CN108498446A - A kind of hair conditioner and preparation method thereof for preventing hair quality impaired - Google Patents
A kind of hair conditioner and preparation method thereof for preventing hair quality impaired Download PDFInfo
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- CN108498446A CN108498446A CN201810755691.4A CN201810755691A CN108498446A CN 108498446 A CN108498446 A CN 108498446A CN 201810755691 A CN201810755691 A CN 201810755691A CN 108498446 A CN108498446 A CN 108498446A
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/35—Ketones, e.g. benzophenone
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/41—Amines
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
- A61K8/447—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof containing sulfur
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- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
- A61K8/65—Collagen; Gelatin; Keratin; Derivatives or degradation products thereof
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- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
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- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/04—Topical preparations for affording protection against sunlight or other radiation; Topical sun tanning preparations
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/002—Preparations for repairing the hair, e.g. hair cure
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/12—Preparations containing hair conditioners
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Abstract
The invention discloses a kind of hair conditioner and preparation method thereof for preventing hair quality impaired, belong to cosmetic field.The present invention is added small molecule keratin of the urea through reduction extraction, L cysteines is added using the rabbit hair as raw material so that keratin solution contains a large amount of cysteines, by addition glycerine and the jojoba oil with hair care effect, increases lubricant effect；Using butyl methoxydibenzoylmethise, octyl salicylate as raw material, two kinds of compoundings, which can absorb UVA, can also absorb UVB, prevent damage of the ultraviolet light to hair, with N vinyl pyrrolidones, dimethylaminopropyl methacrylamide etc. for raw material, initiator is added and is polymerize, elastic film forming agent is obtained through end-vinyl is dimethyl siloxane modified, it can be in the homogeneous film formation of hair surface, film forming thickness very little, be combined with hair surface, toughness it is good, increase the elasticity of hair.The present invention, which solves current hair conditioner, cannot preferably protect hair quality so that hair is withered, follows the string and the problem of flexibility.
Description
Technical field
The invention belongs to cosmetic fields, are specifically related to a kind of hair conditioner and preparation method thereof for preventing hair quality impaired.
Background technology
Hair conditioner is also known as Rinsing, is generally used in pairs with shampoo.Appropriate hair conditioner is uniformly applied on hair after hair washing,
It gently rubs one minute or so, then with clear water rinsed clean, therefore also someone is known as rinsing conditioner.Hair conditioner is divided into from mode of appearance
Two kinds of transparent type and emulsion-type, relatively conventional is emulsion type products in the market.Shampoo is with anion, non-ionic surface
Activating agent provides decontamination and foaming for primary raw material, and the primary raw material of hair conditioner is cationic surfactant.Shampoo
After cleaning hair, hair conditioner is reused, it can neutralize the molecule with anion that remains in hair surface, form monomolecular film,
And the hair of entanglement is made to obey, it is easy to comb.And the hair surface layer of health is by the oil of one group of complete hair scale piece and naturally secret
Fat constitutes the protective film of hair, and the natural protective film of this layer can all be destroyed by excessively washing reason, boiling hot dye, exposure in sunshine, lead to cortex moisture
It is lost in.Keep hair withered, follows the string and flexibility.Hair conditioner is only commonly used, could persistently form the protective film of hair,
Hair is set to escape injury.
Invention content
The technical problems to be solved by the invention：Hair quality cannot be preferably protected for current hair conditioner so that hair
It is withered, it follows the string and the problem of flexibility, provides a kind of hair conditioner and preparation method thereof for preventing hair quality impaired.
In order to solve the above technical problems, the present invention is using technical solution as described below：
A kind of hair conditioner for preventing hair quality impaired, including active permeation renovation agent, prevention of uv damages activating agent, elasticity film forming
Agent；
The preparation method of the active permeation renovation agent, includes the following steps：
Take the rabbit hair through sterile water washing, drying obtains the dry rabbit hair, takes urea in mass ratio 2 ~ 5：0.3~0.6：80 ~ 100 are added L-
Cysteine, deionized water are stirred, and obtain stirring mixture, take the dry rabbit hair in mass ratio 2 ~ 6：10 ~ 15, which are added stirring, mixes
Object is closed, pH to 9 ~ 10 is adjusted, is warming up to 70 ~ 75 DEG C and is stirred, is filtered, is taken filtrate to dialyse, take dialyzate in mass ratio 1 ~ 3：6
~ 9 are added polyethylene glycol-1000 0, stand, obtain standing liquid, take and stand liquid in mass ratio 10 ~ 15：1~3：2 ~ 5 be added glycerine, flash
Bar oil mixing 40 ~ 60min to get active permeation renovation agent.
The preparation method of the prevention of uv damages activating agent, includes the following steps：
Take butyl methoxydibenzoylmethise in mass ratio 3 ~ 5：1 ~ 3 addition octyl salicylate is stirred, and must be stirred
Object a takes 10 ~ 15 portions of stirring mixture a, 6 ~ 9 parts of Tween-80s, 3 ~ 5 parts of cetostearyl alcohols, 3 ~ 5 portions of coconuts according to the mass fraction
Base glucoside, 80 ~ 90 parts of water, 15 ~ 20 parts of isobutyl palmitates are stirred, and are cooled to room temperature to get prevention of uv damages
Activating agent.
The condition that is stirred of the prevention of uv damages activating agent is：It is stirred 30 ~ 50min in 50 ~ 70 DEG C.
It is characterized in that, the preparation method of the elasticity film forming agent, includes the following steps：
Take n-vinyl pyrrolidone, dimethylaminopropyl methacrylamide in mass ratio 5 ~ 9：3~5：3 ~ 7 are added end ethylene
Base dimethyl siloxane is stirred, and obtains mixture, takes mixture in mass ratio 1 ~ 3：8 ~ 10 are added ethyl alcohol, are passed through nitrogen guarantor
Shield is warming up to 65 ~ 75 DEG C of 4 ~ 6h of heat preservation, adds the ammonium persulfate of mixture quality 3 ~ 6%, it is stirred 2 in 70 ~ 75 DEG C ~
4h is cooled to room temperature to get elastic film forming agent.
The preparation method includes the following steps：
According to the mass fraction, 8 ~ 12 parts of elastic film forming agents, 10 ~ 15 portions of prevention of uv damages activating agents, 1 ~ 3 part of ethylene glycol list are taken
Stearate mixes, and is warming up to 70 ~ 80 DEG C and is stirred, obtain mixed liquor a, according to the mass fraction, 7 ~ 10 parts of active permeations is taken to repair
Multiple agent, 100 ~ 150 parts of water, 0.8 ~ 1.5 part of sodium citrate, 1 ~ 3 part of polylysine, 2 ~ 4 parts of grapefruit essence, 4 ~ 6 parts of surface-actives
Agent is stirred in 30 ~ 40 DEG C, obtains mixed liquor b, is taken mixed liquor a to be added in mixed liquor b, is stirred 1 ~ 2h to get preventing from sending out
The impaired hair conditioner of matter.
It is described that take the mass ratio of mixed liquor a and mixed liquor b be 3 ~ 5：8~10.
The surfactant is：Take double hexadecyl trimethyl ammonium chloride in mass ratio 4 ~ 7：2 ~ 4 are added octadecyl
Trimethyl ammonium chloride mixes to get surfactant.
Compared with other methods, advantageous effects are the present invention：
（1）The present invention is added small molecule keratin of the urea through reduction extraction, L-cysteine is added, makes using the rabbit hair as raw material
It obtains keratin solution and contains a large amount of cysteines, the cortical layer of hair can be penetrated into, the hydrophilic radical with exposure in damaged hair
Crosslinking bonding plays the role of reparation, moisturizing, by the way that glycerine is added and with the jojoba oil of hair care, increases lubrication effect
Fruit promotes small molecule keratin to enter hair faster with other active materials, accelerates the onset time of hair conditioner；
（2）For the present invention using butyl methoxydibenzoylmethise, octyl salicylate as raw material, two kinds of compoundings can absorb UVA
UVB can be absorbed, prevents damage of the ultraviolet light to hair, butyl methoxydibenzoylmethise contains can be with amino, carboxylic in hair
Base forms the alcoholic extract hydroxyl group of hydrogen bond, and the ability for forming hydrogen bond is strong, and octyl salicylate introduces ester group and phenyl ring hydroxyl, thermodynamics
Motion intense so that more molecules are adsorbed in hair surface, because hair surface is negatively charged, double hexadecyl front three
Ammonium chloride, octadecyltrimethylammonium chloride built surfactant with the negative electrical charge of hair surface with can mutually inhale
The positive charge drawn makes hair surface cover again so as to effectively adsorb pre- UV resistance damagine activity agent in hair surface
The hydrophobic protection of last layer, can repair the aliphatic acid protective film that hair is lost in because dyeing and perm etc. is nursed, and the electric conductivity of quaternary ammonium salt also can
Reduce hair electrostatic accumulation, reduce hair float and improve Hair setting, so it simultaneously can also make hair become it is smooth,
It is soft；
（3）The present invention with n-vinyl pyrrolidone, dimethylaminopropyl methacrylamide etc. for raw material, be added initiator into
Row polymerization, obtain elastic film forming agent through end-vinyl is dimethyl siloxane modified, can in the homogeneous film formation of hair surface, and at
Film thickness very little, be combined with hair surface, toughness it is good, increase the elasticity of hair, hair conditioner active material be sealed in film
It is inside adsorbed on hair, is wrapped up, introduce dimethyl silicone polymer in film forming matter, Si-O key ratios C- in molecular structure
C key lengths are longer, and bond angle is relatively flat so that obtained elastic film forming agent its polymer chain is very flexible, and is easy rotation
Turn, meanwhile, the surface tension of methyl group is relatively low, so providing very low surface tension of liquid, is easy to spread over hair table
Face, levelability is good, so that the glossiness of hair is promoted.
Specific implementation mode
Active permeation renovation agent：Take the rabbit hair through sterile water washing, drying obtains the dry rabbit hair, takes urea in mass ratio 2 ~ 5：
0.3~0.6：80 ~ 100 addition L-cysteines, deionized water are stirred 20 ~ 30min, obtain stirring mixture, take the dry rabbit hair
In mass ratio 2 ~ 6：10 ~ 15 are added stirring mixture, adjust pH to 9 ~ 10, are warming up to 70 ~ 75 DEG C and are stirred 3 ~ 5h, filter,
It takes filtrate to dialyse 2 ~ 4 days, takes dialyzate in mass ratio 1 ~ 3：6 ~ 9 addition polyethylene glycol-1000 0, standing 18 ~ for 24 hours, it must stand
Liquid takes and stands liquid in mass ratio 10 ~ 15：1~3：2 ~ 5 addition glycerine, jojoba oil mix 40 ~ 60min and are repaiied to get active permeation
Multiple agent.
Prevention of uv damages activating agent：Take butyl methoxydibenzoylmethise in mass ratio 3 ~ 5：1 ~ 3 is added bigcatkin willow
Misery ester, is stirred 20 ~ 30min, must stir mixture a, according to the mass fraction, take 10 ~ 15 parts of stirring mixture a, 6 ~ 9 parts
Tween-80,3 ~ 5 parts of cetostearyl alcohols, 3 ~ 5 parts of coco group glucosides, 80 ~ 90 parts of water, 15 ~ 20 parts of isobutyl palmitates, in 50 ~
70 DEG C are stirred 30 ~ 50min, are cooled to room temperature to get prevention of uv damages activating agent.
Elastic film forming agent：Take n-vinyl pyrrolidone, dimethylaminopropyl methacrylamide in mass ratio 5 ~ 9：3~
5：3 ~ 7 addition end-vinyl dimethyl siloxanes are stirred 20 ~ 30min, obtain mixture, take mixture in mass ratio 1 ~ 3：8~
10 are added the ethyl alcohol that mass fraction is 80%, are passed through nitrogen protection, are warming up to 65 ~ 75 DEG C, keep the temperature 4 ~ 6h, add compounding substances
The ammonium persulfate of amount 3 ~ 6%, is stirred 2 ~ 4h in 70 ~ 75 DEG C, is cooled to room temperature to get elastic film forming agent.
Surfactant：Take double hexadecyl trimethyl ammonium chloride in mass ratio 4 ~ 7：2 ~ 4 are added octadecyl trimethyl
Ammonium chloride mixes to get surfactant.
A kind of preparation method for the hair conditioner for preventing hair quality impaired, includes the following steps：
According to the mass fraction, 8 ~ 12 parts of elastic film forming agents, 10 ~ 15 portions of prevention of uv damages activating agents, 1 ~ 3 part of ethylene glycol list are taken
Stearate mixes, and is warming up to 70 ~ 80 DEG C and is stirred 30 ~ 40min, obtain mixed liquor a, according to the mass fraction, takes 7 ~ 10 parts of work
Property infiltration renovation agent, 100 ~ 150 parts of water, 0.8 ~ 1.5 part of sodium citrate, 1 ~ 3 part of polylysine, 2 ~ 4 parts of grapefruit essence, 4 ~ 6 parts
Surfactant is stirred 20 ~ 30min in 30 ~ 40 DEG C, obtains mixed liquor b, takes mixed liquor a in mass ratio 3 ~ 5：8 ~ 10 are added
Mixed liquor b is stirred 1 ~ 2h to get the hair conditioner for preventing hair quality impaired.
Embodiment 1
Active permeation renovation agent：Take the rabbit hair through sterile water washing, drying obtains the dry rabbit hair, takes urea in mass ratio 2：0.3：80
Addition L-cysteine, deionized water are stirred 20min, obtain stirring mixture, take the dry rabbit hair in mass ratio 2：10 are added
Mixture is stirred, pH to 9 is adjusted, is warming up to 70 DEG C and is stirred 3h, is filtered, takes filtrate to dialyse 2 days, takes dialyzate in mass ratio
1：6 are added polyethylene glycol-1000 0, stand 18h, obtain standing liquid, take and stand liquid in mass ratio 10：1：2 are added glycerine, Jojoba
40min is to get active permeation renovation agent for oil mixing.
Prevention of uv damages activating agent：Take butyl methoxydibenzoylmethise in mass ratio 3：1 addition bigcatkin willow is misery
Ester is stirred 20min, must stir mixture a, according to the mass fraction, take 10 parts of stirring mixture a, 6 parts of Tween-80s, 3 parts
Cetostearyl alcohol, 3 parts of coco group glucosides, 80 parts of water, 15 parts of isobutyl palmitates, are stirred 30min in 50 DEG C, are cooled to
Room temperature is to get prevention of uv damages activating agent.
Elastic film forming agent：Take n-vinyl pyrrolidone, dimethylaminopropyl methacrylamide in mass ratio 5：3：3 add
Enter end-vinyl dimethyl siloxane and be stirred 20min, obtain mixture, takes mixture in mass ratio 1：8 are added mass fraction
For 80% ethyl alcohol, it is passed through nitrogen protection, is warming up to 65 DEG C, 4h is kept the temperature, the ammonium persulfate of mixture quality 3% is added, in 70
DEG C it is stirred 2h, is cooled to room temperature to get elastic film forming agent.
Surfactant：Take double hexadecyl trimethyl ammonium chloride in mass ratio 4：2 are added octadecyl trimethyl chlorination
Ammonium mixes to get surfactant.
A kind of preparation method for the hair conditioner for preventing hair quality impaired, includes the following steps：
According to the mass fraction, 8 parts of elastic film forming agents, 10 portions of prevention of uv damages activating agents, 1 part of ethylene glycol monostearate are taken
Mixing, be warming up to 70 DEG C and be stirred 30min, obtain mixed liquor a, according to the mass fraction, take 7 parts of active permeation renovation agents, 100 parts
Water, 0.8 part of sodium citrate, 1 part of polylysine, 2 parts of grapefruit essence, 4 parts of surfactants, are stirred 20min in 30 DEG C, obtain
Mixed liquor b takes mixed liquor a in mass ratio 3：8 are added mixed liquor b, are stirred 1h to get the hair conditioner for preventing hair quality impaired.
Embodiment 2
Active permeation renovation agent：Take the rabbit hair through sterile water washing, drying obtains the dry rabbit hair, takes urea in mass ratio 3：0.4：90
Addition L-cysteine, deionized water are stirred 25min, obtain stirring mixture, take the dry rabbit hair in mass ratio 4：12 are added
Mixture is stirred, pH to 9.5 is adjusted, is warming up to 73 DEG C and is stirred 4h, is filtered, takes filtrate to dialyse 3 days, takes dialyzate by quality
Than 2：7 are added polyethylene glycol-1000 0, stand 21h, obtain standing liquid, take and stand liquid in mass ratio 12：2：3 be added glycerine, flash
Bar oil mixing 50min to get active permeation renovation agent.
Prevention of uv damages activating agent：Take butyl methoxydibenzoylmethise in mass ratio 4：2 addition bigcatkin willows are misery
Ester is stirred 25min, must stir mixture a, according to the mass fraction, take 12 parts of stirring mixture a, 7 parts of Tween-80s, 4 parts
Cetostearyl alcohol, 4 parts of coco group glucosides, 85 parts of water, 17 parts of isobutyl palmitates, are stirred 40min in 60 DEG C, are cooled to
Room temperature is to get prevention of uv damages activating agent.
Elastic film forming agent：Take n-vinyl pyrrolidone, dimethylaminopropyl methacrylamide in mass ratio 7：4：5 add
Enter end-vinyl dimethyl siloxane and be stirred 25min, obtain mixture, takes mixture in mass ratio 2：9 are added mass fraction
For 80% ethyl alcohol, it is passed through nitrogen protection, is warming up to 70 DEG C, 5h is kept the temperature, the ammonium persulfate of mixture quality 4% is added, in 73
DEG C it is stirred 3h, is cooled to room temperature to get elastic film forming agent.
Surfactant：Take double hexadecyl trimethyl ammonium chloride in mass ratio 5：3 are added octadecyl trimethyl chlorination
Ammonium mixes to get surfactant.
A kind of preparation method for the hair conditioner for preventing hair quality impaired, includes the following steps：
According to the mass fraction, 10 parts of elastic film forming agents, 13 portions of prevention of uv damages activating agents, 2 parts of ethylene glycol monostearates are taken
Ester mixes, and is warming up to 75 DEG C and is stirred 35min, obtain mixed liquor a, according to the mass fraction, takes 9 parts of active permeation renovation agents, 130
Part water, 1.2 parts of sodium citrates, 2 parts of polylysines, 3 parts of grapefruit essence, 5 parts of surfactants, 25min is stirred in 35 DEG C,
Mixed liquor b is obtained, mixed liquor a in mass ratio 4 is taken：9 are added mixed liquor b, are stirred 1.5h to get the hair care for preventing hair quality impaired
Element.
Embodiment 3
Active permeation renovation agent：Take the rabbit hair through sterile water washing, drying obtains the dry rabbit hair, takes urea in mass ratio 5：0.6：100
Addition L-cysteine, deionized water are stirred 30min, obtain stirring mixture, take the dry rabbit hair in mass ratio 6：15 are added
Mixture is stirred, pH to 10 is adjusted, is warming up to 75 DEG C and is stirred 5h, is filtered, takes filtrate to dialyse 4 days, takes dialyzate by quality
Than 3：9 are added polyethylene glycol-1000 0, stand for 24 hours, obtain standing liquid, take and stand liquid in mass ratio 15：3：5 be added glycerine, flash
Bar oil mixing 60min to get active permeation renovation agent.
Prevention of uv damages activating agent：Take butyl methoxydibenzoylmethise in mass ratio 5：3 addition bigcatkin willows are misery
Ester is stirred 30min, must stir mixture a, according to the mass fraction, take 15 parts of stirring mixture a, 9 parts of Tween-80s, 5 parts
Cetostearyl alcohol, 5 parts of coco group glucosides, 90 parts of water, 20 parts of isobutyl palmitates, are stirred 50min in 70 DEG C, are cooled to
Room temperature is to get prevention of uv damages activating agent.
Elastic film forming agent：Take n-vinyl pyrrolidone, dimethylaminopropyl methacrylamide in mass ratio 9：5：7 add
Enter end-vinyl dimethyl siloxane and be stirred 30min, obtain mixture, takes mixture in mass ratio 3：10 are added mass fraction
For 80% ethyl alcohol, it is passed through nitrogen protection, is warming up to 75 DEG C, 6h is kept the temperature, the ammonium persulfate of mixture quality 6% is added, in 75
DEG C it is stirred 4h, is cooled to room temperature to get elastic film forming agent.
Surfactant：Take double hexadecyl trimethyl ammonium chloride in mass ratio 7：4 are added octadecyl trimethyl chlorination
Ammonium mixes to get surfactant.
A kind of preparation method for the hair conditioner for preventing hair quality impaired, includes the following steps：
According to the mass fraction, 12 parts of elastic film forming agents, 15 portions of prevention of uv damages activating agents, 3 parts of ethylene glycol monostearates are taken
Ester mix, be warming up to 80 DEG C and be stirred 40min, obtain mixed liquor a, according to the mass fraction, take 10 parts of active permeation renovation agents,
150 parts of water, 1.5 parts of sodium citrates, 3 parts of polylysines, 4 parts of grapefruit essence, 6 parts of surfactants, are stirred in 40 DEG C
30min obtains mixed liquor b, takes mixed liquor a in mass ratio 5：10 are added mixed liquor b, are stirred 2h to get preventing hair quality impaired
Hair conditioner.
Comparative example 1：It is essentially identical with the preparation method of embodiment 1, it has only the difference is that lacking active permeation renovation agent.
Comparative example 2：It is essentially identical with the preparation method of embodiment 1, it has only the difference is that lacking prevention of uv damages work
Property agent.
Comparative example 3：It is essentially identical with the preparation method of embodiment 1, it has only the difference is that lacking elastic film forming agent.
Comparative example 4：The hair conditioner of Shanghai City company production.
Detection result on probation is carried out to embodiment 1-3 and comparative example the 1-4 product prepared.140 people are randomly selected to implementing
Example 1~3, comparative example 1~4 and commercially available product product are tried out, and daily using once, are used 1 month altogether.Result on trial is counted,
Every using effect total score is 5 points：5 points are best result, indicate fine；4 points are preferable；3 points are that can receive；2 points are bad；
1 point is that cannot receive.It is every average below, result on trial refers to table 1：
Table 1：
In summary, hair conditioner of the invention can preferably protect hair quality so that and hair water moistens, and elasticity and flexibility are all fine,
It is worth of widely use.
Claims (7)
1. a kind of hair conditioner for preventing hair quality impaired, which is characterized in that live including active permeation renovation agent, prevention of uv damages
Property agent, elastic film forming agent；
The preparation method of the active permeation renovation agent, includes the following steps：
Take the rabbit hair through sterile water washing, drying obtains the dry rabbit hair, takes urea in mass ratio 2 ~ 5：0.3~0.6：80 ~ 100 are added L-
Cysteine, deionized water are stirred, and obtain stirring mixture, take the dry rabbit hair in mass ratio 2 ~ 6：10 ~ 15, which are added stirring, mixes
Object is closed, pH to 9 ~ 10 is adjusted, is warming up to 70 ~ 75 DEG C and is stirred, is filtered, is taken filtrate to dialyse, take dialyzate in mass ratio 1 ~ 3：6
~ 9 are added polyethylene glycol-1000 0, stand, obtain standing liquid, take and stand liquid in mass ratio 10 ~ 15：1~3：2 ~ 5 be added glycerine, flash
Bar oil mixing 40 ~ 60min to get active permeation renovation agent.
2. the hair conditioner according to claim 1 for preventing hair quality impaired, which is characterized in that the prevention of uv damages is lived
The preparation method of property agent, includes the following steps：
Take butyl methoxydibenzoylmethise in mass ratio 3 ~ 5：1 ~ 3 addition octyl salicylate is stirred, and must be stirred
Object a takes 10 ~ 15 portions of stirring mixture a, 6 ~ 9 parts of Tween-80s, 3 ~ 5 parts of cetostearyl alcohols, 3 ~ 5 portions of coconuts according to the mass fraction
Base glucoside, 80 ~ 90 parts of water, 15 ~ 20 parts of isobutyl palmitates are stirred, and are cooled to room temperature to get prevention of uv damages
Activating agent.
3. the hair conditioner according to claim 2 for preventing hair quality impaired, which is characterized in that the prevention of uv damages is lived
The condition that is stirred of property agent is：It is stirred 30 ~ 50min in 50 ~ 70 DEG C.
4. the preparation method of the hair conditioner according to claim 1 for preventing hair quality impaired, which is characterized in that the elasticity at
The preparation method of film, includes the following steps：
Take n-vinyl pyrrolidone, dimethylaminopropyl methacrylamide in mass ratio 5 ~ 9：3~5：3 ~ 7 are added end ethylene
Base dimethyl siloxane is stirred, and obtains mixture, takes mixture in mass ratio 1 ~ 3：8 ~ 10 are added ethyl alcohol, are passed through nitrogen guarantor
Shield is warming up to 65 ~ 75 DEG C of 4 ~ 6h of heat preservation, adds the ammonium persulfate of mixture quality 3 ~ 6%, it is stirred 2 in 70 ~ 75 DEG C ~
4h is cooled to room temperature to get elastic film forming agent.
5. a kind of preparation method of hair conditioner for preventing hair quality impaired as described in claim 1 ~ 4 any one, feature exist
In the preparation method includes the following steps：
According to the mass fraction, 8 ~ 12 parts of elastic film forming agents, 10 ~ 15 portions of prevention of uv damages activating agents, 1 ~ 3 part of ethylene glycol list are taken
Stearate mixes, and is warming up to 70 ~ 80 DEG C and is stirred, obtain mixed liquor a, according to the mass fraction, 7 ~ 10 parts of active permeations is taken to repair
Multiple agent, 100 ~ 150 parts of water, 0.8 ~ 1.5 part of sodium citrate, 1 ~ 3 part of polylysine, 2 ~ 4 parts of grapefruit essence, 4 ~ 6 parts of surface-actives
Agent is stirred in 30 ~ 40 DEG C, obtains mixed liquor b, is taken mixed liquor a to be added in mixed liquor b, is stirred 1 ~ 2h to get preventing from sending out
The impaired hair conditioner of matter.
6. the preparation method of the hair conditioner according to claim 5 for preventing hair quality impaired, which is characterized in that described to take mixing
The mass ratio of liquid a and mixed liquor b is 3 ~ 5：8~10.
7. the preparation method of the hair conditioner according to claim 5 for preventing hair quality impaired, which is characterized in that live on the surface
Property agent is：Take double hexadecyl trimethyl ammonium chloride in mass ratio 4 ~ 7：2 ~ 4 are added octadecyltrimethylammonium chloride mixing, i.e.,
Obtain surfactant.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
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