CN108354866A - A kind of preparation method of anti-ageing face mask - Google Patents

A kind of preparation method of anti-ageing face mask Download PDF

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CN108354866A
CN108354866A CN201810341549.5A CN201810341549A CN108354866A CN 108354866 A CN108354866 A CN 108354866A CN 201810341549 A CN201810341549 A CN 201810341549A CN 108354866 A CN108354866 A CN 108354866A
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phases
stirring
agitated kettle
heated
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陈桂芳
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/19Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9789Magnoliopsida [dicotyledons]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/08Anti-ageing preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/41Particular ingredients further characterized by their size
    • A61K2800/413Nanosized, i.e. having sizes below 100 nm
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/59Mixtures
    • A61K2800/592Mixtures of compounds complementing their respective functions
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/59Mixtures
    • A61K2800/592Mixtures of compounds complementing their respective functions
    • A61K2800/5922At least two compounds being classified in the same subclass of A61K8/18

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  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Veterinary Medicine (AREA)
  • Public Health (AREA)
  • General Health & Medical Sciences (AREA)
  • Animal Behavior & Ethology (AREA)
  • Epidemiology (AREA)
  • Birds (AREA)
  • Dermatology (AREA)
  • Mycology (AREA)
  • Microbiology (AREA)
  • Botany (AREA)
  • Biotechnology (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical & Material Sciences (AREA)
  • Inorganic Chemistry (AREA)
  • Gerontology & Geriatric Medicine (AREA)
  • Cosmetics (AREA)

Abstract

The invention discloses a kind of preparation methods of anti-ageing face mask, include the following steps:1 8% glycerine, 1 8% propylene glycol, 0.1 0.3% carbomer, 0.03 0.1% xanthans, 2 6% glycine betaines, 0.1 0.5% creatine, 0.03 0.08% dipotassium glycyrrhizinate, 0.01 0.05% Sodium Hyaluronate, 0.1 0.3% Chlorphenesin, deionized water are mixed to be added in agitated kettle and are heated to 70 85 DEG C, stirring and dissolving is complete, and A phases are made;0.8 1.8% polyglycereol, 3 methyl distearate, 0.5 1% cetostearyl alcohol, 0.5 1.5% octyl polymethyl siloxane, 2.5 4.5% dimethyl silicone polymers are added in agitated kettle and are heated to 70 85 DEG C, B phases are made;B is added to A phases, 1 8min of emulsifying homogeneous is cooled to 40 50 DEG C, and 0.1 0.3% triethanolamine is added and stirs evenly, 0.1 4% Herba Saxifragae extract, 0.1 6% Khotan jade superfine nano powder, 0.1 4% Fructus Canarii extract, 0.5 1% Phenoxyethanol is added, discharges after stirring.The present invention can effectively remove extra free radical, play anti-oxidant, anti-aging effects.

Description

A kind of preparation method of anti-ageing face mask
Technical field
The present invention relates to cosmetic fields, and in particular to a kind of preparation method of anti-ageing face mask.
Background technology
With advancing age, the natural Green Tea Extract of human body, oxidation resistant ability constantly decline, the cell meeting aging of people, The problems such as also will produce pigmentation, pachylosis in appearance of people, human tissue organ also can rapid aging.Free radical is to draw An important factor for playing skin aging, air pollution, pressure, drug etc. can all be such that body generates free radicals.There are one free radical contains Or the molecule of multiple unpaired electrons or a part for molecule, there is the tendency of pairing.Therefore most of free radicals are all very active, Chemism with height.Under normal circumstances, the free radical in human body is in the dynamic equilibrium for constantly generating with removing Among.But free radical is generated excessive or was removed slowly, it can cause body by attacking life macromolecule substance and various cells Various damages, accelerate the ageing process of body, show the variation of gradual aging, such as age pigment deposition, skin corrugation.
Currently, the anti-aging effects unobvious of commercially available common anti-ageing face mask, some also added irritation chemicals Matter, improper use are easy that wrinkle is accelerated to occur and cutis laxa occur, cause skin disease.Therefore, prepare it is a kind of safer, Efficient anti-ageing face mask have become there is an urgent need to.
Invention content
In view of the deficiencies of the prior art, the purpose of the present invention is to provide a kind of preparation methods of anti-ageing face mask.
In order to reach the purpose of the present invention, adopt the following technical scheme that:
A kind of preparation method of anti-ageing face mask, includes the following steps:
(4) by 1-8% glycerine, 1-8% propylene glycol, 0.1-0.3% carbomers, 0.03-0.1% xanthans, 2-6% beets Alkali, 0.1-0.5% creatines, 0.03-0.08% dipotassium glycyrrhizinates, 0.01-0.05% Sodium Hyaluronates, 0.1-0.3% chlorobenzenes are sweet Ether, deionized water mixing are added in agitated kettle and are heated to 70-85 DEG C, and stirring and dissolving is complete, and A phases are made;
(5) by 0.8-1.8% polyglycereol-3-methyl distearates, 0.5-1% cetostearyl alcohols, 0.5-1.5% Octyl polymethyl siloxane, 2.5-4.5% dimethyl silicone polymers, which are added in agitated kettle, is heated to 70-85 DEG C, and B phases are made;
(6) B is added to A phases, emulsifying homogeneous 1-8min is cooled to 40-50 DEG C, and 0.1-0.3% triethanolamines are added and stir It mixes uniformly, 0.1-4% Herba Saxifragae extracts, 0.1-6% Khotan jade superfine nanos powder, 0.1-4% Fructus Canarii extracts, 0.5- is added 1% Phenoxyethanol discharges after stirring.
Wherein, the diameter of the Khotan jade superfine nano powder in above-mentioned steps (3) is between 0.01 nanometer -100 nanometers.
Preferably, the preparation method of the anti-ageing face mask, includes the following steps:
(1) by 2-6% glycerine, 2-6% propylene glycol, 0.15-0.25% carbomers, 0.05-0.08% xanthans, 3-5% Glycine betaine, 0.2-0.4% creatines, 0.03-0.07% dipotassium glycyrrhizinates, 0.02-0.04% Sodium Hyaluronates, 0.15-0.25% Chlorphenesin, deionized water mixing are added in agitated kettle and are heated to 75-85 DEG C, and stirring and dissolving is complete, and A phases are made;
(2) by 1-1.5% polyglycereol-3-methyl distearates, 0.6-0.8% cetostearyl alcohols, 0.6-1.2% Octyl polymethyl siloxane, 2.8-3.8% dimethyl silicone polymers, which are added in agitated kettle, is heated to 75-85 DEG C, and B phases are made;
(3) B is added to A phases, emulsifying homogeneous 3-5min is cooled to 45-50 DEG C, and 0.1-0.3% triethanolamines are added and stir It mixes uniformly, 0.5-3.8% Herba Saxifragae extracts, 0.5-5.5% Khotan jade superfine nanos powder, the extraction of 0.2-3.6% Chinese olives is added Object, 0.6-0.8% Phenoxyethanols, discharge after stirring.
Wherein, the diameter of the Khotan jade superfine nano powder in above-mentioned steps (3) is between 0.01 nanometer -100 nanometers.
Preferably, the preparation method of the anti-ageing face mask, includes the following steps:
(1) by 4% glycerine, 4% propylene glycol, 0.2% carbomer, 0.07% xanthans, 4.5% glycine betaine, 0.3% flesh Acid, the mixing of 0.05% dipotassium glycyrrhizinate, 0.03% Sodium Hyaluronate, 0.2% Chlorphenesin, deionized water are added in agitated kettle and add For heat to 75-85 DEG C, stirring and dissolving is complete, and A phases are made;
(2) by 1.2% polyglycereol-3-methyl distearate, 0.7% cetostearyl alcohol, the poly- methyl of 0.8% octyl Siloxanes, 3% dimethyl silicone polymer, which are added in agitated kettle, is heated to 75-85 DEG C, and B phases are made;
(3) B is added to A phases, emulsifying homogeneous 3-5min is cooled to 45-50 DEG C, and it is equal that the stirring of 0.2% triethanolamine is added It is even, 3.5% Herba Saxifragae extract, 4% Khotan jade superfine nano powder, 2% Fructus Canarii extract, 0.7% Phenoxyethanol is added, fully It discharges after stirring evenly.
Wherein, the diameter of the Khotan jade superfine nano powder in above-mentioned steps (3) is between 0.01 nanometer -100 nanometers.
Following introduce is made to the fractions in the present invention:
Kiss-me, alias gold thread hang lotus, rotten Auricled Hedyotis Herb, stone lotus, spun gold lotus leaf, ear grass, are saxifragaceae plant tiger The herb of Auricled Hedyotis Herb Saxifraga stolonifera Meerb. has wind-dispelling, heat-clearing, removing pattogenic heat from the blood and toxic material from the body and other effects.Kiss-me has It is because wherein containing a large amount of flavone compound, most study is Quercetin, quercitin there are many bioactivity.This Outer its also contains some organic acids, steroid and polyphenol compound, such as Bergenin, protocatechuic acid, succinic acid, nutgall Acid, the ingredient to a coumaric acid, sitosterol, Kaempferol, daucosterol, bergenin etc. with larger medical value.The cards such as Cui Wei Clear kiss-me can pass through the O that degrades2And H2O2For avirulent H2O and O2, remove oxygen radical and lipid peroxidation confrontation tissue Damage, play anti-aging effects.The Kaempferol that contains in kiss-me, Bergenin, Quercetin, quercitin, gallic acid, original The substances such as catechuic acid and sitosterol all have different degrees of antioxidation, illustrate that the content of its antioxidant content is very high.
Chinese olive, alias olive are the famous and high-quality fruits of south China, have promote the production of body fluid to quench thirst, open taste, is aid digestion, solution controls larynx Disease etc. is medicinal and health-care efficacy.The a variety of chemical compositions contained in Chinese olive have higher pharmacological activity, especially can wherein carry Take the superoxides of separation greater activity
- dismutase is O in body2Natural scavenger, protection cell can be played the role of, anti-aging equally has hydroxyl The peroxidase and catalase of the inhibiting effect of base radicals scavenging effect and superoxide radical, this 3 kinds of antioxidases There is mutually coordinated effect when injury caused by extra superoxide anion in removing machine body.
Khotan jade category dolomitic marble and intermediate acidity magmatic rock contact metasomatism and the metamorphic rock formed, Chinese Gem Studies are pointed out For nephrite mohs hardness between 6.0-6.5, the jade that tremolite composition accounts for 98% or more is all named as Khotan jade, includes sudden strain of a muscle More mineral aggregates such as stone, hornblend, actinolite.It is micro- containing 13 kinds of calcium, iron, manganese, zinc, copper etc. in the mineral composition of Khotan jade Secondary element, they are beneficial to human body, and ancient medicine is classical《The Yellow Emperor's Canon of Internal Medicine》、《Tang materia medica》、《Legendary god of farming's book on Chinese herbal medicine》、《Compendium of Materia Medica》 Claim Khotan jade can " enriching yin gas, invigorating kidney yang, except it is middle heat, solution be tired of depressed and discontented, embellish lung, help sound larynx, grow hair, support the five internal organs, peace soul, Dredge blood vessels, bright knowledge ".
Compared with prior art, the present invention has the advantages that:
(1) anti-ageing face mask prepared by the present invention, by Khotan jade superfine nano powder, Herba Saxifragae extract and Fructus Canarii extract Carry out reasonable compatibility, scientific matching makes different effective active composition generate synergistic function, can effectively remove it is extra from By base, anti-oxidant, anti-aging effects are played.
(2) the Khotan jade superfine nano powder in facial mask of the present invention has extremely strong activation, adsorption function, can activate flesh Skin accelerates skin metabolism, while its trace element being rich in can also be that skin supplements the nutrients, and skin is enabled to restore smooth, soft Tender, younger state;Herba Saxifragae extract can remove the damage of oxygen radical and lipid peroxidation confrontation tissue, and Fructus Canarii extract contains There are many antioxidases, can further remove extra free radical, play the role of protection cell, anti-aging.
(3) anti-ageing face mask that prepared by the present invention is mildly non-stimulated to skin, and preparation process is simple, adapts to industrial metaplasia Production.
Specific implementation mode
Below in conjunction with specific embodiment, the present invention is further elaborated.
A kind of formula of anti-ageing face mask prepared by 1-3 of the embodiment of the present invention see the table below 1:
Table 1
A kind of preparation methods of anti-ageing face mask of above-described embodiment 1-3 include the following steps:
(1) by glycerine, propylene glycol, carbomer, xanthans, glycine betaine, creatine, dipotassium glycyrrhizinate, Sodium Hyaluronate, chlorobenzene Sweet ether, deionized water mixing are added in agitated kettle and are heated to 70-85 DEG C, and stirring and dissolving is complete, and A phases are made;
(2) by polyglycereol-3-methyl distearate, cetostearyl alcohol, octyl polymethyl siloxane, poly dimethyl Siloxanes is added in agitated kettle and is heated to 70-85 DEG C, and B phases are made;
(3) B is added to A phases, emulsifying homogeneous 3-5min is cooled to 40-50 DEG C, and it is equal that the stirring of 0.2% triethanolamine is added It is even, 2% Herba Saxifragae extract, 3% Khotan jade superfine nano powder, 2% Fructus Canarii extract, 0.7% Phenoxyethanol is added, fully stirs Discharging after mixing uniformly.
Wherein, in above-mentioned steps (3) diameter of Khotan jade superfine nano powder between 0.01 nanometer -100 nanometers.
Comparative example 1
Difference with embodiment 1 is that Herba Saxifragae extract is not added, other preparation conditions and method are same as Example 1.
Comparative example 2
Difference with embodiment 1 is that Khotan jade superfine nano powder, other preparation conditions and method and 1 phase of embodiment are not added Together.
Comparative example 3
Difference with embodiment 1 is that Fructus Canarii extract is not added, other preparation conditions and method are same as Example 1.
Comparative example 4
Difference with embodiment 1 is that Khotan jade superfine nano powder, Herba Saxifragae extract, Fructus Canarii extract are not added, other Preparation condition and method are same as Example 1.
Embodiment 4
Mouse skin irritant test
(1) test specimen:Anti-ageing face mask prepared by embodiment 1-3;
(2) test method:With reference to (cosmetics health specification) 2007 Ministry of Public Health's health legal system and supervision department;
(3) experimental animal:Small white mouse;
(4) test result:It is anti-to be showed no stimulation using the embodiment 1-3 anti-ageing face masks prepared for 7 days Skin Irritation Tests It answers;It can be seen that anti-ageing face mask prepared by the present invention is mildly non-stimulated.
Embodiment 5
Atraumatic human efficiency evaluates
Detection result on probation is carried out to embodiment 1-3 and comparative example the 1-4 anti-ageing face mask prepared.Test object:Each reality It is 30 women (25-50 Sui) to test group;Test zone:Face;It uses:Once a day, it persistently uses 28 days;Test event: The soft degree of humidity of skin, skin, wrinkle depth.Result on trial see the table below 2:
Table 2
As can be seen from Table 2, the anti-ageing face mask that prepared by embodiment 1-3 shows good guarantor compared with comparative example 1-4 Wet, crease-resistant and anti-aging effects;Embodiment 1-3 shows Khotan jade superfine nano powder, kiss-me extraction compared with comparative example 1-3 Object, Fructus Canarii extract have synergistic function.
Above example only illustrates embodiment of the present invention, and there is no have limitation in any form to the present invention;Appoint What is engaged in professional and technical personnel, all has the ability to make some changes or modification using the technology contents disclosed, becomes equivalent The equivalent embodiment of variation carries out simple modification, equivalent change and modification to the present invention, belongs to according to the technology of the present invention essence In the range of technical solution of the present invention.

Claims (4)

1. a kind of preparation method of anti-ageing face mask, which is characterized in that include the following steps:
(1) by 1-8% glycerine, 1-8% propylene glycol, 0.1-0.3% carbomers, 0.03-0.1% xanthans, 2-6% glycine betaines, 0.1-0.5% creatines, 0.03-0.08% dipotassium glycyrrhizinates, 0.01-0.05% Sodium Hyaluronates, 0.1-0.3% Chlorphenesins, Deionized water mixing, which is added in agitated kettle, is heated to 70-85 DEG C, and stirring and dissolving is complete, and A phases are made;
(2) by 0.8-1.8% polyglycereol-3-methyl distearates, 0.5-1% cetostearyl alcohols, 0.5-1.5% octyls Polymethyl siloxane, 2.5-4.5% dimethyl silicone polymers, which are added in agitated kettle, is heated to 70-85 DEG C, and B phases are made;
(3) B is added to A phases, emulsifying homogeneous 1-8min is cooled to 40-50 DEG C, and it is equal that the stirring of 0.1-0.3% triethanolamines is added It is even, 0.1-4% Herba Saxifragae extracts, 0.1-6% Khotan jade superfine nanos powder, 0.1-4% Fructus Canarii extracts, 0.5-1% is added Phenoxyethanol discharges after stirring.
2. the preparation method of anti-ageing face mask as described in claim 1, which is characterized in that include the following steps:
(1) by 2-6% glycerine, 2-6% propylene glycol, 0.15-0.25% carbomers, 0.05-0.08% xanthans, 3-5% beets Alkali, 0.2-0.4% creatines, 0.03-0.07% dipotassium glycyrrhizinates, 0.02-0.04% Sodium Hyaluronates, 0.15-0.25% chlorobenzenes Sweet ether, deionized water mixing are added in agitated kettle and are heated to 75-85 DEG C, and stirring and dissolving is complete, and A phases are made;
(2) by 1-1.5% polyglycereol-3-methyl distearates, 0.6-0.8% cetostearyl alcohols, 0.6-1.2% octyls Polymethyl siloxane, 2.8-3.8% dimethyl silicone polymers, which are added in agitated kettle, is heated to 75-85 DEG C, and B phases are made;
(3) B is added to A phases, emulsifying homogeneous 3-5min is cooled to 45-50 DEG C, and it is equal that the stirring of 0.1-0.3% triethanolamines is added It is even, be added 0.5-3.8% Herba Saxifragae extracts, 0.5-5.5% Khotan jade superfine nanos powder, 0.2-3.6% Fructus Canarii extracts, 0.6-0.8% Phenoxyethanols discharge after stirring.
3. the preparation method of anti-ageing face mask as claimed in claim 2, which is characterized in that include the following steps:
(1) by 4% glycerine, 4% propylene glycol, 0.2% carbomer, 0.07% xanthans, 4.5% glycine betaine, 0.3% creatine, 0.05% dipotassium glycyrrhizinate, 0.03% Sodium Hyaluronate, 0.2% Chlorphenesin, deionized water mixing are added in agitated kettle and heat To 75-85 DEG C, stirring and dissolving is complete, and A phases are made;
(2) by 1.2% polyglycereol-3-methyl distearate, 0.7% cetostearyl alcohol, 0.8% octyl methyl polysilicone Alkane, 3% dimethyl silicone polymer, which are added in agitated kettle, is heated to 75-85 DEG C, and B phases are made;
(3) B is added to A phases, emulsifying homogeneous 3-5min is cooled to 45-50 DEG C, and 0.2% triethanolamine is added and stirs evenly, adds Enter 3.5% Herba Saxifragae extract, 4% Khotan jade superfine nano powder, 2% Fructus Canarii extract, 0.7% Phenoxyethanol, is sufficiently stirred Discharging after uniformly.
4. the preparation method of anti-ageing face mask as described in claim any one of 1-3, which is characterized in that the step (3) neutralizes The diameter of field jade superfine nano powder is between 0.01 nanometer -100 nanometers.
CN201810341549.5A 2018-04-17 2018-04-17 A kind of preparation method of anti-ageing face mask Withdrawn CN108354866A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110669588A (en) * 2019-11-06 2020-01-10 山东花物堂生物科技有限公司 Distillation method for extracting ginger essential oil and application of distillation method in cosmetics

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110669588A (en) * 2019-11-06 2020-01-10 山东花物堂生物科技有限公司 Distillation method for extracting ginger essential oil and application of distillation method in cosmetics

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Application publication date: 20180803