CN108384646A - A kind of controller switching equipment charged insulating cleaning agent and preparation method thereof - Google Patents
A kind of controller switching equipment charged insulating cleaning agent and preparation method thereof Download PDFInfo
- Publication number
- CN108384646A CN108384646A CN201810226969.9A CN201810226969A CN108384646A CN 108384646 A CN108384646 A CN 108384646A CN 201810226969 A CN201810226969 A CN 201810226969A CN 108384646 A CN108384646 A CN 108384646A
- Authority
- CN
- China
- Prior art keywords
- parts
- cleaning agent
- switching equipment
- controller switching
- charged insulating
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- 239000012459 cleaning agent Substances 0.000 title claims abstract description 36
- 238000002360 preparation method Methods 0.000 title claims abstract description 15
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 41
- 239000003995 emulsifying agent Substances 0.000 claims abstract description 41
- 230000000740 bleeding effect Effects 0.000 claims abstract description 39
- -1 polysiloxane Polymers 0.000 claims abstract description 35
- 239000003381 stabilizer Substances 0.000 claims abstract description 33
- GEWDNTWNSAZUDX-WQMVXFAESA-N (-)-methyl jasmonate Chemical compound CC\C=C/C[C@@H]1[C@@H](CC(=O)OC)CCC1=O GEWDNTWNSAZUDX-WQMVXFAESA-N 0.000 claims abstract description 26
- CYTYCFOTNPOANT-UHFFFAOYSA-N Perchloroethylene Chemical group ClC(Cl)=C(Cl)Cl CYTYCFOTNPOANT-UHFFFAOYSA-N 0.000 claims abstract description 26
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims abstract description 26
- GEWDNTWNSAZUDX-UHFFFAOYSA-N methyl 7-epi-jasmonate Natural products CCC=CCC1C(CC(=O)OC)CCC1=O GEWDNTWNSAZUDX-UHFFFAOYSA-N 0.000 claims abstract description 26
- 239000002904 solvent Substances 0.000 claims abstract description 26
- 229950011008 tetrachloroethylene Drugs 0.000 claims abstract description 26
- 229920001296 polysiloxane Polymers 0.000 claims abstract description 24
- LQZZUXJYWNFBMV-UHFFFAOYSA-N dodecan-1-ol Chemical class CCCCCCCCCCCCO LQZZUXJYWNFBMV-UHFFFAOYSA-N 0.000 claims abstract description 16
- QIGBRXMKCJKVMJ-UHFFFAOYSA-N Hydroquinone Chemical compound OC1=CC=C(O)C=C1 QIGBRXMKCJKVMJ-UHFFFAOYSA-N 0.000 claims abstract description 12
- 239000002994 raw material Substances 0.000 claims abstract description 10
- 150000002148 esters Chemical class 0.000 claims abstract description 7
- 235000014113 dietary fatty acids Nutrition 0.000 claims description 19
- 239000000194 fatty acid Substances 0.000 claims description 19
- 229930195729 fatty acid Natural products 0.000 claims description 19
- 150000004665 fatty acids Chemical class 0.000 claims description 19
- IMNFDUFMRHMDMM-UHFFFAOYSA-N N-Heptane Chemical group CCCCCCC IMNFDUFMRHMDMM-UHFFFAOYSA-N 0.000 claims description 7
- 150000001335 aliphatic alkanes Chemical class 0.000 claims description 7
- SNRUBQQJIBEYMU-UHFFFAOYSA-N dodecane Chemical compound CCCCCCCCCCCC SNRUBQQJIBEYMU-UHFFFAOYSA-N 0.000 claims description 7
- DIOQZVSQGTUSAI-UHFFFAOYSA-N n-butylhexane Natural products CCCCCCCCCC DIOQZVSQGTUSAI-UHFFFAOYSA-N 0.000 claims description 7
- 238000003756 stirring Methods 0.000 claims description 7
- 125000004836 hexamethylene group Chemical group [H]C([H])([*:2])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[*:1] 0.000 claims description 4
- 239000000203 mixture Substances 0.000 claims description 3
- DIOQZVSQGTUSAI-NJFSPNSNSA-N decane Chemical compound CCCCCCCCC[14CH3] DIOQZVSQGTUSAI-NJFSPNSNSA-N 0.000 claims 1
- 238000009738 saturating Methods 0.000 claims 1
- 230000007797 corrosion Effects 0.000 abstract description 5
- 238000005260 corrosion Methods 0.000 abstract description 5
- 239000000428 dust Substances 0.000 abstract description 4
- 230000007812 deficiency Effects 0.000 abstract description 3
- 239000003344 environmental pollutant Substances 0.000 abstract description 3
- 231100000719 pollutant Toxicity 0.000 abstract description 3
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 10
- QYKIQEUNHZKYBP-UHFFFAOYSA-N Vinyl ether Chemical compound C=COC=C QYKIQEUNHZKYBP-UHFFFAOYSA-N 0.000 description 9
- BZHJMEDXRYGGRV-UHFFFAOYSA-N Vinyl chloride Chemical compound ClC=C BZHJMEDXRYGGRV-UHFFFAOYSA-N 0.000 description 6
- 239000012212 insulator Substances 0.000 description 4
- AZQWKYJCGOJGHM-UHFFFAOYSA-N 1,4-benzoquinone Chemical compound O=C1C=CC(=O)C=C1 AZQWKYJCGOJGHM-UHFFFAOYSA-N 0.000 description 2
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 238000009413 insulation Methods 0.000 description 2
- 239000004033 plastic Substances 0.000 description 2
- 229920003023 plastic Polymers 0.000 description 2
- 229920002379 silicone rubber Polymers 0.000 description 2
- 125000001340 2-chloroethyl group Chemical class [H]C([H])(Cl)C([H])([H])* 0.000 description 1
- IAYPIBMASNFSPL-UHFFFAOYSA-N Ethylene oxide Chemical compound C1CO1 IAYPIBMASNFSPL-UHFFFAOYSA-N 0.000 description 1
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000005540 biological transmission Effects 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- SNRUBQQJIBEYMU-NJFSPNSNSA-N dodecane Chemical group CCCCCCCCCCC[14CH3] SNRUBQQJIBEYMU-NJFSPNSNSA-N 0.000 description 1
- 238000010891 electric arc Methods 0.000 description 1
- 230000005684 electric field Effects 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 238000003912 environmental pollution Methods 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 230000003694 hair properties Effects 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
- 229910052739 hydrogen Inorganic materials 0.000 description 1
- 230000007774 longterm Effects 0.000 description 1
- 239000006210 lotion Substances 0.000 description 1
- 239000003595 mist Substances 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 239000005413 snowmelt Substances 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
- 230000009466 transformation Effects 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
- C11D1/825—Mixtures of compounds all of which are non-ionic
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/02—Inorganic compounds ; Elemental compounds
- C11D3/12—Water-insoluble compounds
- C11D3/124—Silicon containing, e.g. silica, silex, quartz or glass beads
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/18—Hydrocarbons
- C11D3/181—Hydrocarbons linear
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/18—Hydrocarbons
- C11D3/185—Hydrocarbons cyclic
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/20—Organic compounds containing oxygen
- C11D3/2093—Esters; Carbonates
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/24—Organic compounds containing halogen
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/24—Organic compounds containing halogen
- C11D3/245—Organic compounds containing halogen containing fluorine
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/37—Polymers
- C11D3/3703—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- C11D3/3707—Polyethers, e.g. polyalkyleneoxides
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/37—Polymers
- C11D3/3703—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- C11D3/373—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds containing silicones
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/43—Solvents
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/008—Polymeric surface-active agents
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
- C11D1/667—Neutral esters, e.g. sorbitan esters
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
- C11D1/72—Ethers of polyoxyalkylene glycols
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Emergency Medicine (AREA)
- Inorganic Chemistry (AREA)
- Detergent Compositions (AREA)
Abstract
The invention discloses a kind of controller switching equipment charged insulating cleaning agents and preparation method thereof, include the raw material of following parts by weight：22 30 parts of tetrachloro-ethylene, 30 45 parts, No. 120 26 35 parts of solvent naphthas of trifluorobichloroethane, 6 15 parts of Ludox, 28 parts of methyl jasmonate, 28 parts of hydroquinone mono fattya nd ester, 37 parts of ethoxylated dodecyl alcohol, 25 parts of polysiloxane, 0.1 0.8 parts of bleeding agent, 0.1 1 parts of emulsifier, 0.1 0.5 parts of stabilizer.The controller switching equipment charged insulating cleaning agent of the present invention can rapidly and thoroughly clear the pollution off, and greasy dirt, dust cleannes are up to 96 99%, flashover caused by can effectively preventing when pollutant is by humidity；The present invention can clean the charging equipment of 300KV or more, to being cleaned the component of equipment without any corrosion and volatilizing comparatively fast, overcome at present the deficiency of charged insulating cleaning agent on the market.
Description
Technical field
The present invention relates to a kind of cleaning agent, specifically a kind of controller switching equipment charged insulating cleaning agent and preparation method thereof.
Background technology
The insulator of long-term running power equipment, especially on-line operation, by industrial emissions in atmospheric environment,
The influence of the environmental factors such as moisture, oxidation, corrosive gas and natural airborne dust in air, surface gradually deposited one layer of synthesis
Dunghill.In the case of dry weather, insulator of these surfaces with dunghill remains to remain higher dielectric level.
However, when encounter mist, dew, drizzle, frost and ice-melt, when the wet weathers such as snow melt, insulator surface can be due in pollution layer
Dissolved salt, acid-base class is soluble in water and forms conductive moisture film, thus leakage current can be made to be flowed through along the surface of insulator.Due to exhausted
The shape of edge, the factors such as structure size influence, and the current density at each position in surface is different, the meeting position bigger in electric current
It is initially formed dry zone, dry zone carries higher voltage, and when electric field strength is sufficiently large, electric current will be on the edge across dry section
Face is discharged, and local arc is generated.When dirty and dampness is more serious, local arc meets or exceeds critical condition, electric arc
The two poles of the earth will be run through, flashover, i.e. pollution flashover occurs.
With the fast development of national economy, net capacity and specified defeated voltage class increase substantially, simultaneous
The development of industrial or agricultural, the environmental pollution has become increasingly serious of some areas, the pollution flashover thing of electric system power transmission and transformation equipment outer insulation
Therefore caused harm and economic loss also getting worse.The insulation cleaning agent pressure resistance used on the market at present is relatively low, generally most
Height can only clean 220KV charging equipments.And this cleaning agent has certain corruption to certain plastics components, silicon rubber component
Corrosion.In addition this cleaning agent volatilization is slower on the market, and cleaning agent is sprayed in cleaned equipment or on component if waved
Hair property is not strong, certainly will have some corrosion to the component especially plastics and silicon rubber component for being cleaned equipment.
Invention content
It is above-mentioned to solve the purpose of the present invention is to provide a kind of controller switching equipment charged insulating cleaning agent and preparation method thereof
The problem of being proposed in background technology.
To achieve the above object, the present invention provides the following technical solutions：
A kind of controller switching equipment charged insulating cleaning agent, includes the raw material of following parts by weight：22-30 parts of tetrachloro-ethylene, trifluoro two
30-45 parts, No. 120 26-35 parts of solvent naphthas of chloroethanes, 6-15 parts of Ludox, 2-8 parts of methyl jasmonate, quinhydrones mono fatty acid
2-8 parts of ester, 3-7 parts of ethoxylated dodecyl alcohol, 2-5 parts of polysiloxane, 0.1-0.8 parts of bleeding agent, emulsifier 0.1-1
Part, 0.1-0.5 parts of stabilizer.
As a further solution of the present invention：Include the raw material of following parts by weight：27 parts of tetrachloro-ethylene, two chloroethene of trifluoro
38 parts, No. 120 30 parts of solvent naphthas of alkane, 11 parts of Ludox, 6 parts of methyl jasmonate, 5 parts of quinhydrones mono fatty acid, laruyl alcohol polyoxy
6 parts of vinethene, 4 parts of polysiloxane, 0.5 part of bleeding agent, 0.9 part of emulsifier, 0.3 part of stabilizer.
As a further solution of the present invention：The stabilizer is one kind in heptane, hexamethylene, dodecane or decane
Or the mixture of a variety of arbitrary proportions.
As a further solution of the present invention：The bleeding agent uses DX bleeding agents.
As a further solution of the present invention：The emulsifier uses O10 emulsifiers or O15 emulsifiers.
A kind of preparation method of controller switching equipment charged insulating cleaning agent, includes the following steps：
（1）According to parts by weight weigh tetrachloro-ethylene, trifluorobichloroethane, No. 120 solvent naphthas, Ludox, methyl jasmonate,
Quinhydrones mono fatty acid, ethoxylated dodecyl alcohol, polysiloxane, bleeding agent, emulsifier and stabilizer, it is spare；
（2）First by tetrachloro-ethylene, trifluorobichloroethane, No. 120 solvent naphthas, Ludox, ethoxylated dodecyl alcohol and poly- organic
Siloxanes is added in stirred tank, is stirred dark conjunction 10-23min, is then reacted 1-2h at 5-8 DEG C；
（3）Methyl jasmonate and quinhydrones mono fatty acid are added into stirred tank, is then stirred to react 35- at 9-13 DEG C
50min；
（4）Bleeding agent, emulsifier and stabilizer are added into stirred tank, be then stirred to react at 15-20 DEG C 1-2h to get at
Product.
As a further solution of the present invention：Step（2）First by tetrachloro-ethylene, trifluorobichloroethane, No. 120 solvent naphthas,
Ludox, ethoxylated dodecyl alcohol and polysiloxane are added in stirred tank, stir it is dark close 16min, then at 7 DEG C
React 1.3h.
As a further solution of the present invention：Step（3）Methyl jasmonate and quinhydrones monoester fat are added into stirred tank
Then acid is stirred to react 42min at 11 DEG C.
As a further solution of the present invention：Step（4）Bleeding agent, emulsifier and stabilizer are added into stirred tank, so
1.5h is stirred to react at 18 DEG C afterwards to get finished product.
Compared with prior art, the beneficial effects of the invention are as follows：
The controller switching equipment charged insulating cleaning agent of the present invention can rapidly and thoroughly clear the pollution off, and greasy dirt, dust cleannes are high
Up to 96-99%, flashover caused by can effectively preventing when pollutant is by humidity；The present invention can clean the electrification of 300KV or more
Equipment overcomes at present charged insulating cleaning agent on the market to being cleaned the component of equipment without any corrosion and volatilizing comparatively fast
Deficiency.
Specific implementation mode
The technical solution of this patent is described in more detail With reference to embodiment.
Embodiment 1
A kind of controller switching equipment charged insulating cleaning agent, includes the raw material of following parts by weight：22 parts of tetrachloro-ethylene, two chloroethene of trifluoro
30 parts, No. 120 26 parts of solvent naphthas of alkane, 6 parts of Ludox, 2 parts of methyl jasmonate, 2 parts of hydroquinone mono fattya nd ester, laruyl alcohol polyoxy
3 parts of vinethene, 2 parts of polysiloxane, 0.1 part of bleeding agent, 0.1 part of emulsifier, 0.1 part of stabilizer.The stabilizer is
Heptane.The bleeding agent uses DX bleeding agents.The emulsifier uses O10 emulsifiers.
A kind of preparation method of controller switching equipment charged insulating cleaning agent, includes the following steps：（1）It is weighed according to parts by weight
Tetrachloro-ethylene, trifluorobichloroethane, No. 120 solvent naphthas, Ludox, methyl jasmonate, quinhydrones mono fatty acid, laruyl alcohol polyoxy
Vinethene, polysiloxane, bleeding agent, emulsifier and stabilizer, it is spare；（2）First by tetrachloro-ethylene, trifluorobichloroethane,
No. 120 solvent naphthas, Ludox, ethoxylated dodecyl alcohol and polysiloxane are added in stirred tank, stir dark close
Then 10min reacts 1h at 5 DEG C；（3）Methyl jasmonate and quinhydrones mono fatty acid are added into stirred tank, then in 9 DEG C
Under be stirred to react 35min；（4）Bleeding agent, emulsifier and stabilizer are added into stirred tank, is then stirred to react at 15 DEG C
1h is to get finished product.
Embodiment 2
A kind of controller switching equipment charged insulating cleaning agent, includes the raw material of following parts by weight：22 parts of tetrachloro-ethylene, two chloroethene of trifluoro
30 parts, No. 120 26 parts of solvent naphthas of alkane, 6 parts of Ludox, 2 parts of methyl jasmonate, 2 parts of hydroquinone mono fattya nd ester, laruyl alcohol polyoxy
3 parts of vinethene, 2 parts of polysiloxane, 0.1 part of bleeding agent, 0.1 part of emulsifier, 0.1 part of stabilizer.The stabilizer is
Hexamethylene.The bleeding agent uses DX bleeding agents.The emulsifier uses O15 emulsifiers.
A kind of preparation method of controller switching equipment charged insulating cleaning agent, includes the following steps：（1）It is weighed according to parts by weight
Tetrachloro-ethylene, trifluorobichloroethane, No. 120 solvent naphthas, Ludox, methyl jasmonate, quinhydrones mono fatty acid, laruyl alcohol polyoxy
Vinethene, polysiloxane, bleeding agent, emulsifier and stabilizer, it is spare；（2）First by tetrachloro-ethylene, trifluorobichloroethane,
No. 120 solvent naphthas, Ludox, ethoxylated dodecyl alcohol and polysiloxane are added in stirred tank, stir dark close
Then 23min reacts 2h at 8 DEG C；（3）Methyl jasmonate and quinhydrones mono fatty acid are added into stirred tank, then in 13
50min is stirred to react at DEG C；（4）Bleeding agent, emulsifier and stabilizer are added into stirred tank, is then stirred to react at 20 DEG C
2h is to get finished product.
Embodiment 3
A kind of controller switching equipment charged insulating cleaning agent, includes the raw material of following parts by weight：27 parts of tetrachloro-ethylene, two chloroethene of trifluoro
38 parts, No. 120 30 parts of solvent naphthas of alkane, 11 parts of Ludox, 6 parts of methyl jasmonate, 5 parts of quinhydrones mono fatty acid, laruyl alcohol polyoxy
6 parts of vinethene, 4 parts of polysiloxane, 0.5 part of bleeding agent, 0.9 part of emulsifier, 0.3 part of stabilizer.The stabilizer is
Dodecane.The bleeding agent uses DX bleeding agents.The emulsifier uses O10 emulsifiers.
A kind of preparation method of controller switching equipment charged insulating cleaning agent, includes the following steps：
（1）According to parts by weight weigh tetrachloro-ethylene, trifluorobichloroethane, No. 120 solvent naphthas, Ludox, methyl jasmonate,
Quinhydrones mono fatty acid, ethoxylated dodecyl alcohol, polysiloxane, bleeding agent, emulsifier and stabilizer, it is spare；（2）First will
Tetrachloro-ethylene, trifluorobichloroethane, No. 120 solvent naphthas, Ludox, ethoxylated dodecyl alcohol and polysiloxane are added to
In stirred tank, stir it is dark close 16min, then react 1.3h at 7 DEG C；（3）Methyl jasmonate and hydrogen are added into stirred tank
Then quinone mono fatty acid is stirred to react 42min at 11 DEG C；（4）Bleeding agent, emulsifier and stabilizer are added into stirred tank,
Then 1.5h is stirred to react at 18 DEG C to get finished product.
Embodiment 4
A kind of controller switching equipment charged insulating cleaning agent, includes the raw material of following parts by weight：23 parts of tetrachloro-ethylene, two chloroethene of trifluoro
44 parts, No. 120 28 parts of solvent naphthas of alkane, 12 parts of Ludox, 3 parts of methyl jasmonate, 3 parts of hydroquinone mono fattya nd ester, laruyl alcohol are poly-
6 parts of ethylene oxide ether, 3 parts of polysiloxane, 0.7 part of bleeding agent, 0.2 part of emulsifier, 0.4 part of stabilizer.The stabilizer
For decane.The bleeding agent uses DX bleeding agents.The emulsifier uses O10 emulsifiers.
A kind of preparation method of controller switching equipment charged insulating cleaning agent, includes the following steps：（1）It is weighed according to parts by weight
Tetrachloro-ethylene, trifluorobichloroethane, No. 120 solvent naphthas, Ludox, methyl jasmonate, quinhydrones mono fatty acid, laruyl alcohol polyoxy
Vinethene, polysiloxane, bleeding agent, emulsifier and stabilizer, it is spare；（2）First by tetrachloro-ethylene, trifluorobichloroethane,
No. 120 solvent naphthas, Ludox, ethoxylated dodecyl alcohol and polysiloxane are added in stirred tank, stir dark close
Then 11min reacts 1.1h at 7 DEG C；（3）Methyl jasmonate and quinhydrones mono fatty acid are added into stirred tank, then in
It is stirred to react 38min at 12 DEG C；（4）Bleeding agent, emulsifier and stabilizer are added into stirred tank, is then stirred at 18 DEG C anti-
Answer 1.2h to get finished product.
Embodiment 5
A kind of controller switching equipment charged insulating cleaning agent, includes the raw material of following parts by weight：28 parts of tetrachloro-ethylene, two chloroethene of trifluoro
32 parts, No. 120 32 parts of solvent naphthas of alkane, 7 parts of Ludox, 7 parts of methyl jasmonate, 7 parts of hydroquinone mono fattya nd ester, laruyl alcohol polyoxy
4 parts of vinethene, 4 parts of polysiloxane, 0.2 part of bleeding agent, 0.8 part of emulsifier, 0.2 part of stabilizer.The stabilizer is
The mixture of heptane, hexamethylene, dodecane or decane.The bleeding agent uses DX bleeding agents.The emulsifier is emulsified using O15
Agent.
A kind of preparation method of controller switching equipment charged insulating cleaning agent, includes the following steps：（1）It is weighed according to parts by weight
Tetrachloro-ethylene, trifluorobichloroethane, No. 120 solvent naphthas, Ludox, methyl jasmonate, quinhydrones mono fatty acid, laruyl alcohol polyoxy
Vinethene, polysiloxane, bleeding agent, emulsifier and stabilizer, it is spare；（2）First by tetrachloro-ethylene, trifluorobichloroethane,
No. 120 solvent naphthas, Ludox, ethoxylated dodecyl alcohol and polysiloxane are added in stirred tank, stir dark close
Then 22min reacts 1.8h at 6 DEG C；（3）Methyl jasmonate and quinhydrones mono fatty acid are added into stirred tank, then in
It is stirred to react 45min at 10 DEG C；（4）Bleeding agent, emulsifier and stabilizer are added into stirred tank, is then stirred at 16 DEG C anti-
Answer 1.9h to get finished product.
The controller switching equipment charged insulating cleaning agent of the present invention can rapidly and thoroughly clear the pollution off, greasy dirt, dust cleaning
Degree is up to 96-99%, flashover caused by can effectively preventing when pollutant is by humidity；The present invention can clean 300KV's or more
It is clear to overcome at present charged insulating on the market to being cleaned the component of equipment without any corrosion and volatilizing comparatively fast for charging equipment
The deficiency of lotion.
The better embodiment of this patent is explained in detail above, but this patent is not limited to above-mentioned embodiment party
Formula, one skilled in the relevant art within the scope of knowledge, can also be under the premise of not departing from this patent objective
It makes a variety of changes.
Claims (9)
1. a kind of controller switching equipment charged insulating cleaning agent, which is characterized in that include the raw material of following parts by weight：Tetrachloro-ethylene
22-30 parts, 30-45 parts, No. 120 26-35 parts of solvent naphthas of trifluorobichloroethane, 6-15 parts of Ludox, methyl jasmonate 2-8
Part, 2-8 parts of hydroquinone mono fattya nd ester, 3-7 parts of ethoxylated dodecyl alcohol, 2-5 parts of polysiloxane, bleeding agent 0.1-0.8
Part, 0.1-1 parts of emulsifier, 0.1-0.5 parts of stabilizer.
2. controller switching equipment charged insulating cleaning agent according to claim 1, which is characterized in that including following parts by weight
Raw material：27 parts of tetrachloro-ethylene, 38 parts, No. 120 30 parts of solvent naphthas of trifluorobichloroethane, 11 parts of Ludox, methyl jasmonate 6
Part, 5 parts of quinhydrones mono fatty acid, 6 parts of ethoxylated dodecyl alcohol, 4 parts of polysiloxane, 0.5 part of bleeding agent, emulsifier 0.9
Part, 0.3 part of stabilizer.
3. controller switching equipment charged insulating cleaning agent according to claim 1, which is characterized in that the stabilizer is heptan
The mixture of one or more arbitrary proportions in alkane, hexamethylene, dodecane or decane.
4. controller switching equipment charged insulating cleaning agent according to claim 1, which is characterized in that the bleeding agent is oozed using DX
Saturating agent.
5. controller switching equipment charged insulating cleaning agent according to claim 1, which is characterized in that the emulsifier uses O10
Emulsifier or O15 emulsifiers.
6. a kind of preparation method of controller switching equipment charged insulating cleaning agent according to any one of claims 1 to 5, which is characterized in that
Include the following steps：
（1）According to parts by weight weigh tetrachloro-ethylene, trifluorobichloroethane, No. 120 solvent naphthas, Ludox, methyl jasmonate,
Quinhydrones mono fatty acid, ethoxylated dodecyl alcohol, polysiloxane, bleeding agent, emulsifier and stabilizer, it is spare；
（2）First by tetrachloro-ethylene, trifluorobichloroethane, No. 120 solvent naphthas, Ludox, ethoxylated dodecyl alcohol and poly- organic
Siloxanes is added in stirred tank, is stirred dark conjunction 10-23min, is then reacted 1-2h at 5-8 DEG C；
（3）Methyl jasmonate and quinhydrones mono fatty acid are added into stirred tank, is then stirred to react 35- at 9-13 DEG C
50min；
（4）Bleeding agent, emulsifier and stabilizer are added into stirred tank, be then stirred to react at 15-20 DEG C 1-2h to get at
Product.
7. the preparation method of controller switching equipment charged insulating cleaning agent according to claim 6, which is characterized in that step（2）
First tetrachloro-ethylene, trifluorobichloroethane, No. 120 solvent naphthas, Ludox, ethoxylated dodecyl alcohol and polysiloxane are added
Enter into stirred tank, stir it is dark close 16min, then react 1.3h at 7 DEG C.
8. the preparation method of controller switching equipment charged insulating cleaning agent according to claim 6, which is characterized in that step（3）
Methyl jasmonate and quinhydrones mono fatty acid are added into stirred tank, is then stirred to react 42min at 11 DEG C.
9. the preparation method of controller switching equipment charged insulating cleaning agent according to claim 6, which is characterized in that step（4）
Bleeding agent, emulsifier and stabilizer are added into stirred tank, 1.5h is then stirred to react at 18 DEG C to get finished product.
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| CN201810226969.9A CN108384646A (en) | 2018-03-20 | 2018-03-20 | A kind of controller switching equipment charged insulating cleaning agent and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201810226969.9A CN108384646A (en) | 2018-03-20 | 2018-03-20 | A kind of controller switching equipment charged insulating cleaning agent and preparation method thereof |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111849650A (en) * | 2020-08-17 | 2020-10-30 | 福建省腾达洁环保工程有限公司 | Network communication electrified maintenance cleaning agent and preparation method thereof |
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|---|---|---|---|---|
| CN104073376A (en) * | 2013-03-31 | 2014-10-01 | 滕州市智星电力电子工程有限公司 | Ultrahigh-voltage charged insulator cleaning agent and preparation method thereof |
| CN105273869A (en) * | 2014-07-24 | 2016-01-27 | 滕州市智星电力电子工程有限公司 | Electrical equipment charged insulation cleaning agent and preparation method thereof |
| CN106190618A (en) * | 2016-07-07 | 2016-12-07 | 无锡市华东电力设备有限公司 | A kind of charged insulating abluent of high pressure equipment |
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2018
- 2018-03-20 CN CN201810226969.9A patent/CN108384646A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104073376A (en) * | 2013-03-31 | 2014-10-01 | 滕州市智星电力电子工程有限公司 | Ultrahigh-voltage charged insulator cleaning agent and preparation method thereof |
| CN105273869A (en) * | 2014-07-24 | 2016-01-27 | 滕州市智星电力电子工程有限公司 | Electrical equipment charged insulation cleaning agent and preparation method thereof |
| CN106190618A (en) * | 2016-07-07 | 2016-12-07 | 无锡市华东电力设备有限公司 | A kind of charged insulating abluent of high pressure equipment |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN111849650A (en) * | 2020-08-17 | 2020-10-30 | 福建省腾达洁环保工程有限公司 | Network communication electrified maintenance cleaning agent and preparation method thereof |
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