CN1083554A - Method for preparation of anti-creasing agent of clothes - Google Patents
Method for preparation of anti-creasing agent of clothes Download PDFInfo
- Publication number
- CN1083554A CN1083554A CN 92110156 CN92110156A CN1083554A CN 1083554 A CN1083554 A CN 1083554A CN 92110156 CN92110156 CN 92110156 CN 92110156 A CN92110156 A CN 92110156A CN 1083554 A CN1083554 A CN 1083554A
- Authority
- CN
- China
- Prior art keywords
- clothes
- microencapsulation
- emulsification
- oil
- beta
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 238000000034 method Methods 0.000 title claims abstract description 8
- 238000002360 preparation method Methods 0.000 title claims description 8
- WHGYBXFWUBPSRW-FOUAGVGXSA-N beta-cyclodextrin Chemical compound OC[C@H]([C@H]([C@@H]([C@H]1O)O)O[C@H]2O[C@@H]([C@@H](O[C@H]3O[C@H](CO)[C@H]([C@@H]([C@H]3O)O)O[C@H]3O[C@H](CO)[C@H]([C@@H]([C@H]3O)O)O[C@H]3O[C@H](CO)[C@H]([C@@H]([C@H]3O)O)O[C@H]3O[C@H](CO)[C@H]([C@@H]([C@H]3O)O)O3)[C@H](O)[C@H]2O)CO)O[C@@H]1O[C@H]1[C@H](O)[C@@H](O)[C@@H]3O[C@@H]1CO WHGYBXFWUBPSRW-FOUAGVGXSA-N 0.000 claims abstract description 16
- 229920000858 Cyclodextrin Polymers 0.000 claims abstract description 14
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 14
- 239000000575 pesticide Substances 0.000 claims abstract description 14
- 239000001116 FEMA 4028 Substances 0.000 claims abstract description 13
- 235000011175 beta-cyclodextrine Nutrition 0.000 claims abstract description 13
- 229960004853 betadex Drugs 0.000 claims abstract description 13
- 238000006243 chemical reaction Methods 0.000 claims abstract description 11
- 238000004945 emulsification Methods 0.000 claims abstract description 9
- 239000002994 raw material Substances 0.000 claims abstract description 5
- 235000013599 spices Nutrition 0.000 claims abstract description 3
- 239000007864 aqueous solution Substances 0.000 claims description 12
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 claims description 9
- 239000000243 solution Substances 0.000 claims description 7
- 238000003756 stirring Methods 0.000 claims description 7
- 239000000203 mixture Substances 0.000 claims description 6
- TUNFSRHWOTWDNC-UHFFFAOYSA-N tetradecanoic acid Chemical compound CCCCCCCCCCCCCC(O)=O TUNFSRHWOTWDNC-UHFFFAOYSA-N 0.000 claims description 6
- DTGKSKDOIYIVQL-WEDXCCLWSA-N (+)-borneol Chemical compound C1C[C@@]2(C)[C@@H](O)C[C@@H]1C2(C)C DTGKSKDOIYIVQL-WEDXCCLWSA-N 0.000 claims description 5
- 229920001661 Chitosan Polymers 0.000 claims description 5
- DTGKSKDOIYIVQL-MRTMQBJTSA-N Isoborneol Natural products C1C[C@@]2(C)[C@H](O)C[C@@H]1C2(C)C DTGKSKDOIYIVQL-MRTMQBJTSA-N 0.000 claims description 5
- CKDOCTFBFTVPSN-UHFFFAOYSA-N borneol Natural products C1CC2(C)C(C)CC1C2(C)C CKDOCTFBFTVPSN-UHFFFAOYSA-N 0.000 claims description 5
- DTGKSKDOIYIVQL-UHFFFAOYSA-N dl-isoborneol Natural products C1CC2(C)C(O)CC1C2(C)C DTGKSKDOIYIVQL-UHFFFAOYSA-N 0.000 claims description 5
- 229940105132 myristate Drugs 0.000 claims description 5
- DSSYKIVIOFKYAU-XCBNKYQSSA-N (R)-camphor Chemical compound C1C[C@@]2(C)C(=O)C[C@@H]1C2(C)C DSSYKIVIOFKYAU-XCBNKYQSSA-N 0.000 claims description 4
- 229930008380 camphor Natural products 0.000 claims description 4
- 239000007788 liquid Substances 0.000 claims description 4
- 239000002304 perfume Substances 0.000 claims description 3
- 239000000047 product Substances 0.000 claims description 3
- HIQIXEFWDLTDED-UHFFFAOYSA-N 4-hydroxy-1-piperidin-4-ylpyrrolidin-2-one Chemical compound O=C1CC(O)CN1C1CCNCC1 HIQIXEFWDLTDED-UHFFFAOYSA-N 0.000 claims description 2
- QTBSBXVTEAMEQO-UHFFFAOYSA-M Acetate Chemical compound CC([O-])=O QTBSBXVTEAMEQO-UHFFFAOYSA-M 0.000 claims description 2
- 239000000706 filtrate Substances 0.000 claims description 2
- WHGYBXFWUBPSRW-UHFFFAOYSA-N Cycloheptaamylose Natural products O1C(C(C2O)O)C(CO)OC2OC(C(C2O)O)C(CO)OC2OC(C(C2O)O)C(CO)OC2OC(C(C2O)O)C(CO)OC2OC(C(O)C2O)C(CO)OC2OC(C(C2O)O)C(CO)OC2OC2C(O)C(O)C1OC2CO WHGYBXFWUBPSRW-UHFFFAOYSA-N 0.000 claims 3
- 241000723346 Cinnamomum camphora Species 0.000 claims 1
- 229960000846 camphor Drugs 0.000 claims 1
- 238000001914 filtration Methods 0.000 claims 1
- 229920002521 macromolecule Polymers 0.000 claims 1
- 239000000463 material Substances 0.000 claims 1
- HFHDHCJBZVLPGP-UHFFFAOYSA-N schardinger α-dextrin Chemical compound O1C(C(C2O)O)C(CO)OC2OC(C(C2O)O)C(CO)OC2OC(C(C2O)O)C(CO)OC2OC(C(O)C2O)C(CO)OC2OC(C(C2O)O)C(CO)OC2OC2C(O)C(O)C1OC2CO HFHDHCJBZVLPGP-UHFFFAOYSA-N 0.000 claims 1
- 239000007787 solid Substances 0.000 claims 1
- 239000004744 fabric Substances 0.000 abstract description 11
- 230000037303 wrinkles Effects 0.000 abstract description 6
- 230000000694 effects Effects 0.000 abstract description 5
- 239000003205 fragrance Substances 0.000 abstract description 3
- 230000002045 lasting effect Effects 0.000 abstract description 3
- 229920005615 natural polymer Polymers 0.000 abstract description 3
- 239000000835 fiber Substances 0.000 abstract description 2
- 239000002775 capsule Substances 0.000 abstract 1
- 238000005538 encapsulation Methods 0.000 abstract 1
- 239000000839 emulsion Substances 0.000 description 3
- TWJNQYPJQDRXPH-UHFFFAOYSA-N 2-cyanobenzohydrazide Chemical compound NNC(=O)C1=CC=CC=C1C#N TWJNQYPJQDRXPH-UHFFFAOYSA-N 0.000 description 1
- AXISYYRBXTVTFY-UHFFFAOYSA-N Isopropyl tetradecanoate Chemical compound CCCCCCCCCCCCCC(=O)OC(C)C AXISYYRBXTVTFY-UHFFFAOYSA-N 0.000 description 1
- 235000021360 Myristic acid Nutrition 0.000 description 1
- 239000012752 auxiliary agent Substances 0.000 description 1
- 230000003796 beauty Effects 0.000 description 1
- 239000008367 deionised water Substances 0.000 description 1
- 229910021641 deionized water Inorganic materials 0.000 description 1
- 230000005611 electricity Effects 0.000 description 1
- 239000003995 emulsifying agent Substances 0.000 description 1
- 239000000796 flavoring agent Substances 0.000 description 1
- 235000019634 flavors Nutrition 0.000 description 1
- 239000002960 lipid emulsion Substances 0.000 description 1
- 239000003094 microcapsule Substances 0.000 description 1
- 239000000376 reactant Substances 0.000 description 1
- 230000003068 static effect Effects 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Images
Landscapes
- Fats And Perfumes (AREA)
- Chemical Or Physical Treatment Of Fibers (AREA)
Abstract
A kind of anti-creasing agent of clothes is to be made up of anti-moth pesticide, perfumery oil, beta-cyclodextrin and shitosan.The present invention is prepared from raw material through technical process such as dissolving, emulsification, mixing, microencapsulation reactions.The present invention is by the fiber molecule strong bonded of natural polymer molecule and fabric, impel the gauffer of fabric and clothes open and flat well-pressed, adopt micro-encapsulation technology simultaneously, make the spices and the anti-moth pesticide that are wrapped in the capsule be able to slow release, play mothproof and effect lasting fragrance the desinsection of clothes and fabric.
Product of the present invention can press clothes and fabric down at 60 ℃, makes it open and flat well-pressed, also can go wrinkle to clothes under no flatiron condition.
Description
Along with The development in society and economy, living standards of the people also improve thereupon, and increasing people is also improving constantly the requirement of dress, not only pursues the style of clothes, and the dress of attention clothes is wanted well-pressed displaying people's beauty in appearance, this just too busy to get away arrangement to clothes.Traditional clothes arrangement is promptly gone to wrinkle well-pressed, is that labour intensity is also big by electricity flatiron, event consumes energy and poor working environment.I prepare a kind of clothes anti-creasing agent after deliberation, it both can be at flatiron clothes and fabric below 60 ℃, make it smooth well-pressed, also can under no flatiron condition, go wrinkle for family and traveller to clothes, and can be according to user's needs, increase lasting diverse fragrant flavour, its function is to utilize the hole of beta-cyclodextrin molecule, to store perfume molecules and anti-moth pesticide, and through the reaction of the microencapsulation of natural polymer, make the spices and the anti-moth pesticide that are wrapped up by microcapsules be able to slow release, play mothproof and effect lasting fragrance, simultaneously owing to the natural polymer molecule, under the effect of auxiliary agent to the desinsection of clothes and fabric, with the fiber molecule strong bonded of fabric, impel the wrinkle Zhe of fabric and clothes open and flat well-pressed.
The objective of the invention is to fill up the blank in market, a kind of clothes anti-creasing agent preparation method be provided, realize that technical scheme of the present invention is:
One, raw material is formed (weight %)
A, anti-creasing agent is formed
Anti-moth pesticide 2～5
Beta-cyclodextrin 0.5～5
Isopropyl myristate 0.5～2
Perfumery oil 0.5～1
5% shitosan acetic acid solution adds to 100
B, anti-moth pesticide is formed
Blue camphorated oil 3～8
Gum Camphor 5～15
Isoborneol fat 5～15
Two, preparation technology's method
(1) anti-moth pesticide preparation technology
(proportioning is 2～5: 1), carry out emulsification respectively, filter then and mix, be mixed into anti-moth pesticide again with water-soluble Gum Camphor filtrate with the 5% beta-cyclodextrin aqueous solution and blue camphorated oil and isoborneol fat.
(2) anti-creasing agent preparation technology
1. pretreatment of raw material
A, the beta-cyclodextrin deionized water dissolving, solid-to-liquid ratio is 5: 95, filter the dissolving back, discards insoluble matter, is the 5% beta-cyclodextrin aqueous solution, as emulsifying agent in the system.
B, shitosan dissolves with acetate, and solid-to-liquid ratio is 5: 95, and filter the dissolving back, discards insoluble matter, is 5% shitosan acetic acid solution.
C, the myristic acid isopropyl ester carries out emulsification with the 5% beta-cyclodextrin aqueous solution (solid-to-liquid ratio is 1: 2～5), crosses then and discards insoluble matter, becomes the myristate emulsion.
D, perfumery oil carries out emulsification (volume ratio is 1: 2～5) with the 5% beta-cyclodextrin aqueous solution, and leaving standstill becomes the perfumery oil emulsion.
2. microencapsulation reaction process
A adds 5% chitosan aqueous solution in the agent of desinsection moth, mix under stirring condition, makes it form particulate and carries out the microencapsulation reaction.
B with myristic acid fat emulsion and perfumery oil emulsion and 5% beta-cyclodextrin aqueous solution, carries out the microencapsulation reaction under stirring condition.
C, with a, b two parts microencapsulation reactant liquor mixes, and adds 5% chitosan aqueous solution, carries out second time microencapsulation and reacts, and is finished product in static 24 hours.
The anti wrinkling agent that the present invention produces has following characteristics:
1, the anti wrinkling agent produced of the present invention has been filled up the blank in market.
2, product of the present invention not only has crease-resistant effect, and it is mothproof and discharge the effect of fragrance to have desinsection concurrently.
3, the present invention is used on clothes or fabric crease-resistant, and every square metre of consumption is 15ml only, and is economical convenient, practicality.
4, anti wrinkling agent both can be used for having the wrinkle of going of flatiron garment fabric condition, also can be used for the wrinkle of going without the clothes that press.
5, anti wrinkling agent can press clothes and fabric at lower temperature below 60 ℃, makes it smooth well-pressed, but conservation of power and reducing labor intensity.
Description of drawings
The encapsulated reaction process flow chart of Fig. 1 anti-creasing agent
Fig. 2 anti-moth pesticide preparation technology flow chart
Claims (4)
1, a kind of method for preparation of anti-creasing agent of clothes comprises anti-moth pesticide, spices, macromolecular compound, it is characterized in that the anti wrinkling agent raw material consists of (weight %)
Anti-moth pesticide 2～5
Perfumery oil 0.5～1
Beta-cyclodextrin 0.5～5
Isopropyl myristate 0.5～2
5% shitosan acetic acid solution adds to 100
Anti-moth pesticide contains in the composition
Blue camphorated oil 3～8
Gum Camphor 5～15
Isoborneol fat 5～15
Above-mentioned raw materials all need dissolve respectively, the reaction of emulsification, microencapsulation.
2, method according to claim 1, it is characterized in that anti-moth pesticide system with blue camphorated oil, isoborneol fat under stirring condition, respectively with the 5% beta-cyclodextrin aqueous solution carry out emulsification, filter blue camphorated oil, isoborneol fat mixes by 1: 3～5 with the ratio of the beta-cyclodextrin aqueous solution, mix again with the camphor filtrate after the water-soluble.
3, method according to claim 1 is characterized in that
A, beta-cyclodextrin filter with water-soluble (Gu: liquid is 5: 95) becomes the 5% cycloheptaamylose aqueous solution;
B dissolves shitosan (liquid-solid ratio is 95: 5) with acetate, removes insoluble matter after filtration, becomes 5% chitosan solution;
C, myristate and perfumery oil use 5% cycloheptaamylose aqueous solution emulsification respectively under stirring condition, myristate, perfumery oil are 1: 2～5 with the ratio of cyclodextrine solution, filter respectively then, leave standstill, and become emulsification myristate and emulsify perfume oil.
4, method according to claim 1 is characterized in that substep carries out the microencapsulation reaction.
A, anti-moth pesticide and 5% chitosan solution mix under stirring condition, carry out the microencapsulation reaction,
B, emulsification myristate and the emulsify perfume oil and the 5% cycloheptaamylose aqueous solution mix under stirring condition, carry out the microencapsulation reaction,
C, with a, b two parts microencapsulation material mixes under stirring condition, adds 5% chitosan solution and carries out the microencapsulation reaction of second step, leaves standstill and is finished product in 24 hours.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 92110156 CN1083554A (en) | 1992-09-04 | 1992-09-04 | Method for preparation of anti-creasing agent of clothes |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 92110156 CN1083554A (en) | 1992-09-04 | 1992-09-04 | Method for preparation of anti-creasing agent of clothes |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN1083554A true CN1083554A (en) | 1994-03-09 |
Family
ID=4944643
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 92110156 Pending CN1083554A (en) | 1992-09-04 | 1992-09-04 | Method for preparation of anti-creasing agent of clothes |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN1083554A (en) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1297706C (en) * | 2003-06-03 | 2007-01-31 | 陈立成 | Crease-proof finishing agent of non-methanol fabric and producing method thereof |
| CN100429345C (en) * | 2006-07-28 | 2008-10-29 | 上海应用技术学院 | Method of perfuming on textile using rose, ambargris, santal mixed essence |
| CN103924320A (en) * | 2014-04-09 | 2014-07-16 | 浙江华峰氨纶股份有限公司 | Spandex with long-acting insect-resistant performance and preparation method thereof |
| CN105297420A (en) * | 2015-11-30 | 2016-02-03 | 无锡新德印染制品有限公司 | Method of performing mothproof treatment on real silk fabric |
-
1992
- 1992-09-04 CN CN 92110156 patent/CN1083554A/en active Pending
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1297706C (en) * | 2003-06-03 | 2007-01-31 | 陈立成 | Crease-proof finishing agent of non-methanol fabric and producing method thereof |
| CN100429345C (en) * | 2006-07-28 | 2008-10-29 | 上海应用技术学院 | Method of perfuming on textile using rose, ambargris, santal mixed essence |
| CN103924320A (en) * | 2014-04-09 | 2014-07-16 | 浙江华峰氨纶股份有限公司 | Spandex with long-acting insect-resistant performance and preparation method thereof |
| CN103924320B (en) * | 2014-04-09 | 2015-12-02 | 浙江华峰氨纶股份有限公司 | A kind of have spandex of long-acting insect protected performance and preparation method thereof |
| CN105297420A (en) * | 2015-11-30 | 2016-02-03 | 无锡新德印染制品有限公司 | Method of performing mothproof treatment on real silk fabric |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN101649254B (en) | Double-layer capsule wall microcapsule essence and preparation method and application thereof | |
| US5071706A (en) | Oily, free-flowing, microcapsules | |
| US5043161A (en) | Small, oily, free-flowing, silky-smooth, talc-like, dry microcapsules and aqueous formulations containing them | |
| US5414079A (en) | Oxidized cellulose | |
| EP0306236A2 (en) | Controlled release formulations | |
| JPH03148206A (en) | Novel cosmetic composition containing chitosan and glucosamine | |
| US20090028916A1 (en) | Loaded Microspheres | |
| CN104755065A (en) | Improvements relating to encapsulated benefit agents | |
| CN105797660B (en) | A kind of method for preparing capsule of oil-soluble etherified amino resin | |
| CN103541227A (en) | Natural essential oil aromatic finishing agent for real silk fabrics and preparation method thereof | |
| CN110433741B (en) | Aromatic antibacterial microcapsule with carbon skeleton and preparation method thereof | |
| CN1083554A (en) | Method for preparation of anti-creasing agent of clothes | |
| CN1073711A (en) | Microcapsule aromatizing agent and preparation method thereof and purposes | |
| CN106074684A (en) | Slow-releasing sachet and preparation method thereof | |
| EP0009540A2 (en) | Fragrance compositions | |
| CN104607119A (en) | Acetic acid styracin nanometer capsule and preparation method thereof | |
| CN114933939A (en) | Essence microcapsule with biodegradable wall material and application thereof in liquid detergent | |
| CN100491510C (en) | Process for preparing nano grade essence perfumery | |
| CN109260029A (en) | A kind of water-soluble nano essential oil micellar solution and preparation method thereof | |
| US20090022764A1 (en) | Organic compounds | |
| CN103070788B (en) | Sustained-release sweet osmanthus perfume | |
| JPH049838B2 (en) | ||
| CN103610665B (en) | A kind of method preparing oil-soluble medicine slow releasing capsule | |
| CN108096217A (en) | A kind of preparation method of tanshinone solid lipid nano particle | |
| CN104758971B (en) | A kind of preparation method of pure natural jasmine solid aromatic |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C06 | Publication | ||
| PB01 | Publication | ||
| C01 | Deemed withdrawal of patent application (patent law 1993) | ||
| WD01 | Invention patent application deemed withdrawn after publication |