CN108384390A - Anti-slip heat-preservation sound-insulation environment-friendly floor coating and preparation method thereof - Google Patents
Anti-slip heat-preservation sound-insulation environment-friendly floor coating and preparation method thereof Download PDFInfo
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- CN108384390A CN108384390A CN201810239461.2A CN201810239461A CN108384390A CN 108384390 A CN108384390 A CN 108384390A CN 201810239461 A CN201810239461 A CN 201810239461A CN 108384390 A CN108384390 A CN 108384390A
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- 238000009413 insulation Methods 0.000 title claims abstract description 107
- 238000000576 coating method Methods 0.000 title claims abstract description 66
- 239000011248 coating agent Substances 0.000 title claims abstract description 63
- 238000002360 preparation method Methods 0.000 title claims abstract description 18
- 238000004321 preservation Methods 0.000 title abstract description 6
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 62
- 229920005989 resin Polymers 0.000 claims abstract description 50
- 239000011347 resin Substances 0.000 claims abstract description 50
- 239000000654 additive Substances 0.000 claims abstract description 43
- 230000000996 additive effect Effects 0.000 claims abstract description 43
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 claims abstract description 30
- 239000002270 dispersing agent Substances 0.000 claims abstract description 23
- 239000002994 raw material Substances 0.000 claims abstract description 23
- 239000002518 antifoaming agent Substances 0.000 claims abstract description 20
- 239000002253 acid Substances 0.000 claims abstract description 19
- 150000002148 esters Chemical class 0.000 claims abstract description 15
- LLHKCFNBLRBOGN-UHFFFAOYSA-N propylene glycol methyl ether acetate Chemical compound COCC(C)OC(C)=O LLHKCFNBLRBOGN-UHFFFAOYSA-N 0.000 claims abstract description 15
- 239000004408 titanium dioxide Substances 0.000 claims abstract description 15
- 150000001875 compounds Chemical class 0.000 claims abstract description 10
- 238000000034 method Methods 0.000 claims abstract description 10
- 239000000945 filler Substances 0.000 claims abstract description 6
- 239000000203 mixture Substances 0.000 claims description 90
- 230000007613 environmental effect Effects 0.000 claims description 39
- 238000003756 stirring Methods 0.000 claims description 31
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 claims description 27
- 238000011049 filling Methods 0.000 claims description 20
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 19
- 238000013329 compounding Methods 0.000 claims description 16
- 230000001965 increasing effect Effects 0.000 claims description 14
- 238000002156 mixing Methods 0.000 claims description 14
- 239000011324 bead Substances 0.000 claims description 12
- NIXOWILDQLNWCW-UHFFFAOYSA-N acrylic acid group Chemical group C(C=C)(=O)O NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 claims description 11
- 239000004925 Acrylic resin Substances 0.000 claims description 10
- 229920000178 Acrylic resin Polymers 0.000 claims description 10
- 238000006243 chemical reaction Methods 0.000 claims description 10
- 229920000180 alkyd Polymers 0.000 claims description 9
- 244000045947 parasite Species 0.000 claims description 9
- 238000004519 manufacturing process Methods 0.000 claims description 8
- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 claims description 7
- 241000276489 Merlangius merlangus Species 0.000 claims description 7
- 239000006004 Quartz sand Substances 0.000 claims description 7
- 239000000919 ceramic Substances 0.000 claims description 7
- 238000001816 cooling Methods 0.000 claims description 7
- 239000007822 coupling agent Substances 0.000 claims description 7
- 235000014113 dietary fatty acids Nutrition 0.000 claims description 7
- 239000000194 fatty acid Substances 0.000 claims description 7
- 229930195729 fatty acid Natural products 0.000 claims description 7
- 150000004665 fatty acids Chemical class 0.000 claims description 7
- 239000011521 glass Substances 0.000 claims description 7
- 239000003595 mist Substances 0.000 claims description 7
- 235000009024 Ceanothus sanguineus Nutrition 0.000 claims description 6
- 235000007516 Chrysanthemum Nutrition 0.000 claims description 6
- 244000062748 Eupatorium adenophorum Species 0.000 claims description 6
- 240000003553 Leptospermum scoparium Species 0.000 claims description 6
- 235000015459 Lycium barbarum Nutrition 0.000 claims description 6
- 229960000892 attapulgite Drugs 0.000 claims description 6
- FPAFDBFIGPHWGO-UHFFFAOYSA-N dioxosilane;oxomagnesium;hydrate Chemical compound O.[Mg]=O.[Mg]=O.[Mg]=O.O=[Si]=O.O=[Si]=O.O=[Si]=O.O=[Si]=O FPAFDBFIGPHWGO-UHFFFAOYSA-N 0.000 claims description 6
- 238000007667 floating Methods 0.000 claims description 6
- 235000013312 flour Nutrition 0.000 claims description 6
- 239000003365 glass fiber Substances 0.000 claims description 6
- 125000002887 hydroxy group Chemical group [H]O* 0.000 claims description 6
- 229910052625 palygorskite Inorganic materials 0.000 claims description 6
- 239000000377 silicon dioxide Substances 0.000 claims description 6
- 239000002904 solvent Substances 0.000 claims description 6
- 229920002126 Acrylic acid copolymer Polymers 0.000 claims description 5
- 241001116389 Aloe Species 0.000 claims description 5
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 5
- 229920000142 Sodium polycarboxylate Polymers 0.000 claims description 5
- QYKIQEUNHZKYBP-UHFFFAOYSA-N Vinyl ether Chemical compound C=COC=C QYKIQEUNHZKYBP-UHFFFAOYSA-N 0.000 claims description 5
- 150000003973 alkyl amines Chemical class 0.000 claims description 5
- 235000011399 aloe vera Nutrition 0.000 claims description 5
- LNENVNGQOUBOIX-UHFFFAOYSA-N azidosilane Chemical class [SiH3]N=[N+]=[N-] LNENVNGQOUBOIX-UHFFFAOYSA-N 0.000 claims description 5
- 239000003054 catalyst Substances 0.000 claims description 5
- 239000003822 epoxy resin Substances 0.000 claims description 5
- 238000001914 filtration Methods 0.000 claims description 5
- 229910021389 graphene Inorganic materials 0.000 claims description 5
- -1 methyl siloxane Chemical class 0.000 claims description 5
- 229920001558 organosilicon polymer Polymers 0.000 claims description 5
- 229920000647 polyepoxide Polymers 0.000 claims description 5
- 150000003839 salts Chemical group 0.000 claims description 5
- 238000005292 vacuum distillation Methods 0.000 claims description 5
- 238000010792 warming Methods 0.000 claims description 5
- 238000001291 vacuum drying Methods 0.000 claims description 4
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 3
- 239000000843 powder Substances 0.000 claims description 2
- 230000004048 modification Effects 0.000 claims 2
- 238000012986 modification Methods 0.000 claims 2
- 244000189548 Chrysanthemum x morifolium Species 0.000 claims 1
- 230000002708 enhancing effect Effects 0.000 claims 1
- 229920000058 polyacrylate Polymers 0.000 claims 1
- 230000007797 corrosion Effects 0.000 abstract description 5
- 238000005260 corrosion Methods 0.000 abstract description 5
- 231100000252 nontoxic Toxicity 0.000 abstract description 4
- 230000003000 nontoxic effect Effects 0.000 abstract description 4
- 238000009776 industrial production Methods 0.000 abstract 1
- 241000723353 Chrysanthemum Species 0.000 description 5
- 230000000694 effects Effects 0.000 description 5
- 239000012467 final product Substances 0.000 description 4
- 239000000463 material Substances 0.000 description 4
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- 229940070721 polyacrylate Drugs 0.000 description 3
- DVKJHBMWWAPEIU-UHFFFAOYSA-N toluene 2,4-diisocyanate Chemical compound CC1=CC=C(N=C=O)C=C1N=C=O DVKJHBMWWAPEIU-UHFFFAOYSA-N 0.000 description 3
- 239000012855 volatile organic compound Substances 0.000 description 3
- 238000010276 construction Methods 0.000 description 2
- 230000006378 damage Effects 0.000 description 2
- 238000001035 drying Methods 0.000 description 2
- 238000009408 flooring Methods 0.000 description 2
- 239000007789 gas Substances 0.000 description 2
- 239000003973 paint Substances 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- SMZOUWXMTYCWNB-UHFFFAOYSA-N 2-(2-methoxy-5-methylphenyl)ethanamine Chemical compound COC1=CC=C(C)C=C1CCN SMZOUWXMTYCWNB-UHFFFAOYSA-N 0.000 description 1
- 241000894006 Bacteria Species 0.000 description 1
- 102000002322 Egg Proteins Human genes 0.000 description 1
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- 206010019233 Headaches Diseases 0.000 description 1
- 206010068319 Oropharyngeal pain Diseases 0.000 description 1
- 201000007100 Pharyngitis Diseases 0.000 description 1
- 235000014676 Phragmites communis Nutrition 0.000 description 1
- 206010035664 Pneumonia Diseases 0.000 description 1
- 206010037423 Pulmonary oedema Diseases 0.000 description 1
- 208000027418 Wounds and injury Diseases 0.000 description 1
- QCWXUUIWCKQGHC-UHFFFAOYSA-N Zirconium Chemical compound [Zr] QCWXUUIWCKQGHC-UHFFFAOYSA-N 0.000 description 1
- 150000001336 alkenes Chemical class 0.000 description 1
- 201000009961 allergic asthma Diseases 0.000 description 1
- 238000005267 amalgamation Methods 0.000 description 1
- 230000001458 anti-acid effect Effects 0.000 description 1
- 208000006673 asthma Diseases 0.000 description 1
- 239000012752 auxiliary agent Substances 0.000 description 1
- 206010006451 bronchitis Diseases 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 231100000357 carcinogen Toxicity 0.000 description 1
- 239000003183 carcinogenic agent Substances 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
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- 229920001577 copolymer Polymers 0.000 description 1
- 238000005336 cracking Methods 0.000 description 1
- 238000005034 decoration Methods 0.000 description 1
- 230000001627 detrimental effect Effects 0.000 description 1
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- 231100000869 headache Toxicity 0.000 description 1
- 229910001385 heavy metal Inorganic materials 0.000 description 1
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- 230000007794 irritation Effects 0.000 description 1
- 230000007774 longterm Effects 0.000 description 1
- 239000006210 lotion Substances 0.000 description 1
- JRZJOMJEPLMPRA-UHFFFAOYSA-N olefin Natural products CCCCCCCC=C JRZJOMJEPLMPRA-UHFFFAOYSA-N 0.000 description 1
- 150000002894 organic compounds Chemical class 0.000 description 1
- 239000005416 organic matter Substances 0.000 description 1
- 210000004681 ovum Anatomy 0.000 description 1
- 208000005333 pulmonary edema Diseases 0.000 description 1
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- 238000007665 sagging Methods 0.000 description 1
- 230000003678 scratch resistant effect Effects 0.000 description 1
- 208000024891 symptom Diseases 0.000 description 1
- 229910052726 zirconium Inorganic materials 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D163/00—Coating compositions based on epoxy resins; Coating compositions based on derivatives of epoxy resins
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/61—Additives non-macromolecular inorganic
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/61—Additives non-macromolecular inorganic
- C09D7/62—Additives non-macromolecular inorganic modified by treatment with other compounds
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/65—Additives macromolecular
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/70—Additives characterised by shape, e.g. fibres, flakes or microspheres
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
- C08K3/20—Oxides; Hydroxides
- C08K3/22—Oxides; Hydroxides of metals
- C08K2003/2237—Oxides; Hydroxides of metals of titanium
- C08K2003/2241—Titanium dioxide
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
- C08K3/20—Oxides; Hydroxides
- C08K3/22—Oxides; Hydroxides of metals
- C08K2003/2244—Oxides; Hydroxides of metals of zirconium
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
- C08K3/24—Acids; Salts thereof
- C08K3/26—Carbonates; Bicarbonates
- C08K2003/265—Calcium, strontium or barium carbonate
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K2201/00—Specific properties of additives
- C08K2201/011—Nanostructured additives
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/02—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group
- C08L2205/025—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group containing two or more polymers of the same hierarchy C08L, and differing only in parameters such as density, comonomer content, molecular weight, structure
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
- C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Paints Or Removers (AREA)
- Compositions Of Macromolecular Compounds (AREA)
Abstract
The invention discloses an anti-slip heat-insulation sound-insulation environment-friendly floor coating and a preparation method thereof, wherein the coating comprises the following raw materials in parts by weight: 90-100 parts of modified compound resin, 7-11 parts of sound insulation additive, 8-14 parts of heat insulation filler, 6-10 parts of anti-skid additive, 20-30 parts of tackifying resin, 2-4 parts of insect-repelling degerming extract, 10-20 parts of mixed dibasic acid ester, 15-20 parts of propylene glycol monomethyl ether acetate, 3-5 parts of titanium dioxide, 0.5-1.5 parts of anti-settling agent, 1-2 parts of film forming agent, 0.4-0.8 part of defoaming agent, 0.8-1.4 parts of flatting agent and 2-4 parts of dispersing agent. The floor coating provided by the invention has the advantages that the floor coating is fine and smooth in surface, excellent in leveling property and touch, good in heat preservation and sound insulation performance, and excellent in skid resistance, friction resistance and corrosion resistance; meanwhile, the raw material components of the invention are safe and reliable, nontoxic and harmless, the raw materials are easy to obtain, the cost is lower, the process is simple, the operation and the realization of industrial production are easy, and the invention has higher practical value and good application prospect.
Description
Technical field
The present invention relates to technical field of coatings, and in particular to a kind of Anti-slide insulation sound insulation environmental protection floor coating and its preparation side
Method.
Background technology
The major function of floor coating is decoration and protection flooring, keeps floor cleaning beautiful, with other ornament materials
Hydraulic type indoor environment is created together.In order to obtain good decorative effect, not according to some use occasions and effect requirements
Together, height also more is required to the making of coating.Common paint adhesion is inadequate, is easy to peel off after drying up;Although having anti-
Alkaline energy, but antiacid corrosive power is relatively not good enough;And the texture of common coating is poor.And it is reached using antiskid effect after coating
Less than standard, it is also to weigh that can cause unnecessary injury, the anti-skidding and wear-resisting property of floor coating to old man and child in this way
One major criterion of coating property, because the non-skid property of coating is directly related to the safety in utilization of people, and wearability
In close relations with the service life of dope layer, wearability, which not enough can not only increase cost of material, can also increase construction cost.
In addition every year because of indoor furniture is fitted up being poisoned to death of occurring or sick number rises year by year, it is seen then that choosing
It is most important to the health of household to select the ornament materials of health, especially healthy coating, but many coating of domestic market
Middle benzene, the exceeded of VOC (volatile organic compounds) seriously affect health.Benzene, VOC are exceeded will to cause room organic contamination,
It is serious to cause the symptoms such as occupant's headache, sore-throat, it is detrimental to health.Free toluene diisocyanate (TDI) is that have
The organic compound of intense irritation gas.There are intense stimulus effect, Long Term Contact or high concentration to skin, eyes and respiratory tract
TDI gases can cause bronchitis, allergic asthma, pneumonia, pulmonary edema.In addition, the use of existing floor paint top grade
Synthetic fatty acid and acrylic acid system performance are good but of high cost, and market is difficult to receive;Other system prices are advantageous, but film
Performance is general, and construction problem is more.
Flooring needs certain heat-insulating property and sound insulation value, existing coating this respect to be also weak simultaneously.
Invention content
In view of the drawbacks of the prior art, the object of the present invention is to provide a kind of Anti-slide insulation sound insulation environmental protection floor coatings, should
Coating is as floor coating, and surface exquisiteness, levelability and sense of touch are more excellent, heat preservation and soundproof better performances, anti-skidding, antifriction
It wipes, fine corrosion resistance;The raw material components of the present invention are safe and reliable simultaneously, and nontoxic, raw material is easy to get, and cost is relatively low, work
Skill is concise, industrialized production easy to operate and realize, has higher practical value and good application prospect.
The present invention solves technical problem and adopts the following technical scheme that:
The present invention provides a kind of Anti-slide insulation sound insulation environmental protection floor coatings, include the raw material of following parts by weight:
Modified 90-100 parts of resin of compounding, 7-11 parts of sound insulation additive, 8-14 parts of thermal insulating filling, additive 6-10 parts anti-skidding, increasing
20-30 parts of resin of property, 2-4 parts of expelling parasite degerming extracting solution, 10-20 parts of mixed dibasic acid ester, propylene glycol methyl ether acetate 15-20
Part, is divided 3-5 parts of titanium dioxide, 0.5-1.5 parts of anti-settling agent, 1-2 parts of film forming agent, 0.4-0.8 parts of antifoaming agent, 0.8-1.4 parts of levelling agent
2-4 parts of powder.
Preferably, the Anti-slide insulation sound insulation environmental protection floor coating includes the raw material of following parts by weight:
Modified 95 parts of resin of compounding, 11 parts of thermal insulating filling, 8 parts of anti-skidding additive, 25 parts of resin of increasing property, drives 9 parts of sound insulation additive
3 parts of worm degerming extracting solution, 15 parts of mixed dibasic acid ester, 18 parts of propylene glycol methyl ether acetate, 4 parts of titanium dioxide, 1 part of anti-settling agent, at
1.5 parts of film, 0.6 part of antifoaming agent, 1.1 parts of levelling agent, 3 parts of dispersant.
Preferably, the sound insulation additive is glass bead, hollow glass fibre, floating bead according to weight ratio 3:1:2 compositions
Mixture;
The thermal insulating filling is attapulgite, oyster shell whiting, silica flour, talcum powder according to weight ratio 3:2:1:The mixture of 2 compositions,
The specification of the high temperature resistant filler was 400 mesh.
Preferably, the anti-skidding additive is nano zircite, nano ceramics micro mist, nano quartz sand according to weight ratio 4:
2:3 are modified, and the method for modifying is:Nano-mixture is added to the azido silanes coupling agent for being equivalent to total weight 3-5%
The ethoxylated alkylamine of S-3046 and total weight 1-3%, stir 2-3h under the conditions of temperature is 55-65 DEG C, and filtering is sent to vacuum
It is 0.08-0.10Mpa in vacuum degree, under conditions of temperature is 85-95 DEG C after dry heat 1-2h in drying box to obtain the final product.
Preferably, the modified compounding process for preparing resins is:By polyorganosiloxane resin, epoxy resin, acrylic resin
According to weight ratio 2:3:1 dissolving in organic solvent, stirs and is warming up to 80-90 DEG C, be added hydroxyl-terminated injecting two methyl siloxane,
Coupling agent and catalyst are uniformly mixed, isothermal reaction 2-4h, after reaction vacuum distillation removal low molecular compound and molten
Then graphene is added in agent into mixture again, be stirred to react 1-2h to get.
Preferably, the reinforced resin is for fatty acid modified low viscosity short oil alkyd resin and without the high hydroxyl short oil alcohol of benzene
Acid resin is according to weight ratio 3:The mixture of 2 compositions.
Preferably, the expelling parasite degerming extracting solution is:Aloe, Eupatorium adenophorum, tea tree, folium artemisiae argyi, Dalmatian chrysanthemum extracting solution press
According to weight ratio 3:1:2:1:The mixture of 2 compositions.
Preferably, the anti-settling agent is polyolefin-wax;The film forming agent is Hydroxylated acrylic resin, and the antifoaming agent is to have
Organosilicon polymer and vinethene are modified acrylic acid copolymer according to weight ratio 2:The mixture of 1 composition, the levelling agent are poly- third
Olefin(e) acid ester copolymer, the dispersant are sodium polycarboxylate salt form dispersant.
The present invention also provides a kind of preparation methods of Anti-slide insulation sound insulation environmental protection floor coating, include the following steps:
Step 1 weighs prepare each component raw material as required;
Step 2, by mixed dibasic acid ester, increasing property resin, sound insulation additive, thermal insulating filling, anti-skidding additive, mixing is sent into high
In temperature be 70-80 DEG C of rotating speed it is 250-350r/min in fast blender, stirs 15-25 minutes, obtain mixture A;
Step 3 modified compounding resin, propylene glycol methyl ether acetate, titanium dioxide, anti-settling agent is added in homogenizer, rotating speed
To continue stirring 15-25 minutes under 400-600r/min, ultrasonic disperse 20-30min systems in ultrasonic wave are placed in dispersant is added
Obtain mixture B;
Step 4 by the mixture B of mixture A, step 3 preparation prepared by film forming agent, antifoaming agent, levelling agent, step 2, is driven
The mixing of worm degerming extracting solution is added in high speed dispersor, rotating speed 5000-6000r/min, and temperature is to be dispersed with stirring at 65-75 DEG C
25-35 minutes, the Anti-slide insulation sound insulation environmental protection floor coating of invention was made in natural cooling.
Preferably, the preparation process of the Anti-slide insulation sound insulation environmental protection floor coating is:
Step 1 weighs prepare each component raw material as required;
Step 2, by mixed dibasic acid ester, increasing property resin, sound insulation additive, thermal insulating filling, anti-skidding additive, mixing is sent into high
In temperature be 75 DEG C of rotating speeds it is 300r/min in fast blender, stirs 20 minutes, obtain mixture A;
Step 3 modified compounding resin, propylene glycol methyl ether acetate, titanium dioxide, anti-settling agent is added in homogenizer, rotating speed
To continue stirring 20 minutes under 500r/min, the obtained mixture B of ultrasonic disperse 25min in ultrasonic wave are placed in dispersant is added;
Step 4 by the mixture B of mixture A, step 3 preparation prepared by film forming agent, antifoaming agent, levelling agent, step 2, is driven
The mixing of worm degerming extracting solution is added in high speed dispersor, rotating speed 5500r/min, and temperature is to be dispersed with stirring 30 minutes at 70 DEG C,
The Anti-slide insulation sound insulation environmental protection floor coating of invention is made in natural cooling.
Compared with prior art, the present invention has following advantageous effect:
(1)A kind of sound insulation additive of Anti-slide insulation sound insulation environmental protection floor coating addition of the present invention is glass bead, hollow glass
Glass fiber, floating bead, the hollow structure of several persons can effectively prevent the propagation of sound, while also certain heat-insulation warm keeping performance.
(2)The present invention a kind of Anti-slide insulation sound insulation environmental protection floor coating addition thermal insulating filling be mainly attapulgite,
Oyster shell whiting, silica flour, talcum powder can be effectively improved the heat preservation and insulation of coating, and oyster shell whiting also has certain kill in addition
Bacterium performance improves the corrosion resistance of coating, while a few persons can form fine and close lotion so that coating is not easy to draw because of overheat
Cracking is played, the performance of coating is improved.
(3)A kind of anti-skidding additive of Anti-slide insulation sound insulation environmental protection floor coating addition of the present invention is predominantly nano oxidized
Zirconium, nano ceramics micro mist, nano quartz sand, several persons can greatly improve the scratch-resistant performance of material, prevent coating surface excessively
It is dangerous caused by smooth, while anti-skidding additive is prepared by modified so that its amalgamation between other compositions is more preferable, in conjunction with more
It is close.
(4)A kind of Anti-slide insulation sound insulation environmental protection floor coating of the present invention, either bulk composition, solvent, auxiliary agent are not
Containing the carcinogens such as benzene and triphen, heavy metal is free of, health performance is excellent, and what is used compounds resin using modified so that
The coating of preparation has preferable levelability, glossiness and flexibility, all strictly controls the amount of volatile organic matter, environmental-protecting performance
It is superior.
(5)A kind of reinforced resin of Anti-slide insulation sound insulation environmental protection floor coating addition of the present invention is predominantly fatty acid modified
Low viscosity short oil alkyd resin and without the high hydroxyl short oil-ity alcohol acid resin of benzene, can effectively improve the sense of touch of coating, bond
Performance is more preferable, and sagging performance is more excellent.
(6)A kind of expelling parasite degerming extracting solution of Anti-slide insulation sound insulation environmental protection floor coating addition of the present invention is mainly reed
Luxuriant growth, Eupatorium adenophorum, tea tree, folium artemisiae argyi, Dalmatian chrysanthemum extracting solution, on the one hand its can effectively kill worm's ovum and mould, prevent terrace
The spot caused by overlong time and worm bite, and on the other hand use vegetal substance, and the chemical combination agent avoided is to human body
Harm.
(7)The present invention a kind of Anti-slide insulation sound insulation environmental protection floor coating be used as floor coating, surface exquisiteness, levelability and
Sense of touch is more excellent, heat preservation and soundproof better performances, anti-skidding, rub resistance, fine corrosion resistance;The raw material group of the present invention simultaneously
Divide securely and reliably, nontoxic, raw material is easy to get, and cost is relatively low, and technique is concise, and industrialized production easy to operate and realize has
Higher practical value and good application prospect.
Specific implementation mode
With reference to specific embodiment, technical scheme in the embodiment of the invention is clearly and completely described, shows
So, described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.Based on the reality in the present invention
Example is applied, every other embodiment obtained by those of ordinary skill in the art without making creative efforts all belongs to
In the scope of protection of the invention.
Embodiment 1.
A kind of Anti-slide insulation sound insulation environmental protection floor coating of the present embodiment, includes the raw material of following parts by weight:
Modified 90 parts of resin of compounding, 8 parts of thermal insulating filling, 6 parts of anti-skidding additive, 20 parts of resin of increasing property, drives 7 parts of sound insulation additive
2 parts of worm degerming extracting solution, 10 parts of mixed dibasic acid ester, 15 parts of propylene glycol methyl ether acetate, 3 parts of titanium dioxide, 0.5 part of anti-settling agent,
1 part of film forming agent, 0.4 part of antifoaming agent, 0.8 part of levelling agent, 2 parts of dispersant.
Sound insulation additive in the present embodiment is glass bead, hollow glass fibre, floating bead according to weight ratio 3:1:2 compositions
Mixture;
The thermal insulating filling is attapulgite, oyster shell whiting, silica flour, talcum powder according to weight ratio 3:2:1:The mixture of 2 compositions,
The specification of the high temperature resistant filler was 400 mesh.
Anti-skidding additive in the present embodiment is nano zircite, nano ceramics micro mist, nano quartz sand according to weight ratio
4:2:3 are modified, and the method for modifying is:Nano-mixture is added to the azido silanes coupling agent for being equivalent to total weight 3%
The ethoxylated alkylamine of S-3046 and total weight 1%, stir 2h under the conditions of temperature is 55 DEG C, and filtering is sent to vacuum drying chamber
It is interior, it is 0.08Mpa in vacuum degree, under conditions of temperature is 85 DEG C after dry heat 1h to obtain the final product.
Being modified in the present embodiment compounds process for preparing resins:By polyorganosiloxane resin, epoxy resin, acrylic resin
According to weight ratio 2:3:1 dissolving in organic solvent, stirs and is warming up to 80 DEG C, addition hydroxyl-terminated injecting two methyl siloxane, idol
Join agent and catalyst, be uniformly mixed, isothermal reaction 2h, after reaction vacuum distillation removal low molecular compound and solvent, so
Graphene is added into mixture again afterwards, be stirred to react 1h to get.
Reinforced resin in the present embodiment is for fatty acid modified low viscosity short oil alkyd resin and without the high hydroxyl short oil of benzene
Alkyd resin is according to weight ratio 3:The mixture of 2 compositions.
Expelling parasite degerming extracting solution in the present embodiment is:Aloe, Eupatorium adenophorum, tea tree, folium artemisiae argyi, Dalmatian chrysanthemum extracting solution press
According to weight ratio 3:1:2:1:The mixture of 2 compositions.
Anti-settling agent in the present embodiment is polyolefin-wax;The film forming agent is Hydroxylated acrylic resin, and the antifoaming agent is
Organosilicon polymer and vinethene are modified acrylic acid copolymer according to weight ratio 2:The mixture of 1 composition, the levelling agent is poly-
Acrylate interpolymer, the dispersant are sodium polycarboxylate salt form dispersant.
A kind of preparation method of Anti-slide insulation sound insulation environmental protection floor coating of the present embodiment, includes the following steps:
Step 1 weighs prepare each component raw material as required;
Step 2, by mixed dibasic acid ester, increasing property resin, sound insulation additive, thermal insulating filling, anti-skidding additive, mixing is sent into high
In temperature be 70 DEG C of rotating speeds it is 250r/min in fast blender, stirs 15 minutes, obtain mixture A;
Step 3 modified compounding resin, propylene glycol methyl ether acetate, titanium dioxide, anti-settling agent is added in homogenizer, rotating speed
To continue stirring 15 minutes under 400r/min, the obtained mixture B of ultrasonic disperse 20min in ultrasonic wave are placed in dispersant is added;
Step 4 by the mixture B of mixture A, step 3 preparation prepared by film forming agent, antifoaming agent, levelling agent, step 2, is driven
The mixing of worm degerming extracting solution is added in high speed dispersor, rotating speed 5000r/min, and temperature is to be dispersed with stirring 25 minutes at 65 DEG C,
The Anti-slide insulation sound insulation environmental protection floor coating of invention is made in natural cooling.
Embodiment 2.
A kind of Anti-slide insulation sound insulation environmental protection floor coating of the present embodiment, includes the raw material of following parts by weight:
Modified 100 parts of resin of compounding, 11 parts of sound insulation additive, 14 parts of thermal insulating filling, 10 parts of anti-skidding additive, increasing property resin 30
Part, 4 parts of expelling parasite degerming extracting solution, 20 parts of mixed dibasic acid ester, 20 parts of propylene glycol methyl ether acetate, 5 parts of titanium dioxide, anti-settling agent
1.5 parts, 2 parts of film forming agent, 0.8 part of antifoaming agent, 1.4 parts of levelling agent, 4 parts of dispersant.
Sound insulation additive in the present embodiment is glass bead, hollow glass fibre, floating bead according to weight ratio 3:1:2 compositions
Mixture;
The thermal insulating filling is attapulgite, oyster shell whiting, silica flour, talcum powder according to weight ratio 3:2:1:The mixture of 2 compositions,
The specification of the high temperature resistant filler was 400 mesh.
Anti-skidding additive in the present embodiment is nano zircite, nano ceramics micro mist, nano quartz sand according to weight ratio
4:2:3 are modified, and the method for modifying is:Nano-mixture is added to the azido silanes coupling agent for being equivalent to total weight 5%
The ethoxylated alkylamine of S-3046 and total weight 3%, stir 3h under the conditions of temperature is 65 DEG C, and filtering is sent to vacuum drying chamber
It is interior, it is 0.10Mpa in vacuum degree, under conditions of temperature is 95 DEG C after dry heat 2h to obtain the final product.
Being modified in the present embodiment compounds process for preparing resins:By polyorganosiloxane resin, epoxy resin, acrylic resin
According to weight ratio 2:3:1 dissolving in organic solvent, stirs and is warming up to 90 DEG C, addition hydroxyl-terminated injecting two methyl siloxane, idol
Join agent and catalyst, be uniformly mixed, isothermal reaction 4h, after reaction vacuum distillation removal low molecular compound and solvent, so
Graphene is added into mixture again afterwards, be stirred to react 2h to get.
Reinforced resin in the present embodiment is for fatty acid modified low viscosity short oil alkyd resin and without the high hydroxyl short oil of benzene
Alkyd resin is according to weight ratio 3:The mixture of 2 compositions.
Expelling parasite degerming extracting solution in the present embodiment is:Aloe, Eupatorium adenophorum, tea tree, folium artemisiae argyi, Dalmatian chrysanthemum extracting solution press
According to weight ratio 3:1:2:1:The mixture of 2 compositions.
Anti-settling agent in the present embodiment is polyolefin-wax;The film forming agent is Hydroxylated acrylic resin, and the antifoaming agent is
Organosilicon polymer and vinethene are modified acrylic acid copolymer according to weight ratio 2:The mixture of 1 composition, the levelling agent is poly-
Acrylate interpolymer, the dispersant are sodium polycarboxylate salt form dispersant.
A kind of preparation method of Anti-slide insulation sound insulation environmental protection floor coating of the present embodiment, includes the following steps:
Step 1 weighs prepare each component raw material as required;
Step 2, by mixed dibasic acid ester, increasing property resin, sound insulation additive, thermal insulating filling, anti-skidding additive, mixing is sent into high
In temperature be 80 DEG C of rotating speeds it is 350r/min in fast blender, stirs 25 minutes, obtain mixture A;
Step 3 modified compounding resin, propylene glycol methyl ether acetate, titanium dioxide, anti-settling agent is added in homogenizer, rotating speed
To continue stirring 25 minutes under 600r/min, the obtained mixture B of ultrasonic disperse 30min in ultrasonic wave are placed in dispersant is added;
Step 4 by the mixture B of mixture A, step 3 preparation prepared by film forming agent, antifoaming agent, levelling agent, step 2, is driven
The mixing of worm degerming extracting solution is added in high speed dispersor, rotating speed 6000r/min, and temperature is to be dispersed with stirring 35 minutes at 75 DEG C,
The Anti-slide insulation sound insulation environmental protection floor coating of invention is made in natural cooling.
Embodiment 3.
A kind of Anti-slide insulation sound insulation environmental protection floor coating of the present embodiment, includes the raw material of following parts by weight:
Modified 95 parts of resin of compounding, 11 parts of thermal insulating filling, 8 parts of anti-skidding additive, 25 parts of resin of increasing property, drives 9 parts of sound insulation additive
3 parts of worm degerming extracting solution, 15 parts of mixed dibasic acid ester, 18 parts of propylene glycol methyl ether acetate, 4 parts of titanium dioxide, 1 part of anti-settling agent, at
1.5 parts of film, 0.6 part of antifoaming agent, 1.1 parts of levelling agent, 3 parts of dispersant.
Sound insulation additive in the present embodiment is glass bead, hollow glass fibre, floating bead according to weight ratio 3:1:2 compositions
Mixture;
The thermal insulating filling is attapulgite, oyster shell whiting, silica flour, talcum powder according to weight ratio 3:2:1:The mixture of 2 compositions,
The specification of the high temperature resistant filler was 400 mesh.
Anti-skidding additive in the present embodiment is nano zircite, nano ceramics micro mist, nano quartz sand according to weight ratio
4:2:3 are modified, and the method for modifying is:Nano-mixture is added to the azido silanes coupling agent for being equivalent to total weight 4%
The ethoxylated alkylamine of S-3046 and total weight 2%, stir 2.5h under the conditions of temperature is 60 DEG C, and filtering is sent to vacuum drying
In case, under the conditions of vacuum degree is 0.09Mpa, is at a temperature of 90 °C after dry heat 1.5h to obtain the final product.
Being modified in the present embodiment compounds process for preparing resins:By polyorganosiloxane resin, epoxy resin, acrylic resin
According to weight ratio 2:3:1 dissolving in organic solvent, stirs and is warming up to 85 DEG C, addition hydroxyl-terminated injecting two methyl siloxane, idol
Join agent and catalyst, be uniformly mixed, isothermal reaction 3h, after reaction vacuum distillation removal low molecular compound and solvent, so
Graphene is added into mixture again afterwards, be stirred to react 1.5h to get.
Reinforced resin in the present embodiment is for fatty acid modified low viscosity short oil alkyd resin and without the high hydroxyl short oil of benzene
Alkyd resin is according to weight ratio 3:The mixture of 2 compositions.
Expelling parasite degerming extracting solution in the present embodiment is:Aloe, Eupatorium adenophorum, tea tree, folium artemisiae argyi, Dalmatian chrysanthemum extracting solution press
According to weight ratio 3:1:2:1:The mixture of 2 compositions.
Anti-settling agent in the present embodiment is polyolefin-wax;The film forming agent is Hydroxylated acrylic resin, and the antifoaming agent is
Organosilicon polymer and vinethene are modified acrylic acid copolymer according to weight ratio 2:The mixture of 1 composition, the levelling agent is poly-
Acrylate interpolymer, the dispersant are sodium polycarboxylate salt form dispersant.
A kind of preparation method of Anti-slide insulation sound insulation environmental protection floor coating of the present embodiment, includes the following steps:
Step 1 weighs prepare each component raw material as required;
Step 2, by mixed dibasic acid ester, increasing property resin, sound insulation additive, thermal insulating filling, anti-skidding additive, mixing is sent into high
In temperature be 75 DEG C of rotating speeds it is 300r/min in fast blender, stirs 20 minutes, obtain mixture A;
Step 3 modified compounding resin, propylene glycol methyl ether acetate, titanium dioxide, anti-settling agent is added in homogenizer, rotating speed
To continue stirring 20 minutes under 500r/min, the obtained mixture B of ultrasonic disperse 25min in ultrasonic wave are placed in dispersant is added;
Step 4 by the mixture B of mixture A, step 3 preparation prepared by film forming agent, antifoaming agent, levelling agent, step 2, is driven
The mixing of worm degerming extracting solution is added in high speed dispersor, rotating speed 5500r/min, and temperature is to be dispersed with stirring 30 minutes at 70 DEG C,
The Anti-slide insulation sound insulation environmental protection floor coating of invention is made in natural cooling.
A kind of Anti-slide insulation sound insulation environmental protection floor coating of the present invention is used as floor coating, and surface is fine and smooth, levelability and tactile
Feel more excellent, heat preservation and soundproof better performances, anti-skidding, rub resistance, fine corrosion resistance;The raw material components of the present invention simultaneously
Securely and reliably, nontoxic, raw material is easy to get, and cost is relatively low, and technique is concise, industrialized production easy to operate and realize, have compared with
High practical value and good application prospect.
It is obvious to a person skilled in the art that invention is not limited to the details of the above exemplary embodiments, Er Qie
In the case of without departing substantially from spirit or essential attributes of the invention, the present invention can be realized in other specific forms.Therefore, no matter
From the point of view of which point, the present embodiments are to be considered as illustrative and not restrictive, and the scope of the present invention is by appended power
Profit requires rather than above description limits, it is intended that all by what is fallen within the meaning and scope of the equivalent requirements of the claims
Variation is included within the present invention.
In addition, it should be understood that although this specification is described in terms of embodiments, but not each embodiment is only wrapped
Containing an independent technical solution, this description of the specification is merely for the sake of clarity, and those skilled in the art should
It considers the specification as a whole, the technical solutions in the various embodiments may also be suitably combined, forms those skilled in the art
The other embodiment being appreciated that.
Claims (10)
1. a kind of Anti-slide insulation sound insulation environmental protection floor coating, which is characterized in that include the raw material of following parts by weight:
Modified 90-100 parts of resin of compounding, 7-11 parts of sound insulation additive, 8-14 parts of thermal insulating filling, additive 6-10 parts anti-skidding, increasing
20-30 parts of resin of property, 2-4 parts of expelling parasite degerming extracting solution, 10-20 parts of mixed dibasic acid ester, propylene glycol methyl ether acetate 15-20
Part, is divided 3-5 parts of titanium dioxide, 0.5-1.5 parts of anti-settling agent, 1-2 parts of film forming agent, 0.4-0.8 parts of antifoaming agent, 0.8-1.4 parts of levelling agent
2-4 parts of powder.
2. a kind of Anti-slide insulation sound insulation environmental protection floor coating according to claim 1, which is characterized in that the Anti-slide insulation
Sound insulation environmental protection floor coating includes the raw material of following parts by weight:
Modified 95 parts of resin of compounding, 11 parts of thermal insulating filling, 8 parts of anti-skidding additive, 25 parts of resin of increasing property, drives 9 parts of sound insulation additive
3 parts of worm degerming extracting solution, 15 parts of mixed dibasic acid ester, 18 parts of propylene glycol methyl ether acetate, 4 parts of titanium dioxide, 1 part of anti-settling agent, at
1.5 parts of film, 0.6 part of antifoaming agent, 1.1 parts of levelling agent, 3 parts of dispersant.
3. a kind of Anti-slide insulation sound insulation environmental protection floor coating according to claim 1 or 2, which is characterized in that the sound insulation
Additive is glass bead, hollow glass fibre, floating bead according to weight ratio 3:1:The mixture of 2 compositions;
The thermal insulating filling is attapulgite, oyster shell whiting, silica flour, talcum powder according to weight ratio 3:2:1:The mixture of 2 compositions,
The specification of the high temperature resistant filler was 400 mesh.
4. a kind of Anti-slide insulation sound insulation environmental protection floor coating according to claim 1 or 2, which is characterized in that described anti-skidding
Additive is nano zircite, nano ceramics micro mist, nano quartz sand according to weight ratio 4:2:3 are modified, the modification side
Method is:Nano zircite, nano ceramics micro mist, nano quartz sand are mixed, the azido silanes for being equivalent to total weight 3-5% are added
The ethoxylated alkylamine of coupling agent S-3046 and total weight 1-3% stir 2-3h under the conditions of temperature is 55-65 DEG C, and filtering is sent
It is 0.08-0.10Mpa in vacuum degree, under conditions of temperature is 85-95 DEG C after dry heat 1-2h i.e. to vacuum drying chamber
.
5. a kind of Anti-slide insulation sound insulation environmental protection floor coating according to claim 1 or 2, which is characterized in that the modification
Compounding process for preparing resins is:By polyorganosiloxane resin, epoxy resin, acrylic resin according to weight ratio 2:3:1 has been dissolved in
In solvent, stirs and be warming up to 80-90 DEG C, addition hydroxyl-terminated injecting two methyl siloxane, coupling agent and catalyst mix equal
Even, isothermal reaction 2-4h, vacuum distillation removal low molecular compound and solvent, are then added into mixture again after reaction
Graphene, be stirred to react 1-2h to get.
6. a kind of Anti-slide insulation sound insulation environmental protection floor coating according to claim 1 or 2, which is characterized in that the enhancing
Resin is for fatty acid modified low viscosity short oil alkyd resin and without the high hydroxyl short oil-ity alcohol acid resin of benzene according to weight ratio 3:2 compositions
Mixture.
7. a kind of Anti-slide insulation sound insulation environmental protection floor coating according to claim 1 or 2, which is characterized in that the expelling parasite
Degerming extracting solution is:Aloe, Eupatorium adenophorum, tea tree, folium artemisiae argyi, Dalmatian chrysanthemum extracting solution according to weight ratio 3:1:2:1:2 compositions
Mixture.
8. a kind of Anti-slide insulation sound insulation environmental protection floor coating according to claim 1 or 2, which is characterized in that described anti-settling
Agent is polyolefin-wax;The film forming agent is Hydroxylated acrylic resin, and the antifoaming agent is that organosilicon polymer and vinethene are modified
Acrylic acid copolymer is according to weight ratio 2:The mixture of 1 composition, the levelling agent are polyacrylate copolymer, the dispersant
For sodium polycarboxylate salt form dispersant.
9. a kind of method preparing Anti-slide insulation sound insulation environmental protection floor coating as claimed in claim 1 or 2, which is characterized in that
Include the following steps:
Step 1 weighs prepare each component raw material as required;
Step 2, by mixed dibasic acid ester, increasing property resin, sound insulation additive, thermal insulating filling, anti-skidding additive, mixing is sent into high
In temperature be 70-80 DEG C of rotating speed it is 250-350r/min in fast blender, stirs 15-25 minutes, obtain mixture A;
Step 3 modified compounding resin, propylene glycol methyl ether acetate, titanium dioxide, anti-settling agent is added in homogenizer, rotating speed
To continue stirring 15-25 minutes under 400-600r/min, ultrasonic disperse 20-30min systems in ultrasonic wave are placed in dispersant is added
Obtain mixture B;
Step 4 by the mixture B of mixture A, step 3 preparation prepared by film forming agent, antifoaming agent, levelling agent, step 2, is driven
The mixing of worm degerming extracting solution is added in high speed dispersor, rotating speed 5000-6000r/min, and temperature is to be dispersed with stirring at 65-75 DEG C
25-35 minutes, the Anti-slide insulation sound insulation environmental protection floor coating of invention was made in natural cooling.
10. a kind of preparation method of Anti-slide insulation sound insulation environmental protection floor coating according to claim 9, which is characterized in that
The step is:
Step 1 weighs prepare each component raw material as required;
Step 2, by mixed dibasic acid ester, increasing property resin, sound insulation additive, thermal insulating filling, anti-skidding additive, mixing is sent into high
In temperature be 75 DEG C of rotating speeds it is 300r/min in fast blender, stirs 20 minutes, obtain mixture A;
Step 3 modified compounding resin, propylene glycol methyl ether acetate, titanium dioxide, anti-settling agent is added in homogenizer, rotating speed
To continue stirring 20 minutes under 500r/min, the obtained mixture B of ultrasonic disperse 25min in ultrasonic wave are placed in dispersant is added;
Step 4 by the mixture B of mixture A, step 3 preparation prepared by film forming agent, antifoaming agent, levelling agent, step 2, is driven
The mixing of worm degerming extracting solution is added in high speed dispersor, rotating speed 5500r/min, and temperature is to be dispersed with stirring 30 minutes at 70 DEG C,
The Anti-slide insulation sound insulation environmental protection floor coating of invention is made in natural cooling.
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