CN108477153A - A kind of thickening aids compound aqueous suitable for glyphosate and Mediben - Google Patents
A kind of thickening aids compound aqueous suitable for glyphosate and Mediben Download PDFInfo
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- CN108477153A CN108477153A CN201810323941.7A CN201810323941A CN108477153A CN 108477153 A CN108477153 A CN 108477153A CN 201810323941 A CN201810323941 A CN 201810323941A CN 108477153 A CN108477153 A CN 108477153A
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- Prior art keywords
- glyphosate
- mediben
- compound aqueous
- thickening aids
- thickening
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
- A01N25/30—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests characterised by the surfactants
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
- A01N25/02—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests containing liquids as carriers, diluents or solvents
- A01N25/04—Dispersions, emulsions, suspoemulsions, suspension concentrates or gels
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N37/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
- A01N37/36—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing at least one carboxylic group or a thio analogue, or a derivative thereof, and a singly bound oxygen or sulfur atom attached to the same carbon skeleton, this oxygen or sulfur atom not being a member of a carboxylic group or of a thio analogue, or of a derivative thereof, e.g. hydroxy-carboxylic acids
- A01N37/38—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing at least one carboxylic group or a thio analogue, or a derivative thereof, and a singly bound oxygen or sulfur atom attached to the same carbon skeleton, this oxygen or sulfur atom not being a member of a carboxylic group or of a thio analogue, or of a derivative thereof, e.g. hydroxy-carboxylic acids having at least one oxygen or sulfur atom attached to an aromatic ring system
- A01N37/40—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing at least one carboxylic group or a thio analogue, or a derivative thereof, and a singly bound oxygen or sulfur atom attached to the same carbon skeleton, this oxygen or sulfur atom not being a member of a carboxylic group or of a thio analogue, or of a derivative thereof, e.g. hydroxy-carboxylic acids having at least one oxygen or sulfur atom attached to an aromatic ring system having at least one carboxylic group or a thio analogue, or a derivative thereof, and one oxygen or sulfur atom attached to the same aromatic ring system
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N57/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds
- A01N57/18—Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds having phosphorus-to-carbon bonds
- A01N57/20—Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds having phosphorus-to-carbon bonds containing acyclic or cycloaliphatic radicals
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- Life Sciences & Earth Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Health & Medical Sciences (AREA)
- Pest Control & Pesticides (AREA)
- Agronomy & Crop Science (AREA)
- Plant Pathology (AREA)
- Engineering & Computer Science (AREA)
- Dentistry (AREA)
- Wood Science & Technology (AREA)
- Zoology (AREA)
- Environmental Sciences (AREA)
- Toxicology (AREA)
- Dispersion Chemistry (AREA)
- Chemical & Material Sciences (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The invention discloses a kind of thickening aids compound aqueous suitable for glyphosate and Mediben, are mainly made of according to a certain percentage water soluble surfactant active such as dodecyl polyoxyethylene groups amine oxide, lauroyl Sodium Glycinate, oleamide propyl betaine and alkyl glycosides.The auxiliary agent is compound aqueous to glyphosate and Mediben to have excellent thickening power, and aqua heatproof cold resistance is good.
Description
Technical field
The invention belongs to technical field of pesticide, and in particular to a kind of insecticides adjuvant more particularly to glyphosate and Mediben are multiple
Thickening aids with aqua.
Background technology
Glyphosate is now widely used large-tonnage steriland herbicide, due to not scientifical use for a long time, is caused miscellaneous
Careless resistance rapidly develops, and especially broad leaved weed resistance development in part is extremely rapid.In order to slow down the development of glyphosate-resistant weeds,
And improve glyphosate herbicide speed and expand herbicide controlling spectrum, pesticide producing enterprise is mixed with Mediben using glyphosate, and studies system
Both standby mix preparation, wherein most commonly seen with aqua.
Ammonium salt, isopropyl amine salt and the dimethylamine salt and Mediben of glyphosate all have preferable water solubility, can prepare
At the aqua of high-content, still, when the two exists simultaneously in same aqueous solution, it may occur that saponification or even layering and precipitating.
Currently, researcher mainly utilizes the surfactant micellar solubilization of high concentration, solves low content glyphosate and Mediben is mixed
The stability of Heshui agent, but the stability without solving high-content mixing aqua, with more making with certain adhesiveness
Thickening type mixing aqua product.
The auxiliary agent of the present invention is to be directed to the physicochemical property of glyphosate and Mediben in aqueous solution, and that specially researches and develops is compound
Auxiliary agent is made of a variety of water soluble surfactant actives, and the present invention is that one kind can improve high content glyphosate and Mediben is multiple
Additives Products with aqua stability, it is often more important that the present invention has excellent thickening property to the compound aqueous of the two.
Invention content:
The purpose of the present invention is to provide a kind of thickening aids compound aqueous suitable for glyphosate and Mediben.
The purpose of the present invention is what is be accomplished by the following way:
A kind of thickening aids compound aqueous suitable for glyphosate and Mediben, the thickening aids are mainly by dodecane
Base polyoxyethylene groups amine oxide, lauroyl Sodium Glycinate, oleamide propyl betaine and alkyl glycosides composition.
It is preferred that above-mentioned dodecyl polyoxyethylene groups amine oxide, lauroyl Sodium Glycinate, oleamide propyl betaine and
The weight ratio of alkyl glycosides is 20-40:5-10:10-20:10-30.Weight content of the principle active component in auxiliary agent be
45%-100%.
Above-mentioned glyphosate is that any one water soluble salt form exists in ammonium salt, isopropyl amine salt, dimethylamine salt.
The above-mentioned thickening aids compound aqueous suitable for glyphosate and Mediben, it is specific composed of the following components:
Auxiliary agent of the present invention is compound aqueous to the glyphosate and Mediben of a variety of contents to have significant, stable thickening property
Energy.The auxiliary agent is suitable for glyphosate content 20-50%, and Mediben content 0.1-20%'s is compound aqueous, and the auxiliary agent is particularly suitable
In glyphosate content 30-40%, Mediben content 2-10%'s is compound aqueous.
Dosage of the above-mentioned thickening aids compound aqueous suitable for glyphosate and Mediben compound aqueous is 10%-
15%.
Beneficial effects of the present invention compared with the prior art:
1, auxiliary agent thickening properties of the invention are notable, are suitable for thickening type glyphosate and Mediben is compound aqueous.
2, auxiliary agent of the invention has excellent surfactant property of solubilizing for glyphosate and Mediben are compound aqueous,
Suitable for glyphosate content 20-50%, Mediben content 0.1-20%'s is compound aqueous, especially suitable for glyphosate content 30-
40%, Mediben content 2-10%'s is compound aqueous, and well, heat resistance is good for the stabilization of made various aquas.
3, auxiliary agent of the invention is applied widely, and it is arbitrary to be suitable for ammonium salt, isopropyl amine salt or dimethylamine salt of glyphosate etc.
A kind of salt is compound aqueous with Mediben dimethylamine salt.
Specific embodiment
By following embodiment, the present invention is further described, but does not illustrate that the present invention is limited to these implementations
Example.
Embodiment 1
A kind of thickening aids compound aqueous suitable for glyphosate and Mediben, are matched by following substance according to mass percent
It makes:
Embodiment 2
A kind of thickening aids compound aqueous suitable for glyphosate and Mediben, are matched by following substance according to mass percent
It makes:
Embodiment 3
A kind of thickening aids compound aqueous suitable for glyphosate and Mediben, are matched by following substance according to mass percent
It makes:
Embodiment 4
A kind of thickening aids compound aqueous suitable for glyphosate and Mediben, are matched by following substance according to mass percent
It makes:
Embodiment 5
A kind of thickening aids compound aqueous suitable for glyphosate and Mediben, are matched by following substance according to mass percent
It makes:
Embodiment 6
A kind of thickening aids compound aqueous suitable for glyphosate and Mediben, are matched by following substance according to mass percent
It makes:
Embodiment 7
A kind of thickening aids compound aqueous suitable for glyphosate and Mediben, are matched by following substance according to mass percent
It makes:
Embodiment 8
A kind of thickening aids compound aqueous suitable for glyphosate and Mediben, are matched by following substance according to mass percent
It makes:
Embodiment 9
38% glyphosate+Mediben (30+8) aqua, is formulated by mass percentage by following substance:
38% glyphosate+Mediben (30+8) aqua glyphosate exists with ammonium salts, and Mediben is with dimethylamine salt shape
Formula exists.Aqua appearance is in the sticky flowable liquids of homogeneous phase transparent, and viscosity is 300mPa.s (25 DEG C), cold heat storage stability
Well, the problems such as said preparation stores 30d at -10 DEG C and 54 DEG C respectively, no layering and precipitation, dilution stability is good (to be utilized
342ppm standard hard waters, which dilute, stands 18h at 20 times, 30 DEG C, no layering and precipitation), meet national standard and FAO standards, it is water-soluble
Property is good.
Embodiment 10
32% glyphosate+Mediben (30+2) aqua, is formulated by mass percentage by following substance:
32% glyphosate+Mediben (30+2) aqua glyphosate exists with ammonium salts, and Mediben is with dimethylamine salt shape
Formula exists.Aqua appearance is in the sticky flowable liquids of homogeneous phase transparent, and viscosity is 280mPa.s (25 DEG C), cold heat storage stability
Well, the problems such as said preparation stores 30d at -10 DEG C and 54 DEG C respectively, no layering and precipitation, dilution stability is good (to be utilized
342ppm standard hard waters, which dilute, stands 18h at 20 times, 30 DEG C, no layering and precipitation), meet national standard and FAO standards, it is water-soluble
Property is good.
Embodiment 11
45% glyphosate+Mediben (35+10) aqua, is formulated by mass percentage by following substance:
45% glyphosate+Mediben (35+10) aqua glyphosate exists in the form of isopropyl amine salt, and Mediben is with dimethylamine
Salt form exists.Aqua appearance is in the sticky flowable liquids of homogeneous phase transparent, and viscosity is 400mPa.s (25 DEG C), and cold and hot storage is steady
Qualitative good, the problems such as said preparation stores 30d at -10 DEG C and 54 DEG C respectively, no layering and precipitation, dilution stability is good (sharp
It is diluted with 342ppm standard hard waters and stands 18h at 20 times, 30 DEG C, no layering and precipitation), meet national standard and FAO standards, water
Dissolubility is good.
Embodiment 12
40% glyphosate+Mediben (35+5) aqua, is formulated by mass percentage by following substance:
40% glyphosate+Mediben (35+5) aqua glyphosate exists in the form of isopropyl amine salt, and Mediben is with dimethylamine
Salt form exists.
Aqua appearance is in the sticky flowable liquids of homogeneous phase transparent, and viscosity is 500mPa.s (25 DEG C), and cold and hot storage is stablized
Property good, the problems such as said preparation stores 30d at -10 DEG C and 54 DEG C respectively, no layering and precipitation, dilution stability is good (to be utilized
342ppm standard hard waters, which dilute, stands 18h at 20 times, 30 DEG C, no layering and precipitation), meet national standard and FAO standards, it is water-soluble
Property is good.
Embodiment 13
38% glyphosate+Mediben (35+3) aqua, has following substance to be formulated by mass percentage:
38% glyphosate+Mediben (35+3) aqua glyphosate and Mediben exist in the form of dimethylamine salt.
Aqua appearance is in the sticky flowable liquids of homogeneous phase transparent, and viscosity is 350mPa.s (25 DEG C), and cold and hot storage is stablized
Property good, the problems such as said preparation stores 30d at -10 DEG C and 54 DEG C respectively, no layering and precipitation, dilution stability is good (to be utilized
342ppm standard hard waters, which dilute, stands 18h at 20 times, 30 DEG C, no layering and precipitation), meet national standard and FAO standards, it is water-soluble
Property is good.
Embodiment 14
50% glyphosate+Mediben (40+10) aqua, is formulated by mass percentage by following substance:
50% glyphosate+Mediben (40+10) aqua glyphosate and Mediben exist in the form of dimethylamine salt.
Aqua appearance is in the sticky flowable liquids of homogeneous phase transparent, and viscosity is 450mPa.s (25 DEG C), and cold and hot storage is stablized
Property good, the problems such as said preparation stores 30d at -10 DEG C and 54 DEG C respectively, no layering and precipitation, dilution stability is good (to be utilized
342ppm standard hard waters, which dilute, stands 18h at 20 times, 30 DEG C, no layering and precipitation), meet national standard and FAO standards, it is water-soluble
Property is good.
Comparative example 1
45% glyphosate+Mediben (35+10) aqua, is formulated by mass percentage by following substance:
45% glyphosate+Mediben (35+10) aqua glyphosate exists in the form of isopropyl amine salt, and Mediben is with dimethylamine
Salt form exists.The flowable liquids that obtained aqua appearance is translucent, viscosity are only 10mPa.s (25 DEG C), said preparation room
Temperature places 2d, occurs being layered and has Precipitation phenomenon.
Comparative example 2
45% glyphosate+Mediben (35+10) aqua, has following substance to be formulated by mass percentage:
45% glyphosate+Mediben (35+10) aqua glyphosate exists in the form of isopropyl amine salt, and Mediben is with dimethylamine
Salt form exists.The transparent flowable liquids of obtained aqua appearance, viscosity are 300mPa.s (25 DEG C), and said preparation is at 54 DEG C
3d is stored, lamination occurs.
Test example 1
The 4 kinds of glyphosates and Mediben of embodiment 9,10,12,13 are compound aqueous.
Comparison medicament:30% gyphosate solution (commercially available).
Control object:The weeds such as lamb's-quarters, Horseweed Herb, annual gramineae.
Test method:According to the area of experimental plot, good various medicaments of precise, and after being watered dilution, using bearing
Formula sprayer carries out even spraying, the dedicated Fan spray head of sprinkler selection herbicide.
15d, 30d observe weeds death condition, and the activity of weeding of more various medicaments after medicine respectively.
The embodiment of the present invention preparation Herbicidal Testing Trials effect see the table below 1 (15d after medicine) and table 2 (30d after medicine)
1 field control effectiveness test result of table (15d after medicine)
2 field control effectiveness test result of table (30d after medicine)
The test of pesticide effectiveness the result shows that, the present invention have excellent synergistic effect.
Claims (8)
1. a kind of thickening aids compound aqueous suitable for glyphosate and Mediben, it is characterised in that the thickening aids are main
It is made of dodecyl polyoxyethylene groups amine oxide, lauroyl Sodium Glycinate, oleamide propyl betaine and alkyl glycosides.
2. the thickening aids compound aqueous suitable for glyphosate and Mediben according to claim 1, it is characterised in that ten
The weight ratio of dialkyl group polyoxyethylene groups amine oxide, lauroyl Sodium Glycinate, oleamide propyl betaine and alkyl glycosides
For 20-40:5-10:10-20:10-30.
3. according to the thickening aids compound aqueous suitable for glyphosate and Mediben described in claim 1, it is characterised in that
Weight content of the principle active component in auxiliary agent is 45%-100%.
4. according to the thickening aids compound aqueous suitable for glyphosate and Mediben described in claim 1, it is characterised in that
The glyphosate is that any one water soluble salt form exists in ammonium salt, isopropyl amine salt, dimethylamine salt, and Mediben is with diformazan
Amine salt form exists.
5. according to the thickening aids compound aqueous suitable for glyphosate and Mediben described in claim 1, it is characterised in that
It is specific composed of the following components:
6. according to the thickening aids compound aqueous suitable for glyphosate and Mediben described in claim 1, it is characterised in that
The auxiliary agent is suitable for glyphosate content 20-50%, and Mediben content 0.1-20%'s is compound aqueous.
7. according to the thickening aids compound aqueous suitable for glyphosate and Mediben described in claim 1, it is characterised in that
The auxiliary agent is suitable for glyphosate content 30-40%, and Mediben content 2-10%'s is compound aqueous.
8. according to the thickening aids compound aqueous suitable for glyphosate and Mediben described in claim 1, it is characterised in that
Dosage of the auxiliary agent in compound aqueous is 10%-15%.
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Cited By (4)
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CN110476968A (en) * | 2019-08-19 | 2019-11-22 | 南京拓际生物科技有限公司 | The low bubble low amounts type glufosinate-ammonium of one kind and glyphosate surfactant and its preparation process |
CN111034738A (en) * | 2019-12-30 | 2020-04-21 | 江苏腾龙生物药业有限公司 | Dicamba and glyphosate compound aqueous solution and preparation method thereof |
WO2021093271A1 (en) * | 2019-11-12 | 2021-05-20 | 南京华洲药业有限公司 | Beta cypermethrin nano aqueous agent, preparation method therefor and use thereof |
CN114431226A (en) * | 2022-02-21 | 2022-05-06 | 广东粤港澳大湾区国家纳米科技创新研究院 | Thickening aid suitable for high-salt water aqua |
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Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
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CN110476968A (en) * | 2019-08-19 | 2019-11-22 | 南京拓际生物科技有限公司 | The low bubble low amounts type glufosinate-ammonium of one kind and glyphosate surfactant and its preparation process |
WO2021093271A1 (en) * | 2019-11-12 | 2021-05-20 | 南京华洲药业有限公司 | Beta cypermethrin nano aqueous agent, preparation method therefor and use thereof |
CN111034738A (en) * | 2019-12-30 | 2020-04-21 | 江苏腾龙生物药业有限公司 | Dicamba and glyphosate compound aqueous solution and preparation method thereof |
CN114431226A (en) * | 2022-02-21 | 2022-05-06 | 广东粤港澳大湾区国家纳米科技创新研究院 | Thickening aid suitable for high-salt water aqua |
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