CN108485838A - Clothes detergent - Google Patents
Clothes detergent Download PDFInfo
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- CN108485838A CN108485838A CN201810537453.6A CN201810537453A CN108485838A CN 108485838 A CN108485838 A CN 108485838A CN 201810537453 A CN201810537453 A CN 201810537453A CN 108485838 A CN108485838 A CN 108485838A
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- cortex moutan
- clothes
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/88—Ampholytes; Electroneutral compounds
- C11D1/94—Mixtures with anionic, cationic or non-ionic compounds
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/20—Organic compounds containing oxygen
- C11D3/2003—Alcohols; Phenols
- C11D3/2065—Polyhydric alcohols
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/26—Organic compounds containing nitrogen
- C11D3/33—Amino carboxylic acids
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/36—Organic compounds containing phosphorus
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/38—Products with no well-defined composition, e.g. natural products
- C11D3/382—Vegetable products, e.g. soya meal, wood flour, sawdust
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/48—Medical, disinfecting agents, disinfecting, antibacterial, germicidal or antimicrobial compositions
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/02—Anionic compounds
- C11D1/12—Sulfonic acids or sulfuric acid esters; Salts thereof
- C11D1/14—Sulfonic acids or sulfuric acid esters; Salts thereof derived from aliphatic hydrocarbons or mono-alcohols
- C11D1/146—Sulfuric acid esters
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/88—Ampholytes; Electroneutral compounds
- C11D1/90—Betaines
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Wood Science & Technology (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Emergency Medicine (AREA)
- Detergent Compositions (AREA)
Abstract
The invention discloses a kind of clothes detergents, including following materials by weight percentage：Lauryl sodium sulfate 5 9%；Cocoamidopropyl betaine 2 6%；Laruyl alcohol sulfate ammonium salt 2 6%；Cortex Moutan extract 0.1 0.9%；Glycerine 0.5 2.5%；Surplus is water.The clothes detergent of the present invention, can effectively remove dirt, environmentally safe, safe and non-toxic, non-stimulated to human skin, wash rear noresidue, and have the function of restraining and sterilizing bacteria.
Description
Technical field
The present invention relates to a kind of detergent more particularly to a kind of clothes detergents.
Background technology
Detergent (Detergent) is by wash clean process for cleaning by the product of particular formulation.Key component is usual
It is made of surfactant, builder and additive etc..There are many type of detergent, according to the type for removing dirt, can be divided into
Heavy duty detergent and light-duty detergent；It is more powdery, bulk, paste, pulpous state and liquid etc. can be divided into according to the shape of product
Kind form.
For clothes washing, to there is detergency in the clothes detergent of the prior art not strong and the shortcomings of be easy to hinder hand mostly.
Invention content
In view of the deficienciess of the prior art, technical problem to be solved by the invention is to provide a kind of clothes washings
Agent.
The present invention specifically adopts the following technical scheme that：
A kind of clothes detergent, including following materials by weight percentage：
Lauryl sodium sulfate 5-9%；
Cocoamidopropyl betaine 2-6%；
Laruyl alcohol sulfate ammonium salt 2-6%；
Glycerine 0.5-2.5%；
Surplus is water.
Lauryl sodium sulfate, No. CAS：151-21-3.Cocoamidopropyl betaine, No. CAS：86438-79-1.Month
Cinnamic alcohol sulfate ammonium salt, No. CAS：2235-54-3.Glycerine, No. CAS：56-81-5.
Preferably,
A kind of clothes detergent, including following materials by weight percentage：
Lauryl sodium sulfate 5-9%；
Cocoamidopropyl betaine 2-6%；
Laruyl alcohol sulfate ammonium salt 2-6%；
Cortex Moutan extract 0.1-0.9%；
Glycerine 0.5-2.5%；
Surplus is water.
Moutan bark, Chinese medicine name.For ranunculaceae peony dry root skin.Originate in the ground such as Anhui, Sichuan, Henan, Shandong.
It is bitter, pungent, it is slightly cold, the thoughts of returning home, liver and kidney channel have clearing heat and cooling blood, activate blood circulation and disperse blood clots, reducing the asthenic fever and other effects.《Compendium of Materia Medica》：" tree peony
Skin controls the few cloudy, the moon four of fainting of brothers and lies prostrate fire through blood system.Gai Fuhuo, that is, yin fire, yin fire are that mutually fire, ancient prescription only control mutually fire with this,
Therefore Zhong Jing shenqi pills use it.Descendant is specially controlling mutually fire with amur cork tree, does not know that the work(of the root bark of tree peony more wins.Red colored person's profit, white flower person mend, people
Also seldom realize, preferably distinguish it.”《Collected statements on the herbal foundation》：" Shen visit can Mr. say：It presses《Deep Shi Fang》With moutan bark, same to Radix Angelicae Sinensis, radix rehmanniae preparata are then mended
Blood；The then blood-breaking of same curcuma zedoary, peach kernel；Same Radix Rehmanniae, connects then cool blood at a kind of reed mentioned in ancient books；Same Chinese cassia tree, baked ginger then warm up blood；Same Rhizoma Chuanxiong, RADIX PAEONIAE ALBA are then adjusted
Blood；The same root of bidentate achyranthes, safflower are then invigorated blood circulation；Same matrimony vine, donkey-hide gelatin then green blood；Same rhizoma cyperi the root of bidentate achyranthes, returns, rhizome of chuanxiong, but can regulating the qi flowing in the channels and and blood.With regard to
Fire in the moon, it is non-to be gone with rhizoma anemarrhenae, RADIX PAEONIAE ALBA；Postpartum all diseases, it is non-with return, rhizome of chuanxiong, beneficial mother cannot go.Be intended to again it is pleasant soothing the liver, and
With green peel, radix bupleuri；Opened up to phlegm it is strongly fragrant, and with fritillaria, the tuber of pinellia.If when for the apocenosis of ulcer section, eliminating toxic, cool blood, frankincense must be assisted, do not had
Medicine, the root of Dahurain angelica, Rhizoma Et Radix Notopterygii, Fructus Forsythiae, honeysuckle generation are having Ji.Moutan bark clears away heart-fire, and supports kidney and liver, sharp envelope, and control four through blood system
Fu Huo.Gas medicine in blood.It is kind to control that woman's passages through which vital energy circulates is obstructed and postpartum extravesated blood is more than.Bleeding from five sense organs or subcutaneous tissue haematemesis is controlled again, and uterine bleeding drenches blood, falls and flutter the stasis of blood
Blood, all vim and vigour are disease, and system can control it.Its gas perfume is covered, perfume (or spice) can the promoting circulation of blood with regulating the qi flowing in the channels；Its bitter, hardship can following gas and stop blooding；
Its is cool in nature, it is cool can be with blood and green blood；Its taste is again pungent, pungent to push away old blood, and causes new blood.Therefore the side Zhen Quan controls woman's blood because of heat
And will be withered, lumbar vertebrae pain, night hot polydipsia adds moutan bark most to test again with four objects.Ancient prescription is rushed with this with controlling mutually to attack with fire again, deficiency of Yin hair
Heat.It presses again《This warp》Main fever and chills, apoplexy Chi Zong, convulsion, all diseases of frightened epilepsy perverse trend, total blood system that belongs to is eyes afflicted with calaract.Right fever and chills, apoplexy, this refers to wound
The apoplexy of the cold invasion of blood chamber by heat, wind among non-finger old man deficiency of vital energy coma due to blocking of the respiratory system.Its literary elder generation with two word of fever and chills, being followed by Chi Zong frightened epilepsies can
Know, Kuang Chi Zong, frightened epilepsy, positive blood are obtained hot and cashed, and fever and chills belong to few main person of sun institute again.”《Bencao Jingshu》：" moutan bark, taste
Bitter and micro-pungent, gas are cold and nontoxic, pungent poly- with dissipating bind, bitter cold removes blood-head, enters blood system, the key medicine of cool blood heat.Fever and chills person, the deficiency of Yin
The time of blood-head.Apoplexy Chi Zong, convulsion, frightened epilepsy, all yin asthenia generating intrinsic heat, the event of nutrient QI and blood being insufficient.Heat go then blood it is cool, cool then new blood is raw, cloudy
Gas is multiple, the multiple then fire of cloudy gas it is not scorching and without the card because of hot air wind producing, therefore know master's.Ulcerative carbuncle person, heat are stopped up blood stasis and are formed.Cool blood row
Blood, therefore treat ulcerative carbuncle.Pungent to dissipate blood, hardship can purge heat, therefore can stay house stomach except blood system perverse trend and disease heavily fortified point hemostasis.Dirty category is cloudy and store essential substances,
It likes to dislike heat clearly, heat is removed then the five internal organs and certainly pacified.《It does not record》And gas headache visitor's heat when main, exhaustion or lesion of the five internal organs labor gas, head pain in the back person, expel the heat-evil cool blood
Work(.Main warp arteries and veins is obstructed again by Zhen Quan, and blood drips pain in the back, this all blood time withered because of heat.Blood second of the three ten-day periods of the hot season fire, non-this does not remove, therefore controls
Hectic fever due to yin is lossless and children's smallpox variola sore, blood-head.Dong Yuan calls stomach accumulated heat of having a guilty conscience, and internal heat is vehement very, deficiency of heart-QI person, with moutan bark
For monarch, also this anticipates.”
Commercially available raw material may be used in the Cortex Moutan extract.The Cortex Moutan extract, can also be by following methods
It is prepared：Moutan bark is crushed, 40 mesh sieve is crossed, moutan bark powder is obtained, by 80-120g moutan barks powder and 1000-1500mL water
Mixing, 20-40 minutes are stood at 20-30 DEG C, are ultrasonically treated 35-55 minutes, using 300 mesh filter-cloth filterings, are obtained filtrate and filter
Slag；Filter residue and the ethanol water that 800-1200mL volume fractions are 70-80% mix, small in 60-70 DEG C of refluxing extraction 2-4
When, using 300 mesh filter-cloth filterings, filtrate is obtained, merges filtrate twice, the density for being concentrated under reduced pressure into 65 DEG C is 1.05-1.10g/
ML, obtains Cortex Moutan extract, and the condition of the supersound process is：60-70 DEG C of ultrasonic temperature, ultrasonic power 100-200W surpass
Acoustic frequency 15-25kHz.
Preferably, the Cortex Moutan extract is prepared by following methods：Moutan bark is crushed, 40 mesh sieve is crossed, obtains
80-120g moutan barks powder and 1000-1500mL water are mixed, 20-40 minutes are stood at 20-30 DEG C by moutan bark powder, are ultrasonically treated
20-30 minutes, interval was then sonicated 10-20 minutes after 1-3 minutes, is ultrasonically treated 5-10 minutes after being spaced 1-3 minutes again,
Using 300 mesh filter-cloth filterings, filtrate and filter residue are obtained；Filter residue and the ethyl alcohol that 800-1200mL volume fractions are 70-80% are water-soluble
Liquid mixes, and in 60-70 DEG C of refluxing extraction 2-4 hour, using 300 mesh filter-cloth filterings, obtains filtrate, merges filtrate twice, depressurize
The density for being concentrated into 65 DEG C is 1.05-1.10g/mL, obtains Cortex Moutan extract, the condition of the supersound process is：Ultrasonic temperature
60-70 DEG C, ultrasonic power 100-200W, supersonic frequency 15-25kHz of degree.
A kind of clothes detergent, including following materials by weight percentage：
Lauryl sodium sulfate 5-9%；
Cocoamidopropyl betaine 2-6%；
Laruyl alcohol sulfate ammonium salt 2-6%；
Cortex Moutan extract 0.1-0.9%；
Glycerine 0.5-2.5%；
Chelating agent 0.1-0.7%；
Surplus is water.
The chelating agent is sodium phytate (No. CAS：14306-25-3) and/or four sodium (CAS of iminodisuccinic acid
Number：144538-83-0).
Preferably, the chelating agent is the sodium phytate and 65-75wt% iminodisuccinic acids four of 25-35wt%
The mixture of sodium.
In the present invention, if inventor does not make special explanation, each raw material are all with substance content 100%
It calculates.
The present invention can commonly use each universal method of the industry to prepare.For example, heating water to 60-80 DEG C, add
Enter lauryl sodium sulfate, Cocoamidopropyl betaine, laruyl alcohol sulfate ammonium salt, glycerine and Cortex Moutan extract (if
Have in formula), it stirs 20-60 minutes, is cooled to 30-40 DEG C, add chelating agent (if having in formula), 5-10 points of stirring
Clock.
The clothes detergent of the present invention, can effectively remove dirt, it is environmentally safe, safe and non-toxic, to human skin without
Stimulation, washes rear noresidue, and have the function of restraining and sterilizing bacteria.
Specific implementation mode
It is further illustrated the present invention below by the mode of embodiment, but does not therefore limit the present invention to the reality
It applies among a range.In the following examples, the experimental methods for specific conditions are not specified, according to conventional methods and conditions, or according to quotient
Product specification selects.
Embodiment 1
A kind of clothes detergent, including following materials by weight percentage：
Lauryl sodium sulfate 7%；
Cocoamidopropyl betaine 4%；
Laruyl alcohol sulfate ammonium salt 4%；
Glycerine 1.5%；
Surplus is water.
70 DEG C are heated water to, lauryl sodium sulfate, Cocoamidopropyl betaine, laruyl alcohol sulfate ammonium salt is added
And glycerine, it stirs 40 minutes, is cooled to 35 DEG C, you can the clothes detergent of the present invention is made.
Embodiment 2
A kind of clothes detergent, including following materials by weight percentage：
Lauryl sodium sulfate 7%；
Cocoamidopropyl betaine 4%；
Laruyl alcohol sulfate ammonium salt 4%；
Cortex Moutan extract 0.5%；
Glycerine 1.5%；
Surplus is water.
70 DEG C are heated water to, lauryl sodium sulfate, Cocoamidopropyl betaine, bay alcohol sulfuric ester ammonium is added
Salt, glycerine and Cortex Moutan extract stir 40 minutes, are cooled to 35 DEG C, you can the clothes detergent of the present invention is made.
The Cortex Moutan extract is prepared by following methods：Moutan bark is crushed, 40 mesh sieve is crossed, obtains moutan bark
100g moutan barks powder and 1200mL water are mixed, 30 minutes are stood at 25 DEG C by powder, are ultrasonically treated 48 minutes, using 300 mesh filter clothes
Filtering, obtains filtrate and filter residue；The ethanol water that filter residue and 1000mL volume fractions are 75% mixes, in 65 DEG C of refluxing extractions
3 hours, using 300 mesh filter-cloth filterings, filtrate is obtained, merges filtrate twice, pressure is 0.02MPa, temperature is 65 DEG C of decompressions
The density for being concentrated into 65 DEG C is 1.08g/mL, obtains Cortex Moutan extract, the condition of the supersound process is：Ultrasonic temperature 65
DEG C, ultrasonic power 150W, supersonic frequency 20kHz.
Embodiment 3
A kind of clothes detergent, including following materials by weight percentage：
Lauryl sodium sulfate 7%；
Cocoamidopropyl betaine 4%；
Laruyl alcohol sulfate ammonium salt 4%；
Cortex Moutan extract 0.5%；
Glycerine 1.5%；
Chelating agent sodium phytate 0.4%；
Surplus is water.
70 DEG C are heated water to, lauryl sodium sulfate, Cocoamidopropyl betaine, bay alcohol sulfuric ester ammonium is added
Salt, glycerine and Cortex Moutan extract stir 40 minutes, are cooled to 35 DEG C, add chelating agent, stir 8 minutes, you can this is made
The clothes detergent of invention.
The Cortex Moutan extract is prepared by following methods：Moutan bark is crushed, 40 mesh sieve is crossed, obtains moutan bark
100g moutan barks powder and 1200mL water are mixed, 30 minutes are stood at 25 DEG C by powder, are ultrasonically treated 48 minutes, using 300 mesh filter clothes
Filtering, obtains filtrate and filter residue；The ethanol water that filter residue and 1000mL volume fractions are 75% mixes, in 65 DEG C of refluxing extractions
3 hours, using 300 mesh filter-cloth filterings, filtrate is obtained, merges filtrate twice, pressure is 0.02MPa, temperature is 65 DEG C of decompressions
The density for being concentrated into 65 DEG C is 1.08g/mL, obtains Cortex Moutan extract, the condition of the supersound process is：Ultrasonic temperature 65
DEG C, ultrasonic power 150W, supersonic frequency 20kHz.
Embodiment 4
A kind of clothes detergent, including following materials by weight percentage：
Lauryl sodium sulfate 7%；
Cocoamidopropyl betaine 4%；
Laruyl alcohol sulfate ammonium salt 4%；
Cortex Moutan extract 0.5%；
Glycerine 1.5%；
Four sodium 0.4% of chelating agent iminodisuccinic acid；
Surplus is water.
70 DEG C are heated water to, lauryl sodium sulfate, Cocoamidopropyl betaine, bay alcohol sulfuric ester ammonium is added
Salt, glycerine and Cortex Moutan extract stir 40 minutes, are cooled to 35 DEG C, add chelating agent, stir 8 minutes, you can this is made
The clothes detergent of invention.
The Cortex Moutan extract is prepared by following methods：Moutan bark is crushed, 40 mesh sieve is crossed, obtains moutan bark
100g moutan barks powder and 1200mL water are mixed, 30 minutes are stood at 25 DEG C by powder, are ultrasonically treated 48 minutes, using 300 mesh filter clothes
Filtering, obtains filtrate and filter residue；The ethanol water that filter residue and 1000mL volume fractions are 75% mixes, in 65 DEG C of refluxing extractions
3 hours, using 300 mesh filter-cloth filterings, filtrate is obtained, merges filtrate twice, pressure is 0.02MPa, temperature is 65 DEG C of decompressions
The density for being concentrated into 65 DEG C is 1.08g/mL, obtains Cortex Moutan extract, the condition of the supersound process is：Ultrasonic temperature 65
DEG C, ultrasonic power 150W, supersonic frequency 20kHz.
Embodiment 5
A kind of clothes detergent, including following materials by weight percentage：
Lauryl sodium sulfate 7%；
Cocoamidopropyl betaine 4%；
Laruyl alcohol sulfate ammonium salt 4%；
Cortex Moutan extract 0.5%；
Glycerine 1.5%；
Chelating agent 0.4%；
Surplus is water.
70 DEG C are heated water to, lauryl sodium sulfate, Cocoamidopropyl betaine, bay alcohol sulfuric ester ammonium is added
Salt, glycerine and Cortex Moutan extract stir 40 minutes, are cooled to 35 DEG C, add chelating agent, stir 8 minutes, you can this is made
The clothes detergent of invention.
The chelating agent is the mixture of four sodium of sodium phytate and 70wt% iminodisuccinic acids of 30wt%.
The Cortex Moutan extract is prepared by following methods：Moutan bark is crushed, 40 mesh sieve is crossed, obtains moutan bark
100g moutan barks powder and 1200mL water are mixed, 30 minutes are stood at 25 DEG C by powder, are ultrasonically treated 48 minutes, using 300 mesh filter clothes
Filtering, obtains filtrate and filter residue；The ethanol water that filter residue and 1000mL volume fractions are 75% mixes, in 65 DEG C of refluxing extractions
3 hours, using 300 mesh filter-cloth filterings, filtrate is obtained, merges filtrate twice, pressure is 0.02MPa, temperature is 65 DEG C of decompressions
The density for being concentrated into 65 DEG C is 1.08g/mL, obtains Cortex Moutan extract, the condition of the supersound process is：Ultrasonic temperature 65
DEG C, ultrasonic power 150W, supersonic frequency 20kHz.
Embodiment 6
A kind of clothes detergent, including following materials by weight percentage：
Lauryl sodium sulfate 7%；
Cocoamidopropyl betaine 4%；
Laruyl alcohol sulfate ammonium salt 4%；
Cortex Moutan extract 0.5%；
Glycerine 1.5%；
Chelating agent 0.4%；
Surplus is water.
70 DEG C are heated water to, lauryl sodium sulfate, Cocoamidopropyl betaine, bay alcohol sulfuric ester ammonium is added
Salt, glycerine and Cortex Moutan extract stir 40 minutes, are cooled to 35 DEG C, add chelating agent, stir 8 minutes, you can this is made
The clothes detergent of invention.
The chelating agent is the mixture of four sodium of sodium phytate and 70wt% iminodisuccinic acids of 30wt%.
The Cortex Moutan extract is prepared by following methods：Moutan bark is crushed, 40 mesh sieve is crossed, obtains moutan bark
100g moutan barks powder and 1200mL water are mixed, 30 minutes are stood at 25 DEG C by powder, are ultrasonically treated 25 minutes, after being spaced 2 minutes again
It is ultrasonically treated 15 minutes, is ultrasonically treated 8 minutes after being spaced 2 minutes again, using 300 mesh filter-cloth filterings, obtains filtrate and filter residue；
The ethanol water that filter residue and 1000mL volume fractions are 75% mixes, in 65 DEG C of refluxing extractions 3 hours, using 300 mesh filter clothes
Filtering, obtains filtrate, merges filtrate twice, pressure is 0.02MPa, temperature is that 65 DEG C of density for being concentrated under reduced pressure into 65 DEG C are
1.08g/mL, obtains Cortex Moutan extract, and the condition of the supersound process is：65 DEG C, ultrasonic power 150W of ultrasonic temperature, ultrasound
Frequency 20kHz.
Test case 1：Clean effect is tested
JB-02 albumen soiled cottons are tested before washing and with clothes detergent to JB-02 soiled cottons according to GB/T13174-2008
Whiteness value difference after washing.By environment friendly laundry liquid the whiteness difference result divided by standard front and back to JB-02 soiled cotton decontaminations washing
The liquid detergent whiteness difference front and back to JB-02 soiled cotton decontaminations washing evaluates clean effect as a result, as decontamination index, with this,
Specific data are shown in Table 1.
Specific experiment condition：A concentration of 2g/L of 250ppm hard water, clothes detergent, washing 20 minutes, temperature be 28 DEG C, adopt
With 60 turns defined RQHL types vertical washing machine, rotating speed/min.
Table 1：Clean effect test result table
| Decontamination index (JB-02 albumen soiled cotton) | |
| Embodiment 2 | 0.85 |
| Embodiment 3 | 0.93 |
| Embodiment 4 | 0.95 |
| Embodiment 5 | 1.02 |
Test case 2：Fungistatic effect is tested
Fungistatic effect is tested：Clothes detergent 5g and water 40g are mixed, stirred to complete with 100-200 revs/min at 45 DEG C
Dissolving, is configured to 1g：The sample solution of 8mL, with reference to application No. is the bacteriostatic tests in embodiment in 201511016139.6 6
The fungistatic effect of method test sample solution on E. coli (ATCC 25922).
Fungistatic effect is tested, and specific test result is shown in Table 2.
Table 2：Fungistatic effect test result table
| Antibacterial circle diameter, mm | |
| Embodiment 1 | 8.9 |
| Embodiment 2 | 10.2 |
| Embodiment 3 | 11.7 |
| Embodiment 4 | 12.0 |
| Embodiment 5 | 12.8 |
| Embodiment 6 | 13.5 |
The clothes detergent of the present invention, can effectively remove dirt, it is environmentally safe, safe and non-toxic, to human skin without
Stimulation, washes rear noresidue, and have the function of restraining and sterilizing bacteria.
The preferred embodiment of the present invention has been described in detail above.It should be appreciated that those skilled in the art without
It needs creative work according to the present invention can conceive and makes many modifications and variations.Therefore, all technologies in the art
Personnel are available by logical analysis, reasoning, or a limited experiment on the basis of existing technology under this invention's idea
Technical solution, all should be in the protection domain being defined in the patent claims.
Claims (6)
1. a kind of clothes detergent, including following materials by weight percentage：
Lauryl sodium sulfate 5-9%；
Cocoamidopropyl betaine 2-6%；
Laruyl alcohol sulfate ammonium salt 2-6%；
Glycerine 0.5-2.5%；
Surplus is water.
2. a kind of clothes detergent, including following materials by weight percentage：
Lauryl sodium sulfate 5-9%；
Cocoamidopropyl betaine 2-6%；
Laruyl alcohol sulfate ammonium salt 2-6%；
Cortex Moutan extract 0.1-0.9%；
Glycerine 0.5-2.5%；
Surplus is water.
3. clothes detergent as claimed in claim 2, which is characterized in that the Cortex Moutan extract is prepared by following methods
It obtains：Moutan bark is crushed, moutan bark powder is obtained, 80-120g moutan barks powder and 1000-1500mL water are mixed, at 20-30 DEG C
20-40 minutes are stood, is ultrasonically treated 35-55 minutes, filtrate and filter residue is obtained by filtration；Filter residue and 800-1200mL volume fractions are
The ethanol water of 70-80% mixes, and in 60-70 DEG C of refluxing extraction 2-4 hour, is obtained by filtration filtrate, and merging filtrate twice subtracts
It is 1.05-1.10g/mL that pressure, which is concentrated into density, obtains Cortex Moutan extract, the condition of the supersound process is：Ultrasonic temperature 60-
70 DEG C, ultrasonic power 100-200W, supersonic frequency 15-25kHz.
4. clothes detergent as claimed in claim 2, which is characterized in that the Cortex Moutan extract is prepared by following methods
It arrives：Moutan bark is crushed, moutan bark powder is obtained, 80-120g moutan barks powder and 1000-1500mL water are mixed, it is quiet at 20-30 DEG C
It sets 20-40 minutes, is ultrasonically treated 20-30 minutes, interval is then sonicated 10-20 minutes after 1-3 minutes, is spaced 1-3 points again
It is ultrasonically treated 5-10 minutes after clock, filtrate and filter residue is obtained by filtration；Filter residue and the second that 800-1200mL volume fractions are 70-80%
Alcohol solution mixes, and in 60-70 DEG C of refluxing extraction 2-4 hour, is obtained by filtration filtrate, and merging filtrate twice is concentrated under reduced pressure into 65
DEG C density be 1.05-1.10g/mL, obtain Cortex Moutan extract, the condition of the supersound process is：Ultrasonic temperature 60-70
DEG C, ultrasonic power 100-200W, supersonic frequency 15-25kHz.
5. the clothes detergent as described in any one of claim 1-4, which is characterized in that former including following weight percentage
Material：
Lauryl sodium sulfate 5-9%；
Cocoamidopropyl betaine 2-6%；
Laruyl alcohol sulfate ammonium salt 2-6%；
Cortex Moutan extract 0.1-0.9%；
Glycerine 0.5-2.5%；
Chelating agent 0.1-0.7%；
Surplus is water.
6. clothes detergent as claimed in claim 5, which is characterized in that the chelating agent is sodium phytate and/or Asia
Four sodium of amino disuccinic acid.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201810537453.6A CN108485838B (en) | 2018-05-30 | 2018-05-30 | Clothes cleaning agent |
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| CN201810537453.6A CN108485838B (en) | 2018-05-30 | 2018-05-30 | Clothes cleaning agent |
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| CN109321390A (en) * | 2018-11-29 | 2019-02-12 | 中国农业科学院兰州畜牧与兽药研究所 | A kind of bloodstain cleaning agent and its preparation and application |
| CN111893007A (en) * | 2020-08-11 | 2020-11-06 | 山东中佳药业有限公司 | Chlorogenic acid-containing composition and application thereof in disinfection and antibiosis |
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| CN108485838B (en) | 2020-06-16 |
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Inventor after: He Zhiyong Inventor after: Lu Aiming Inventor before: Lu Aiming |
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Effective date of registration: 20200521 Address after: 363000 No.8 Shugang Road, Fugong Town, Longhai City, Zhangzhou City, Fujian Province Applicant after: FUJIAN MENGJIAOLAN DAILY CHEMICALS Co.,Ltd. Address before: 215332 2-5 new East residence, Huaqiao Town, Kunshan City, Suzhou, Jiangsu. Applicant before: Lu Aiming |
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Denomination of invention: Laundry detergent Effective date of registration: 20220614 Granted publication date: 20200616 Pledgee: Bank of China Limited Longhai sub branch Pledgor: FUJIAN MENGJIAOLAN DAILY CHEMICALS Co.,Ltd. Registration number: Y2022350000061 |