CN108451778B - Transparent gel hair care composition and preparation method thereof - Google Patents
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Abstract
The invention discloses a transparent gel hair care composition and a preparation method thereof. The clear gel hair care composition comprises: 0.1-50% of cationic surfactant, which is quaternary ammonium salt R4N+X‑A characteristic compound or a precursor capable of generating the structural characteristic through chemical reaction, wherein R is4Are respectively CH3-or C10‑C25While at least one R is CH3-and at least one R is C10‑C25Long chain of saturated alkanes; x represents anion with chemical valence of-1, including chloride ion, lactate ion, and citrate ion; 0.1-5% of humectant containing micromolecular polyalcohol or macromolecular polymer; 0.1-10% of hair conditioner, 0.1-30% of cosolvent, 0.05-1.0% of preservative and 0.5-2.0% of essence; the balance of deionized water. The composition has a transparent gel state, can provide excellent moisturizing and conditioning effects for hair, effectively improve the wet rinsing, wet combing and dry combing properties of the hair, reduce the electrostatic effect of the hair, and enable the hair to be softer and smoother.
Description
Technical Field
The invention relates to a skin care composition, belongs to the technical field of daily chemical products, and particularly relates to a transparent gel hair care composition and a preparation method thereof.
Background
With the improvement of living standard of people, on the basis of solving the problem of satiety, people pay more attention to the external image of the people, and more people pursue beautiful, fashionable and personalized appearance. Thus, hair, which is an attachment to human skin, plays an increasingly important role in beautifying the appearance of individuals. The behaviors of dyeing and scalding hair and the like are more and more common, and in the process of dyeing and scalding hair, operations such as bleaching, high temperature, strong alkali, dyeing and the like can cause damage to hair scales and loss of nutrient contents, and finally problems of dry hair, rough hair, dull hair, stiff hair and the like are caused. It is therefore highly desirable to have a product for improving and repairing damaged hair for everyday care.
With regard to hair care, a number of approaches have been developed, including the use of two-in-one products such as shampoos, conditioners, hair treatments, essential hair oils, and the like. Although the two-in-one shampoo is convenient to use, the two-in-one shampoo emphasizes the washing and hair care effects. Along with the increasing attention of consumers to hair care, the requirements of washing and protecting separation are also increased, so that the separation of washing and protecting hair is a development trend; in recent years, the market is the massive emergence of hair conditioner and hairdressing gel products and the great increase of sales volume, and the trend of washing and protecting separation is also being proved.
In the traditional hair conditioner and hairdressing gel type hair care products, cetostearyl alcohol is used as a substrate without exception, so that the products are in a milky cream shape, and the transparent gel hair conditioner partially using carbomer as the substrate has the problem that the carbomer generates a flocculation reaction with a cationic conditioner in the products to influence the stability of the products.
Disclosure of Invention
The invention aims to provide a transparent gel hair care composition which can provide excellent moisturizing and conditioning effects for hair, effectively improve the wet rinsing, wet combing and dry combing properties of the hair, reduce the electrostatic effect of the hair and enable the hair to be softer and smoother.
Another object of the present invention is to provide a method for preparing the above transparent gel hair care composition.
The invention provides a transparent gel hair care composition, which comprises the following components in percentage by weight:
0.1-50% of cationic surfactant which is quaternary ammonium salt R4N+X-A characteristic compound or a precursor capable of generating the structural characteristic through chemical reaction, wherein R is4Are respectively CH3-or C10-C25While at least one R is CH3-and at least one R is C10-C25Long chain of saturated alkanes; x represents anion with chemical valence of-1, including chloride ion, lactate ion, and citrate ion;
0.1-15% of humectant which is a raw material with hair moisturizing function and contains micromolecular polyalcohol or macromolecular polymer;
0.1-10% of hair conditioning agent;
0.1-30% of cosolvent;
0.05-1.0% of preservative;
0.5-2.0% of essence;
the balance of deionized water.
According to the transparent gel hair care composition, the weight of the cationic surfactant preferably accounts for 1.0-15% of the total weight of the composition, and the cationic surfactant comprises dicetyl dimethyl ammonium chloride, dipalmitoyloxyethyl dimethyl ammonium chloride, dioctadecyl dimethyl ammonium chloride, behenyl trimethyl ammonium chloride, tricetyl methyl ammonium chloride, stearamidopropyl dimethyl ammonium salt and precursors thereof, preferably dicetyl dimethyl ammonium chloride and precursors thereof.
The humectant preferably comprises from 2 to 10% by weight of the total composition; the humectant comprises glycerin, propylene glycol, pentaerythritol, sorbitol, sodium pyrrolidone carboxylate (PCA-Na), vitamin B5 (panthenol), water-soluble ceramide, lactic acid, and hyaluronic acid; lactic acid is preferred.
The weight of the cosolvent preferably accounts for 2-8% of the total weight of the composition; the cosolvent is alcohols, such as glycerol, propylene glycol, pentaerythritol, and sorbitol; among them, propylene glycol and glycerin are preferable, and propylene glycol is most preferable.
In addition, the invention also provides a preparation method of the transparent gel hair care composition, which comprises the following steps:
1) respectively weighing water, partial cationic surfactant, humectant, hair conditioner, cosolvent, preservative and essence according to the weight percentage;
2) dissolving other cationic surfactant in cosolvent;
3) adding water under stirring;
4) adding humectant, hair conditioner, antiseptic, and essence.
In the preparation method, in the step 1), the process of dissolving part of the cationic surfactant in the cosolvent needs heating, and the temperature is 50-85 ℃; in the step 2), the essence can be firstly dissolved in a small amount of cosolvent and added into the system to ensure the transparency of the system.
The transparent gel hair care composition and the preparation method thereof can achieve the following technical effects:
1) the hair conditioner comprises water, a cationic surfactant, a humectant, a hair conditioner, a cosolvent, a preservative and essence; wherein the cationic surfactant in the composition serves as a softening conditioner for hair and provides a matrix framework of the composition by utilizing the liquid crystal thickening effect of the cationic surfactant; the lactic acid is used as a humectant, and can reduce the pH of the system, so that the pH of the composition is closer to the skin of a human body, the composition is milder, and the irritation of the composition to the skin is avoided; the micromolecular polyalcohol can be used as a solvent of the cationic surfactant and can also provide a moisturizing effect; together with silicone grease, perfume, preservatives, etc. in the formulation, a clear gel hair care composition with superior rinsing and conditioning properties is formed.
2) After the composition is used for nursing the damaged hair caused by scalding and dyeing, the unhealthy states of the hair, such as roughness, dullness, dryness, coarseness and hardness, can be obviously improved, which shows that the composition has the effects of improving the damaged hair and enabling the hair to be smooth, moist and glossy.
Drawings
FIG. 1 is a polarized light microscope photograph of a clear gel hair care composition obtained in example 1 of the present invention.
FIG. 2 is a polarized light microscope photograph of a clear gel hair care composition obtained in example 2 of the present invention.
FIG. 3 is a polarized light microscope photograph of a clear gel hair care composition obtained in example 3 of the present invention.
Detailed Description
The transparent gel hair care composition comprises the following components in percentage by weight: 0.1-50% of cationic surfactant, 0.1-5% of humectant, 0.1-10% of hair conditioner, 0.1-30% of cosolvent, 0.05-1.0% of preservative, 0.5-2.0% of essence and the balance of deionized water.
The cationic surfactant is used as an essential component of the hair care composition, has the effect of conditioning hair, has positive charges, can neutralize and combine negative charges carried by the hair, reduces the static electricity of the hair, and is attached to the surface of the hair after being combined with the hair, so that the hair is softer and smoother, and the aim of effectively improving the hair roughness and the hair hardness is fulfilled.
Lactic acid is used as a humectant, so that on one hand, the lactic acid has excellent moisturizing performance, can effectively moisturize hair, and repair the problems of hair roughness and dryness, and meanwhile, the lactic acid is used as a pH regulator of a system, so that the pH of the system is weakly acidic and is closer to the pH of a scalp, and the product has less stimulation to the scalp and is milder.
The invention utilizes the property that the essential component of the hair care composition, namely the cationic surfactant, has a transparent paste body which spontaneously forms a liquid crystal structure with certain thickness in a specific concentration range, completely abandons the technical scheme that the conventional hair care compositions such as hair conditioner, hairdressing gel and the like take cetearyl alcohol as a matrix, and the cationic surfactant not only serves as the conditioner of the hair care composition, but also serves as the matrix material of the composition, thereby achieving the aim of killing two birds with one stone, reducing the product cost and improving the use efficiency of the cationic conditioner.
The transparent gel hair care composition and the method for preparing the same according to the present invention will be described in further detail with reference to the following specific preferred examples, but the present invention is not limited to the following examples. The following percentages are all by weight.
The component structures of the compositions are illustrated by the following examples 1-6, and various compositions are evaluated by the effect test examples.
Example 1
A transparent gel hair care composition comprises the following components in percentage by weight:
7% of dicetyl dimethyl ammonium chloride;
0.5 percent of lactic acid;
propylene glycol 10% (co-solvent);
1% of water-soluble dimethiconol;
0.5 percent of essence;
0.1 percent of preservative
The balance of deionized water.
The preparation method of the transparent gel hair care composition comprises the following steps:
1) respectively weighing water, dicetyl dimethyl ammonium chloride, lactic acid, water-soluble dimethiconol, propylene glycol, a preservative and essence according to the weight percentage;
2) dissolving dicetyl dimethyl ammonium chloride in propylene glycol;
3) adding water under stirring;
4) adding lactic acid, water-soluble dimethiconol, preservative and essence.
Example 2
A transparent gel hair care composition comprises the following components in percentage by weight:
behenyl trimethyl ammonium chloride 2.5%;
0.2 percent of sodium hyaluronate;
propylene glycol (cosolvent) 6%;
polyquaternium-71%;
0.7 percent of essence;
0.1% of preservative;
the balance of deionized water.
The above clear gel hair care composition was prepared in the same manner as in example 1.
Example 3
A transparent gel hair care composition comprises the following components in percentage by weight:
dipalmitoyloxyethyl dimethyl ammonium chloride 12%;
1.5% of sodium pyrrolidone carboxylate;
propylene glycol (cosolvent) 17%;
guar hydroxypropyl trimonium chloride 0.8%;
0.8% of essence;
0.1% of preservative;
the balance of deionized water.
The above clear gel hair care composition was prepared in the same manner as in example 1.
Example 4
A transparent gel hair care composition comprises the following components in percentage by weight:
tricetylmethyl ammonium chloride 25%;
sorbitol 4%;
17% of glycerol (cosolvent);
70.8 percent of polyquaternium;
0.8% of essence;
0.1% of preservative;
the balance of deionized water.
The above clear gel hair care composition was prepared in the same manner as in example 1.
Example 5
A transparent gel hair care composition comprises the following components in percentage by weight:
dipalmitoyloxyethyl dimethyl ammonium chloride 30%;
0.8 percent of lactic acid;
25% of glycerol (cosolvent);
guar hydroxypropyl trimonium chloride 0.8%;
0.8% of essence;
0.1% of preservative;
the balance of deionized water.
The above clear gel hair care composition was prepared in the same manner as in example 1.
Example 6
A transparent gel hair care composition comprises the following components in percentage by weight:
dipalmitoyloxyethyl dimethyl ammonium chloride 12%;
2% of glycerol;
10% of propylene glycol (cosolvent);
70.6 percent of polyquaternium;
0.8% of essence;
0.1% of preservative;
the balance of deionized water.
The above clear gel hair care composition was prepared in the same manner as in example 1.
Examples of Effect test
The compositions of examples 1-6 of the present invention are rinse-off hair care compositions, the use of which comprises the steps of:
1) washing hair with appropriate amount of shampoo, and towel wiping hair to semi-dry state;
2) taking 10-50g of the composition (determined according to the amount of hair), uniformly coating the composition on the hair, and keeping for 3-5 minutes;
3) washing the hair composition with water.
In addition, as shown in FIGS. 1 to 3, there are shown polarized light microscope pictures (polarized light microscope, 400 times magnification) of the transparent gel hair care compositions obtained in examples 1 to 3 of the present invention. It can be seen that: the composition forms a liquid crystal structure, so that an onion phase pattern is presented under a polarized light microscope, and the liquid crystal structure plays an important role in improving the stability of the composition.
Test example 1
The compositions of examples 1 to 6 were used to treat the hair of test persons who had been subjected to permanent waving and dyeing treatment, had dry, thick and stiff hair (application method: after washing out the hair, 30 to 50g of the composition was uniformly applied to the hair in accordance with the amount of the hair, and after 5 minutes was rinsed out with water), and evaluation was made in a sensory evaluation from three aspects of smoothness, moisture and softness of the hair after use. The evaluation results are shown in Table 1.
TABLE 1 organoleptic evaluation of the compositions of examples 1-6
Note: the full score is 10 points, and the higher the score is, the more satisfied the score is
The problems of hair roughness, dryness, hair thickness and hair hardness exist in the test persons subjected to the ironing and dyeing treatment, and the hair ironing and dyeing are a process of damaging the self structure of the hair by using chemical substances under a high-temperature condition to dye or re-shape the hair, and the process can cause serious damage to the hair, open scales of the hair, lose nutrient substances and reduce the water retention capacity, so that the hair roughness, dryness and hair thickness are finally caused.
As can be seen from Table 1, after the damaged hair is treated by the compositions of examples 1 to 6, the hair quality of the tested person is obviously improved, and the overall satisfaction is higher, because the compositions contain the cationic surfactant with hair conditioning effect, and during the use process, the cationic surfactant with positive charge is adsorbed on the surface of the hair with negative charge, and a layer of protective film is formed on the surface of the hair, so that on one hand, the frizzy feeling caused by excessive charge generated by mutual friction between hairs is reduced, and on the other hand, the cationic surfactant can smooth the hair scales on the surface of the hair opened by damage, so that the hair is soft and smooth, and the water retention performance is better; in conclusion, the composition has excellent care effect on hair damaged by scalding and dyeing.
The various embodiments provided by the invention can be combined in any way according to the needs, and the technical scheme obtained by the combination is also in the scope of the invention.
The above description is only a preferred embodiment of the present invention, and is not intended to limit the present invention in any way, so that any simple modification, equivalent change and modification made to the above embodiment according to the technical spirit of the present invention are within the scope of the technical solution of the present invention.
Claims (8)
1. A transparent gel hair care composition is characterized by comprising the following components in percentage by weight:
1-20% of cationic surfactant which is dipalmitoyloxyethyldimethyl ammonium chloride, stearamidopropyl dimethyl ammonium salt or has quaternary ammonium salt R4N+X-Any one of the compounds of feature R4Are respectively CH3-or C10-C25While at least one R is CH3-and at least one R is C10-C25Long chain of saturated alkanes; x represents anion with chemical valence of-1, including chloride ion, lactate ion, and citrate ion;
0.1-5% of humectant which is a raw material with hair moisturizing function and contains micromolecular polyalcohol or macromolecular polymer;
0.1-10% of hair conditioning agent; the hair conditioner is macromolecular natural or artificially modified and synthesized cationic polymer; or one or a mixture of two of water-soluble polydimethylsiloxane;
0.1-30% of cosolvent; the cosolvent is alcohol and has a general formula CnH2n+2-x(OH)x，n≥3，x≥2；
0.05-1.0% of preservative;
0.5-2.0% of essence;
the balance of deionized water.
2. A clear gel hair care composition according to claim 1, characterized in that: the cationic surfactant is one or more selected from dicetyl dimethyl ammonium chloride, dioctadecyl dimethyl ammonium chloride, behenyl trimethyl ammonium chloride and tricetyl methyl ammonium chloride.
3. A clear gel hair care composition according to claim 1, characterized in that: the cationic surfactant is selected from dicetyl dimethyl ammonium chloride.
4. A clear gel hair care composition according to claim 1, characterized in that: the weight of the humectant accounts for 0.1 to 3 percent of the total weight of the composition;
the humectant is one or more of glycerol, propylene glycol, pentaerythritol, sorbitol, sodium pyrrolidone carboxylate, vitamin B5, water soluble ceramide, lactic acid, and hyaluronic acid polyethylene glycol.
5. A clear gel hair care composition according to claim 1, characterized in that: the cosolvent is one or more of glycerol, propylene glycol, glycerol, pentaerythritol and sorbitol.
6. A clear gel hair care composition according to claim 1, characterized in that: the cationic polymer is selected from one or more of cationic cellulose, cationic guar gum, polyquaternium-7 and polyquaternium-52.
7. A clear gel hair care composition according to claim 1, characterized in that: the weight of the cosolvent accounts for 2-8% of the total weight of the composition.
8. A clear gel hair care composition according to claim 7, characterized in that: the cosolvent is one or more of propylene glycol, isopropanol, glycerol and pentaerythritol.
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Effective date of registration: 20221024 Address after: 515834 Liannan Industrial Zone, Chenghai District, Shantou City, Guangdong Province Patentee after: Guangdong Mingchen Daily Chemical Co.,Ltd. Address before: 515834 Liannan Industrial Zone, Lianxia Town, Chenghai District, Shantou City, Guangdong Province Patentee before: MINGCHEN HEALTH Co.,Ltd. |
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