CN108379873A - The device recycled for ethyl alcohol in extraction of traditional Chinese medicine - Google Patents
The device recycled for ethyl alcohol in extraction of traditional Chinese medicine Download PDFInfo
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- CN108379873A CN108379873A CN201810319703.9A CN201810319703A CN108379873A CN 108379873 A CN108379873 A CN 108379873A CN 201810319703 A CN201810319703 A CN 201810319703A CN 108379873 A CN108379873 A CN 108379873A
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D11/00—Solvent extraction
- B01D11/02—Solvent extraction of solids
- B01D11/0292—Treatment of the solvent
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D15/00—Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
- B01D15/08—Selective adsorption, e.g. chromatography
- B01D15/10—Selective adsorption, e.g. chromatography characterised by constructional or operational features
- B01D15/18—Selective adsorption, e.g. chromatography characterised by constructional or operational features relating to flow patterns
- B01D15/1864—Selective adsorption, e.g. chromatography characterised by constructional or operational features relating to flow patterns using two or more columns
- B01D15/1871—Selective adsorption, e.g. chromatography characterised by constructional or operational features relating to flow patterns using two or more columns placed in series
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D15/00—Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
- B01D15/08—Selective adsorption, e.g. chromatography
- B01D15/10—Selective adsorption, e.g. chromatography characterised by constructional or operational features
- B01D15/20—Selective adsorption, e.g. chromatography characterised by constructional or operational features relating to the conditioning of the sorbent material
- B01D15/203—Equilibration or regeneration
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Analytical Chemistry (AREA)
- Treatment Of Liquids With Adsorbents In General (AREA)
- Solid-Sorbent Or Filter-Aiding Compositions (AREA)
Abstract
The present invention is used for the device that ethyl alcohol recycles in extraction of traditional Chinese medicine, contain evaporator, first, second condenser, adsorption column group, first, second fluid reservoir, photometer and external steam, the evaporator can use extractor or concentration tank or rectifying column to replace, evaporator is connect by pipeline with the first condenser, first condenser is connect by pipeline and check valve with the adsorption column group containing several adsorption columns, adsorption column group is passed through into pipeline, check valve and photometer are connect with the first fluid reservoir, the quality of recycling ethyl alcohol is controlled by photometer, qualified ethanol solution after processing is received in the storage of first fluid reservoir；Underproof ethanol solution enters the second condenser through vapor form, and storage is contained in the second fluid reservoir to utilize again.The recycling of ethyl alcohol, activated carbon energy on-line regeneration, high degree of automation have saved cost and time, the quality of recycling ethyl alcohol are made to meet standards of pharmacopoeia in present invention energy online processing, on-line monitoring extraction of traditional Chinese medicine, have the function of to Chinese medicine production positive.
Description
Technical field
The invention belongs to chemical solvents to be recycled technical field, specifically, being related to a kind of in extraction of traditional Chinese medicine
The method and apparatus of ethyl alcohol recycling.
Technical background
Pharmacopeia both domestic and external has clear and strict requirements to the quality of raw material in pharmacy procedure and auxiliary material.In China,
Ethyl alcohol would generally be used as solvent in the extraction process of many Chinese medicines, enterprise is to used etoh solvent often again from section
The theory of about cost and green manufacturing, which is set out, to be recycled and is reused.But extracting the ethyl alcohol recycled after medicinal material can contain
The quality of fresh ethanol is not achieved in the ingredient of some medicinal materials, quality.Compare pharmacopoeia of each country (China, the U.S., European Union, Britain and
Japan) standard the ethyl alcohol of recycling is detected, it is found that its quality is that the standard of pharmacopeia is not achieved.For this case,
On the basis of being difficult to change current extracting technique of Chinese medicine and existing producing equipment quickly, researches and develops and the ethyl alcohol of recycling is carried out
On-line checking and impurity removing technology and device, so that the quality of recycling ethyl alcohol is reached standards of pharmacopoeia just becomes very important thing in the industry
Feelings.
Invention content
The invention aims to solve the above problems, a kind of dress recycled for ethyl alcohol in extraction of traditional Chinese medicine is provided
It sets, it carries out online processing using adsorption column group to ethyl alcohol, can reduce transmission upwards of movement, cost-effective and time；Use photometer
It is monitored on-line, can guarantee that the ethyl alcohol after recycling meets the requirement of pharmacopeia；And detect underproof ethyl alcohol can be through adsorption column group
The rotation of each adsorption column handles and can the activated carbon on-line regeneration in attached column can be reduced the workload for the activated carbon that changes the outfit, and energy
Activated carbon is set to recycle；It wants easy to operation, improves the degree of automation, should have positive impetus to Chinese medicine production.
To achieve the above object, this invention takes following technical schemes.
A kind of device recycled for ethyl alcohol in extraction of traditional Chinese medicine, which is characterized in that contain evaporator, the first condensation
Device, the second condenser, adsorption column group, the first fluid reservoir, the second fluid reservoir, photometer and external steam are filled in the evaporator
There are alcohol mixture to be recycled (including ethyl alcohol water mixed solution or Chinese medicine ethanol extract or ethyl alcohol and medicinal material mixture), institute
The steam (vapor) outlet for stating evaporator is connect by pipeline with the steam inlet of the first condenser, and the outlet of first condenser passes through
Pipeline is connect with the entrance of adsorption column group, and the adsorption column group contains several adsorption columns, and the outlet of the adsorption column group passes through pipe
Road and check valve are connect with photometric entrance, and the photometric outlet is connected by the entrance of pipeline and the first fluid reservoir
It connects, first fluid reservoir storage is received through adsorption column group treated ethanol solution；Outside the connection of one end of the adsorption column group
Steam：The external steam is connect by pipeline and check valve with adsorption column group；When the recycling ethyl alcohol of adsorption column group processing is by institute
State photometer detection it is unqualified when, close the outlet valve of first condenser, external steam drawn by pipeline and check valve
Enter adsorption column group, the activated carbon in adsorption column group is regenerated using steam；The secondary steaming that the adsorption column group regeneration generates
The steam inlet that vapour enters the second condenser by pipeline and check valve connect, the outlet of second condenser by pipeline and
Second fluid reservoir connects, and the condensed liquid of the second condenser is received in second fluid reservoir storage.
Further, the evaporator can use extractor or concentration tank or rectifying column to replace, and ethyl alcohol is housed in the extractor
With the mixture of medicinal material, to be recycled is the ethyl alcohol in the dregs of a decoction；Ethanol extract containing traditional Chinese medicine ingredients is housed in the concentration tank,
To be recycled is the ethyl alcohol in extracting solution；The mixed solution or precipitation solution of ethyl alcohol and water are housed in the rectifying column, it is to be recycled
The mixed solution or the ethyl alcohol in precipitation solution for being ethyl alcohol and water.
Further, steam (vapor) outlet pipeline, bottom are equipped with equipped with solid discharge pipeline at the top of the extractor；Described
The top of concentration tank is equipped with vapor liquid export pipeline, bottom is equipped with extracting solution inlet ductwork.
Further, the adsorption column group contains more than two adsorption columns, and several adsorption columns are connected in parallel.
Further, the adsorption column use jacket type structure, each adsorption column contain top board net, support expanded metals, chuck,
First nozzle (be recycling ethanol entrance port), the second nozzle (being indirect steam outlet), third nozzle (being Boiler Steam entrance), the
Four nozzles (being chuck condensation-water drain) and the 5th nozzle (being the outlet of recycling ethyl alcohol after processing).
Further, the adsorbent that the adsorption column group uses is activated carbon.
A kind of device recycled for ethyl alcohol in extraction of traditional Chinese medicine, which is characterized in that contain evaporator, the first condensation
Device, the second condenser, the first adsorption column, the second adsorption column, third adsorption column, the first fluid reservoir, the second fluid reservoir, photometer and
External steam, in the evaporator equipped with alcohol mixture to be recycled (including ethyl alcohol water mixed solution or the extraction of Chinese medicine ethyl alcohol
Liquid or ethyl alcohol and medicinal material mixture), the steam (vapor) outlet of the evaporator is connect by pipeline with the steam inlet of the first condenser,
The outlet of first condenser by pipeline and check valve respectively with the first adsorption column, the second adsorption column and that are connected in parallel
The entrances of three adsorption columns connects, the outlet of first adsorption column, the second adsorption column and third adsorption column respectively by pipeline and
Check valve is connect with photometric entrance, and the photometric outlet is connect by pipeline with the entrance of the first fluid reservoir, institute
It states the storage of the first fluid reservoir to receive through adsorption column group treated ethanol solution, first adsorption column, the second adsorption column and third are inhaled
One end of attached column is separately connected external steam；It, will when the recycling ethyl alcohol of the first adsorption column processing is unqualified through photometer detection
The inlet and outlet non-return valve switches of first adsorption column enable second adsorption column and continue to the inlet and outlet check valve of the second adsorption column
Adsorption treatment, while external steam is introduced into the first adsorption column by pipeline and check valve, using in the first adsorption column of steam pair
Activated carbon regenerated；Using third adsorption column as station set, first adsorption column, the second adsorption column and third absorption
Column can cycle operation by this method：When the recycling ethyl alcohol of the second adsorption column processing is unqualified through photometer detection, second is inhaled
The inlet and outlet non-return valve switches of attached column enable the third adsorption column and continue at absorption to the inlet and outlet check valve of third adsorption column
Reason, while external steam is introduced into the second adsorption column by pipeline and check valve, use the activity in the second adsorption column of steam pair
Charcoal is regenerated；Using the first adsorption column as station set；When the recycling ethyl alcohol of third adsorption column processing detects not through photometer
When qualified, by the inlet and outlet check valve of the inlet and outlet non-return valve switches of third adsorption column to the first adsorption column, described first is enabled
Adsorption column continues adsorption treatment, while external steam is introduced third adsorption column by pipeline and check valve, uses steam pair the
Activated carbon in three adsorption columns is regenerated；Using the second adsorption column as station set；First adsorption column is regenerated secondary
Steam by its pipeline and check valve enters the second condenser, and (or the regenerated indirect steam of the second adsorption column passes through its pipe
Road and check valve enter the second condenser or the regenerated indirect steam of third adsorption column by its pipeline and check valve into
Enter the second condenser), the outlet of second condenser is connect by pipeline with the second fluid reservoir, and the second fluid reservoir storage is received
For the indirect steam of first adsorption column, the second adsorption column or third adsorption column through the condensed liquid of the second condenser, it can conduct
The raw material of ethyl alcohol is recycled with rectifying column.
Further, the evaporator can use extractor or concentration tank or rectifying column to replace, and ethyl alcohol is housed in the extractor
With the mixture of medicinal material, to be recycled is the ethyl alcohol in the dregs of a decoction；Ethanol extract containing traditional Chinese medicine ingredients is housed in the concentration tank,
To be recycled is the ethyl alcohol in extracting solution；The mixed solution or precipitation solution of ethyl alcohol and water are housed in the rectifying column, it is to be recycled
The mixed solution or the ethyl alcohol in precipitation solution for being ethyl alcohol and water.
Further, steam (vapor) outlet pipeline, bottom are equipped with equipped with solid discharge pipeline at the top of the extractor；Described
The top of concentration tank is equipped with vapor liquid export pipeline, bottom is equipped with extracting solution inlet ductwork.
The present invention is used for the good effect of device that ethyl alcohol recycles in extraction of traditional Chinese medicine：
(1) it uses adsorption column group to carry out online processing to ethyl alcohol, reduces transmission upwards of movement, it can the cost-effective and time.
(2) with Ultraviolet sensor (photometer), treated, and ethyl alcohol is monitored on-line, can guarantee the ethyl alcohol symbol after recycling
Close the requirement of pharmacopeia；It detects each adsorption column of the unqualified ethyl alcohol through adsorption column group and carries out rotation processing and by the work in preceding adsorption column
Property charcoal carries out on-line regeneration with steam, reduces the workload for the activated carbon that changes the outfit, activated carbon is enable to be recycled for multiple times.
(3) the device of the invention can carry out meeting pharmacopeia under the premise of not changing existing Chinese medicine extraction equipment and technique
The recycling of ethyl alcohol, reasonable design is easy to operation, and high degree of automation, has the function of to Chinese medicine production positive.
Description of the drawings
Fig. 1 is the structure and connection relationship diagram for the device that the present invention is recycled for ethyl alcohol in extraction of traditional Chinese medicine.
Fig. 2 is the part-structure enlarged drawing of Fig. 1.
Fig. 3 is the uv atlas that ethyl alcohol is recycled in the dregs of a decoction
Fig. 4 is the uv atlas that ethyl alcohol is recycled in extracting solution.
Fig. 5 is the uv atlas that ethyl alcohol is recycled in precipitation solution.
Label in figure is respectively：
1, evaporator；201, the first condenser；
202, the second condenser；3, adsorption column group；
301, the first adsorption column；302, the second adsorption column；
303, third adsorption column；401, the first check valve；
402, the second check valve；403, third check valve；
404, the 4th check valve；405, the 5th check valve；
406, the 6th check valve；407, the 7th check valve；
408, the 8th check valve；409, the 9th check valve；
410, the tenth check valve；411, the 11st check valve；
412, the 12nd check valve；413, the 13rd check valve；
414, the 14th check valve；415, the 15th check valve；
416, the 16th check valve；417, the 17th check valve；
418, the 18th check valve；419, the 19th check valve；
501, the first fluid reservoir；502, the second fluid reservoir；
6, photometer；7, external steam；
8, top board net；9, expanded metals is supported；
10, chuck；11, pressure gauge；
12, thermometer；13, drain valve；
1401, the first nozzle；1402, the second nozzle；
1403, third nozzle；1404, the 4th nozzle；
1405, the 5th nozzle.
Specific implementation mode
Specific implementation mode of the present invention for the device that ethyl alcohol in extraction of traditional Chinese medicine recycles is provided below in conjunction with attached drawing,
It should be noted that the implementation embodiment not limited to the following of the present invention.
Referring to Fig. 1.A kind of device recycled for ethyl alcohol in extraction of traditional Chinese medicine, contains evaporator 1, the first condenser
201, the second condenser 202, adsorption column group 3, the first fluid reservoir 501, the second fluid reservoir 502, photometer 6 and external steam 7.
The evaporator 1 is equipped with alcohol mixture to be recycled (including ethyl alcohol water mixed solution or Chinese medicine ethanol extract
Or ethyl alcohol and medicinal material mixture).
Evaporator 1 in apparatus of the present invention can be replaced with extractor, equipped with ethyl alcohol and medicinal material in the extractor
Mixture, to be recycled is the ethyl alcohol in the dregs of a decoction, therefore, is set equipped with steam (vapor) outlet pipeline, bottom at the top of the extractor
There is solid discharge pipeline.
Evaporator 1 in apparatus of the present invention can be replaced with concentration tank, equipped with containing traditional Chinese medicine ingredients in the concentration tank
Ethanol extract, to be recycled is the ethyl alcohol in extracting solution, therefore, vapor liquid outlet is equipped at the top of the concentration tank
Road, bottom are equipped with extracting solution inlet ductwork.
Evaporator 1 in apparatus of the present invention can also be replaced with rectifying column, equipped with ethyl alcohol and water in the rectifying column
Mixed solution or precipitation solution, the mixed solution or the ethyl alcohol in precipitation solution that be recycled be ethyl alcohol and water.
Condensed water water inlet pipe, the 16th check valve 416 and outlet pipe are equipped on first condenser 201.Described
Second condenser 202 is equipped with condensed water water inlet pipe, the 17th check valve 417 and outlet pipe.
Adsorption column group 3 in apparatus of the present invention uses three adsorption columns --- the first adsorption column 301, the second adsorption column 302
With third adsorption column 303.First adsorption column 301, the second adsorption column 302 and third adsorption column 303 use jacket type structure,
Each adsorption column contains top board net 8, support expanded metals 9, chuck 10, the first nozzle 1401 --- and it is recycling ethanol entrance port, second
Nozzle 1402 --- is that indirect steam exports, third nozzle 1403 --- being Boiler Steam entrance, the 4th nozzle 1404 --- is
Chuck condensation-water drain, the 5th nozzle 1405 --- it is the outlet of recycling ethyl alcohol after processing (referring to Fig. 2).First adsorption column
301, the adsorbent that the second adsorption column 302 and third adsorption column 303 use is activated carbon.By first adsorption column 301, second
Adsorption column 302 and third adsorption column 303 are connected in parallel.
The steam (vapor) outlet of the evaporator 1 is connect by pipeline with the steam inlet of the first condenser 201,
The steam (vapor) outlet of first condenser 201 is passed through into pipeline and the first check valve 401, the second check valve 402 and third
Check valve 403 is separately connected entrance (the first nozzle of the first adsorption column 301, the second adsorption column 302 and third adsorption column 303
1401), by the outlet (the 5th nozzle 1405) of first adsorption column 301, the second adsorption column 302 and third adsorption column 303 point
The entrance of the photometer 6 is not connected to by pipeline and the 7th check valve 407, the 8th check valve 408, the 9th check valve 409,
The outlet of the photometer 6 is connect by pipeline with the entrance of the first fluid reservoir 501, the storage of the first fluid reservoir 501 is received
Through the first adsorption column 301 or the second adsorption column 302 or third adsorption column 303 treated ethanol solution.
By one end (third nozzle 1403) of first adsorption column 301, the second adsorption column 302 and third adsorption column 303
It is connect respectively with external steam (7) by pipeline and the tenth check valve 410, the 11st check valve 411, the 12nd check valve 412；
In this way, when the recycling ethyl alcohol of the first adsorption column 301 processing detects unqualified through the photometer 6, it can be by the first adsorption column 301
Inlet and outlet the first check valve 401, the 7th check valve 407 switch to the second adsorption column 302 inlet and outlet the second check valve 402,
8th check valve 408 enables second adsorption column 302 and continues adsorption treatment, while external steam 7 is passed through pipeline and the tenth
Check valve 410 introduces the first adsorption column 301, is regenerated using the activated carbon in the first adsorption column of steam pair 301；Third is inhaled
Attached column 303 is used as station set.
First adsorption column 301, the second adsorption column 302 and third adsorption column 303 can be with above-mentioned formula cycle operations, i.e.,：
When the recycling ethyl alcohol of the second adsorption column 302 processing detects unqualified through photometer 6, the second adsorption column 302 is imported and exported the
Two check valves 402, the 8th check valve 408 switch to the third check valve 403 of the inlet and outlet of third adsorption column 303, the 9th check valve
409, it enables the third adsorption column 303 and continues adsorption treatment, meanwhile, external steam 7 is passed through into pipeline and the 11st check valve
411 introduce the second adsorption column 302, are regenerated using the activated carbon in the second adsorption column of steam pair 302.By the first adsorption column
301 are used as station set.
When third adsorption column 303 processing recycling ethyl alcohol detect unqualified through photometer 6 when, by third adsorption column 303 into
The third check valve 403 of outlet, the 9th check valve 409 switch to the first check valve 401 of the first adsorption column 301 inlet and outlet, the
Seven check valves 407 enable first adsorption column 301 and continue adsorption treatment, meanwhile, external steam 7 is passed through into pipeline and the tenth
Two check valves 412 introduce third adsorption column 303, are regenerated to the activated carbon in third adsorption column 303 using steam；By second
Adsorption column 302 is used as station set.
First adsorption column, 301 regenerated indirect steam passes through pipeline and the 4th check valve 404 through the second nozzle 1402
Into the second condenser 202, (or second adsorption column, 302 regenerated indirect steam passes through its pipeline and the 5th check valve
405 is unidirectional by its pipeline and the 6th into the second condenser 202 or 303 regenerated indirect steam of the third adsorption column
Valve 406 enters the second condenser 202), meanwhile, the folder of the first adsorption column 301 (the second adsorption column 302 and third adsorption column 303)
By pipeline and the 13rd check valve 413, (the 14th check valve the 414, the 15th is single through the 4th nozzle 1404 for condensed water in set
To valve 415) and the discharge outward of drain valve 13.
The outlet of second condenser 202 is connect by pipeline with the second fluid reservoir 502, second fluid reservoir
502 storages receive indirect steam that the first adsorption column 301 or the second adsorption column 302 or third adsorption column 303 generate through the second condenser
202 condensed liquid.The ethyl alcohol recycled in second fluid reservoir 502 eventually enters into rectifying column, as the raw material recycled again.
The 3 presented below Application Examples using alcohol recovering device of the present invention.
Application Example 1
Ethyl alcohol water mixed solution or Chinese medicine ethanol extract or ethyl alcohol are recycled using the alcohol recovering device equipped with evaporator 1
With the ethyl alcohol in medicinal material mixture.The steam (vapor) outlet of the evaporator 1 is connect with the steam inlet of the first condenser 201, it will
The condensate outlet of first condenser 201 is connect with the entrance of adsorption column group 3, by the liquid outlet of the adsorption column group 3
It is connect with the entrance of photometer 6, the outlet of the photometer 6 is connect with the entrance of the first fluid reservoir 501；First liquid storage
Tank 501 receives ethanol solution after processing.
The steam that 3 regenerated indirect steam of the adsorption column group is passed through into steam (vapor) outlet and pipeline and the second condenser 202
Entrance connects, and the second condenser 202 is connect by tube body with the second fluid reservoir 502, the second condenser 202 is cold by indirect steam
Liquid after solidifying flows into the second fluid reservoir 502.
Application Example 2
Substantially with Application Example 1, except that：Ginkgo is equipped with using the alcohol recovering device recycling equipped with extractor
The ginkgo dregs of a decoction after leaf extraction, recycle the ethyl alcohol in the dregs of a decoction.The ethyl alcohol of recycling directly surveys ultraviolet spectra (referring to Fig. 3), finds it
Absorbance is not met《Chinese Pharmacopoeia》Requirement, continue with.Ethyl alcohol is recycled again after 3 adsorption treatment of adsorption column group, then with purple
External spectrum detects：It was found that its absorbance meets《Chinese Pharmacopoeia》Requirement, illustrate this recycling of the tired device to ethanol in medicine residue
There is positive effect.
Application Example 3
Substantially with Application Example 1, except that：Using the alcohol recovering device recycling Radix Salviae Miltiorrhizae extraction equipped with concentration tank
The ethyl alcohol of ethyl alcohol in liquid, recycling directly surveys ultraviolet spectra (referring to Fig. 4), it is found that its absorbance is not met《Chinese Pharmacopoeia》Want
It asks, continues with.Recycling ethyl alcohol detects after 3 adsorption treatment of adsorption column group, then with ultraviolet spectra again：It was found that its absorbance meets
《Chinese Pharmacopoeia》Requirement, illustrate that this tired device has positive effect to the recycling of ethyl alcohol in red sage root extract.
Application Example 4
Substantially with Application Example 1, except that：It is mixed using the alcohol recovering device recycling ethanol water equipped with rectifying column
The ethyl alcohol in solution or precipitation solution is closed, the ethyl alcohol of recycling directly surveys ultraviolet spectra (referring to Fig. 5), it is found that its absorbance is not met
《Chinese Pharmacopoeia》Requirement, continue with.Recycling ethyl alcohol detects after 3 adsorption treatment of adsorption column group, then with ultraviolet spectra again：Hair
Its existing absorbance meets《Chinese Pharmacopoeia》Requirement, illustrate the device of the invention to ethyl alcohol in ethyl alcohol water mixed solution or precipitation solution
Recycling have positive effect.
Claims (9)
1. a kind of device recycled for ethyl alcohol in extraction of traditional Chinese medicine, which is characterized in that contain evaporator (1), the first condensation
Device (201), the second condenser (202), adsorption column group (3), the first fluid reservoir (501), the second fluid reservoir (502), photometer (6)
With external steam (7), alcohol mixture to be recycled is housed in the evaporator (1), the steam (vapor) outlet of the evaporator (1) is logical
Piping is connect with the steam inlet of the first condenser (201), and the outlet of first condenser (201) passes through pipeline and absorption
The entrance of column group (3) connects, and the adsorption column group (3) contains several adsorption columns, and the outlet of the adsorption column group (3) passes through pipeline
It is connect with check valve with the entrance of photometer (6), the outlet of the photometer (6) passes through pipeline and the first fluid reservoir (501)
Entrance connection, first fluid reservoir (501) storage receives through adsorption column group (3) treated ethanol solution；In the adsorption column
One end connection external steam (7) of group (3)：The external steam (7) is connect by pipeline and check valve with adsorption column group (3)；
When the recycling ethyl alcohol of adsorption column group (3) processing is unqualified by the photometer (6) detection, first condenser is closed
(201) external steam (7) is introduced adsorption column group (3), using steam to adsorption column group by outlet valve by pipeline and check valve
(3) activated carbon in is regenerated；The indirect steam that the adsorption column group (3) regeneration generates enters the by pipeline and check valve
The steam inlet of two condensers (202) connects, and the outlet of second condenser (202) passes through pipeline and the second fluid reservoir
(502) it connects, the second condenser (202) condensed liquid is received in second fluid reservoir (502) storage.
2. the device according to claim 1 recycled for ethyl alcohol in extraction of traditional Chinese medicine, which is characterized in that the evaporation
Device (1) can use extractor or concentration tank or rectifying column to replace, and the mixture of ethyl alcohol and medicinal material is housed in the extractor, to be recycled
Be ethyl alcohol in the dregs of a decoction；Ethanol extract containing traditional Chinese medicine ingredients is housed, to be recycled is in extracting solution in the concentration tank
Ethyl alcohol；The mixed solution or precipitation solution of ethyl alcohol and water are housed, to be recycled is the mixed solution of ethyl alcohol and water in the rectifying column
Or the ethyl alcohol in precipitation solution.
3. the device according to claim 2 recycled for ethyl alcohol in extraction of traditional Chinese medicine, which is characterized in that carried described
The top of tank is taken to be equipped with steam (vapor) outlet pipeline, bottom equipped with solid discharge pipeline；It is equipped with vapor liquid at the top of the concentration tank
Export pipeline, bottom are equipped with extracting solution inlet ductwork.
4. the device according to claim 1 recycled for ethyl alcohol in extraction of traditional Chinese medicine, which is characterized in that the absorption
Column group (3) contains more than two adsorption columns, and several adsorption columns are connected in parallel.
5. the device according to claim 4 recycled for ethyl alcohol in extraction of traditional Chinese medicine, which is characterized in that the absorption
Column uses jacket type structure, each adsorption column to contain top board net (8), support expanded metals (9), chuck (10), the first nozzle
(1401) --- recycling ethanol entrance port, the second nozzle (1402) --- being indirect steam outlet, third nozzle (1403) --- are
Boiler Steam entrance, the 4th nozzle (1404) --- chuck condensation-water drain, the 5th nozzle (1405) --- recycle second after processing
The outlet of alcohol.
6. the device according to claim 1 recycled for ethyl alcohol in extraction of traditional Chinese medicine, which is characterized in that the absorption
The adsorbent that column group (3) uses is activated carbon.
7. a kind of device recycled for ethyl alcohol in extraction of traditional Chinese medicine, which is characterized in that contain evaporator (1), the first condensation
Device (201), the second condenser (202), the first adsorption column (301), the second adsorption column (302), third adsorption column (303), first
Fluid reservoir (501), the second fluid reservoir (502), photometer (6) and external steam (7), in the evaporator (1) equipped with to be recycled
Alcohol mixture (including ethyl alcohol water mixed solution or Chinese medicine ethanol extract or ethyl alcohol and medicinal material mixture), the evaporator
(1) steam (vapor) outlet is connect by pipeline with the steam inlet of the first condenser (201), and the first condenser (201) go out
Mouthful by pipeline and check valve respectively with the first adsorption column (301), the second adsorption column (302) and third adsorption column that are connected in parallel
(303) entrance connection, the outlet point of first adsorption column (301), the second adsorption column (302) and third adsorption column (303)
It is not connect with the entrance of photometer (6) by pipeline and check valve, the outlet of the photometer (6) is stored up by pipeline and first
The entrance of flow container (501) connects, and the first fluid reservoir (501) storage is received through adsorption column group (3) treated ethanol solution, described
One end of first adsorption column (301), the second adsorption column (302) and third adsorption column (303) is separately connected external steam (7)；When
When the recycling ethyl alcohol of first adsorption column (301) processing is unqualified through photometer (6) detection, by the disengaging of the first adsorption column (301)
Mouth non-return valve switches enable second adsorption column (302) and continue at absorption to the inlet and outlet check valve of the second adsorption column (302)
Reason, while external steam (7) is introduced into the first adsorption column (301) by pipeline and check valve, use the first adsorption column of steam pair
(301) activated carbon in is regenerated；It regard third adsorption column (303) as station set, first adsorption column (301), the
Two adsorption columns (302) and third adsorption column (303) can cycle operations by this method：When the recycling of the second adsorption column (302) processing
When ethyl alcohol is unqualified through photometer (6) detection, by the inlet and outlet non-return valve switches of the second adsorption column (302) to third adsorption column
(303) inlet and outlet check valve enables the third adsorption column (303) and continues adsorption treatment, while external steam (7) being passed through
Pipeline and check valve introduce the second adsorption column (302), are regenerated using the activated carbon in the second adsorption column of steam pair (302)；
It regard the first adsorption column (301) as station set；When the recycling ethyl alcohol of third adsorption column (303) processing is detected through photometer (6)
When unqualified, by the inlet and outlet non-return valve switches of third adsorption column (303) to the inlet and outlet check valve of the first adsorption column (301),
It enables first adsorption column (301) and continues adsorption treatment, while external steam (7) is introduced into third by pipeline and check valve
Adsorption column (303) regenerates the activated carbon in third adsorption column (303) using steam；By the second adsorption column (302) conduct
Station set；The regenerated indirect steam of first adsorption column (301) enters the second condenser by its pipeline and check valve
(202) (or second adsorption column (302) regenerated indirect steam enters the second condenser by its pipeline and check valve
(202) or the third adsorption column (303) regenerated indirect steam enters the second condenser by its pipeline and check valve
(202)), the outlet of second condenser (202) is connect by pipeline with the second fluid reservoir (502), second fluid reservoir
(502) storage receive the first adsorption column (301), the second adsorption column (302) or third adsorption column (303) indirect steam through second condensation
Device (202) condensed liquid, it can be as the raw material for recycling ethyl alcohol with rectifying column.
8. the device according to claim 7 recycled for ethyl alcohol in extraction of traditional Chinese medicine, which is characterized in that the evaporation
Device (1) can use extractor or concentration tank or rectifying column to replace, and the mixture of ethyl alcohol and medicinal material is housed in the extractor, to be recycled
Be ethyl alcohol in the dregs of a decoction；Ethanol extract containing traditional Chinese medicine ingredients is housed, to be recycled is in extracting solution in the concentration tank
Ethyl alcohol；The mixed solution or precipitation solution of ethyl alcohol and water are housed, to be recycled is the mixed solution of ethyl alcohol and water in the rectifying column
Or the ethyl alcohol in precipitation solution.
9. the device according to claim 8 recycled for ethyl alcohol in extraction of traditional Chinese medicine, which is characterized in that carried described
The top of tank is taken to be equipped with steam (vapor) outlet pipeline, bottom equipped with solid discharge pipeline；It is equipped with vapor liquid at the top of the concentration tank
Export pipeline, bottom are equipped with extracting solution inlet ductwork.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110237888A (en) * | 2019-05-13 | 2019-09-17 | 杭州谈笑电子商务有限公司 | A kind of alcohol extraction procedure |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101138686A (en) * | 2007-07-23 | 2008-03-12 | 沈军 | Method for extracting active ingredient of natural product and uses thereof |
| CN102363085A (en) * | 2011-11-11 | 2012-02-29 | 惠州市众惠能源科技有限公司 | Method and special device for extracting and concentrating water extraction liquid medicine of Chinese medicine |
| CN103007571A (en) * | 2012-12-19 | 2013-04-03 | 温州市天龙轻工设备有限公司 | Alcohol-recyclable medicine extracting device and process thereof |
| CN103908799A (en) * | 2014-04-30 | 2014-07-09 | 江西中医药大学 | Extracting and concentrating all-in-one machine |
| CN206980170U (en) * | 2017-05-10 | 2018-02-09 | 天津中医药大学 | A kind of Chinese medicine ethanol extracts rapid concentration equipment integrating |
-
2018
- 2018-04-11 CN CN201810319703.9A patent/CN108379873B/en active Active
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101138686A (en) * | 2007-07-23 | 2008-03-12 | 沈军 | Method for extracting active ingredient of natural product and uses thereof |
| CN102363085A (en) * | 2011-11-11 | 2012-02-29 | 惠州市众惠能源科技有限公司 | Method and special device for extracting and concentrating water extraction liquid medicine of Chinese medicine |
| CN103007571A (en) * | 2012-12-19 | 2013-04-03 | 温州市天龙轻工设备有限公司 | Alcohol-recyclable medicine extracting device and process thereof |
| CN103908799A (en) * | 2014-04-30 | 2014-07-09 | 江西中医药大学 | Extracting and concentrating all-in-one machine |
| CN206980170U (en) * | 2017-05-10 | 2018-02-09 | 天津中医药大学 | A kind of Chinese medicine ethanol extracts rapid concentration equipment integrating |
Non-Patent Citations (2)
| Title |
|---|
| 宋竹田: "中药提取过程中乙醇的回收和套用", 《化工与医药工程》 * |
| 詹益兴主编: "《化工小商品生产法 第10集》", 31 March 1992, 湖南科学技术出版社 * |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110237888A (en) * | 2019-05-13 | 2019-09-17 | 杭州谈笑电子商务有限公司 | A kind of alcohol extraction procedure |
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