CN108497491A - A kind of extracting method of Xinhui tangerine peel functional components - Google Patents
A kind of extracting method of Xinhui tangerine peel functional components Download PDFInfo
- Publication number
- CN108497491A CN108497491A CN201810218741.5A CN201810218741A CN108497491A CN 108497491 A CN108497491 A CN 108497491A CN 201810218741 A CN201810218741 A CN 201810218741A CN 108497491 A CN108497491 A CN 108497491A
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- China
- Prior art keywords
- tangerine peel
- functional components
- minutes
- xinhui tangerine
- crystal
- Prior art date
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- 238000000034 method Methods 0.000 title claims abstract description 25
- 241000675108 Citrus tangerina Species 0.000 title claims abstract 7
- 239000000126 substance Substances 0.000 claims abstract description 18
- 229930003935 flavonoid Natural products 0.000 claims abstract description 12
- 150000002215 flavonoids Chemical class 0.000 claims abstract description 12
- 235000017173 flavonoids Nutrition 0.000 claims abstract description 12
- 150000004676 glycans Chemical class 0.000 claims abstract description 12
- 150000008442 polyphenolic compounds Chemical class 0.000 claims abstract description 12
- 235000013824 polyphenols Nutrition 0.000 claims abstract description 12
- 239000005017 polysaccharide Substances 0.000 claims abstract description 12
- 229920001282 polysaccharide Polymers 0.000 claims abstract description 12
- 239000000341 volatile oil Substances 0.000 claims abstract description 10
- 239000013078 crystal Substances 0.000 claims description 15
- 238000000605 extraction Methods 0.000 claims description 12
- 239000000287 crude extract Substances 0.000 claims description 10
- 230000005684 electric field Effects 0.000 claims description 10
- 239000012530 fluid Substances 0.000 claims description 10
- 108010059892 Cellulase Proteins 0.000 claims description 5
- 230000002411 adverse Effects 0.000 claims description 5
- 229940106157 cellulase Drugs 0.000 claims description 5
- 238000010265 fast atom bombardment Methods 0.000 claims description 5
- 238000000746 purification Methods 0.000 claims description 5
- 238000000108 ultra-filtration Methods 0.000 claims description 5
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 4
- 238000002844 melting Methods 0.000 claims description 2
- 230000008018 melting Effects 0.000 claims description 2
- 239000003643 water by type Substances 0.000 claims description 2
- 238000011084 recovery Methods 0.000 abstract description 6
- 235000015114 espresso Nutrition 0.000 abstract 1
- 241001672694 Citrus reticulata Species 0.000 description 24
- 238000004821 distillation Methods 0.000 description 3
- IDGUHHHQCWSQLU-UHFFFAOYSA-N ethanol;hydrate Chemical compound O.CCO IDGUHHHQCWSQLU-UHFFFAOYSA-N 0.000 description 3
- 238000010438 heat treatment Methods 0.000 description 3
- 239000003921 oil Substances 0.000 description 2
- 206010011224 Cough Diseases 0.000 description 1
- 206010062717 Increased upper airway secretion Diseases 0.000 description 1
- 208000006673 asthma Diseases 0.000 description 1
- 230000006835 compression Effects 0.000 description 1
- 238000007906 compression Methods 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 235000013399 edible fruits Nutrition 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000000284 extract Substances 0.000 description 1
- 210000004072 lung Anatomy 0.000 description 1
- 230000001151 other effect Effects 0.000 description 1
- 208000026435 phlegm Diseases 0.000 description 1
- 235000013619 trace mineral Nutrition 0.000 description 1
- 239000011573 trace mineral Substances 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/105—Plant extracts, their artificial duplicates or their derivatives
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
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- Life Sciences & Earth Sciences (AREA)
- Botany (AREA)
- Mycology (AREA)
- Health & Medical Sciences (AREA)
- Nutrition Science (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Fats And Perfumes (AREA)
- Extraction Or Liquid Replacement (AREA)
Abstract
The invention discloses a kind of extracting methods of Xinhui tangerine peel functional components, using various ways, collaboration is handled this method step by step, finally obtained Xinhui tangerine peel functional components are rich in volatile oil, Flavonoid substances, polysaccharide and polyphenols, recovery rate is greatly improved compared to Conventional espresso method, and simple process and low cost.
Description
Technical field
The present invention relates to the field of fruit surface functional components extraction, more particularly to a kind of Xinhui tangerine peel functional components
Extracting method.
Background technology
Citrus chachiensis hortorum is best with Xinhui tangerine peel, there is eliminating the phlegm, relieving asthma, moisten the lung and relieve the cough and other effects, various trace elements are rich in,
It is well received by consumers.Jiangmen City of Guangdong Province Xinhui District is the Genuine producing area of citrus chachiensis hortorum, is the township of Chinese dried orange peel, Xinhui tangerine peel
It ranks first of the Triratna of Guangdong, plantation is with a long history, and Xinhui tangerine peel is national geography sign protection product.It is rich in and waves in Xinhui tangerine peel
The substances such as hair oil, Flavonoid substances, polysaccharide and Polyphenols have good health-care efficacy to human body.
Invention content
Technical problem to be solved by the invention is to provide a kind of extracting method of Xinhui tangerine peel functional components, this method
The recovery rate of the substances such as volatile oil, Flavonoid substances, polysaccharide and the Polyphenols of Xinhui tangerine peel functional components extract of extraction
It is greatly improved compared to conventional method.
The present invention solve above-mentioned technical problem technical solution be：
A kind of extracting method of Xinhui tangerine peel functional components, include the following steps for：
（1）The Xinhui tangerine peel of aged 3-8 is cleaned up, use electric field strength for the impulse electric field of 30-50kV/cm at
200-500 μ s are managed, then frequency is used to be handled for the ultrasonic wave of 30-50kHz and microwave cooperating, repeatedly collaboration processing 4-6 times, every time
Processing 5-8 minutes, midfeather 30 minutes crush for use；
（2）Dried Tangerine Peel is dissolved in the closed container of 80-90% ethanol waters, it is 10-20 kV's that container, which is placed in pressure,
It in hyperbaric environment, is heated to 80-90 DEG C and is kept for 30-50 minutes, then cellulase is added in a reservoir and carries out assisted extraction, simultaneously
Microwave treatment 20-40 minutes, isolated treatment fluid A；
（3）Treatment fluid A is freezed 12-16 hours at -10 DEG C, first crystal is precipitated, then freeze 24-30 hours at -25 DEG C,
Second batch crystal is precipitated, uses frequency to be handled for 20-40kHz ultrasonic waves and microwave cooperating in whole process, two batches crystal is closed
And melting is heated, it is preserved at 0 DEG C, obtains crude extract；
（4）Crude extract is combined using high speed adverse current chromatogram and fast atom bombardment MS and carries out further extraction purification, then is passed through
The Xinhui tangerine peel functional components rich in volatile oil, Flavonoid substances, polysaccharide and Polyphenols etc. are obtained after ultrafiltration.
The present invention has the following advantages that compared with prior art and effect：The relatively traditional extracting method of the present invention, volatilization
The recovery rate of the substances such as oil, Flavonoid substances, polysaccharide and Polyphenols greatly improves.Present invention process is simple, at low cost.
Specific implementation mode
Further detailed description is done to the present invention with reference to embodiment, embodiments of the present invention are not limited thereto.
Embodiment 1
A kind of extracting method of Xinhui tangerine peel functional components is by step：
（1）Aged 3 years Xinhui tangerine peels are cleaned up, electric field strength is used to handle 200 for the impulse electric field of 30kV/cm
μ s, then frequency is used to be handled for the ultrasonic wave of 30kHz and microwave cooperating, collaboration processing 4 times repeatedly is 5 minutes per treatment, intermediate
Interval 30 minutes crushes for use；
（2）Dried Tangerine Peel is dissolved in the closed container of 80% ethanol water, container is placed in the hyperbaric environment that pressure is 10kV
In, it is heated to 80 DEG C and is kept for 30 minutes, then cellulase is added in a reservoir and carries out assisted extraction, while microwave treatment 20 is divided
Clock, isolated treatment fluid A；
（3）Treatment fluid A is freezed 12 hours at -10 DEG C, first crystal is precipitated, then freeze 24 hours at -25 DEG C, is precipitated the
Two batches of crystal use in whole process frequency to be handled for 20kHz ultrasonic waves and microwave cooperating, and it is molten that two batches crystal is merged heating
Melt, is preserved at 0 DEG C, obtain crude extract；
（4）Crude extract is combined using high speed adverse current chromatogram and fast atom bombardment MS and carries out further extraction purification, then is passed through
The Xinhui tangerine peel functional components rich in volatile oil, Flavonoid substances, polysaccharide and Polyphenols etc. are obtained after ultrafiltration.
After testing, the relatively traditional distillation extracting method of the present invention, volatile oil, Flavonoid substances, polysaccharide and Polyphenols etc.
The recovery rate of substance greatly improves.Present invention process is simple, at low cost.
Embodiment 2
（1）Aged 6 years Xinhui tangerine peels are cleaned up, electric field strength is used to handle 400 for the impulse electric field of 40kV/cm
μ s, then frequency is used to be handled for the ultrasonic wave of 40kHz and microwave cooperating, collaboration processing 5 times repeatedly is 6 minutes per treatment, intermediate
Interval 30 minutes crushes for use；
（2）Dried Tangerine Peel is dissolved in the closed container of 85% ethanol water, container is placed in the hyperbaric environment that pressure is 15kV
In, it is heated to 85 DEG C and is kept for 40 minutes, then cellulase is added in a reservoir and carries out assisted extraction, while microwave treatment 30 is divided
Clock, isolated treatment fluid A；
（3）Treatment fluid A is freezed 14 hours at -10 DEG C, first crystal is precipitated, then freeze 28 hours at -25 DEG C, is precipitated the
Two batches of crystal use in whole process frequency to be handled for 30kHz ultrasonic waves and microwave cooperating, and it is molten that two batches crystal is merged heating
Melt, is preserved at 0 DEG C, obtain crude extract；
（4）Crude extract is combined using high speed adverse current chromatogram and fast atom bombardment MS and carries out further extraction purification, then is passed through
The Xinhui tangerine peel functional components rich in volatile oil, Flavonoid substances, polysaccharide and Polyphenols etc. are obtained after ultrafiltration.
After testing, the relatively traditional distillation extracting method of the present invention, volatile oil, Flavonoid substances, polysaccharide and Polyphenols etc.
The recovery rate of substance greatly improves.Present invention process is simple, at low cost.
Embodiment 3
（1）Aged 8 years Xinhui tangerine peels are cleaned up, electric field strength is used to handle 500 for the impulse electric field of 50kV/cm
μ s, then frequency is used to be handled for the ultrasonic wave of 50kHz and microwave cooperating, collaboration processing 6 times repeatedly is 8 minutes per treatment, intermediate
Interval 30 minutes crushes for use；
（2）Dried Tangerine Peel is dissolved in the closed container of 90% ethanol water, container is placed in the high compression ring that pressure is 20 kV
It in border, is heated to 90 DEG C and is kept for 50 minutes, then cellulase is added in a reservoir and carries out assisted extraction, while microwave treatment 40 is divided
Clock, isolated treatment fluid A；
（3）Treatment fluid A is freezed 16 hours at -10 DEG C, first crystal is precipitated, then freeze 30 hours at -25 DEG C, is precipitated the
Two batches of crystal use in whole process frequency to be handled for 40kHz ultrasonic waves and microwave cooperating, and it is molten that two batches crystal is merged heating
Melt, is preserved at 0 DEG C, obtain crude extract；
（4）Crude extract is combined using high speed adverse current chromatogram and fast atom bombardment MS and carries out further extraction purification, then is passed through
The Xinhui tangerine peel functional components rich in volatile oil, Flavonoid substances, polysaccharide and Polyphenols etc. are obtained after ultrafiltration.
After testing, the relatively traditional distillation extracting method of the present invention, volatile oil, Flavonoid substances, polysaccharide and Polyphenols etc.
The recovery rate of substance greatly improves.Present invention process is simple, at low cost.
Claims (1)
1. a kind of extracting method of Xinhui tangerine peel functional components, which is characterized in that include the following steps：
（1）The Xinhui tangerine peel of aged 3-8 is cleaned up, use electric field strength for the impulse electric field of 30-50kV/cm at
200-500 μ s are managed, then frequency is used to be handled for the ultrasonic wave of 30-50kHz and microwave cooperating, repeatedly collaboration processing 4-6 times, every time
Processing 5-8 minutes, midfeather 30 minutes crush for use；
（2）By step（1）It handles obtained Dried Tangerine Peel to be dissolved in the closed container of 80-90% ethanol waters, container is placed in
Pressure is to be heated to 80-90 DEG C in the hyperbaric environment of 10-20 kV and kept for 30-50 minutes, then cellulase is added in a reservoir
Carry out assisted extraction, while microwave treatment 20-40 minutes, isolated treatment fluid A；
（3）Treatment fluid A is freezed 12-16 hours at -10 DEG C, first crystal is precipitated, then freeze 24-30 hours at -25 DEG C,
Second batch crystal is precipitated, uses frequency to be handled for 20-40kHz ultrasonic waves and microwave cooperating in whole process, two batches crystal is closed
And melting is heated, it is preserved at 0 DEG C, obtains crude extract；
（4）Crude extract is combined using high speed adverse current chromatogram and fast atom bombardment MS and carries out further extraction purification, then is passed through
The Xinhui tangerine peel functional components rich in volatile oil, Flavonoid substances, polysaccharide and Polyphenols etc. are obtained after ultrafiltration.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810218741.5A CN108497491A (en) | 2018-03-16 | 2018-03-16 | A kind of extracting method of Xinhui tangerine peel functional components |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810218741.5A CN108497491A (en) | 2018-03-16 | 2018-03-16 | A kind of extracting method of Xinhui tangerine peel functional components |
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| Publication Number | Publication Date |
|---|---|
| CN108497491A true CN108497491A (en) | 2018-09-07 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201810218741.5A Withdrawn CN108497491A (en) | 2018-03-16 | 2018-03-16 | A kind of extracting method of Xinhui tangerine peel functional components |
Country Status (1)
| Country | Link |
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| CN (1) | CN108497491A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110498827A (en) * | 2019-08-27 | 2019-11-26 | 浙江理工大学 | A method of extracting flavonoid glycoside from orange peel |
| CN115651090A (en) * | 2022-10-31 | 2023-01-31 | 五邑大学 | Preparation method and application of polysaccharide extract of pericarpium citri reticulatae enriched with lactobacillus |
-
2018
- 2018-03-16 CN CN201810218741.5A patent/CN108497491A/en not_active Withdrawn
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110498827A (en) * | 2019-08-27 | 2019-11-26 | 浙江理工大学 | A method of extracting flavonoid glycoside from orange peel |
| CN110498827B (en) * | 2019-08-27 | 2020-08-18 | 浙江理工大学 | Method for extracting flavonoid glycoside from orange peel |
| CN115651090A (en) * | 2022-10-31 | 2023-01-31 | 五邑大学 | Preparation method and application of polysaccharide extract of pericarpium citri reticulatae enriched with lactobacillus |
| CN115651090B (en) * | 2022-10-31 | 2024-04-26 | 广东新宝堂制药有限公司 | Preparation method and application of wide orange peel polysaccharide extract enriched with lactobacillus |
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| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| WW01 | Invention patent application withdrawn after publication | ||
| WW01 | Invention patent application withdrawn after publication |
Application publication date: 20180907 |