CN108358601A - A kind of full impregnated polished glazed tile and preparation method thereof - Google Patents
A kind of full impregnated polished glazed tile and preparation method thereof Download PDFInfo
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- CN108358601A CN108358601A CN201810163368.8A CN201810163368A CN108358601A CN 108358601 A CN108358601 A CN 108358601A CN 201810163368 A CN201810163368 A CN 201810163368A CN 108358601 A CN108358601 A CN 108358601A
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- C04B35/626—Preparing or treating the powders individually or as batches ; preparing or treating macroscopic reinforcing agents for ceramic products, e.g. fibres; mechanical aspects section B
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- C04B35/626—Preparing or treating the powders individually or as batches ; preparing or treating macroscopic reinforcing agents for ceramic products, e.g. fibres; mechanical aspects section B
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- C04B35/626—Preparing or treating the powders individually or as batches ; preparing or treating macroscopic reinforcing agents for ceramic products, e.g. fibres; mechanical aspects section B
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- C04B2235/34—Non-metal oxides, non-metal mixed oxides, or salts thereof that form the non-metal oxides upon heating, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
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Abstract
The invention discloses a kind of full impregnated polished glazed tiles and preparation method thereof, and in terms of parts by weight, the full impregnated polished glazed tile includes mainly following components：22 42 parts of ball clay, 12 18 parts of albite, 5 12 parts of silica flour, 8 15 parts of wollastonite, 47 parts of water mill feldspar in powder, 14 parts of waterglass, 0.4 0.8 parts of water-reducing agent, 0.3 0.6 parts of green body reinforcing agent, 44 70 parts of deionized water.The preparation method includes raw material preparation, ball milling, mist projection granulating, punch forming, calcining and polishing.Full impregnated polished glazed tile prepared by the present invention solves traditional polished bricks case shell, three-dimensional and imitation stone effect obscure it is bad, have developed the super application expected so that imitation stone effect is more true to nature, while having preferable permeability resistance, glossiness, preparation method is simple, is suitable for industrialized production.
Description
Technical field
The present invention relates to technical field of construction and decoration materials, and in particular to a kind of full impregnated polished glazed tile and preparation method thereof.
Background technology
Polished bricks are one kind of all-body tile, by the surface of all-body tile green body by a kind of brick of light made of polishing, are
The popular novel decorative ceramic material of recent domestic, surface is by polishing, and the surface of polished bricks is than all-body tile light
Clean is more.
Polished bricks are compared with lithotome, no radioactive element, and lithotome category minerals without high temperature sintering, therefore contain
Individual trace-level activity elements, Long Term Contact can be harmful；Polished bricks are harmless；When lithotome is due to diagenesis
Between, rock stratum depth difference aberration it is larger, polished bricks are through allotment meticulously, substantially colorless difference consistent with batch product pattern；Polished bricks are anti-
Bending strength is big, and lithotome leads to tightness degree, intensity not since self-assembling formation, time of becoming a useful person, weathering etc. are not quite similar
One；Polished bricks are suppressed by thousands of t hydraulic press, then through 1200 DEG C or more high temperature sinterings, and intensity is high；Polished bricks brick body is thin, weight
Gently, lithotome because intensity it is low, therefore it is larger to process thickness, heavy, increases the weighing load of floor building, forms potential prestige
The side of body, cost increase, and increase the difficulties such as transport, paving.
Meanwhile polished bricks have the characteristics that freeze proof antifouling, acid-fast alkali-proof, light is magnificent, sustains its quality through age, polished bricks are hard resistance to
Mill, is suitble to use in most interior spaces in addition to toilet, kitchen, for example is used for balcony, and decoration of exterior wall etc. makes polishing
Brick is largely used.
But polished bricks are mainly using traditional apparatus for distributing polish after cloth at present, Recipe is opposite
Fairly simple, white material and saturating material temperature degree are not much different, and case shell unobvious, not very good simulated effect exists simultaneously anti-
The poor situation of permeability, glossiness.
Based on this, it is necessary to a kind of full impregnated polished glazed tile and preparation method thereof is provided, to solve prior art presence
The problem of.
Invention content
In view of the above-mentioned analysis to the prior art, a kind of full impregnated polished glazed tile of present invention offer and preparation method thereof,
The ceramic tile solves traditional polished bricks case shell, three-dimensional and imitation stone effect obscures bad, has developed the super application expected so that
Imitation stone effect is more true to nature, while having preferable permeability resistance, glossiness, and preparation method is simple, is suitable for industrialized production.
In order to achieve the above object, the present invention is achieved through the following technical solutions：
A kind of full impregnated polished glazed tile, in terms of parts by weight, the full impregnated polished glazed tile includes mainly following components：
22-42 parts of ball clay；
12-18 parts of albite；
5-12 parts of silica flour；
8-15 parts of wollastonite；
4-7 parts of water mill feldspar in powder
1-4 parts of waterglass；
0.4-0.8 parts of water-reducing agent；
0.3-0.6 parts of green body reinforcing agent；
44-70 parts of deionized water
Preferably, in terms of parts by weight, the full impregnated polished glazed tile includes mainly following components：
30 parts of ball clay；
15 parts of albite；
8.5 parts of silica flour；
11.5 parts of wollastonite；
5.5 parts of water mill feldspar in powder
2.05 parts of waterglass；
0.6 part of water-reducing agent；
0.5 part of green body reinforcing agent；
57 parts of deionized water.
Preferably, the water-reducing agent is polycarboxylate water-reducer.
Preferably, the green body reinforcing agent is by sodium carboxymethylcellulose, polyvinyl alcohol, polyvinyl butyral and poly- second
One or more of glycol.
The present invention also provides a kind of preparation methods of full impregnated polished glazed tile, include the following steps：
Step 1：Raw material preparation:Each raw material is weighed by regulation number, and carries out mixing outfit, obtains mixture a1；
Step 2：Ball milling：In step 1 mixture a1 and deionized water be added in ball mill and carry out mixed grinding, form slurry
a2；
Step 3：Mist projection granulating：Slurry a1 injections in step 2 are in the spray drying tower dried it, is granulated, is formed
Powder a3；
Step 4：Punch forming：Press machine is added in powder a3 in step 3 and carries out cloth, punch forming, obtains ceramic tile blank
a4；
Step 5：Calcining：Ceramic tile blank a4 in step 4 is put into kiln and is calcined, full impregnated ceramic tile a5 is obtained；
Step 6：Polishing：Full impregnated ceramic tile a5 in step 5 is polished process, obtains full impregnated polished glazed tile.
Preferably, the condition of the ball milling in step 2：To grind 40-60min under 400-500rpmn speed.
Preferably, the pressure of the press machine in step 4 is 30-40Mpa.
Preferably, the firing temperature calcined in step 5 is 1150-1250 DEG C, the time of firing is 50-60 minutes.
Compared with prior art, the present invention having following advantageous effect：
（1）The present invention solves traditional polished bricks case shell, three-dimensional and imitation stone effect obscure it is bad, by having developed super material
Application so that imitation stone effect is more true to nature, while having preferable permeability resistance, glossiness, and preparation method is simple, science close
Reason, it is of low cost, it is suitable for industrialized production.
（2）The present invention does not quote material containing zirconium source material, is directly selecting ball clay, albite, silica flour, wollastonite, water mill
Feldspar in powder is reasonably arranged in pairs or groups by each component so that ceramic tile obtained 3-5 degree higher than common ceramic tile, surface is smooth, radioactivity
It is not exceeded, meet the requirement of national standard, reaches environmental protection and energy saving effect；Pass through experiment, hardness >=7 of polished glazed tile of the invention
Grade；Acid-fast alkali-proof is UA grades；Radioactivity is Ira≤0.6, Ir≤0.8；Flexural strength is 41-45Mpa, and the performance of test is not
But meet the requirement of production technology standard, it is even more excellent.
（3）The present invention mainly with making an addition in ball mill in slurry, plays dilution by the addition water-reducing agent, waterglass
Effect, the mobile performance of slurry can be improved, the water content in slurry can be reduced to suitable level, in order to follow-up
Prepared by the powder of technique, avoid slurry moisture excessive and influence spray tower and be granulated quality and cost.It is few by introducing in formula
Green body reinforcing agent substitution prior partial ball clay is measured, use the content of ball clay is reduced, is helped to improve before and after body drying by force
Degree, contributes to optimization of C/C composites structure, reduces the usage amount of clay, is conducive to the promotion of product light transmittance, is burnt into the quickening of speed
And formulation cost is reduced, while raw material resources are in short supply positive guiding to alleviating.
（4）The preparation process of the full impregnated polished glazed tile of the present invention is simple, industrialized production easy to implement.
Specific implementation mode
Form by the following examples is described in further detail the above of the present invention again, but should not be by this
The range for being interpreted as the above-mentioned theme of the present invention is only limitted to following embodiment, all based on the technology realized belonging to the above of the present invention
It all belongs to the scope of the present invention.
Embodiment 1
A kind of full impregnated polished glazed tile, in terms of parts by weight, the full impregnated polished glazed tile includes mainly following components：
22 parts of ball clay；
12 parts of albite；
5 parts of silica flour；
8 parts of wollastonite；
4 parts of water mill feldspar in powder
1 part of waterglass；
0.4 part of water-reducing agent；
0.3 part of green body reinforcing agent；
44 parts of deionized water.
Wherein, the water-reducing agent is polycarboxylate water-reducer.
Wherein, the green body reinforcing agent is by sodium carboxymethylcellulose, polyvinyl alcohol, polyvinyl butyral and polyethylene glycol
One or more of.
The present invention also provides a kind of preparation methods of full impregnated polished glazed tile, include the following steps：
Step 1：Raw material preparation:Each raw material is weighed by regulation number, and carries out mixing outfit, obtains mixture a1；
Step 2：Ball milling：In step 1 mixture a1 and deionized water be added in ball mill and carry out mixed grinding, form slurry
a2；
Step 3：Mist projection granulating：Slurry a1 injections in step 2 are in the spray drying tower dried it, is granulated, is formed
Powder a3；
Step 4：Punch forming：Press machine is added in powder a3 in step 3 and carries out cloth, punch forming, obtains ceramic tile blank
a4；
Step 5：Calcining：Ceramic tile blank a4 in step 4 is put into kiln and is calcined, full impregnated ceramic tile a5 is obtained；
Step 6：Polishing：Full impregnated ceramic tile a5 in step 5 is polished process, obtains full impregnated polished glazed tile.
Wherein, the condition of the ball milling in step 2：To grind 40min under 400rpmn speed.
Wherein, the pressure of the press machine in step 4 is 30Mpa.
Wherein, the firing temperature calcined in step 5 is 1150 DEG C, and the time of firing is 50 minutes.
Embodiment 2
A kind of full impregnated polished glazed tile, in terms of parts by weight, the full impregnated polished glazed tile includes mainly following components：
42 parts of ball clay；
18 parts of albite；
12 parts of silica flour；
15 parts of wollastonite；
7 parts of water mill feldspar in powder
4 parts of waterglass；
0.8 part of water-reducing agent；
0.6 part of green body reinforcing agent；
70 parts of deionized water.
Wherein, the water-reducing agent is polycarboxylate water-reducer.
Wherein, the green body reinforcing agent is by sodium carboxymethylcellulose, polyvinyl alcohol, polyvinyl butyral and polyethylene glycol
One or more of.
The present invention also provides a kind of preparation methods of full impregnated polished glazed tile, include the following steps：
Step 1：Raw material preparation:Each raw material is weighed by regulation number, and carries out mixing outfit, obtains mixture a1；
Step 2：Ball milling：In step 1 mixture a1 and deionized water be added in ball mill and carry out mixed grinding, form slurry
a2；
Step 3：Mist projection granulating：Slurry a1 injections in step 2 are in the spray drying tower dried it, is granulated, is formed
Powder a3；
Step 4：Punch forming：Press machine is added in powder a3 in step 3 and carries out cloth, punch forming, obtains ceramic tile blank
a4；
Step 5：Calcining：Ceramic tile blank a4 in step 4 is put into kiln and is calcined, full impregnated ceramic tile a5 is obtained；
Step 6：Polishing：Full impregnated ceramic tile a5 in step 5 is polished process, obtains full impregnated polished glazed tile.
Wherein, the condition of the ball milling in step 2：To grind 60min under 500rpmn speed.
Wherein, the pressure of the press machine in step 4 is 40Mpa.
Wherein, the firing temperature calcined in step 5 is 1250 DEG C, and the time of firing is 60 minutes.
Embodiment 3
A kind of full impregnated polished glazed tile, in terms of parts by weight, the full impregnated polished glazed tile includes mainly following components：
30 parts of ball clay；
15 parts of albite；
8.5 parts of silica flour；
11.5 parts of wollastonite；
5.5 parts of water mill feldspar in powder
2.05 parts of waterglass；
0.6 part of water-reducing agent；
0.5 part of green body reinforcing agent；
57 parts of deionized water.
Wherein, the water-reducing agent is polycarboxylate water-reducer.
Wherein, the green body reinforcing agent is by sodium carboxymethylcellulose, polyvinyl alcohol, polyvinyl butyral and polyethylene glycol
One or more of.
The present invention also provides a kind of preparation methods of full impregnated polished glazed tile, include the following steps：
Step 1：Raw material preparation:Each raw material is weighed by regulation number, and carries out mixing outfit, obtains mixture a1；
Step 2：Ball milling：In step 1 mixture a1 and deionized water be added in ball mill and carry out mixed grinding, form slurry
a2；
Step 3：Mist projection granulating：Slurry a1 injections in step 2 are in the spray drying tower dried it, is granulated, is formed
Powder a3；
Step 4：Punch forming：Press machine is added in powder a3 in step 3 and carries out cloth, punch forming, obtains ceramic tile blank
a4；
Step 5：Calcining：Ceramic tile blank a4 in step 4 is put into kiln and is calcined, full impregnated ceramic tile a5 is obtained；
Step 6：Polishing：Full impregnated ceramic tile a5 in step 5 is polished process, obtains full impregnated polished glazed tile.
Wherein, the condition of the ball milling in step 2：To grind 50min under 450rpmn speed.
Wherein, the pressure of the press machine in step 4 is 35Mpa.
Wherein, the firing temperature calcined in step 5 is 1200 DEG C, and the time of firing is 55 minutes.
It is merely a preferred embodiment of the present invention, is not intended to restrict the invention, although with reference to aforementioned implementation described in upper
Invention is explained in detail for example, for those skilled in the art, still can be to foregoing embodiments
Recorded technical solution is modified or equivalent replacement of some of the technical features.All spirit in the present invention
Within principle, any modification, equivalent replacement, improvement and so on should all be included in the protection scope of the present invention.
Claims (8)
1. a kind of full impregnated polished glazed tile, which is characterized in that in terms of parts by weight, the full impregnated polished glazed tile includes mainly with the following group
Point：
22-42 parts of ball clay；
12-18 parts of albite；
5-12 parts of silica flour；
8-15 parts of wollastonite；
4-7 parts of water mill feldspar in powder
1-4 parts of waterglass；
0.4-0.8 parts of water-reducing agent；
0.3-0.6 parts of green body reinforcing agent；
44-70 parts of deionized water.
2. full impregnated polished glazed tile according to claim 1, which is characterized in that in terms of parts by weight, the full impregnated polishes porcelain
Brick includes mainly following components：
30 parts of ball clay；
15 parts of albite；
8.5 parts of silica flour；
11.5 parts of wollastonite；
5.5 parts of water mill feldspar in powder
2.05 parts of waterglass；
0.6 part of water-reducing agent；
0.5 part of green body reinforcing agent；
57 parts of deionized water.
3. full impregnated polished glazed tile according to claim 1, which is characterized in that the water-reducing agent is polycarboxylate water-reducer.
4. full impregnated polished glazed tile according to claim 1, which is characterized in that the green body reinforcing agent is by carboxymethyl cellulose
One or more of sodium, polyvinyl alcohol, polyvinyl butyral and polyethylene glycol.
5. a kind of preparation method according to claims 1-4 any one of them full impregnated polished glazed tiles, which is characterized in that packet
Include following steps：
Step 1：Raw material preparation:Each raw material is weighed by regulation number, and carries out mixing outfit, obtains mixture a1；
Step 2：Ball milling：In step 1 mixture a1 and deionized water be added in ball mill and carry out mixed grinding, form slurry
a2；
Step 3：Mist projection granulating：Slurry a1 injections in step 2 are in the spray drying tower dried it, is granulated, is formed
Powder a3；
Step 4：Punch forming：Press machine is added in powder a3 in step 3 and carries out cloth, punch forming, obtains ceramic tile blank
a4；
Step 5：Calcining：Ceramic tile blank a4 in step 4 is put into kiln and is calcined, full impregnated ceramic tile a5 is obtained；
Step 6：Polishing：Full impregnated ceramic tile a5 in step 5 is polished process, obtains full impregnated polished glazed tile.
6. the preparation method of full impregnated polished glazed tile according to claim 5, which is characterized in that the item of the ball milling in step 2
Part：To grind 40-60min under 400-500rpmn speed.
7. the preparation method of full impregnated polished glazed tile according to claim 5, which is characterized in that press machine in step 4
Pressure is 30-40Mpa.
8. the preparation method of full impregnated polished glazed tile according to claim 5, which is characterized in that the firing calcined in step 5
Temperature is 1150-1250 DEG C, and the time of firing is 50-60 minutes.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| IT201800009672A1 (en) * | 2018-10-22 | 2020-04-22 | Caolino Panciera Spa | ADDITIVED CERAMIC MIX |
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| CN101948302A (en) * | 2010-09-15 | 2011-01-19 | 高邑县力马建陶有限公司 | Totally transparent micropowder polished ceramic tile |
| CN103979999A (en) * | 2014-05-21 | 2014-08-13 | 佛山市东鹏陶瓷有限公司 | Full-impregnated travertine ceramic tile |
| CN106495493A (en) * | 2016-10-11 | 2017-03-15 | 常州市鼎日环保科技有限公司 | A kind of preparation method of crystallite stone ceramic tile |
| CN107324789A (en) * | 2017-07-12 | 2017-11-07 | 合肥信亚达智能科技有限公司 | A kind of full impregnated micropowder polished ceramic tile and preparation method thereof |
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| CN103979999A (en) * | 2014-05-21 | 2014-08-13 | 佛山市东鹏陶瓷有限公司 | Full-impregnated travertine ceramic tile |
| CN106495493A (en) * | 2016-10-11 | 2017-03-15 | 常州市鼎日环保科技有限公司 | A kind of preparation method of crystallite stone ceramic tile |
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