CN108525341B - Plant effective component extraction equipment for preparing medical raw materials - Google Patents

Plant effective component extraction equipment for preparing medical raw materials Download PDF

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Publication number
CN108525341B
CN108525341B CN201810239310.7A CN201810239310A CN108525341B CN 108525341 B CN108525341 B CN 108525341B CN 201810239310 A CN201810239310 A CN 201810239310A CN 108525341 B CN108525341 B CN 108525341B
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crushing
plant
extraction
grinding
ultrasonic
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CN108525341A (en
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孙学中
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Nanjing Zelang Medical Technology Co Ltd
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Nanjing Zelang Medical Technology Co Ltd
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D11/00Solvent extraction
    • B01D11/02Solvent extraction of solids
    • B01D11/0261Solvent extraction of solids comprising vibrating mechanisms, e.g. mechanical, acoustical
    • B01D11/0265Applying ultrasound
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D11/00Solvent extraction
    • B01D11/02Solvent extraction of solids
    • B01D11/0207Control systems
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D11/00Solvent extraction
    • B01D11/02Solvent extraction of solids
    • B01D11/028Flow sheets
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D3/00Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/14Fractional distillation or use of a fractionation or rectification column
    • B01D3/32Other features of fractionating columns ; Constructional details of fractionating columns not provided for in groups B01D3/16 - B01D3/30
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D5/00Condensation of vapours; Recovering volatile solvents by condensation
    • B01D5/0003Condensation of vapours; Recovering volatile solvents by condensation by using heat-exchange surfaces for indirect contact between gases or vapours and the cooling medium
    • B01D5/0006Coils or serpentines
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D9/00Crystallisation
    • B01D9/0018Evaporation of components of the mixture to be separated
    • B01D9/0031Evaporation of components of the mixture to be separated by heating
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B02CRUSHING, PULVERISING, OR DISINTEGRATING; PREPARATORY TREATMENT OF GRAIN FOR MILLING
    • B02CCRUSHING, PULVERISING, OR DISINTEGRATING IN GENERAL; MILLING GRAIN
    • B02C15/00Disintegrating by milling members in the form of rollers or balls co-operating with rings or discs
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B02CRUSHING, PULVERISING, OR DISINTEGRATING; PREPARATORY TREATMENT OF GRAIN FOR MILLING
    • B02CCRUSHING, PULVERISING, OR DISINTEGRATING IN GENERAL; MILLING GRAIN
    • B02C23/00Auxiliary methods or auxiliary devices or accessories specially adapted for crushing or disintegrating not provided for in preceding groups or not specially adapted to apparatus covered by a single preceding group
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B02CRUSHING, PULVERISING, OR DISINTEGRATING; PREPARATORY TREATMENT OF GRAIN FOR MILLING
    • B02CCRUSHING, PULVERISING, OR DISINTEGRATING IN GENERAL; MILLING GRAIN
    • B02C23/00Auxiliary methods or auxiliary devices or accessories specially adapted for crushing or disintegrating not provided for in preceding groups or not specially adapted to apparatus covered by a single preceding group
    • B02C23/18Adding fluid, other than for crushing or disintegrating by fluid energy
    • B02C23/24Passing gas through crushing or disintegrating zone
    • B02C23/30Passing gas through crushing or disintegrating zone the applied gas acting to effect material separation

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Physics & Mathematics (AREA)
  • Food Science & Technology (AREA)
  • Acoustics & Sound (AREA)
  • Mechanical Engineering (AREA)
  • Thermal Sciences (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Automation & Control Theory (AREA)
  • Disintegrating Or Milling (AREA)
  • Extraction Or Liquid Replacement (AREA)

Abstract

The invention discloses plant active ingredient extraction equipment for preparing medicinal raw materials, wherein an ultramicro crushing mechanism is arranged in an installation box, and an active ingredient extraction mechanism is arranged at the lower part of the ultramicro crushing mechanism; the effective component extraction mechanism comprises an extractor and an efficient cleaning device, the extractor comprises an extractor vessel, the bottom of the extractor vessel is connected with a dry powder guide tube and a water slurry guide tube through guide tubes, the upper part of the extractor vessel is connected with an extraction liquid adding box, the extraction liquid adding box is connected with a filling tube, the efficient cleaning device comprises an ultrasonic generator, an ultrasonic transducer and an ultrasonic amplitude-increasing rod, the output end of the ultrasonic generator is electrically connected with the input end of the ultrasonic transducer, the output end of the ultrasonic transducer is electrically connected with the electric energy input end of the ultrasonic amplitude-increasing rod, the ultrasonic amplitude-increasing rod penetrates through the lower bottom surface of the extractor vessel and extends into the extractor vessel, separation of impurities and effective components in plants to be extracted is achieved, and the subsequent step of separating the effective components in.

Description

Plant effective component extraction equipment for preparing medical raw materials
Technical Field
The invention relates to the field of biological pharmacy, in particular to a plant effective component extraction device for preparing a medicine raw material.
Background
The plant extract industry has been developed in the last 20 years and is an emerging industry combining the industries of medicine, fine chemicals and agriculture. The plant extract refers to a substance extracted or processed from a plant (whole or a part of the plant) by using a proper solvent or method, and can be used in the pharmaceutical industry, the food industry, the health industry, the beauty industry and other industries. The plant extract is a product formed by taking plants as raw materials, directionally obtaining and concentrating one or more active ingredients in the plants through a physical and chemical extraction and separation process according to the requirements of the application of an extracted final product, and not changing the structures of the active ingredients. According to different components of the extracted plants, glycoside, acid, polyphenol, polysaccharide, terpenoid, flavone, alkaloid and the like are formed; according to different properties, the plant oil can be divided into vegetable oil, extract, powder, crystalline lens and the like.
The data shows that in the first half 2014, 1074 enterprises in China export plant extract commodities to the outside, and the quantity of the exported plant extract commodities is slightly increased compared with that of the exported enterprises in the same period in the last year. The export account of the civil enterprises is up to 50.4%, the civil enterprises are far ahead, and the contribution is the largest. The percentage of "three-funded" businesses immediately following this is up to 35.4%. The plant extract industry in China is developed for less than 20 years, and people's camp plant extract enterprises grow and develop under the condition of lack of ' care ', so that the challenge of coping with financial ' tsunami ' is continuously strengthened.
Under the influence of new medical models, plant extract products with functionality or activity are gaining favor. At present, the plant extract industry develops more and more rapidly, exceeds the growth rate of the drug market and becomes an independent new industry. With the rise of the plant extract market worldwide, the Chinese plant extract industry must become a new strategic pillar industry for the development of national economy and society.
The plant extract is the main force of export of Chinese medicine commodities, and the export accounts for more than 40 percent of the total export of Chinese medicine products. Although the plant extract industry is an emerging industry, it has developed rapidly over the last two decades. Statistical data show that the export of Chinese plant extracts reaches 11.3 hundred million dollars in 2011, the year-by-year increase is 47%, and the composite increase rate in 2002-2011 reaches 21.91%. Plant extracts are the first commodity category for export of traditional Chinese medicine in excess of 10 billion dollars.
However, the existing method for separating and extracting the effective components of the plants has the following defects:
(1) in the prior art, in the process of separating and extracting effective components of plants, because the plants are not crushed sufficiently, the crushed particles of the plants are large, and the crushed particles of the plants are not in sufficient contact with a leaching solution, a small amount of effective components in the plants are extracted, and the extraction rate of the effective components of the plants is not high;
(2) in the prior art, in the process of separating and extracting the effective components of the plants, the temperature of the plants rises when the plants are crushed and ground, so that the effective components in the plants volatilize, the bioactivity of the effective components of the plants is possibly reduced, and the extraction rate and the quality of the effective components of the plants are reduced;
(3) in the prior art, in the process of extracting effective components of plants, the extracting solution of the effective components of the plants is often distilled, condensed and recycled to obtain the effective components in the plants, when the effective components in the plants are sensitive to heat, the method causes adverse effects on the effective components of the plants, and meanwhile, the purity of the effective components of the plants obtained by the method is not high.
Disclosure of Invention
In order to overcome the defects of the prior art scheme, the invention provides the plant effective component extraction equipment for preparing the medicinal raw materials, which ensures the biological activity of the plant effective components, greatly improves the extraction rate of the effective components, has the characteristics of safety, high efficiency and high quality, and can effectively solve the problems in the background art.
The technical scheme adopted by the invention for solving the technical problems is as follows:
a plant active ingredient extraction device for preparing medicinal raw materials comprises an installation box, wherein a coarse crushing and feeding device is arranged at the top of the installation box, an ultramicro crushing mechanism is arranged at the upper part in the installation box, an active ingredient extraction mechanism is arranged at the lower part of the ultramicro crushing mechanism, a continuous material guide device is connected between the active ingredient extraction mechanism and the ultramicro crushing mechanism, and a two-stage purification mechanism is arranged below the active ingredient extraction mechanism;
the superfine grinding mechanism comprises a fine grinding device, the right end of the fine grinding device is movably connected with an auxiliary grinding device, the fine grinding device comprises a grinding barrel, the grinding barrel is installed in an installation box and is connected with a driving motor, a grinding roller is arranged in the grinding barrel, a plurality of rows of supporting springs are arranged between the grinding roller and the inner wall of the grinding barrel, and the supporting springs are adjacent to each other, a grinding disc is arranged between the supporting springs, and the grinding disc is fixedly installed on the grinding roller.
Furthermore, the inner surface of the crushing barrel is provided with a cylindrical crushing groove, the bottom surface of the cylindrical crushing groove is in sliding contact with the crushing disc, the cylindrical crushing groove is fixedly connected with one end of the supporting spring, two ends of the cylindrical crushing groove are provided with columnar guide discs with right-angled triangle-shaped cross sections, and the columnar guide discs are fixedly installed on the inner wall of the crushing barrel.
Further, supplementary reducing mechanism is including being the fan housing of round table face form, the fan housing right flank is equipped with the air inlet, and the air inlet has the liquid nitrogen container through pipe connection, fixed mounting has auxiliary fan in the fan housing, auxiliary fan left side is equipped with the electric heat silk screen, the electric heat silk screen left side is equipped with ultraviolet tube, be equipped with the reflection lens around the ultraviolet tube.
Further, coarse crushing feed arrangement includes feeder hopper and crushing pipe, feeder hopper and crushing pipe fixed connection, it has two striker plates to articulate in the feeder hopper, the striker plate top is equipped with limit baffle, and limit baffle fixed mounting is on the feeder hopper inner wall, fixedly connected with reset spring between striker plate and the feeder hopper inner wall, crushing intraductal movable mounting has two crushing posts, two all be equipped with crushing groove on the crushing post, and two crushing groove interlocks on the crushing post are connected, are located left crushing post transmission is connected with crushing motor, crushing motor fixed mounting is on the trailing flank in the install bin.
Further, continuous guide device includes left dry powder guiding tube and the water slurry guiding tube on right side, dry powder guiding tube movable mounting is at crushing bucket left end, be equipped with a plurality of spoilers in the dry powder guiding tube, the spoiler interval sets up on the side about the dry powder guiding tube, be equipped with the arc filter chamber in the water slurry guiding tube, the filter is installed to arc filter chamber bottom, movable mounting has the blowdown wheel in the arc filter chamber, blowdown wheel right side detachably is equipped with the blowdown groove, and the blowdown groove passes install bin right flank and movable mounting on the install bin, the blowdown wheel includes the movable rod, equidistant a plurality of blowdown separation blades that are equipped with on the movable rod, and the surface sliding contact on blowdown separation blade and the filter.
Further, the filter includes fixed frame, fixed frame bottom fixed mounting has the supporting network, there are four fixed plates that the cross-section is 'L' shape at fixed frame top through hinge movable mounting, fixedly connected with fixed spring between fixed plate and the supporting network, and the fixed plate left surface after fixing contacts with the laminating of fixed frame internal surface.
Further, the effective component extraction mechanism comprises a leaching device and a high-efficiency cleaning device, the leaching device comprises a leaching vessel, the bottom of the leaching vessel is connected with a dry powder guide pipe and a slurry guide pipe through guide pipes, a leaching plate is fixedly mounted in the middle of the leaching vessel, a plurality of conical leaching holes are formed in the leaching plate, a leaching agent adding box is connected to the upper portion of the leaching vessel, the leaching agent adding box is connected with a filling pipe, and a liquid level meter is fixedly mounted at the top end of the leaching vessel.
Furthermore, the efficient cleaning device comprises an ultrasonic generator, an ultrasonic transducer and an ultrasonic amplitude-increasing rod, wherein the ultrasonic generator, the ultrasonic transducer and the ultrasonic amplitude-increasing rod are fixedly installed in the installation box, the output end of the ultrasonic generator is electrically connected with the input end of the ultrasonic transducer, the output end of the ultrasonic transducer is electrically connected with the electric energy input end of the ultrasonic amplitude-increasing rod, and the ultrasonic amplitude-increasing rod penetrates through the lower bottom surface of the leaching vessel and extends into the leaching vessel.
Further, two-stage purification mechanism includes distillation recovery unit and recrystallization purification device, distillation recovery unit includes heating cup and condensation recoverer, heating cup top movable mounting has sealed lid, and sealed lid sets up to bilayer structure, bottom surface fixed mounting has the distillation heater in the heating cup, still be equipped with the distillation flask in the heating cup, the laminating is installed and is removed miscellaneous filter paper on the distillation flask inner wall, distillation flask top and sealed lid inner circle movable mounting, condensation recoverer and sealed lid fixed connection, the condensation recoverer sets up to spiral helicine three layer construction.
Further, the recrystallization purification device comprises a water bath cup, a water bath heater is fixedly mounted at the bottom of the water bath cup, a recrystallization vessel is arranged in the water bath cup, a gas collection cover is movably mounted at the top of the water bath cup, a conical drainage plate is arranged on the lower surface of the gas collection cover, the top end of the gas collection cover is connected with a condensation recoverer, an exhaust pipe is further connected to the top end of the gas collection cover, and the exhaust pipe penetrates through the right side face of the installation box and is fixedly mounted on the installation box.
Furthermore, an intelligent control device is arranged on the installation box and comprises a singlechip, the singlechip is electrically connected with a display, silicon controlled rectifiers are electrically connected between the output end of the singlechip and the ultrasonic generator, the distillation heater and the water bath heater, the output end of the single chip microcomputer is electrically connected with the liquid level meter, the output end of the single chip microcomputer is also electrically connected with a dry powder electromagnetic valve, a water slurry electromagnetic valve, a distillation temperature sensor, a recrystallization temperature sensor and a leachate adding electromagnetic valve, the dry powder electromagnetic valve is arranged between the crushing barrel and the dry powder guide pipe, the water slurry electromagnetic valve is arranged between the crushing barrel and the water slurry guide pipe, the distillation temperature sensor is fixedly arranged on the heating cup, the recrystallization temperature sensor is fixedly arranged on the inner wall of the water bath cup, and the leachate adding electromagnetic valve is arranged between the leachate adding box and the leaching vessel.
Compared with the prior art, the invention has the beneficial effects that:
(1) the coarse crushing feeding device provided by the invention can be used for primarily crushing the plants to be extracted, so that the plants to be extracted can be crushed into a smaller volume, the loss of an ultramicro crushing mechanism is reduced, the crushing effect is greatly improved, and the extraction rate of effective components of the plants to be extracted is improved;
(2) the superfine grinding mechanism provided by the invention is used for carrying out secondary fine grinding on the preliminarily ground plant to be extracted, so that the plant to be extracted can be ground into a smaller volume, and the biological cell walls of the effective components in the plant to be extracted are damaged, so that the effective components in the plant to be extracted are fully exposed in the extracting solution, and the extraction rate of the effective components in the plant to be extracted is greatly improved;
(3) the effective component extraction mechanism extracts the effective components in the crushed plants to be extracted, so that the separation of impurities and the effective components in the plants to be extracted is realized, the subsequent step of separating the effective components in the plants to be extracted is simplified, and the extraction period of the effective components of the plants to be extracted is shortened;
(4) the continuous material guide device conveys the plants to be extracted after being crushed in the superfine crushing mechanism to the effective component extraction mechanism, so that continuous production is realized, and the production efficiency is greatly improved;
(5) the two-stage purification mechanism of the invention separates and purifies the extract of the effective components of the plant to be extracted, and not only can obtain more effective components of the plant, but also can improve the purity of the purification by a two-stage purification mode.
Drawings
FIG. 1 is a schematic view of the overall structure of the present invention;
FIG. 2 is a schematic structural view of a fine grinding apparatus according to the present invention;
FIG. 3 is a schematic view of the coarse crushing feeding device according to the present invention;
FIG. 4 is a schematic view of the structure of the continuous material guiding device of the present invention
FIG. 5 is a schematic view of a filter according to the present invention;
FIG. 6 is a schematic diagram of the construction of the leaching plate of the present invention;
FIG. 7 is a schematic view of the sealing cap of the present invention;
FIG. 8 is a schematic view of a condensate recoverer according to the present invention;
FIG. 9 is a schematic cross-sectional view of a condensate recovery device according to the present invention;
FIG. 10 is a schematic structural diagram of an intelligent control device according to the present invention;
FIG. 11 is a schematic view of the structure of the effective component extraction mechanism of the present invention.
Reference numbers in the figures:
1-installing a box; 2-a coarse crushing feeding device; 3-an ultramicro crushing mechanism; 4-an active ingredient extraction mechanism; 5-continuous material guiding device; 6-a two-stage purification mechanism; 7-a fine crushing device; 8-an auxiliary crushing device; 9-a leacher; 10-cylindrical pulverizing tank; 11-high efficiency cleaning means; 12-distillation recovery unit; 13-a recrystallization purification unit; 14-an intelligent control device; 15-drainage grooves; 16-a barrier net; 17 a movable groove; 18-a connecting strip; 19-a transmission rod; 20-rotating the handle; 21-mounting grooves;
201-a feed hopper; 202-a crushing tube; 203-striker plate; 204-a limit baffle; 205-a return spring; 206-crushing column; 207-a crushing tank; 208-a grinding motor;
501-dry powder guiding tube; 502-slurry guide tube; 503-spoiler; 504-arc filter chamber; 505-a filter; 506-a pollution discharge wheel; 507-a sewage draining tank;
701-a crushing barrel; 702-a drive motor; 703-crushing rollers; 704-a support spring; 705-grinding plate;
801-wind collecting cover; 802-an air inlet; 803-liquid nitrogen container; 804-auxiliary fan; 805-electric heating wire mesh; 806-ultraviolet lamp tube; 807-mirror plate;
901-a leaching vessel; 902-leaching plate; 903-extraction holes; 904-leachate addition tank; 906-a liquid level meter;
1101-an ultrasonic generator; 1102-an ultrasonic transducer; 1103-ultrasonic horn;
1201-heating cup; 1202-condensation recoverer; 1203-sealing cover; 1204-distillation heater; 1205-a distillation flask; 1206-impurity removing filter paper;
1301-water bath cup; 1302-water bath heater; 1303-recrystallization vessel; 1304-gas collection cover; 1305-a drainage plate; 1306-an exhaust pipe;
1401-single chip microcomputer; 1402-a display; 1403-thyristor; 1404-dry powder solenoid valve; 1405-water slurry electromagnetic valve; 1406-distillation temperature sensor; 1407-recrystallization temperature sensor; 1408-leachate addition solenoid valve;
5051-fixing frames; 5052-supporting the net; 5053, fixing a plate; 5054-fixing the spring;
5061-a movable bar; 5062-blowdown catch.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
As shown in fig. 1 to 11, the present invention provides a plant active ingredient extraction apparatus for preparing pharmaceutical raw materials, which includes an installation box 1, a coarse crushing feeding device 2 is disposed at the top of the installation box 1, an ultra-fine crushing mechanism 3 is disposed at the upper portion in the installation box 1, an active ingredient extraction mechanism 4 is disposed at the lower portion of the ultra-fine crushing mechanism 3, a continuous material guiding device 5 is connected between the active ingredient extraction mechanism 4 and the ultra-fine crushing mechanism 3, and a two-stage purification mechanism 6 is disposed below the active ingredient extraction mechanism 4.
In this embodiment, coarsely smash feed arrangement 2 and treat to extract the plant and carry out preliminary crushing, can smash the plant that will wait to extract into less volume, reduce the loss to superfine grinding mechanism, simultaneously also promoted kibbling effect greatly, superfine grinding mechanism 3 carries out secondary fine crushing to the preliminary kibbling plant that waits to extract, can smash the plant that waits to extract into littleer volume, the biological cell wall of active ingredient in the plant that waits to extract has been destroyed simultaneously, make active ingredient fully expose in the plant that waits to extract in the extract, the extraction rate of active ingredient in the plant that waits to extract has improved greatly, active ingredient extraction mechanism 4 extracts the active ingredient in the plant that waits to extract after smashing, the separation of active ingredient in impurity and the plant that waits to extract has been realized, the step of the follow-up active ingredient separation in the plant that waits to extract has been simplified, continuous guiding device 5 carries the plant that waits to extract after smashing in the superfine grinding mechanism 3 to extract the active ingredient extraction mechanism and extracts the mechanism In 4, realized serialization production, promoted the efficiency of production greatly, the separation and purification that the extract of the active ingredient of the plant was carried out is treated to two-stage purification mechanism 6, through the two-stage purification mode, not only can acquire more plant active ingredient, the purity of purification is higher simultaneously.
The superfine crushing mechanism 3 comprises a fine crushing device 7, an auxiliary crushing device 8 is movably connected to the right end of the fine crushing device 7, the fine crushing device 7 comprises a crushing barrel 701, the crushing barrel 701 is installed in the installation box 1, the crushing barrel 701 is connected with a driving motor 702, a crushing roller 703 is arranged in the crushing barrel 701, a plurality of rows of supporting springs 704 are arranged between the crushing roller 703 and the inner wall of the crushing barrel 701, a crushing disc 705 is arranged between the adjacent supporting springs 704, and the crushing disc 705 is fixedly installed on the crushing roller 703.
In the embodiment, the superfine grinding mechanism 3 finely grinds the preliminarily ground plants to be extracted for the second time, so as to grind the plants to be extracted into smaller volume, and simultaneously destroy the biological cell walls of the active ingredients in the plants to be extracted, so that the active ingredients in the plants to be extracted are fully exposed in the extracting solution, thereby greatly improving the extraction rate of the active ingredients in the plants to be extracted, in the embodiment, when the driving motor 702 works, the grinding barrel 701 rotates along with the same, the grinding roller 703 connected with the inner wall of the grinding barrel 701 through the supporting spring 704 rotates along with the grinding barrel 701 under the tangential force of the supporting spring 704, because the centrifugal force of the grinding roller 703 is greater than the upward elastic force of the supporting spring 704 when the grinding roller 703 is subjected to the self gravity and rotates, the bottom end of the grinding disc 703 always collides with the bottom of the grinding barrel 701 to enable the plants to be extracted positioned in the grinding barrel 701 to be repeatedly rolled, finally, the plant to be extracted is crushed into fine powder or slurry, the biological cell walls of the plant to be extracted are damaged, and the effective components in the biological cell walls are exposed, so that the extraction rate of the effective components in the plant to be extracted is greatly improved, and the extraction cost of the effective components is reduced.
The inner surface of the crushing barrel 701 is provided with a cylindrical crushing groove 10, the bottom surface of the cylindrical crushing groove 10 is in sliding contact with a crushing disc 705, the cylindrical crushing groove 10 is fixedly connected with one end of a supporting spring 704, two ends of the cylindrical crushing groove 10 are provided with cylindrical guide discs with right-angled triangle sections, and the cylindrical guide discs are fixedly arranged on the inner wall of the crushing barrel 701.
In this embodiment, the cylindrical pulverizing tank 10 provides a pulverizing place for the plants to be extracted, one end of the supporting spring 704 is fixedly installed in the cylindrical pulverizing tank 10, the other end of the supporting spring 704 is fixedly installed on the pulverizing roller 703, the pulverizing disk 705 on the pulverizing roller 703 collides with the bottom of the cylindrical pulverizing tank 10 in the rotating process to realize the pulverization of the plants to be extracted, in the present embodiment, the cylindrical pulverizing groove 10 is arranged so that the plant to be extracted in the pulverizing barrel 701 always falls into the cylindrical pulverizing groove 10 for pulverizing and grinding the plant to be extracted, the end of the cylindrical guiding plate close to the cylindrical pulverizing groove 10 is flush with the bottom of the cylindrical pulverizing groove 10, the cylindrical guiding plate 11 is arranged, so that the plants to be extracted being crushed and ground in the crushing barrel 701 are slid into the cylindrical crushing tank 10, the plant to be extracted is more fully crushed and ground, so that the obtaining efficiency of the effective components in the plant to be extracted is improved.
Supplementary reducing mechanism 8 is including being the wind-collecting cover 801 of round table face form, wind-collecting cover 801 right flank is equipped with air inlet 802, and air inlet 802 has liquid nitrogen tank 803 through pipe connection, fixed mounting has auxiliary fan 804 in the wind-collecting cover 801, auxiliary fan 804 left side is equipped with electric heat silk screen 805, electric heat silk screen 805 left side is equipped with ultraviolet tube 806, be equipped with reflection lens 807 around ultraviolet tube 806.
In this embodiment, supplementary reducing mechanism 8 is used for assisting smart reducing mechanism 7 to accomplish the crushing grinding of waiting to extract the plant better, supplementary reducing mechanism 8 treats through spun liquid nitrogen and extracts the plant and carries out the cold-ization processing, treat that the plant of extracting cold-ization processing back is more fragile, not only can make to be extracted the plant smash ground more abundant, improve the rate of acquisition of active ingredient in waiting to extract the plant, reduced simultaneously and waited to extract the plant and smashed the temperature rise of grinding in-process, the biological activity that has prevented high temperature from causing plant active ingredient and descend, the quality of active ingredient in the plant has been promoted.
In this embodiment, when the plant to be extracted is dry solid, the rotation speed of the auxiliary fan 804 is adjusted when the plant to be extracted is pulverized and ground, and when the plant to be extracted is pulverized into fine particles, the fine particles are blown to the left end of the pulverizing barrel 701 under the action of the wind force of the auxiliary fan 804;
when the plant to be extracted is large in particle size after being crushed and ground, the plant to be extracted cannot be blown to the left end of the crushing barrel 701 by the blowing of the auxiliary fan 804, and the plant to be extracted is always positioned in the cylindrical crushing groove 10 until being ground into fine particles and finally blown to the left end of the crushing barrel 701.
In this embodiment, auxiliary fan 804 also through silicon controlled rectifier electric connection to following singlechip 1401 on, the control signal given through singlechip 1401 realizes the regulation of auxiliary fan 804 wind speed, auxiliary fan 804 has played the effect of screening at the in-process that the plant that waits to extract is smashed and is ground, auxiliary fan 804 blows to the plant that waits to extract with liquid nitrogen tank 803 exhaust nitrogen gas simultaneously, the speed of waiting to extract the plant crushing and grinding has been accelerated, the quality of the plant active ingredient after also having promoted simultaneously acquireing, when the plant that waits to extract is the active plant for kibbling, auxiliary fan 804 blows to the plant that waits to extract with liquid nitrogen tank 803 exhaust nitrogen gas, the better faster completion of supplementary fine crushing device 7 is waited to extract the crushing and grinding of plant.
When the plants to be extracted are crushed and ground, the ultraviolet lamp 806 works, and under the reflection action of the reflector 807, ultraviolet rays are reflected to the primarily crushed plants to be extracted to sterilize the primarily crushed plants to be extracted, so that the activity of effective components in the plants to be extracted caused by bacteria carried on the surfaces of the plants to be extracted is prevented from being damaged.
Before the next extraction of the effective components of the plants, the inside of the crushing barrel 701 needs to be cleaned, and the specific steps are as follows: an appropriate amount of cleaning water is added into the crushing barrel 701, the driving motor 702, the auxiliary fan 804, the electric heating wire mesh 805 and the ultraviolet lamp tube 806 are turned on, the liquid nitrogen tank 803 air valve is closed at the same time, the cleaning water cleans the crushing barrel 701 in the rotating process, after the cleaning is finished, hot air blown out by the auxiliary fan 804 dries and dries the inside of the crushing barrel 701, ultraviolet light generated by the ultraviolet lamp tube 805 sterilizes and sterilizes the inside of the crushing barrel 701, and pollution of residual substances and bacteria in the crushing barrel 701 to the next operation is avoided.
Coarse crushing feed arrangement 2 includes feeder hopper 201 and crushing pipe 202, feeder hopper 201 and crushing pipe 202 fixed connection, it has two striker plates 203 to articulate in the feeder hopper 201, striker plate 203 top is equipped with limit baffle 204, and limit baffle 204 fixed mounting is on feeder hopper 201 inner wall, fixedly connected with reset spring 205 between striker plate 203 and the feeder hopper 201 inner wall, crushing pipe 202 interior movable mounting has two crushing post 206, two all be equipped with crushing groove 207 on crushing post 206, and two crushing groove 207 interlocks on crushing post 206 are connected, are located left crushing post 206 transmission is connected with crushing motor 208, crushing motor 208 fixed mounting is on the trailing flank in install bin 1.
In the embodiment, the rough grinding feeding device 2 carries out preliminary grinding on the plants to be extracted, can grind the plants to be extracted into smaller volume, reduces the loss of the ultramicro grinding mechanism, and simultaneously greatly improves the grinding effect, in the embodiment, the plant to be extracted is added into the feed hopper 201, the pressure generated by the plant to be extracted baffle plate 203 on the baffle plate 203 is greater than the elastic force of the return spring 205 on the baffle plate, the baffle plate 203 rotates downwards for a certain angle, the middle position of the baffle plate 203 on both sides of the feed hopper 201 has a crack, the plant to be extracted on the baffle plate 203 falls into the bottom of the feed hopper 201 from the crack, after the plant to be extracted on the baffle plate 203 falls into the bottom of the feed hopper 201, the baffle plate 203 recovers to the original position under the action of the elastic force of the return spring 205, and the two baffle plates 203 are folded to realize the sealing of the feed hopper 201.
After the plants to be extracted slide down from the baffle plate 203 and fall onto the crushing column 206, the crushing column 206 rotates under the driving of the crushing motor 208, the plants to be extracted on the crushing column 206 are crushed by the crushing groove 207 in the rotating process of the crushing column 206, and finally fall into the crushing barrel 701 for secondary crushing and grinding.
Particularly, in the rotating process of the two crushing columns 206, the crushing groove 207 on one crushing column 206 is matched with the convex part on the other crushing column 206, and in the rotating process, the crushing groove 207 on one crushing column 206 is meshed with the crushing groove 207 on the other crushing column 206, so that the crushing effect of the plant to be extracted is improved.
Continuous guide device 5 includes left dry powder guide tube 501 and water slurry guide tube 502 on right side, dry powder guide tube 501 movable mounting is at crushing bucket 701 left end, be equipped with a plurality of spoilers 503 in the dry powder guide tube 501, the spoiler 503 interval sets up on dry powder guide tube 501 left and right sides, be equipped with arc filter chamber 504 in the water slurry guide tube 502, filter 505 is installed to arc filter chamber 504 bottom, movable mounting has blowdown wheel 506 in the arc filter chamber 504, blowdown wheel 506 right side detachably is equipped with blowdown groove 507, and blowdown groove 507 passes 1 right flank of install bin and movable mounting on install bin 1, blowdown wheel 506 includes movable rod 5061, equidistant a plurality of blowdown separation blades 5062 that are equipped with on movable rod 5061, and blowdown separation blade 5062 and filter 505 upper surface sliding contact.
In the embodiment, the continuous material guide device 5 conveys the plant to be extracted crushed in the superfine crushing mechanism 3 to the effective component extraction mechanism 4, thereby realizing continuous production, greatly improving the production efficiency, in the embodiment, the continuous material guiding device 5 adopts different material guiding modes for the plants to be extracted which are crushed by the dry method and the wet method, when the plant to be extracted is a dry solid matter, the pulverized and ground powder enters the effective component extraction mechanism 4 through the dry powder guide pipe 501, the plant that waits to extract in the crushing bucket 701 is blown under the effect of auxiliary blower 804 after being smashed and ground, blows in dry powder guide tube 501 in the cylindricality crushing groove 10 in the crushing bucket 804, and the powder is in dry powder guide tube 501 the effect of the baffler 503 resistance of receiving, and the speed that the powder flows slows down, has avoided powder flow velocity to cause the powder to discharge and has overflowed when the dry powder guide tube at the excessive speed.
When the plant to be extracted is an active plant, the slurry obtained by pulverizing and grinding the plant to be extracted enters the effective component extraction mechanism 4 from the slurry guide pipe 502, and in this embodiment, the specific connection mode between the slurry guide pipe 502 and the pulverizing barrel 701 is as follows: the inner surface of the right end of the cylindrical crushing tank 10 on the crushing barrel 701 is provided with a drainage groove 15, the drainage groove 15 is provided with a blocking net 16, the outer surface of the right end of the cylindrical crushing tank 10 on the crushing barrel 701 is provided with a movable groove 17 with a 'shaped cross section, a connecting strip 18 with a' shaped cross section is slidably connected on the movable groove 17, the bottom end of the connecting strip 18 is communicated and connected with the water slurry guide pipe 502, in the rotating process of the crushing barrel 701, the connecting strip 18 keeps still, the ground plant slurry in the crushing barrel 701 is discharged through the connecting strip 18, the left side of the drainage groove 15 is slightly recessed, the plant slurry is convenient to collect and discharge, and the blocking net 16 is arranged, so that dry powder to be extracted and ground by plants is prevented from being discharged from the drainage groove 15.
In the process of discharging the plant slurry to be extracted, the slurry after crushing and grinding the plant to be extracted enters the slurry guide pipe 502, the slurry falls onto the sewage discharge baffle 5062, the kinetic energy of the slurry when falling is converted into the kinetic energy of the sewage discharge wheel 506 when rotating, and in the process of rotating the sewage discharge wheel, the residue filtered by the filter 505 is discharged from the bottom of the arc-shaped filter cavity 504 by a belt in the process of rotating the sewage discharge baffle 5062 and is finally discharged through the sewage discharge groove 507.
The filter 505 comprises a fixed frame 5051, a support net 5052 is fixedly installed at the bottom of the fixed frame 5051, four fixing plates 5053 with L-shaped cross sections are movably installed at the top of the fixed frame 5051 through hinges, a fixing spring 5054 is fixedly connected between the fixing plates 5053 and the support net 5052, and the left side face of the fixed fixing plate 5053 is in contact with the inner surface of the fixed frame 5051 in an attaching manner.
In the embodiment, the filter 505 separates insoluble substances in plant slurry to be extracted, the bottom of the arc-shaped installation cavity 504 is provided with the installation groove 21, the filter 505 is detachably installed in the installation groove 21 at the bottom of the arc-shaped filter cavity 504, filter screens with different densities are selected according to the size of residues in the ground plant slurry, the type of the filter screens is determined and then the filter screens are installed on the filter 505, so that the plant slurry to be extracted can be filtered, and after insoluble substances in the plant slurry to be extracted are removed, the subsequent steps of extracting effective components in plants to be extracted are simplified.
In this embodiment, the specific installation method of the filter screen is as follows: the filter installation method comprises the steps of firstly expanding a fixing plate 5053 around a fixing frame 5051, then flatly laying a selected filter screen on a support screen 5052, finally loosening the fixing plate 5053, restoring the fixing plate 5053 to the original position under the action of elastic force of a fixing spring 5054, and enabling the filter screen to be firmly fixed between the fixing plate 5053 and the support screen 5052.
The effective component extraction mechanism 4 comprises an extractor 9 and an efficient cleaning device 11, the extractor 9 comprises an extraction vessel 901, the bottom of the extraction vessel 901 is connected with a dry powder guide pipe 501 and a slurry guide pipe 502 through guide pipes, an extraction plate 902 is fixedly installed in the middle of the extraction vessel 901, a plurality of conical extraction holes 903 are formed in the extraction plate 902, the upper portion of the extraction vessel 901 is connected with an extraction liquid adding box 904, the extraction liquid adding box 904 is connected with an injection pipe 905, and the top end of the extraction vessel 901 is fixedly provided with a liquid level meter 906.
In this embodiment, the effective component extraction mechanism 4 extracts effective components in the crushed plant to be extracted, so as to separate impurities from the effective components in the plant to be extracted, and simplify the subsequent step of separating the effective components in the plant to be extracted, the effective component extraction mechanism 4 absorbs the effective components in the plant in the slurry through the leachate, and then separates the effective components of the plant from the leachate through the subsequent step, so as to extract the effective components of the plant, wherein the leachate addition tank 904 is used for storing the leachate, the filling pipe 905 passes through the left side surface of the installation tank 1 and is fixedly installed on the left side surface of the installation tank 1, the filling pipe 905 is used for adding the leachate in the leachate addition tank 904, and the setting of the liquid level meter 906 can detect the liquid level in the leaching vessel 901, so as to avoid overflow of the leachate.
When the plant to be extracted is a dry plant, the powder generated by crushing and grinding the plant to be extracted enters the extractor 9 through the dry powder guide pipe 501, the powder of the plant to be extracted enters the extraction vessel 901 and then contacts with the extraction liquid, and the extraction liquid absorbs the active ingredients in the plant to be extracted, wherein the extraction plate 902 and the conical extraction hole 903 are arranged, so that the situation that the plant powder to be extracted directly floats to the upper surface of the extraction liquid when entering the extraction vessel 901 is avoided, the absorption rate of the plant active ingredients by the extraction liquid is slowed down, and meanwhile, the conical extraction hole 903 arranged in an inverted manner prevents the plant powder to be extracted from settling on the upper surface of the extraction plate 902, and the accumulation of the plant powder to be extracted on the extraction plate 902 is reduced.
When the plant to be extracted is an active plant, the slurry generated by crushing and grinding the plant to be extracted enters the extractor 9 through the slurry guide pipe 502, the plant slurry to be extracted enters the extraction vessel 901 and then fully contacts with the leachate, the leachate absorbs the active ingredients in the plant slurry to be extracted, the leachate absorbing the active ingredients of the plant to be extracted is separated from the leachate through the subsequent steps, and the extraction of the active ingredients of the plant can be realized.
The efficient cleaning device 11 comprises an ultrasonic generator 1101, an ultrasonic transducer 1102 and an ultrasonic amplitude transformer 1103, wherein the ultrasonic generator 1101, the ultrasonic transducer 1102 and the ultrasonic amplitude transformer 1103 are all fixedly installed in the installation box 1, the output end of the ultrasonic generator 1101 is electrically connected with the input end of the ultrasonic transducer 1102, the output end of the ultrasonic transducer 1102 is electrically connected with the electric energy input end of the ultrasonic amplitude transformer 1103, and the ultrasonic amplitude transformer 1103 penetrates through the lower bottom surface of the leaching vessel 901 and extends into the leaching vessel 901.
In this embodiment, the efficient cleaning device 11 provides high-frequency vibration to realize sufficient contact between the leachate and the plant powder or the slurry to be extracted, so as to accelerate the absorption rate of the leachate to the effective components in the plant to be extracted, thereby shortening the period of extraction of the effective components in the plant, meanwhile, the efficient cleaning device 11 can also clean the leacher 9, after the leacher 9 is added with proper cleaning water, the high-frequency vibration provided by the efficient cleaning device 11 can make the stains attached to the leacher 9 fall off, and a certain cleaning effect is achieved.
In this embodiment, the ultrasonic generator 1101 is configured to convert the commercial power into a high-frequency alternating current corresponding to the ultrasonic transducer 1102 to drive the ultrasonic transducer 1102 to operate, the ultrasonic transducer 1102 converts the high-frequency electric power output by the ultrasonic generator 1101 into mechanical power (i.e., ultrasonic waves) and transmits the mechanical power, and the ultrasonic booster 1103 transmits the high-frequency vibration generated by the ultrasonic transducer 1102 into the extractor 9 to provide the stable high-frequency vibration to the extractor 9.
The two-stage purification mechanism 6 comprises a distillation recovery device 12 and a recrystallization purification device 13, the distillation recovery device 12 comprises a heating cup 1201 and a condensation recoverer 1202, a sealing cover 1203 is movably mounted at the top of the heating cup 1201, the sealing cover 1203 is arranged to be of a double-layer structure, a distillation heater 1204 is fixedly mounted on the inner bottom surface of the heating cup 1201, a distillation bottle 1205 is further arranged in the heating cup 1201, impurity-removing filter paper 1206 is mounted on the inner wall of the distillation bottle 1205 in a fit mode, the top end of the distillation bottle 1205 is movably mounted in the inner ring of the sealing cover 1203, the condensation recoverer 1202 is fixedly connected with the sealing cover 1203, and the condensation recoverer 1202 is arranged to be of.
In this embodiment, the two-stage purification mechanism 6 separates and purifies the leachate which absorbs the plant effective components by distillation recovery and recrystallization methods to obtain relatively pure plant effective components, wherein the distillation recovery device 12 can perform primary coarse separation according to the difference of the boiling points of the substances in the leachate, the primary product obtained after the primary separation has higher purity, and the primary product is then purified by recrystallization to obtain more pure plant effective components.
The purification method for distillation recovery comprises the following steps: after the leachate of the plant active ingredients reaches the distillation flask 1205, a proper amount of water is added into the heating cup 1201, meanwhile, the distillation heater 1204 is turned on to heat the water in the heating cup 1201, the distillation flask 1205 is heated in a water bath heating mode, all parts of the distillation flask 1205 are uniformly heated in the water bath heating mode, the distillation temperature is conveniently controlled, and then the distillation separation extraction is carried out according to the boiling points of all substances in the leachate of the plant active ingredients.
The distillation separation extraction is sequentially separated from low boiling point to high boiling point, when the boiling point of the impurities in the plant effective component leaching solution is larger than the boiling point of the effective components and is lower than the boiling point of the effective components, the impurities lower than the boiling point of the effective components are firstly subjected to distillation separation, then the effective components are subjected to distillation separation and recovery, and the remaining liquid is directly poured out without distillation separation, so that the process of separating the plant effective components is simplified, and the extraction efficiency of the plant effective components is accelerated.
In this embodiment, the sealing cover 1203 is set as a double-layer structure, the external channel is a steam overflow channel, which avoids explosion danger caused by too high air pressure in the heating cup 1201 during heating, the internal channel of the sealing cover 1203 provides a circulating channel for impurities and gases of active ingredients in the plant active ingredient leachate, which is convenient for separating impurities from active ingredients, the impurity-removing filter paper 1206 is replaceably installed on the inner wall of the distillation flask 1205, when the plant active ingredients are distilled and separated, the internal impurities may be crystallized and separated out, the impurities in the distillation flask 1205 can be removed by replacing the impurity-removing filter paper, which avoids pollution caused by next extraction operation, and meanwhile, in order to prevent the plant active ingredients from crystallizing and separating out, a sufficient amount of leachate is added during the extraction process of the plant active ingredients, the condensation recoverer 1202 is set, which can condense and recover the steam of the plant active ingredients, obtaining the product of primary separation and purification of the effective components of the plants.
Wherein condensation recoverer 1202 downward sloping certain angle installation, steam and the vapor condensation of plant active ingredient flow to recrystallization purification device 13 in the condensation recoverer 1202 of being convenient for, condensation recoverer 1202 sets up to the heliciform, the tube side of steam condensation has been increased, the effect of condensation has been promoted greatly, condensation recoverer 1202 sets up to three layer construction, loop through the steam of plant active ingredient or impurity from inside to outside among the three layer construction, flowing water, vapor, wherein flowing water flows into high-end outflow from the bottom, can make flowing water be full of the middle level pipeline, promote the effect of condensation.
The recrystallization purification device 13 comprises a water bath cup 1301, a water bath heater 1302 is fixedly installed at the bottom of the water bath cup 1301, a recrystallization vessel 1303 is arranged in the water bath cup 1301, a gas collection cover 1304 is movably installed at the top of the water bath cup 1301, a conical flow guide plate 1305 is arranged on the lower surface of the gas collection cover 1304, the top end of the gas collection cover 1304 is connected with a condensation recoverer 1202, an exhaust pipe 1306 is further connected to the top end of the gas collection cover 1304, and the exhaust pipe 1306 penetrates through the right side face of the installation box 1 and is fixedly installed on the installation box 1.
In this embodiment, the recrystallization purification device 13 heats and concentrates the solution of the plant effective components to be extracted, when the solvent of the solution of the plant effective components to be extracted is reduced by evaporation, the concentration of the plant effective components to be extracted is increased, and when the concentration of the plant effective components to be extracted is greater than the solubility of the plant effective components in the solvent, the plant effective components to be extracted can be crystallized out, so that relatively pure crystals of the plant effective components to be extracted can be obtained in the recrystallization vessel 1303.
The specific method for recrystallization purification comprises the following steps: the primary product of the plant effective components to be extracted, which is condensed and recovered by the condensation recoverer 12, flows to the recrystallization vessel 1303, a proper amount of water is added into the water bath cup 1301 firstly, then the water bath heater 1302 is turned on, the water bath heater 1302 works to heat the water in the water bath cup 1301, the water temperature in the water bath cup 1301 rises to provide a proper heating temperature for the water bath vessel 1303, the solvent in the primary product in the water bath vessel 1303 volatilizes, the plant effective components to be extracted are crystallized and separated out along with the continuous volatilization of the solvent, finally, the water bath heater 1302 is turned off, and the crystals of the plant effective components to be extracted in the water bath vessel 1303 are collected.
Wherein the liquid that the innermost layer of condensation recoverer 1202 flows leads to recrystallization ware 1303, the outermost layer of flowing comdenstion water of condensation recoverer 1202 flows into in the water bath cup 1301 through the drainage plate 1305, can supply the water yield of water bath cup 1301, steam escape in gas collection lid 1304 and blast pipe 1306 can be with the recrystallization ware 1303 of water bath cup 1301 and, avoid steam to get into the install bin 1 inside, influence holistic working property, conical surface's drainage plate 1305 has not only played the guide comdenstion water and has got into water bath cup 1301, also avoided steam condensation among the recrystallization process to flow back to in the recrystallization ware 1303 simultaneously, the progress of recrystallization process has been accelerated.
The installation box 1 is provided with an intelligent control device 14, the intelligent control device 14 comprises a single chip microcomputer 1401, the single chip microcomputer 1401 is electrically connected with a display 1402, the output end of the single chip microcomputer 1401, an ultrasonic generator 1101, a distillation heater 1204 and a water bath heater 1302 are electrically connected with a silicon controlled rectifier 1403, the output end of the single chip microcomputer 1401 is electrically connected with a liquid level meter 906, the output end of the single chip microcomputer 1401 is also electrically connected with a dry powder electromagnetic valve 1404, a water slurry electromagnetic valve 1405, a distillation temperature sensor 1406, a recrystallization temperature sensor 1407 and a leachate adding electromagnetic valve 1408, the dry powder electromagnetic valve 1404 is installed between the crushing barrel 701 and the dry powder guide pipe 501, the water slurry electromagnetic valve 1405 is installed between the crushing barrel 701 and the water slurry guide pipe 502, the distillation temperature sensor 1406 is fixedly installed on the heating cup 1201, and the recrystallization temperature sensor 1407 is fixedly installed, the leachate adding electromagnetic valve is arranged between the leachate adding box and the leaching vessel.
In this embodiment, the single chip 1401 monitors each device in the installation box 1 in real time through the real-time information transmitted from each sensor and takes corresponding measures, so that the process of extracting the effective components of the plants is orderly performed.
The specific control mode of the singlechip is as follows: the single-chip microcomputer 1401 obtains the water bath temperature during distillation and recrystallization through the distillation temperature sensor 1406 and the recrystallization temperature sensor 1407, when the detected temperature is higher than the required temperature, the single-chip microcomputer 1401 sends a trigger signal to the silicon controlled rectifier 1403, the silicon controlled rectifier 1403 is in a cut-off state, the distillation heater 1204 and the water bath heater 1302 stop working, the distillation thermometer and the water bath temperature are reduced, and the required temperature is reached; when the detected temperature is lower than the required temperature, the single chip microcomputer 140 sends a trigger signal to the thyristor 1403, and the heating powers of the distillation heater 1204 and the water bath heater 1302 are changed by changing the trigger angle of the trigger signal, so that the distillation temperature and the water bath temperature reach the required temperature.
The single chip 1401 controls the dry powder electromagnetic valve 1404 and the water slurry electromagnetic valve 1405 to be switched off by sending triggering signals to the dry powder electromagnetic valve 1404 and the water slurry electromagnetic valve 1405, so that the continuous material guide device 5 is controlled.
The single chip 1401 obtains the height of the liquid level in the leaching vessel 901 through the liquid level meter 906, controls the switching-off of the leachate adding electromagnetic valve 1408 according to the liquid level height of the leaching vessel 901, controls the leachate adding electromagnetic valve 1408 to be opened to add the leachate when the amount of the leachate is small, and controls the leachate adding electromagnetic valve to stop adding the leachate when the amount of the leachate reaches the required amount.
The single chip 1401 realizes the switching of the ultrasonic generator 1101 by sending a trigger signal to the silicon controlled rectifier 1403, accelerates the absorption of the leaching solution on the effective components of the plants to be extracted, and can clean the leacher 9.
The display 1402 electrically connected to the single chip 1401 selects a touch display screen, can determine the operation condition of each device according to information displayed on the touch display screen, and can control the operation state of each device through the touch screen.
It is particularly noted that other electrical appliances in this embodiment can be connected through the relay single-chip microcomputer 1401, and the switching of the electrical appliances is realized through the trigger signal sent by the single-chip microcomputer 1401 to the relay, which is convenient for controlling the electrical appliances in the device.
It will be evident to those skilled in the art that the invention is not limited to the details of the foregoing illustrative embodiments, and that the present invention may be embodied in other specific forms without departing from the spirit or essential attributes thereof. The present embodiments are therefore to be considered in all respects as illustrative and not restrictive, the scope of the invention being indicated by the appended claims rather than by the foregoing description, and all changes which come within the meaning and range of equivalency of the claims are therefore intended to be embraced therein. Any reference sign in a claim should not be construed as limiting the claim concerned.

Claims (8)

1. A plant active ingredient draws equipment for preparation of medical raw materials, includes install bin (1), its characterized in that: an ultramicro crushing mechanism (3) is arranged at the upper part in the installation box (1), and an effective component extraction mechanism (4) is arranged at the lower part of the ultramicro crushing mechanism (3); the effective component extraction mechanism (4) comprises an extractor (9) and an efficient cleaning device (11), the extractor (9) comprises an extraction vessel (901), the bottom of the extraction vessel (901) is connected with a dry powder guide pipe (501) and a water slurry guide pipe (502) through guide pipes, an extraction plate (902) is fixedly installed in the middle of the extraction vessel (901), a plurality of conical extraction holes (903) are formed in the extraction plate (902), an extraction liquid adding box (904) is connected to the upper portion of the extraction vessel (901), a filling pipe (905) is connected to the extraction liquid adding box (904), a liquid level meter (906) is fixedly installed at the top end of the extraction vessel (901), the efficient cleaning device (11) comprises an ultrasonic generator (1101), an ultrasonic transducer (1102) and an ultrasonic amplification rod (1103), the ultrasonic generator (1101), The ultrasonic transducer (1102) and the ultrasonic booster (1103) are fixedly installed in the installation box (1), the output end of the ultrasonic generator (1101) is electrically connected with the input end of the ultrasonic transducer (1102), the output end of the ultrasonic transducer (1102) is electrically connected with the electric energy input end of the ultrasonic booster (1103), and the ultrasonic booster (1103) penetrates through the lower bottom surface of the leaching vessel (901) and extends into the leaching vessel (901);
a two-stage purification mechanism (6) is arranged below the effective component extraction mechanism (4), the two-stage purification mechanism (6) comprises a distillation recovery device (12) and a recrystallization purification device (13), the distillation recovery device (12) comprises a heating cup (1201) and a condensation recoverer (1202), a sealing cover (1203) is movably arranged at the top of the heating cup (1201), the sealing cover (1203) is arranged to be of a double-layer structure, a distillation heater (1204) is fixedly arranged on the inner bottom surface of the heating cup (1201), a distillation flask (1205) is also arranged in the heating cup (1201), impurity removing filter paper (1206) is attached and installed on the inner wall of the distillation flask (1205), the top end of the distillation bottle (1205) is movably mounted with the inner ring of the sealing cover (1203), the condensation recoverer (1202) is fixedly connected with the sealing cover (1203), and the condensation recoverer (1202) is of a spiral three-layer structure;
the recrystallization purification device (13) comprises a water bath cup (1301), a water bath heater (1302) is fixedly installed at the bottom of the water bath cup (1301), a recrystallization vessel (1303) is arranged in the water bath cup (1301), an air collection cover (1304) is movably installed at the top of the water bath cup (1301), a conical drainage plate (1305) is arranged on the lower surface of the air collection cover (1304), the top end of the air collection cover (1304) is connected with a condensation recoverer (1202), an exhaust pipe (1306) is further connected to the top end of the air collection cover (1304), and the exhaust pipe (1306) penetrates through the right side face of the installation box (1) and is fixedly installed on the installation box (1).
2. The plant active ingredient extraction apparatus for pharmaceutical raw material preparation according to claim 1, characterized in that: the superfine grinding mechanism (3) comprises a fine grinding device (7), an auxiliary grinding device (8) is movably connected to the right end of the fine grinding device (7), the fine grinding device (7) comprises a grinding barrel (701), the grinding barrel (701) is installed in an installation box (1), the grinding barrel (701) is connected with a driving motor (702), grinding rollers (703) are arranged in the grinding barrel (701), a plurality of rows of supporting springs (704) are arranged between the grinding rollers (703) and the inner wall of the grinding barrel (701), a grinding disc (705) is arranged between every two adjacent supporting springs (704), and the grinding disc (705) is fixedly installed on the grinding rollers (703).
3. The plant active ingredient extraction apparatus for pharmaceutical raw material preparation according to claim 2, characterized in that: the inner surface of the crushing barrel (701) is provided with a cylindrical crushing groove (10), the bottom surface of the cylindrical crushing groove (10) is in sliding contact with a crushing disc (705), the cylindrical crushing groove (10) is fixedly connected with one end of a supporting spring (704), two ends of the cylindrical crushing groove (10) are provided with cylindrical guide discs with right-angled triangle-shaped cross sections, and the cylindrical guide discs are fixedly installed on the inner wall of the crushing barrel (701).
4. The plant active ingredient extraction apparatus for pharmaceutical raw material preparation according to claim 2, characterized in that: supplementary reducing mechanism (8) are including being fan housing (801) of circular truncated cone face form, fan housing (801) right flank is equipped with air inlet (802), and air inlet (802) have liquid nitrogen tank (803) through pipe connection, fixed mounting has supplementary fan (804) in fan housing (801), supplementary fan (804) left side is equipped with electric heat silk screen (805), electric heat silk screen (805) left side is equipped with ultraviolet tube (806), be equipped with reflecting lens (807) around ultraviolet tube (806).
5. The plant active ingredient extraction apparatus for pharmaceutical raw material preparation according to claim 1, characterized in that: the mounting box (1) top is equipped with coarse crushing feed arrangement (2), coarse crushing feed arrangement (2) includes feeder hopper (201) and crushing pipe (202), feeder hopper (201) and crushing pipe (202) fixed connection, it has two striker plates (203) to articulate in feeder hopper (201), striker plate (203) top is equipped with limit baffle (204), and limit baffle (204) fixed mounting is on feeder hopper (201) inner wall, fixedly connected with reset spring (205) between striker plate (203) and feeder hopper (201) inner wall, movable mounting has two crushing post (206) in crushing pipe (202), two all be equipped with crushing groove (207) on crushing post (206), and crushing groove (207) interlock on two crushing post (206) is connected, be located the left crushing post (206) transmission is connected with crushing motor (208), the crushing motor (208) is fixedly arranged on the rear side surface in the installation box (1).
6. The plant active ingredient extraction apparatus for pharmaceutical raw material preparation according to claim 2, characterized in that: a continuous material guiding device (5) is connected between the effective component extracting mechanism (4) and the superfine grinding mechanism (3), the continuous material guiding device (5) comprises a dry powder guiding pipe (501) at the left side and a water slurry guiding pipe (502) at the right side, the dry powder guiding pipe (501) is movably mounted at the left end of a grinding barrel (701), a plurality of flow baffles (503) are arranged in the dry powder guiding pipe (501), the flow baffles (503) are arranged on the left side and the right side of the dry powder guiding pipe (501) at intervals, an arc-shaped filtering cavity (504) is arranged in the water slurry guiding pipe (502), a filter (505) is mounted at the bottom of the arc-shaped filtering cavity (504), a sewage discharging wheel (506) is movably mounted in the arc-shaped filtering cavity (504), a sewage discharging groove (507) is detachably arranged at the right side of the sewage discharging wheel (506), and the sewage discharging groove (507) penetrates through the right side of, the blowdown wheel (506) includes movable rod (5061), equidistant a plurality of blowdown separation blades (5062) that are equipped with of movable rod (5061), and blowdown separation blade (5062) and filter (505) upper surface sliding contact.
7. The plant active ingredient extraction apparatus for pharmaceutical raw material preparation according to claim 6, characterized in that: the filter (505) comprises a fixed frame (5051), a supporting net (5052) is fixedly installed at the bottom of the fixed frame (5051), four fixing plates (5053) with L-shaped sections are movably installed at the top of the fixed frame (5051) through hinges, a fixing spring (5054) is fixedly connected between the fixing plates (5053) and the supporting net (5052), and the left side face of the fixed fixing plate (5053) is in fit contact with the inner surface of the fixed frame (5051).
8. The plant active ingredient extraction apparatus for pharmaceutical raw material preparation according to claim 6, characterized in that: the intelligent control device (14) is installed on the installation box (1), the intelligent control device (14) comprises a single chip microcomputer (1401), the single chip microcomputer (1401) is electrically connected with a display (1402), controllable silicon (1403) is electrically connected between the output end of the single chip microcomputer (1401) and the ultrasonic generator (1101), the distillation heater (1204) and the water bath heater (1302), the output end of the single chip microcomputer (1401) is electrically connected with a liquid level meter (906), the output end of the single chip microcomputer (1401) is also electrically connected with a dry powder electromagnetic valve (1404), a water slurry electromagnetic valve (1405), a distillation temperature sensor (1406), a recrystallization temperature sensor (1407) and a leachate adding electromagnetic valve (1408), the dry powder electromagnetic valve (1404) is installed between the crushing barrel (701) and the dry powder guide pipe (501), and the water slurry electromagnetic valve (1405) is installed between the crushing barrel (701) and the water slurry guide pipe (502), the distillation temperature sensor (1406) is fixedly installed on the heating cup (1201), the recrystallization temperature sensor (1407) is fixedly installed on the inner wall of the water bath cup (1301), and the leachate adding electromagnetic valve (1408) is installed between the leachate adding box (904) and the leaching vessel (901).
CN201810239310.7A 2018-03-22 2018-03-22 Plant effective component extraction equipment for preparing medical raw materials Active CN108525341B (en)

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Application Number Priority Date Filing Date Title
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CN108525341A CN108525341A (en) 2018-09-14
CN108525341B true CN108525341B (en) 2021-01-01

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CN111701274B (en) * 2020-07-04 2021-01-22 青岛市第五人民医院 Traditional chinese medicine draws enrichment facility
CN112704903A (en) * 2020-11-30 2021-04-27 镇江波菲尔生物科技有限公司 Extraction equipment for biological medicine capable of reducing bacterial breeding
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