnetostriction materials, such as the metglas of magnetostrictive effect, Ferrite Material only say piezoelectric material as an example
This piezoelectric materials of PZT are illustrated, can equally be changed to the piezoelectric materials such as other barium titanates, lead titanates, lead magnesium niobate titanate.And
For T-type structure, it is only exemplified by glass as an example, it can also be exchanged with the preferable material of some other hardness, such as metal material
Material etc..
Claims (5)
1. a kind of adjustable magneto-electric coupled composite material of resonance mode, it is mainly by negative magnetostriction material nickel sheet, piezoelectric material
Pb(Zr,Ti)O3(PZT), direct magnetostriction material (Terfenol-D) and basal plane composition, it is characterised in that in piezoelectric material PZT
Front be bonded with direct magnetostriction material Terfenol-D, be bonded with negative magnetostriction material nickel sheet in its reverse side, then will pressure
The either end of electric material PZT is vertically fixed on basal plane, forms a kind of cantilever beam structure;The thickness of positive and negative magnetostriction materials
Than being 1:0.4~2, wherein Terfenol-D magnetostriction along its length, the polarization through-thickness of PZT, nickel magnetostriction
Along its length.
2. the adjustable magneto-electric coupled composite material of a kind of resonance mode according to claim 1, it is characterised in that described
The thickness ratio of positive and negative magnetostriction materials is 1:0.4, or be 1:1, or be 1:2.
3. the adjustable magneto-electric coupled composite material of a kind of resonance mode according to claim 1, it is characterised in that described
Basal plane material is metal either glass or plastics.
4. the adjustable magneto-electric coupled composite material of a kind of resonance mode according to claim 1, it is characterised in that described
Bonding is epoxy resin with adhesive.
5. a kind of preparation method of the adjustable magneto-electric coupled composite material of resonance mode, it is characterised in that specifically include following step
Suddenly:
Step 1:With one holder with T-type structure of glass preparation.
Step 2:It chooses the identical direct magnetostriction material Terfenol-D of size and negative magnetostriction material nickel sheet is each a piece of,
The PZT pieces of the big 2.5~5mm of both ends size are chosen again, first use adhesive by direct magnetostriction material Terfenol-D and piezoelectricity
Material PZT is bonded together, and both ends leave some space, and is then again sticked to negative magnetostriction material nickel sheet with epobond epoxyn
The reverse side of PZT, and, wherein direct magnetostriction material Terfenol-D and negative magnetostriction material corresponding with positive Terfenol-D
Expect that the thickness ratio of nickel sheet is 1:0.4~2.
Step 3:By the sample in step 2, adheres on a basal plane of the T-type structure of step 1 or on other basal planes, put
It sets after drying, forms a kind of adjustable magneto-electric coupled composite material of the resonance mode of cantilever beam structure.
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CN109671844A (en) * | 2018-12-28 | 2019-04-23 | 郑州轻工业学院 | A kind of magnetoelectricity gyroscope with high q-factor |
CN110672906A (en) * | 2019-09-25 | 2020-01-10 | 南京理工大学 | Differential current sensor for measuring electrified alternating current straight wire |
CN110794345A (en) * | 2019-11-07 | 2020-02-14 | 青岛大学 | FM/FE/FM multiferroic heterojunction and magnetoelectric coupling sensor |
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CN114251336A (en) * | 2021-11-05 | 2022-03-29 | 湖北塞思博科技有限公司 | Preparation method and detection method of cantilever beam structure magnetoelectric antenna and magnetoelectric antenna |
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CN114251336A (en) * | 2021-11-05 | 2022-03-29 | 湖北塞思博科技有限公司 | Preparation method and detection method of cantilever beam structure magnetoelectric antenna and magnetoelectric antenna |
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