CN108484110A - A kind of formula for ceramic 3D printing pug - Google Patents
A kind of formula for ceramic 3D printing pug Download PDFInfo
- Publication number
- CN108484110A CN108484110A CN201810663500.1A CN201810663500A CN108484110A CN 108484110 A CN108484110 A CN 108484110A CN 201810663500 A CN201810663500 A CN 201810663500A CN 108484110 A CN108484110 A CN 108484110A
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- Prior art keywords
- printing
- pug
- ceramic
- formula
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Classifications
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B33/00—Clay-wares
- C04B33/02—Preparing or treating the raw materials individually or as batches
- C04B33/13—Compounding ingredients
- C04B33/1305—Organic additives
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B33—ADDITIVE MANUFACTURING TECHNOLOGY
- B33Y—ADDITIVE MANUFACTURING, i.e. MANUFACTURING OF THREE-DIMENSIONAL [3-D] OBJECTS BY ADDITIVE DEPOSITION, ADDITIVE AGGLOMERATION OR ADDITIVE LAYERING, e.g. BY 3-D PRINTING, STEREOLITHOGRAPHY OR SELECTIVE LASER SINTERING
- B33Y70/00—Materials specially adapted for additive manufacturing
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B33/00—Clay-wares
- C04B33/02—Preparing or treating the raw materials individually or as batches
- C04B33/13—Compounding ingredients
- C04B33/1315—Non-ceramic binders
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/48—Organic compounds becoming part of a ceramic after heat treatment, e.g. carbonising phenol resins
- C04B2235/483—Si-containing organic compounds, e.g. silicone resins, (poly)silanes, (poly)siloxanes or (poly)silazanes
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Ceramic Engineering (AREA)
- Materials Engineering (AREA)
- Dispersion Chemistry (AREA)
- Structural Engineering (AREA)
- Organic Chemistry (AREA)
- Manufacturing & Machinery (AREA)
- Inks, Pencil-Leads, Or Crayons (AREA)
Abstract
The invention discloses a kind of formulas for ceramic 3D printing pug, the clay for weighing 100 900g first is placed in container, it is 50 200 ten thousand viscous silicone oil that 10 20g atoleines and 30 90g viscosity are added in a reservoir, it is sufficiently stirred, octyl phenol polyoxyethylene ether is added in pug and stirs 30min, homogeneous, Tween 60 is added, it is uniformly mixed, it stands and the pug prepared is packed into barrel, it adjusts instrument parameter and carries out 3D printing, preparation process of the present invention is simple, operation is easy, stickiness and mobility matching are preferable, it is easy to be molded, sample discharging is smooth, pug formula is mainly used for the 3D printing of ceramics.
Description
Technical field
The invention belongs to 3D printing field of material technology, in particular for the formula of ceramic 3D printing pug.
Background technology
3D printing technique is also known as three-dimensional printing technology, be one kind based on digital model file, with powdery metal
Or the adhesive materials such as plastics, construct the technology of object by layer-by-layer printing.It is without mechanical processing or any mould
Tool, the part of any shape can be generated directly from computer graphics data, great advantage is formed to shaped piece, to
The lead time for greatly shortening product improves productivity and reduces production cost.
Currently, the development of ceramic 3D printing lag behind metal and it is high molecular be primarily due to have pug it is higher
It is required that.Ceramic material is generally made of inorganic non-metallic material, dispersant, binder, surfactant and other serial auxiliary materials.
The basic demand of this pug is that the particle of inorganic non-metallic material is necessarily less than 1 μm, and even particle distribution is not reunited,
Caking property cannot be too big, good fluidity, and the matching problem of stickiness and mobility is key therein.
Invention content
The case where based on the prior art, have that global formation, controllability be good, work the purpose of the present invention is to provide one kind
Skill is simply and the formula for ceramics 3D printing pug of high mechanical properties.
In order to realize that above-mentioned technical purpose, the technical solution adopted by the present invention be：
A kind of formula for ceramic 3D printing pug, formula are made of following raw material：
100-900 parts of clay；
10-20 parts of binder；
30-90 parts of silicone oil；
2-10 parts of octyl phenol polyoxyethylene ether；
1-7 parts of Tween-60.
Further, the binder is paraffin oil.
A kind of formula, preparing process for ceramic 3D printing pug comprising following steps：
1）Clay is weighed to be placed in container；
2）Binder and silicone oil are sequentially added in the container equipped with clay, is then sufficiently stirred mixing, mixture is made；
3）In step 2）Octyl phenol polyoxyethylene ether is added in mixture obtained and continues to stir 30min, makes its homogeneous, then
Tween-60 is added, after remixing uniformly, carries out stewing process, you can is made for ceramic 3D printing pug.
Wherein, octyl phenol polyoxyethylene ether and Tween-60 are surfactant.
Further, step 2）The viscosity of middle silicone oil is viscous for 50-200 ten thousand.
By the application for ceramic 3D printing pug made from above-mentioned processing method, the 3D printing for using it for ceramics is former
Material.
Using above-mentioned technical solution, the present invention program have the advantage that for：The present invention uses above-mentioned formula scheme
Prepared ceramic material has stickiness and mobility matching preferable, discharges in print procedure smooth and be easy to be molded, separately
Outside, bright spot of the invention further includes：（1）Preparation process is simple, and operation is easy；（2）Stickiness and mobility matching are preferable, are easy into
Type.
Description of the drawings
The present invention is further elaborated with reference to the accompanying drawings and detailed description：
Fig. 1 is that the embodiment of the present invention 1 prints the product schematic diagram after pug sintered；
Fig. 2 is that the embodiment of the present invention 2 prints the product schematic diagram after pug sintered.
Specific implementation mode
A kind of formula for ceramic 3D printing pug, formula are made of following raw material：
100-900 parts of clay；
10-20 parts of binder；
30-90 parts of silicone oil；
2-10 parts of octyl phenol polyoxyethylene ether；
1-7 parts of Tween-60.
Further, the binder is paraffin oil.
A kind of formula, preparing process for ceramic 3D printing pug comprising following steps：
1）Clay is weighed to be placed in container；
2）Binder and silicone oil are sequentially added in the container equipped with clay, is then sufficiently stirred mixing, mixture is made；
3）In step 2）Octyl phenol polyoxyethylene ether is added in mixture obtained and continues to stir 30min, makes its homogeneous, then
Tween-60 is added, after remixing uniformly, carries out stewing process, you can is made for ceramic 3D printing pug.
Wherein, octyl phenol polyoxyethylene ether and Tween-60 are surfactant.
Further, step 2）The viscosity of middle silicone oil is viscous for 50-200 ten thousand.
Embodiment 1
A kind of formula, preparing process for ceramic 3D printing pug comprising following steps：
1）600 g clays are weighed to be placed in container；
2）It is 1,000,000 viscous silicone oil that 10 g paraffin oils and 30 g viscosity are sequentially added in the container equipped with clay, then by it
It is sufficiently stirred mixing, mixture is made；
3）In step 2）3 g octyl phenol polyoxyethylene ether are added in mixture obtained and continue to stir 30min, make its homogeneous,
Then 2 g Tween-60 are added, after remixing uniformly, carry out stewing process, you can are made for ceramic 3D printing pug；
4）The printing pug prepared is packed into barrel, parameter carries out 3D printing together for adjustment 3D printing, and obtained product is burnt
Shown in product schematic diagram 1 after knot.
Embodiment 2
A kind of formula, preparing process for ceramic 3D printing pug comprising following steps：
1）500 g clays are weighed to be placed in container；
2）It is 1,500,000 viscous silicone oil that 15 g paraffin oils and 45 g viscosity are sequentially added in the container equipped with clay, then by it
It is sufficiently stirred mixing, mixture is made；
3）In step 2）5 g octyl phenol polyoxyethylene ether are added in mixture obtained and continue to stir 30min, make its homogeneous,
Then 4 g Tween-60 are added, after remixing uniformly, carry out stewing process, you can are made for ceramic 3D printing pug；
4）The printing pug prepared is packed into barrel, parameter carries out 3D printing together for adjustment 3D printing, and obtained product is burnt
Shown in product schematic diagram 2 after knot.
Embodiment 3
A kind of formula, preparing process for ceramic 3D printing pug comprising following steps：
1）100 g clays are weighed to be placed in container；
2）It is 2,000,000 viscous silicone oil that 20 g paraffin oils and 90 g viscosity are sequentially added in the container equipped with clay, then by it
It is sufficiently stirred mixing, mixture is made；
3）In step 2）10 g octyl phenol polyoxyethylene ether are added in mixture obtained and continue to stir 30min, make its homogeneous,
Then 7 g Tween-60 are added, after remixing uniformly, carry out stewing process, you can are made for ceramic 3D printing pug；
4）The printing pug prepared is packed into barrel, parameter carries out 3D printing together for adjustment 3D printing
The foregoing is merely presently preferred embodiments of the present invention, all equivalent changes done according to scope of the present invention patent with repair
Decorations should all belong to the covering scope of the present invention.
Claims (5)
1. a kind of formula for ceramic 3D printing pug, it is characterised in that：Its formula is made of following raw material：
100-900 parts of clay；
10-20 parts of binder；
30-90 parts of silicone oil；
2-10 parts of octyl phenol polyoxyethylene ether；
1-7 parts of Tween-60.
2. a kind of formula for ceramic 3D printing pug according to claim 1, it is characterised in that：The binder is
Paraffin oil.
3. a kind of formula, preparing process for ceramic 3D printing pug according to claim 1 or claim 2, it is characterised in that：Its
Include the following steps：
1）Clay is weighed to be placed in container；
2）Binder and silicone oil are sequentially added in the container equipped with clay, is then sufficiently stirred mixing, mixture is made；
3）In step 2）Octyl phenol polyoxyethylene ether is added in mixture obtained and continues to stir 30min, makes its homogeneous, then
Tween-60 is added, after remixing uniformly, carries out stewing process, you can is made for ceramic 3D printing pug.
4. a kind of formula, preparing process for ceramic 3D printing pug according to claim 3, it is characterised in that：Step
2）The viscosity of middle silicone oil is viscous for 50-200 ten thousand.
5. the processing method as claimed in claim 3 application obtained for ceramic 3D printing pug, it is characterised in that：It is used
In the 3D printing raw material of ceramics.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810663500.1A CN108484110A (en) | 2018-06-25 | 2018-06-25 | A kind of formula for ceramic 3D printing pug |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810663500.1A CN108484110A (en) | 2018-06-25 | 2018-06-25 | A kind of formula for ceramic 3D printing pug |
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| Publication Number | Publication Date |
|---|---|
| CN108484110A true CN108484110A (en) | 2018-09-04 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201810663500.1A Pending CN108484110A (en) | 2018-06-25 | 2018-06-25 | A kind of formula for ceramic 3D printing pug |
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| Country | Link |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CH715480A1 (en) * | 2018-10-30 | 2020-04-30 | Alpla Werke Alwin Lehner Gmbh & Co Kg | Plastic container, in particular for flowable and free-flowing filling material, the container body having at least one support structure. |
| CN111362667A (en) * | 2020-04-09 | 2020-07-03 | 福建造物蛛智能制造有限公司 | Water-based ceramic material for 3D printing and preparation method thereof |
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| WO2016024863A1 (en) * | 2014-08-15 | 2016-02-18 | Ihc Holland Ie B.V. | Deposition of clay structures |
| CN105503147A (en) * | 2015-12-24 | 2016-04-20 | 成都新柯力化工科技有限公司 | Clay material for 3D printing and preparation method of clay material |
| CN105503146A (en) * | 2015-12-24 | 2016-04-20 | 成都新柯力化工科技有限公司 | Clay material for laser sintering 3D printing and preparation method of clay material |
| CN105645923A (en) * | 2015-12-24 | 2016-06-08 | 成都新柯力化工科技有限公司 | Filamentous clay material for 3D printing and preparation method thereof |
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| CN106396620A (en) * | 2016-09-07 | 2017-02-15 | 济南大学 | Preparation of rapid prototyping black pottery powder material used for 3DP (three-dimensional printing) process |
| CN107090726A (en) * | 2017-06-26 | 2017-08-25 | 王蒙 | A kind of printing assistant |
| CN107098717A (en) * | 2017-04-07 | 2017-08-29 | 武汉理工大学 | A kind of 3 D-printing molding method for preparing of filtering porous ceramics |
| CN107304238A (en) * | 2016-04-20 | 2017-10-31 | 天津市有为印刷包装有限公司 | A kind of printing ink powder adhesive composition and preparation method thereof |
| CN107512898A (en) * | 2017-08-14 | 2017-12-26 | 河海大学常州校区 | A kind of 3D printing clay material and preparation method thereof |
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2018
- 2018-06-25 CN CN201810663500.1A patent/CN108484110A/en active Pending
Patent Citations (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2016024863A1 (en) * | 2014-08-15 | 2016-02-18 | Ihc Holland Ie B.V. | Deposition of clay structures |
| CN105174907A (en) * | 2015-06-30 | 2015-12-23 | 成都新柯力化工科技有限公司 | 3D printing clay material and preparation method thereof |
| CN105503147A (en) * | 2015-12-24 | 2016-04-20 | 成都新柯力化工科技有限公司 | Clay material for 3D printing and preparation method of clay material |
| CN105503146A (en) * | 2015-12-24 | 2016-04-20 | 成都新柯力化工科技有限公司 | Clay material for laser sintering 3D printing and preparation method of clay material |
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| CN107304238A (en) * | 2016-04-20 | 2017-10-31 | 天津市有为印刷包装有限公司 | A kind of printing ink powder adhesive composition and preparation method thereof |
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| CN107098717A (en) * | 2017-04-07 | 2017-08-29 | 武汉理工大学 | A kind of 3 D-printing molding method for preparing of filtering porous ceramics |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CH715480A1 (en) * | 2018-10-30 | 2020-04-30 | Alpla Werke Alwin Lehner Gmbh & Co Kg | Plastic container, in particular for flowable and free-flowing filling material, the container body having at least one support structure. |
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| CN111362667A (en) * | 2020-04-09 | 2020-07-03 | 福建造物蛛智能制造有限公司 | Water-based ceramic material for 3D printing and preparation method thereof |
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| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20180904 |
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| RJ01 | Rejection of invention patent application after publication |