CN108373725A - Anti- distillation bottoming slurry of one kind and its preparation method and application - Google Patents
Anti- distillation bottoming slurry of one kind and its preparation method and application Download PDFInfo
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- CN108373725A CN108373725A CN201810227313.9A CN201810227313A CN108373725A CN 108373725 A CN108373725 A CN 108373725A CN 201810227313 A CN201810227313 A CN 201810227313A CN 108373725 A CN108373725 A CN 108373725A
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- China
- Prior art keywords
- distillation
- bottoming
- slurry
- parts
- bottoming slurry
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Classifications
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D133/00—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Coating compositions based on derivatives of such polymers
- C09D133/04—Homopolymers or copolymers of esters
- C09D133/06—Homopolymers or copolymers of esters of esters containing only carbon, hydrogen and oxygen, the oxygen atom being present only as part of the carboxyl radical
- C09D133/08—Homopolymers or copolymers of acrylic acid esters
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D133/00—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Coating compositions based on derivatives of such polymers
- C09D133/02—Homopolymers or copolymers of acids; Metal or ammonium salts thereof
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/61—Additives non-macromolecular inorganic
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/02—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group
- C08L2205/025—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group containing two or more polymers of the same hierarchy C08L, and differing only in parameters such as density, comonomer content, molecular weight, structure
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
- C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Curing Cements, Concrete, And Artificial Stone (AREA)
Abstract
The present invention provides a kind of anti-distillation bottoming to starch, and counts in parts by weight, including 5~20 parts of 30~60 parts of acrylic polymer, 15~30 parts of activated carbon, 6~8 parts of dispersant and water.The anti-distillation bottoming slurry has preferable adhesive force and stronger decoloring ability, it is applied and is starched as bottoming between Printing and clothes, the ground colour of coating and dyestuff in clothes and impurity can be absorbed well, it prevents ground colour and impurity from rising or moving to white rubber cement or mill base surface, improves the yields of Printing.The present invention also provides the preparation method of above-mentioned anti-distillation bottoming slurry and the applications in garment printing.
Description
Technical field
The present invention relates to garment printing technology field, more particularly to a kind of anti-distillation bottoming slurry and preparation method thereof and answer
With.
Background technology
Nowadays, people usually by white rubber cement or mill base by silk screen printing on clothes, to form various colors
Character pattern obtains Printing, which is also referred to as printing technology.However, being generally comprised in the preparation process of clothes various
Dyestuff and coating cause various dyestuffs and coating in clothes usually can distil or infiltrate into white rubber cement or mill base surface, go out
Printing also greatly reduces in existing Huang point, stain or other color dots, the situation for not only bringing appearance not beautiful to Printing
Various performances.
Accordingly, it is desirable to provide a kind of bottoming slurry between Printing and clothes, bottoming slurry can prevent in clothes
Various dyestuffs and coating sublime up into white rubber cement or mill base surface, to solve the above problems.
Invention content
An object of the present invention is to provide a kind of anti-distillation bottoming slurry, can prevent the various dyestuffs in clothes and coating liter
China to white rubber cement or mill base surface.
The second object of the present invention is to provide the preparation method of above-mentioned anti-distillation bottoming slurry.
The third object of the present invention is to provide above-mentioned anti-distillation bottoming and starches the application in garment printing.
To achieve the above object, the present invention provides a kind of anti-distillation bottoming to starch, and counts in parts by weight, including：
Wherein, the number of acrylic polymer can be selected as 30 parts, 40 parts, 50 parts, 60 parts；The number of activated carbon can be with
It is selected as 15 parts, 20 parts, 25 parts, 30 parts；The number of dispersant can be selected as 6 parts, 7 parts, 8 parts；The number of water can be selected as 5 parts,
10 parts, 15 parts, 20 parts.
The present invention provides a kind of anti-distillation bottoming to starch, and refers to that various dyestuffs and the painting that can be prevented in clothes are starched in the bottoming
Material sublimes up into white rubber cement or mill base surface.The anti-distillation bottoming slurry utilizes third using acrylic polymer as material of main part
The preferable adhesion of alkene acids polymers can well be combined with Printing, moreover it is possible to be oozed mutually with white rubber cement or mill base
Thoroughly, the binding force between them is greatly improved, while utilizing activated carbon large specific surface area, activity height, particle with pore more and tool
There is stronger decoloring ability, effectively the ground colour of coating and dyestuff in clothes and impurity can be absorbed, prevent ground colour
Rise or move to white rubber cement or mill base surface.In addition, activated carbon is scattered in acrylic polymer well using dispersant
It closes in object, improves absorbability of the anti-distillation bottoming slurry to the ground colour of coating and dyestuff.
Preferably, the acrylic polymer of the present invention is butyl polyacrylate, polyacrylic acid double methyl esters, polyacrylic acid second
It is one or more in ester and polyacrylic acid.It is further preferable that acrylic polymer is butyl polyacrylate, polyacrylic acid pair
The mixture of methyl esters, polyethyl acrylate and polyacrylic acid can effectively improve white using above-mentioned acrylic polymer
Adhesive force between Printing and anti-distillation bottoming slurry prepared by rubber cement or mill base, also has and improves the anti-of anti-distillation bottoming slurry
Ageing properties.
Preferably, the dispersant of the present invention is in triethyl group hexyl phosphoric acid, lauryl sodium sulfate and methyl anyl alcohol
It is one or more.
Preferably, activated carbon can be coaly activated carbon, wood activated charcoal.It is anti-containing this when being made using wood activated charcoal
The clothes of distillation bottoming slurry can be detected by NEEDLE DETETOR so that the warning level of NEEDLE DETETOR detection is 9-11 grades, is further expanded
The scope of application of anti-distillation bottoming slurry.Granularity in particular by wood activated charcoal is 0.63mm~2.00mm, decolorizing efficiency
It is high.
Preferably, the pH value of the anti-distillation bottoming slurry of the present invention is 6.5~7, pH value is starched in the anti-distillation bottoming of the range
With excellent stability.
Preferably, the solid content of the anti-distillation bottoming slurry of the present invention is 43%~45%, anti-liter of the solid content in the range
The strong adhesive force of magnificent bottoming slurry.
Preferably, the viscosity of the anti-distillation bottoming slurry of the present invention is 100cps, the knot of the anti-distillation bottoming slurry under the viscosity
Resultant force is preferably.
Preferably, the water of the present invention can be pure water, distilled water or deionized water.
The present invention also provides a kind of preparation method of anti-distillation bottoming slurry, step includes：
1) acrylic polymer of formula ratio and part water are uniformly mixed, obtain raw material A；
2) dispersant of formula ratio and remaining water is added in the activated carbon of formula ratio, stirs evenly, obtains raw material B；With
And
3) raw material A is added in the raw material B, is stirred evenly, obtain anti-distillation bottoming slurry.
It first passes through acrylic polymer and part water being uniformly mixed and obtains raw material A, adequately dissolved acrylic compounds
Polymer makes it be uniformly dispersed；Raw material B will be obtained in the dispersant of activated carbon addition formula ratio and remaining water simultaneously, passed through
Activated carbon is uniformly dispersed by dispersant, then raw material A is mixed with raw material B, to make activated carbon uniformly penetrate into original
Expect in A, uniformly mixed with acrylic polymer, the anti-distillation bottoming slurry each component finally obtained is uniform, is reached during use
To optimum efficiency.
The present invention also provides a kind of above-mentioned anti-distillation bottoming to starch the application in garment printing.
Anti- distillation bottoming slurry provided by the invention is applied in garment printing, and stamp prepared by white rubber cement or mill base is become
Bottoming slurry between product and clothes, the ground colour of the coating and dyestuff that can be effectively prevented in clothes rise or move to white
Rubber cement or mill base surface ensure that the appearance of Printing and properties are unaffected.
Specific implementation mode
The technical solution further illustrated the present invention below by specific implementation mode, but do not constitute and the present invention is appointed
What is limited.
Embodiment 1
Anti- distillation bottoming slurry, is counted in parts by weight, including：
The preparation method of above-mentioned anti-distillation bottoming slurry, step include：
1) 30 parts of butyl polyacrylate and 5 parts of water are uniformly mixed, obtain raw material A；
2) it by the triethyl group hexyl phosphoric acid and 5 parts of water of 20 parts of 6 parts of coaly activated carbon addition, stirs evenly, obtains raw material
B；And
3) it will be added in raw material B, stir evenly in raw material A, obtain anti-distillation bottoming slurry.
Embodiment 2
The anti-distillation bottoming of the present embodiment is starched, and is counted in parts by weight, including：
The preparation method of the anti-distillation bottoming slurry of the present embodiment, step include：
1) by 5 parts of butyl polyacrylates, the double methyl esters of 5 parts of polyacrylic acid, 7 parts of polyethyl acrylates and 13 parts of polyacrylic acid and
5 parts of water are uniformly mixed, and obtain raw material A；
2) it by the triethyl group hexyl phosphoric acid and 5 parts of water of 20 parts of 6 parts of coaly activated carbon addition, stirs evenly, obtains raw material
B；And
3) it will be added in raw material B, stir evenly in raw material A, obtain anti-distillation bottoming slurry.
Embodiment 3
The anti-distillation bottoming of the present embodiment is starched, and is counted in parts by weight, including：
The preparation method of the anti-distillation bottoming slurry of the present embodiment is same as Example 2, therefore, it does not elaborate herein.
Embodiment 4
The anti-distillation bottoming of the present embodiment is starched, and is counted in parts by weight, including：
The preparation method of the anti-distillation bottoming slurry of the present embodiment is same as Example 2, therefore, it does not elaborate herein.
Embodiment 5
The anti-distillation bottoming of the present embodiment is starched, and is counted in parts by weight, including：
The preparation method of the anti-distillation bottoming slurry of the present embodiment is same as Example 2, therefore, it does not elaborate herein.
Comparative example 1
The anti-distillation bottoming slurry of this comparative example, is counted in parts by weight, including：
30 parts of butyl polyacrylate；
6 parts of triethyl group hexyl phosphoric acid；And
10 parts of distilled water.
The preparation method of the anti-distillation bottoming slurry of this comparative example is same as Example 1, therefore, it does not elaborate herein.
The anti-distillation bottoming slurry that embodiment 1-5 and comparative example 1 are obtained is detected, test result is shown in Table 1.
The method of inspection：
Anti- distillation bottoming slurry is printed on clothes by wash durability, and wash water, note are carried out to product using 60 DEG C of warm water
The time being initially separated is starched in anti-distillation bottoming on record clothes.
Anti- distillation test, anti-distillation bottoming slurry is printed on clothes, then over print white size, is completed in printing technology
Afterwards, 185 DEG C are adjusted to using pressing machine, stamp are deployed troops on garrison duty into press, is then had a power failure, it is allowed to rest in pressing machine, record the time,
Take out calico observation white size surface whether spottiness.
NEEDLE DETETOR is tested, when being detected by NEEDLE DETETOR, the relied on magnetic field environment of detection can by the difference of conductivity and
Variation, and then cause the fluctuation of immediate current being associated, the size of curent change determines the height of NEEDLE DETETOR warning level,
Currently, the warning level of NEEDLE DETETOR detection has 1~11 grade, the grade the low more explanation contains magnetic metal foreign matter.
Performance test results are starched in 1 anti-distillation bottoming of table
| Wash durability | Anti- distillation test | NEEDLE DETETOR detects | |
| Embodiment 1 | 80min is detached | 10h spottiness | 7 grades |
| Embodiment 2 | 120min is not detached | 10h spottiness | 7 grades |
| Embodiment 3 | 120min is not detached | 11h immaculates | 11 grades |
| Embodiment 4 | 120min is not detached | 11h immaculates | 11 grades |
| Embodiment 5 | 120min is not detached | 11h immaculates | 11 grades |
| Comparative example 1 | 10min is detached | 2h spottiness | 11 grades |
As seen from Table 1, anti-distillation bottoming slurry using the present invention compared with Example 1, has excellent wash durability
Tested with anti-distillation, the reason is that in embodiment 1-5 using activated carbon large specific surface area, activity is high, particle with pore is more and have compared with
The ground colour of coating and dyestuff in clothes and impurity can effectively be absorbed, prevent ground colour from rising by strong decoloring ability
Or move to white rubber cement or mill base surface.In addition, although the NEEDLE DETETOR detection of embodiment 1 is relatively good, which beats
Prime cement does not have completely prevents various dyestuffs in clothes and coating from subliming up into white rubber cement or mill base surface, without real price
Value.
Compared with Example 2, the wash durability in embodiment 2 is far above embodiment 1 to embodiment 1, the reason is that embodiment 2
Middle acrylic polymer is the mixture of butyl polyacrylate, the double methyl esters of polyacrylic acid, polyethyl acrylate and polyacrylic acid,
Printing and anti-distillation bottoming prepared by white rubber cement or mill base can be effectively improved using above-mentioned acrylic polymer
Adhesive force between slurry also has the anti-aging property for improving anti-distillation bottoming slurry.
Compared with Example 3, the NEEDLE DETETOR detection of embodiment 3 is much better than embodiment 2 to embodiment 2, the reason is that wooden activity
The conductivity of charcoal is much smaller than coaly activated carbon, and the bottoming slurry prepared using coaly activated carbon may when being detected by NEEDLE DETETOR
The clothes for causing immediate current to fluctuate, causing NEEDLE DETETOR warning level relatively low, and the anti-distillation bottoming of wood activated charcoal is used to starch
It can be detected well by NEEDLE DETETOR.Meanwhile the anti-distillation test of embodiment 3 is also good compared with embodiment 2, it may be possible to due in the body
Wood activated charcoal is higher than coaly activated carbon to the absorption of the ground colour of coating and dyestuff in clothes in system.
Finally, it should be noted that the above embodiments are merely illustrative of the technical solutions of the present invention rather than is protected to the present invention
The limitation of range is protected, although the present invention is described in detail with reference to preferred embodiment, the invention is not limited in above
Embodiments of the disclosure, and modification, equivalent combinations that various essence according to the present invention carry out should be covered.
Claims (9)
1. a kind of anti-distillation bottoming slurry, which is characterized in that it counts in parts by weight, including：
2. anti-distillation bottoming slurry as described in claim 1, which is characterized in that the acrylic polymer is polyacrylic acid fourth
It is one or more in ester, polyacrylic acid double methyl esters, polyethyl acrylate and polyacrylic acid.
3. anti-distillation bottoming slurry as described in claim 1, which is characterized in that the dispersant selected from triethyl group hexyl phosphoric acid,
It is one or more in lauryl sodium sulfate and methyl anyl alcohol.
4. anti-distillation bottoming slurry as described in claim 1, which is characterized in that the activated carbon is wood activated charcoal.
5. anti-distillation bottoming slurry as described in claim 1, which is characterized in that the pH value of the anti-distillation bottoming slurry for 6.5~
7。
6. anti-distillation bottoming slurry as described in claim 1, which is characterized in that the solid content of the anti-distillation bottoming slurry is 43%
~45%.
7. anti-distillation bottoming slurry as described in claim 1, which is characterized in that the viscosity that the anti-distillation bottoming is starched is
100cps。
8. the preparation method of the anti-distillation bottoming slurry as described in claim 1~7 any one, which is characterized in that its step packet
It includes：
1) acrylic polymer of formula ratio and part water are uniformly mixed, obtain raw material A；
2) dispersant of formula ratio and remaining water is added in the activated carbon of formula ratio, stirs evenly, obtains raw material B；And
3) raw material A is added in the raw material B, is stirred evenly, obtain anti-distillation bottoming slurry.
9. the application in garment printing is starched in a kind of anti-distillation bottoming as described in claim 1~7 any one.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810227313.9A CN108373725A (en) | 2018-03-19 | 2018-03-19 | Anti- distillation bottoming slurry of one kind and its preparation method and application |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810227313.9A CN108373725A (en) | 2018-03-19 | 2018-03-19 | Anti- distillation bottoming slurry of one kind and its preparation method and application |
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| CN108373725A true CN108373725A (en) | 2018-08-07 |
Family
ID=63019092
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115216982A (en) * | 2022-08-15 | 2022-10-21 | 喻盛 | Natural dry baking-free process water-based paint digital direct injection method |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115216982A (en) * | 2022-08-15 | 2022-10-21 | 喻盛 | Natural dry baking-free process water-based paint digital direct injection method |
| CN115216982B (en) * | 2022-08-15 | 2024-03-08 | 喻盛 | Digital direct spraying method for water-based paint in natural drying baking-free procedure |
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Application publication date: 20180807 |