CN108497548A - A kind of stem of noble dendrobium medicinal extract and its application in cigarette - Google Patents
A kind of stem of noble dendrobium medicinal extract and its application in cigarette Download PDFInfo
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- CN108497548A CN108497548A CN201810251818.9A CN201810251818A CN108497548A CN 108497548 A CN108497548 A CN 108497548A CN 201810251818 A CN201810251818 A CN 201810251818A CN 108497548 A CN108497548 A CN 108497548A
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- noble dendrobium
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/24—Treatment of tobacco products or tobacco substitutes by extraction; Tobacco extracts
- A24B15/26—Use of organic solvents for extraction
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/12—Steaming, curing, or flavouring tobacco
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- General Chemical & Material Sciences (AREA)
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Abstract
The present invention provides a kind of stem of noble dendrobium medicinal extract and its application in cigarette, and the stem of noble dendrobium medicinal extract is made by the method for following steps：By stem of noble dendrobium stem crushed after being dried, dendrobe powder is obtained, then gained dendrobe powder is added to the in the mixed solvent of ethyl alcohol and ethyl acetate, the volume ratio of ethyl alcohol and ethyl acetate is 1：1, after being heated to reflux a period of time, filtrate is left and taken in filtering, and filtering is residue obtained wash repeatedly with the mixed solvent and leave and take washing lotion, merge obtained by filtrate and washing lotion, remove under reduced pressure after solvent to get the stem of noble dendrobium medicinal extract.The stem of noble dendrobium medicinal extract is added in cigarette, can preferably reduce the irritation of cigarette, cover miscellaneous gas, improve sweet degree, improve pleasant impression, keep cigarette perfume finer and smoother, soft.
Description
Technical field
The invention belongs to cigarette additive technical fields, and in particular to a kind of stem of noble dendrobium medicinal extract and its application in cigarette.
Background technology
Cigarette irritation refer to cigarette in combustion flue gas to the human body sensories organ such as oral cavity, throat, nasal cavity, eyes
Caused by slight or significant discomfort.The strong cigarette of irritation often covers cigarette perfume, and flue gas is after sucking oral cavity, tongue
Portion can obviously feel bitter taste or pungent, feel that the tip of the tongue is dry and astringent later, as having eaten immature persimmon；Flue gas enters with air
During lung, obvious stimulation is had to throat, throat is caused to tighten, causes strong cough；When being breathed out from nasal cavity, make nose
Chamber is dry and astringent, generates the breath for the people that chokes；Meanwhile flue gas stimulation eyes cause to shed tears, make one to be not felt by the intrinsic fragrance of cigarette and
Taste.Since the difference of tobacco leaf type, planting environment, weather conditions, harvesting opportunity, baking process and alcoholization technique etc. is made
At influence, make its appearance, physical behavior, chemical composition and inherent quality etc. generate larger difference, and inevitably generate
Slight or significant bad breath, such as the smell of soil, pollen gas, green grass gas, rosin gas, withered and burnt smell, the miscellaneous gas of region.Cause
How this, reduce the irritation of cigarette and cover miscellaneous gas and inhale comfort level with the product for improving cigarette, become an important research
Project.
The stem of noble dendrobium is orchid, and stem is straight, fleshy hypertrophy in slightly oblate cylindricality, and the florescence is white in the 4-5 months, is grown on more
Intermountain, a large amount of artificial breeding, mainly originate in subtropical zone, such as Anhui, Sichuan, Guizhou, Yunnan, Guangxi etc..The stem of noble dendrobium
In golden yellow after stem is dry, it is important Chinese medicine, is rich in carbohydrate, glycoside, alcohols, aldehydes, acids, lipid and amine chemical combination
Object has sweet taste, tart flavour, causes fragrant and pharmacological properties, and due to the presence of these organic compounds so that the stem of noble dendrobium has anti-swollen
Tumor, anticoagulation, anti-cataract, anti-acetylcholinesterase, anti-liver injury, adjusts blood glucose, adjusts machine anti-oxidant, antifatigue, antibacterial
Body is immune, excitement intestinal tube, reinforcing stomach reg fluid, nourishing Yin and clearing heat, protection nerve, promotees the multi-efficiencies such as digestion, promotion salivary secretion, now makees
It is widely applied in tea, wine, food and drug for drug and health products.
The researchers of tobacco business also are being dedicated to the stem of noble dendrobium for integrating a variety of benefits being applied in cigarette,
Such as Chinese invention patent CN102715650A discloses a kind of application of Dendrobium officinale polysaccharide in cigarette, the iron sheet stone
The dosage of dry measure used in former times polysaccharide is 0.02 ‰ -0.2 ‰ of tobacco quality in cigarette, and the preparation method of the Dendrobium officinale polysaccharide includes：It will
Dendrobium candidum extracts in water after dry, pulverize after cleaning, and obtains extracting solution, through centrifuging and being filtered by vacuum after cooling, filtrate is true
Sky concentration, obtains concentrate；It is centrifuged after concentrate alcohol precipitation, collects precipitation, up to dendrobium candidum Thick many candies after freeze-drying.But
Only containing carbohydrate and a small amount of alcohols and acid compounds in the dendrobium polysaccharide that the patent water raises, when the addition of dendrobium polysaccharide
When amount is smaller with pipe tobacco proportion, reduces the irritating effect of cigarette and be not obvious, and when the additive amount of dendrobium polysaccharide and pipe tobacco ratio
It weighs to after 0.2 ‰, contents of saccharide is excessively high, and it is thin out to instead result in smoke, and generates miscellaneous gas, and pleasant impression owes comfortable；For another example middle promulgated by the State Council
Bright patent CN105132162A discloses a kind of stem of noble dendrobium triacetyl glycerine extract and its application in cigarette：It is dry to clean
Dry, grain size is that the dendrobium candidum powder of 20-40 mesh is raw material, and triacetyl glycerine is extractant, and use first is heated to reflux
Mode is extracted, and stem of noble dendrobium triacetyl glycerine extract then is prepared by ultrasonic wave extraction.The triacetyl glycerine of the stem of noble dendrobium
Extract main component is flavor matters and the drugs such as esters, aldehydes, ketone, dendrobium candidum element, can reduce cigarette irritation,
Cigarette foreign gas is covered, but due to lacking carbohydrate and acid compounds, the alkaline matters such as the nicotine in pipe tobacco and flue gas can not be neutralized,
Sweet sense cannot be increased, and when additive amount is larger, dendrobium candidum element class too high levels generate stem of noble dendrobium taste instead, cover cigarette perfume.
Invention content
The present invention for the problem of stem of noble dendrobium medicinal extract is applied to cigarette in the prior art, provide a kind of stem of noble dendrobium medicinal extract and
Its application in cigarette is added in cigarette, can preferably reduce the irritation of cigarette, cover miscellaneous gas, improve sweet degree,
Improve pleasant impression, keep cigarette perfume finer and smoother, soft.
The present invention adopts the following technical scheme that：
A kind of stem of noble dendrobium medicinal extract is made by the method for following steps：By stem of noble dendrobium stem crushed after being dried, dendrobe powder is obtained, then
Gained dendrobe powder is added to the in the mixed solvent of ethyl alcohol and ethyl acetate, the volume ratio of ethyl alcohol and ethyl acetate is 1：1, heating
It flows back after a period of time, filtrate is left and taken in filtering, and filtering is residue obtained to be washed repeatedly with the mixed solvent and leave and take washing lotion, is merged
Gained filtrate and washing lotion remove under reduced pressure after solvent to get the stem of noble dendrobium medicinal extract.
Preferably, the w/v of the dendrobe powder and the mixed solvent is 1g:（2~10）mL.
Application of the above-mentioned stem of noble dendrobium medicinal extract in cigarette, the stem of noble dendrobium medicinal extract are added with 0.10 ‰ ~ 0.15 ‰ weight percent
It is added in pipe tobacco and uses.
Preferably, it after stem of noble dendrobium medicinal extract being diluted with solvent, is uniformly sprayed on pipe tobacco.
Beneficial effects of the present invention are as follows：
Medicinal extract used in the present invention is the stem of Dendrobium dry extracts obtained as mixed extractant solvent using ethyl alcohol and ethyl acetate, is prepared
Simply, at low cost, less energy consumption, property is stablized, and has no toxic side effect；Meanwhile with the stem of noble dendrobium water or three triacetins that are previously reported
Ester extract is compared, the chemical composition type contained is more, content higher, especially carbohydrate, glycoside, alcohols, aldehydes, acid
The compounds such as class, lipid and amine, they have sweet taste, tart flavour, cause fragrant and pharmacological properties, are added in cigarette, can be more preferable
Ground reduces the irritation of cigarette, covers miscellaneous gas, improve sweet degree, improve pleasant impression, keep cigarette perfume finer and smoother, soft, is more suitable as
The additive of cigarette.
Specific implementation mode
In order to keep the technical purpose, technical solution and advantageous effect of the present invention clearer, with reference to specific embodiment
Technical scheme of the present invention is further illustrated.
Embodiment 1
A kind of stem of noble dendrobium medicinal extract, is prepared by the following method to obtain：Stem of noble dendrobium stem is put into vacuum drying oven, drying temperature is preferred
40 ~ 70 DEG C, in the present embodiment, 40 DEG C of constant temperature are selected, fully after drying, in natural cooling in baking oven, are taken out；Then 200 are weighed
Stem of noble dendrobium stem after g dryings, is crushed with grinder, obtains dendrobe powder, and the purpose of crushing is to make the granularity of dendrobe powder as far as possible
Carefully, it is convenient for the high efficiency extraction of wherein ingredient；Gained dendrobe powder is transferred completely into the round-bottomed flask of 1000 mL, adds 375
mL 95%（Mass fraction）Ethyl alcohol and 375 mL ethyl acetate in the mixed solvent, heating water bath flow back 8h, stop heating after,
Filtrate is left and taken in filtering while hot, and filtering is residue obtained to wash three times with aforementioned mixed solvent and leave and take washing lotion, merging filtrate and washing lotion,
After cooling, solvent is removed under reduced pressure, obtain orange red thick liquid, the as ethyl alcohol of the stem of noble dendrobium and the extraction leaching of ethyl acetate mixed solvent
Cream has great stem of noble dendrobium taste and fragrant and sweet taste.
Embodiment 2
A kind of stem of noble dendrobium medicinal extract, is prepared by the following method to obtain：Stem of noble dendrobium stem is put into vacuum drying oven, in 60 DEG C of constant temperature items
After fully being dried under part, in natural cooling in baking oven, take out；Then the stem of noble dendrobium stem after 200 g dryings is weighed, with grinder powder
It is broken, obtain dendrobe powder；Gained dendrobe powder is transferred completely into the round-bottomed flask of 1500 mL, adds 500 mL 95%（Quality
Score）Ethyl alcohol and 500mL ethyl acetate in the mixed solvent, heating water bath flow back 6h, stop heating after, while hot filtering leave and take
Filtrate, filtering is residue obtained to wash twice with aforementioned mixed solvent and leaves and takes washing lotion, merging filtrate and washing lotion, after cooling, decompression
Solvent is evaporated off, obtains orange red thick liquid, the as ethyl alcohol of the stem of noble dendrobium and ethyl acetate mixed solvent extracts medicinal extract, has very big
Stem of noble dendrobium taste and fragrant and sweet taste.
The contrast test of the Herba Dendrobii extract of different solvents extraction
1）Experimental design
1. raw material：Stem of noble dendrobium stem；
2. extracting method：Respectively with water, triacetyl glycerine and absolute ethyl alcohol and ethyl acetate（Volume ratio 1:1）Mixing it is molten
Extractant is made in agent, and by the organic matter being heated to reflux in the fully extraction stem of noble dendrobium, the stem of noble dendrobium medicinal extract of three kinds of different solvents extraction is made；
3. the application method of extract：The stem of noble dendrobium medicinal extract that three kinds of different solvents extract is dissolved in ethyl alcohol and distilled water respectively（Volume
Than 1:4）In the mixed solvent, be then added in pipe tobacco with gradient proportion, cigarette be made；
4. to add the cigarette made by the pipe tobacco of medicinal extract as experiment cigarette, and experiment cigarette is carried comprising water, three triacetins
Ester carries and absolute ethyl alcohol and ethyl acetate carry three groups, while will be not added with cigarette made by the pipe tobacco of medicinal extract cigarette as a contrast
Branch carries out comparison by judging panel and smokes panel test.
Extracting method is respectively described below：
Water extracting process：By stem of noble dendrobium stem be put into 60 DEG C of constant-temperature vacuum baking ovens it is fully dry after, in natural cooling in baking oven, take
Go out.200 g are weighed, are crushed with grinder, are transferred in 1000 mL round-bottomed flasks, 750 mL distilled water are added, oil bath adds
8~10 h of heat reflux are filtered while hot after stopping heating, and the distillation water washing of residue heat three times, after filtrate cooling, steam by decompression
Except solvent, pale yellow viscous liquid is obtained, i.e. the water of the stem of noble dendrobium extracts extractum A, has weaker pungent fragrant and certain sweet taste.
Triacetyl glycerine extracting process：By stem of noble dendrobium stem be put into 60 DEG C of constant-temperature vacuum baking ovens it is fully dry after, in baking oven
Interior natural cooling is taken out.200 g are weighed, are crushed with grinder, are transferred in 1000 mL round-bottomed flasks, 750 mL tri- are added
Acetoglyceride, 6~8 h of heating mantle heats reflux are filtered, the triacetyl glycerine of residue heat is washed while hot after stopping heating
It washs three times, after filtrate cooling, removes solvent under reduced pressure, obtain orange-yellow thick liquid, i.e. the triacetyl glycerine extraction leaching of the stem of noble dendrobium
Cream B has certain sweet taste and higher fragrance.
Ethyl alcohol and ethyl acetate mixed extractant solvent method：It is fully dry that stem of noble dendrobium stem is put into 60 DEG C of constant-temperature vacuum baking ovens
Afterwards, it in natural cooling in baking oven, takes out.200 g are weighed, are crushed with grinder, are transferred in 1000 mL round-bottomed flasks, then are added
Enter the ethyl alcohol and 375 mL ethyl acetate of 375 mL 95%, 6~8 h of heating water bath reflux are filtered while hot after stopping heating, residual
Ethyl alcohol and ethyl acetate mixed solvent of the slag with 95%（Volume ratio 1：1）Washing three times, after filtrate cooling, removes solvent under reduced pressure, obtains
To orange red thick liquid, i.e. the ethyl alcohol of the stem of noble dendrobium and ethyl acetate mixed solvent extracts medicinal extract C, has great stem of noble dendrobium taste and perfume (or spice)
Sweet taste.
Three kinds of above-mentioned stem of noble dendrobium extractum As, B and the C of equivalent are weighed respectively, and use ethyl alcohol and distilled water respectively（Volume ratio 1:4）
It is diluted to the solution that mass percent is 5%, three kinds of medicinal extract solution of gained are uniformly sprayed on pipe tobacco, is made different molten respectively
Agent extraction stem of noble dendrobium extractum A, B or C and pipe tobacco weight percent be followed successively by 0.05 ‰, 0.1 ‰, 0.15 ‰, 0.20 ‰ plus
Expect that pipe tobacco, sealing place 4 h, is put into 100 DEG C of baking oven drying, is then humidified to standard moisture with distilled water（12%）, roll into reality
Test cigarette；The control cigarette not fed, experiment cigarette and the control equal equilibrium water conten of cigarette are set simultaneously（Humidity 60% ± 2%, temperature
25±1℃）It smokes panel test after 24 h.
2）Composition detection
With Agilent7890A-5975C type gas chromatograph-mass spectrometers（Anjelen Sci. ＆ Tech. Inc of the U.S.）With 400-MR nuclear magnetic resonance
Spectrometer（VARIAN Oncology Systems）The ingredient of three kinds of extractum As, B and C are analyzed, it is as a result as follows：
1. the water extraction medicinal extract ingredient of the stem of noble dendrobium is mainly rhamnose (rhamnose), arabinose (arabinose), mannose
(mannose), glucose (glucose) also contains a small amount of hentriacontanol (hentriacontanol), the white black false hellebore of dihydro
Alcohol (dihydrogen resveratrol), cupreol (β-sitosterol), dendrophnol (dendrophenol), vanillic aldehyde
(vanillin), syringic acid (syringic acid), vanillic acid (vanillic acid), para hydroxybenzene propionic acid (4-
Hydroxybenzene propanoic acid), hydroxycinnamic acid (4-hydroxycinnamic acid), ferulic acid
(ferulic acid), P-hydroxybenzoic acid (4-hydroxybenzoic acid), hexadecanoic acid (palmitic acid), ten
Seven alkanoic acids (daturic acid), naringenin (naringetol), rheum emodin (emodin), (+)-syringaresinol ((+)-
The organic substances such as syringaresinol).
2. the triacetyl glycerine extraction medicinal extract ingredient of the stem of noble dendrobium is mainly coniferyl aldehyde (coniferaldehyde), syringaldehyde
(syringaldehyde), 5- acetyl-o-methyls furfural (5-acetoxymethyl furfural), meta-methoxy cinnaldehydrum (3-
Methoxycinnamicaldehyde), 5 hydroxymethyl furfural (5-hydroxymethyl-2-furaldehyde), vanillic aldehyde
(vanillin), (+)-syringaresinol ((+)-syringaresinol), escoparone (scoparone), methyl succinate
(succinic acid methyl ester), para hydroxybenzene methyl propionate (methyl 3- (4-hydroxyphenyl)
Propionate), ferulic acid hexacosane ester (hexacosyl (E)-ferulate), digitalis lactone (digitalis
Lactone), 3 ', 5,5 ', 7- tetrahydroxys flavanone (3 ', 5,5 ', 7-tetracarbonyl dihydrogen
Flavonoids), daucosterol (daucosterol), dendrobium candidum element A (dendrobium officinale A), iron sheet stone
Dry measure used in former times element B (dendrobium officinale B), dendrobium candidum element C (dendrobium officinale C), dendrobium candidum
Plain D (dendrobium officinale D), dendrobium candidum element E (dendrobium officinale E), dendrobium candidum element F
(dendrobium officinale F), dendrobium candidum element G (dendrobium officinale G), dendrobium candidum element H
(dendrobium officinale H), dendrobium candidum element I (dendrobium officinale I), dendrobium candidum element J
(dendrobium officinale J), dendrobium candidum element K (dendrobium officinale K), dendrobium candidum element L
(dendrobium officinale L), dendrobium candidum element M (dendrobium officinale M), dendrobium candidum element N
(dendrobium officinale N), dendrobium candidum element O (dendrobium officinale O), dendrobium candidum element P
(dendrobium officinale P), dendrobium candidum element Q (dendrobium officinale Q) also contains micro
The organic substances such as carbohydrate, acids, glycoside.
Ethyl alcohol and ethyl acetate mixed solvent the extraction medicinal extract ingredient of the stem of noble dendrobium are abundant, are carried far more than water or triacetyl glycerine
Medicinal extract is taken, includes mainly：Rhamnose (rhamnose), arabinose (arabinose), mannose (mannose), glucose
(glucose), hentriacontanol (hentriacontanol), dihydro resveratrol (dihydrogen resveratrol), β-
Sitosterol (β-sitosterol), dendrophnol (dendrophenol), coniferyl aldehyde (coniferaldehyde), syringaldehyde
(syringaldehyde), 5- acetyl-o-methyls furfural (5-acetoxymethyl furfural), meta-methoxy cinnaldehydrum (3-
Methoxycinnamicaldehyde), 5 hydroxymethyl furfural (5-hydroxymethyl-2-furaldehyde), vanillic aldehyde
(vanillin), syringic acid (syringic acid), vanillic acid (vanillic acid), para hydroxybenzene propionic acid (4-
Hydroxybenzene propanoic acid), hydroxycinnamic acid (4-hydroxycinnamic acid), ferulic acid
(ferulic acid), P-hydroxybenzoic acid (4-hydroxybenzoic acid), hexadecanoic acid (palmitic acid), ten
Seven alkanoic acids (daturic acid), naringenin (naringetol), rheum emodin (emodin), (+)-syringaresinol ((+)-
Syringaresinol), escoparone (scoparone), methyl succinate (succinic acid methyl ester), right
Hydroxy phenylpropionic acid methyl esters (methyl 3- (4-hydroxyphenyl) propionate), ferulic acid hexacosane ester
(hexacosyl (E)-ferulate), digitalis lactone (digitalis lactone), 3 ', 5,5 ', 7- tetrahydroxys dihydro are yellow
Ketone (3 ', 5,5 ', 7-tetracarbonyl dihydrogen flavonoids), N-p- coumaric acyl tyrasamines (N-p-
Coumaroyltyramine), trans- N- (4- leptodactylines) ferulic amide (trans-N- (4-hydroxy ethyl
Benzene) feruloyloctopamine), daucosterol (daucosterol), 6- hydroxyl -2,5- dimethoxy -1,4- phenanthrenequione
(6-hydroxy-2,5-dimethoxy-1,4-phenanthrenequinone), 4,5- dihydroxy -2- methoxyl groups -9,10- two
Hydrogen phenanthrene (4,5-dihydroxy-2-methoxy-9,10-dihydrophenanthrene), 4- hydroxymethyl phenyl propionic acid ethers (4-
Hydroxymethyl phenyl propionate ether), 2,6- dimethoxy 1,4-benzoquinone (2,3-dimethoxy-5-
Methyl-p-benzoquinone), 4- allyls -2,6- dimethoxy glucosides (4-allylbase-2,6-
Dimethoxy glycosidase), 3- hydroxyls -1- (4- hydroxyl -3,5- dimethoxy benzenes) -1- acetone (3-hydroxy-1-
(4-hydroxy-3,5-dimethoxy benzene) -1-acetone), 2,7- dihydroxy -3,4- dimethoxys -9,10- two
Hydrogen phenanthrene (2,7-dihydroxy-3,4-dimethoxy-9,10-dihydrophenanthrene), 3- hydroxyl -2,4,7- front threes
Oxygroup -9,10- dihydro phenanthrenes (3-hydroxy-2,4,7-trimethoxy-9,10-dihydrophenanthrene), 3,7- bis-
Hydroxyl -2,4- dimethoxy -9,10- dihydro phenanthrenes (3,7-dihydroxy-2,4-dimethoxy-9,10-
Dihydrophenanthrene), 2,7- dihydroxy -3,4- dimethoxys phenanthrene (2,7-dihydroxy-3,4-
Dimethoxyphenanthrene), 3,7- dihydroxy -2,4- dimethoxys phenanthrene (3,7-dihydroxy-2,4-
Dimethoxyphenanthrene), 3- hydroxyls -2,4,7- trimethoxies phenanthrene (3-hydroxy-2,4,7-
Trimethoxyphenanthrene), 3,4,7- trihydroxies -2- methoxyl groups phenanthrene (3,4,7-trihydroxy-2-
Methoxyphenanthrene), β-daucosterol (β-daucosterol), benzyl alcohol-O- β-D- glucopyranosides
(phenylcarbinol-O- β-D-glucopyranoside), Isorhamnetin -3-O- α-L- rhamnopyranosyls (1 → 2)-β-D- pyrroles
Glucopyranoside glycosides (rhamnetin-3-O- α-L- rhamnose base 1 → 2)-β-D-glucopyranoside), 3,4,5-
Trimethoxy-benzene -1-O- β-D- glucopyranosides (3,4,5-trimethoxybenzene-1-O- β-D-
Glucopyranoside), 2,6- dimethoxy-4 's-hydroxyl phenol -1-O- beta-glucosidases (2,6-dimethoxy-4-
Hydroxy phenol-1-O- β-glucoside), Syringin (syringin), (+)-syringaresinol ((+)-
Syringaresinol),-O- of syringaresinol -4 ' β-D- lists glucoside (syringaresinol-4 '-O- β-D-
Monoglucoside), P-hydroxybenzoic acid (4-hydroxybenzoic acid), dendrobium candidum element A (dendrobium
Officinale A), dendrobium candidum element B (dendrobium officinale B), dendrobium candidum element C (dendrobium
Officinale C), dendrobium candidum element D (dendrobium officinale D), dendrobium candidum element E (dendrobium
Officinale E), dendrobium candidum element F (dendrobium officinale F), dendrobium candidum element G (dendrobium
Officinale G), dendrobium candidum element H (dendrobium officinale H), dendrobium candidum element I (dendrobium
Officinale I), dendrobium candidum element J (dendrobium officinale J), dendrobium candidum element K (dendrobium
Officinale K), dendrobium candidum element L (dendrobium officinale L), dendrobium candidum element M (dendrobium
Officinale M), dendrobium candidum element N (dendrobium officinale N), dendrobium candidum element O (dendrobium
Officinale O), dendrobium candidum element P (dendrobium officinale P), dendrobium candidum element Q (dendrobium
Officinale Q) etc. organic substances.
3）It smokes panel test comparison
Stem of noble dendrobium extractum A, B and C that three kinds of distinct methods extract are added to the cigarette of three kinds of different sizes by the present invention（It is denoted as one kind
Cigarette, two class cigarette and three classes cigarette, and successively according to the hard great Jin circles of China Tobacco Henan Industrial Co., Ltd's Bright Yellow, gold
The standard that rolls of leaf Small object and Red-Flag Canal rolls）In, by sensory evaluating smoking, probe into its shadow to kinds of cigarettes aesthetic quality
It rings, is as a result shown in Table 1, table 2 and table 3 respectively.
It is learnt by constituent analysis, the water extraction medicinal extract main component of the stem of noble dendrobium is sweet substance and acidic materials, due to these
The presence of organic compound makes its medicinal extract have special property.Speculated by the smoking result of table 1：The water of the stem of noble dendrobium extracts medicinal extract
It is added in pipe tobacco, the alkaline matters such as the nicotine in pipe tobacco and flue gas can be neutralized, increase sweet sense, reduce cigarette irritation, but
It is mainly saccharide compound in the medicinal extract, after medicinal extract, which is added to the weight percent in pipe tobacco, reaches 0.20 ‰, contents of saccharide
Excessively high, smoke is thin out, and generates miscellaneous gas, and pleasant impression owes comfortable, simultaneously as lack ester type compound in medicinal extract, the flue gas of cigarette
Fragrance does not improve.
The water of 1 stem of noble dendrobium of table extracts medicinal extract flavoring smoking result
It is learnt by constituent analysis, the triacetyl glycerine extraction medicinal extract main component of the stem of noble dendrobium is esters, aldehydes, ketone, iron sheet stone
The flavor matters such as dry measure used in former times element and drug make its medicinal extract have special property due to the presence of these organic compounds.By table 2
Smoking result speculates：The triacetyl glycerine extraction medicinal extract of the stem of noble dendrobium is added in pipe tobacco, can improve fragrance, improve mouthfeel, reduce
Cigarette irritation covers cigarette foreign gas, but after medicinal extract is added to the weight percent in pipe tobacco and reaches 0.20 ‰, dendrobium candidum
Plain class too high levels generate stem of noble dendrobium taste, cover cigarette perfume, generate miscellaneous gas, pleasant impression owes comfortable, simultaneously as lacking carbohydrate in medicinal extract
And acid compounds, medicinal extract can not neutralize the alkaline matters such as the nicotine in pipe tobacco and flue gas, can not increase sweet sense.
The triacetyl glycerine of 2 stem of noble dendrobium of table extracts medicinal extract flavoring smoking result
It is learnt by constituent analysis, ethyl alcohol and ethyl acetate mixed solvent the extraction medicinal extract of the stem of noble dendrobium contain stem of noble dendrobium water and three acetic acid are sweet
The ingredients of two kinds of grease extraction medicinal extract, due to the presence of these organic compounds, the characteristics of making it combine both medicinal extract.By
Known to the smoking result of table 3：Stem of noble dendrobium medicinal extract of the present invention have clear improvement and modify cigarette smoke, cover miscellaneous gas, reduce irritation,
Mitigate bitter and peppery feeling, increase sweet degree, promoting or transferring fragrance degree of hair, improvement suction taste and pleasant impression effect thoroughly, compensates for water and three vinegar well
Deficiency between two kinds of extraction medicinal extract of acid glyceride, has reached more preferably function and effect, but medicinal extract is added to the weight in pipe tobacco
After percentage reaches 0.20 ‰, there are stem of noble dendrobium flavour of a drug, smoke is thin out, and generates miscellaneous gas, and medicinal extract taste covers cigarette perfume, it is therefore proposed that with
Amount：0.10‰~0.15‰.
The ethyl alcohol and ethyl acetate of 3 stem of noble dendrobium of table extract medicinal extract flavoring smoking result
Therefore, expert's identification of smokeing panel test thinks that ethyl alcohol and ethyl acetate mixed solvent the extraction medicinal extract of the stem of noble dendrobium are substantially reduced stimulation
Property, cover miscellaneous gas, improve pleasant impression, mitigate bitter and peppery feeling, increase sweet degree, make pleasant impression alcohol and and comfortably act on；But this medicinal extract
When the weight percent being added in pipe tobacco reaches 0.20 ‰, perfume quantity increases, but flue gas sinks, and cigarette perfume is destroyed, and smoke is thin out,
Irritation increases, and pleasant impression owes comfortable, and medicinal extract taste covers cigarette perfume, it is proposed that dosage is 0.10 ‰ ~ 0.15 ‰.
4）Conclusion
Only containing carbohydrate and a small amount of alcohols and acid compounds in the water extraction medicinal extract of the stem of noble dendrobium, the triacetyl glycerine of the stem of noble dendrobium carries
It includes the substances such as esters, aldehydes, ketone, dendrobium candidum to take medicinal extract mainly, and carbohydrate, alcohols and acids content are seldom, using ethyl alcohol
More rich with the stem of noble dendrobium medicinal extract ingredient of ethyl acetate mixed solvent extraction, compounds content is more, contains the water extraction of the stem of noble dendrobium
The triacetyl glycerine of medicinal extract and the stem of noble dendrobium extracts the ingredient of two kinds of medicinal extract of medicinal extract.Due to the presence of these compounds, make it have
The property of both medicinal extract is compensated for respectively well using water and triacetyl glycerine as between two kinds of medicinal extract obtained by extractant
Deficiency, reached more preferably function and effect.
It should be noted last that：Technical scheme of the present invention that the above embodiments are only illustrative and not limiting is any right
The equivalent replacement and do not depart from the modification of spirit and scope of the invention or local replacement that the present invention carries out, should all cover in this hair
Within bright protective scope of the claims.
Claims (4)
1. a kind of stem of noble dendrobium medicinal extract, which is characterized in that be made by the method for following steps：By stem of noble dendrobium stem crushed after being dried, obtain
To dendrobe powder, then gained dendrobe powder is added to the in the mixed solvent of ethyl alcohol and ethyl acetate, the body of ethyl alcohol and ethyl acetate
Product is than being 1：1, after being heated to reflux a period of time, filtrate is left and taken in filtering, and filtering is residue obtained to be washed repeatedly with the mixed solvent
And washing lotion is left and taken, merge gained filtrate and washing lotion, removes under reduced pressure after solvent to get the stem of noble dendrobium medicinal extract.
2. stem of noble dendrobium medicinal extract according to claim 1, which is characterized in that the weighing body of the dendrobe powder and the mixed solvent
Product is than being 1g:（2~10）mL.
3. application of the stem of noble dendrobium medicinal extract in cigarette described in claim 1, which is characterized in that the stem of noble dendrobium medicinal extract with 0.10 ‰ ~
0.15 ‰ weight percent, which is added in pipe tobacco, to be used.
4. application of the stem of noble dendrobium medicinal extract according to claim 3 in cigarette, which is characterized in that stem of noble dendrobium medicinal extract solvent is dilute
After releasing, uniformly it is sprayed on pipe tobacco.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109864326A (en) * | 2019-03-20 | 2019-06-11 | 福建绿色黄金生物科技有限公司 | One grows tea and dendrobium nobile composition, preparation method and applications |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106947599A (en) * | 2017-04-27 | 2017-07-14 | 河南中烟工业有限责任公司 | A kind of cigarette quick-fried pearl HERBA DENDROBII essence and its application in cigarette |
| CN107319637A (en) * | 2016-04-28 | 2017-11-07 | 湖南中烟工业有限责任公司 | A kind of extracting method of the electronic cigarette basic smoke raw material of tobacco source |
-
2018
- 2018-03-26 CN CN201810251818.9A patent/CN108497548A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107319637A (en) * | 2016-04-28 | 2017-11-07 | 湖南中烟工业有限责任公司 | A kind of extracting method of the electronic cigarette basic smoke raw material of tobacco source |
| CN106947599A (en) * | 2017-04-27 | 2017-07-14 | 河南中烟工业有限责任公司 | A kind of cigarette quick-fried pearl HERBA DENDROBII essence and its application in cigarette |
Non-Patent Citations (1)
| Title |
|---|
| 李丹丹等: "铁皮石斛改善卷烟评吸品质的物质基础研究", 《昆明理工大学学报(自然科学版)》 * |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109864326A (en) * | 2019-03-20 | 2019-06-11 | 福建绿色黄金生物科技有限公司 | One grows tea and dendrobium nobile composition, preparation method and applications |
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Application publication date: 20180907 |