CN108329812A - A kind of flame-proof antibiotic composite building coating and preparation method thereof - Google Patents
A kind of flame-proof antibiotic composite building coating and preparation method thereof Download PDFInfo
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- CN108329812A CN108329812A CN201711469578.1A CN201711469578A CN108329812A CN 108329812 A CN108329812 A CN 108329812A CN 201711469578 A CN201711469578 A CN 201711469578A CN 108329812 A CN108329812 A CN 108329812A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D133/00—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Coating compositions based on derivatives of such polymers
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D175/00—Coating compositions based on polyureas or polyurethanes; Coating compositions based on derivatives of such polymers
- C09D175/04—Polyurethanes
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/14—Paints containing biocides, e.g. fungicides, insecticides or pesticides
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/18—Fireproof paints including high temperature resistant paints
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
- C08K3/20—Oxides; Hydroxides
- C08K3/22—Oxides; Hydroxides of metals
- C08K2003/221—Oxides; Hydroxides of metals of rare earth metal
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
- C08K3/20—Oxides; Hydroxides
- C08K3/22—Oxides; Hydroxides of metals
- C08K2003/2255—Oxides; Hydroxides of metals of molybdenum
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/32—Phosphorus-containing compounds
- C08K2003/321—Phosphates
- C08K2003/322—Ammonium phosphate
- C08K2003/323—Ammonium polyphosphate
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K2201/00—Specific properties of additives
- C08K2201/011—Nanostructured additives
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
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- Plant Pathology (AREA)
- Paints Or Removers (AREA)
Abstract
The present invention discloses a kind of flame-proof antibiotic composite building coating, including the raw material of following mass fraction is prepared：20 parts of aqueous polyurethane, 21 parts of polyurethane acrylate resin, 17 parts of water-based acrylic resin lotion, 3 parts of sodium metasilicate, 2 parts of ammonium polyphosphate, 2 parts of amber sulfonate, 0.5 part of silanes antifoaming agent, 70 parts of deionized water.Invention additionally discloses a kind of methods preparing above-mentioned Environmental Protective Water-paint.The present invention has the advantages that environmental protection, good flame retardation effect.
Description
Technical field
The present invention relates to technical field of environmental protection paint more particularly to a kind of flame-proof antibiotic composite building coating and its preparations
Method.
Background technology
It is every with water as solvent or to make the coating of decentralized medium, it all can be described as water paint.According to adhesive in coating
Classification, water paint are divided into two major classes：The natural water paint of natural materials or minerals (such as potassium silicate) and artificial synthesized
The petrochemical industry water paint of resin (such as acrylic resin).Only the water paint of artificial synthetic resin's class is explained herein
It states.
Water paint includes water soluble paint, water-reducible coating, 3 kinds of water-dispersible paint (latex paint).It is water-soluble
Coating be using water-soluble resin as film forming matter, using polyvinyl alcohol and its various modifiers as representative, in addition to this also water-soluble alcohol
Acid resin, water-soluble epoxy resin and inorganic polymer water-base resin etc..The water paint of the prior art mostly uses halogen flame,
It is larger to environmental hazard, and the water paint of the prior art is to be improved in terms of flame retardant property.In addition, the coating of the prior art
Antibacterial effect, strength stability it is to be improved.
Invention content
In view of the deficiencies of the prior art, the present invention provides environmental protection, good flame retardation effect, good anti-bacterial effect, stable mechanical properties
Flame-proof antibiotic composite building coating and preparation method thereof.
The present invention is realized by following technological means solves above-mentioned technical problem：A kind of flame-proof antibiotic composite building painting
Material, including the raw material of following mass fraction are prepared：20~35 parts of aqueous polyurethane, water-based acrylic resin lotion 17~42
Part, 3~6 parts of sodium metasilicate, 2~4 parts of ammonium polyphosphate, 2~4 parts of amber sulfonate, 10~15 parts of gelatin, 1~3 part of molybdenum oxide, oxygen
Change 2~3 parts of yttrium, 1~2 part of nano-silver ionic, 0.5~2 part of silanes antifoaming agent, 50~70 parts of deionized water.
Preferably, 30 parts of aqueous polyurethane, 36 parts of water-based acrylic resin lotion, 4 parts of sodium metasilicate, 2 parts of ammonium polyphosphate, amber
3 parts of amber sulfonate, 12 parts of gelatin, 2 parts of molybdenum oxide, 2 parts of yttrium oxide, 1 part of nano-silver ionic, 1 part of silanes antifoaming agent, deionization
60 parts of water.
Preferably, including the raw material of following mass fraction is prepared：32 parts of aqueous polyurethane, water-based acrylic resin breast
30 parts of liquid, 5 parts of sodium metasilicate, 3 parts of ammonium polyphosphate, 3 parts of amber sulfonate, 13 parts of gelatin, 3 parts of molybdenum oxide, yttrium oxide 3 part, nanometer
1.5 parts of silver ion, 1.5 parts of silanes antifoaming agent, 65 parts of deionized water.
Preferably, including the raw material of following mass fraction is prepared：25 parts of aqueous polyurethane, water-based acrylic resin breast
35 parts of liquid, 4 parts of ammonium polyphosphate, 2 parts of amber sulfonate, 11 parts of gelatin, 2 parts of molybdenum oxide, 2.5 parts of yttrium oxide, is received 5 parts of sodium metasilicate
2 parts of nano silver ion, 0.5 part of silanes antifoaming agent, 67 parts of deionized water.
Invention additionally discloses a kind of methods preparing above-mentioned flame-proof antibiotic composite building coating, include the following steps：
(1) at room temperature, aqueous polyurethane, water-based acrylic resin lotion are mixed with deionized water, in 300~350r/
5min is stirred under conditions of min；
(2) gelatin is added into the system of step (1), under the conditions of 60~90 DEG C, 300~350r/min react 20~
30min；
(3) sodium metasilicate, ammonium polyphosphate are added into step (2), it is anti-under the conditions of 30~35 DEG C, 300~350r/min
Answer 2~3min；
(4) molybdenum oxide, yttrium oxide, nano-silver ionic are added into the system of step (3), in room temperature, 400~1800r/
20~30min is reacted under the conditions of min；
(5) amber sulfonate is added into the system of step (4), is reacted under the conditions of room temperature, 600~1000r/min
10~15min；
(6) silanes antifoaming agent is added into the system of step (5), is reacted under the conditions of room temperature, 200~300r/min
3~6min obtains product.
The advantage of the invention is that：The present invention, as material of main part, avoids use using hydrophilic water-base resin
The use for the oil-based solvent that DMF, acetone etc. are detrimental to health；Halogen flame, safety are replaced using silicon, phosphorus fire retardant compounding
It is harmless；Its viscosity of coating using the present invention can reach 3300cp or more, and the resistance to combustion time is up to 15min, after the 1h that burns, quality
Retention rate is 86% or more.Using natural degradable gelatin as reinforcing agent, the intensity of coating is improved；Made using rare earth oxide
For adsorbent, the harmful ion in external environment can be appropriately adsorbed；Molybdenum oxide, nano-silver ionic are appropriately added as particle
On the one hand antiseptic can improve the mechanical strength of coating, on the other hand can provide good antibacterial effect.
Specific implementation mode
In order to make the object, technical scheme and advantages of the embodiment of the invention clearer, below in conjunction with the embodiment of the present invention,
Technical scheme in the embodiment of the invention is clearly and completely described, it is clear that described embodiment is the present invention one
Divide embodiment, instead of all the embodiments.Based on the embodiments of the present invention, those of ordinary skill in the art are not making
The every other embodiment obtained under the premise of creative work, shall fall within the protection scope of the present invention.
Embodiment 1
The present embodiment discloses a kind of flame-proof antibiotic composite building coating, including following mass fraction raw material prepare and
At：20 parts of aqueous polyurethane, 17 parts of water-based acrylic resin lotion, 3 parts of sodium metasilicate, 2 parts of ammonium polyphosphate, 2 parts of amber sulfonate,
10 parts of gelatin, 1 part of molybdenum oxide, 2 parts of yttrium oxide, 1 part of nano-silver ionic, 0.5 part of silanes antifoaming agent, 50 parts of deionized water.
Invention additionally discloses a kind of methods preparing above-mentioned flame-proof antibiotic composite building coating, include the following steps：
(1) at room temperature, aqueous polyurethane, water-based acrylic resin lotion are mixed with deionized water, 300r/min's
Under the conditions of stir 5min；
(2) gelatin is added into the system of step (1), reacts 20min under the conditions of 60 DEG C, 300r/min；
(3) sodium metasilicate, ammonium polyphosphate are added into step (2), react 2min under the conditions of 30 DEG C, 300r/min；
(4) molybdenum oxide, yttrium oxide, nano-silver ionic are added into the system of step (3), in room temperature, 400r/min items
20~30min is reacted under part；
(5) amber sulfonate is added into the system of step (4), reacts 10min under the conditions of room temperature, 600r/min；
(6) silanes antifoaming agent is added into the system of step (5), reacts 3min under the conditions of room temperature, 200r/min,
Obtain product.
Embodiment 2
The present embodiment discloses a kind of flame-proof antibiotic composite building coating, including following mass fraction raw material prepare and
At：30 parts of aqueous polyurethane, 36 parts of water-based acrylic resin lotion, 4 parts of sodium metasilicate, 2 parts of ammonium polyphosphate, 3 parts of amber sulfonate,
12 parts of gelatin, 2 parts of molybdenum oxide, 2 parts of yttrium oxide, 1 part of nano-silver ionic, 1 part of silanes antifoaming agent, 60 parts of deionized water.
Invention additionally discloses a kind of methods preparing above-mentioned flame-proof antibiotic composite building coating, include the following steps：
(1) at room temperature, aqueous polyurethane, water-based acrylic resin lotion are mixed with deionized water, 330r/min's
Under the conditions of stir 7min；
(2) gelatin is added into the system of step (1), reacts 30min under the conditions of 70 DEG C, 350r/min；
(3) sodium metasilicate, ammonium polyphosphate are added into step (2), react 2min under the conditions of 35 DEG C, 350r/min；
(4) molybdenum oxide, yttrium oxide, nano-silver ionic are added into the system of step (3), in room temperature, 600r/min items
20min is reacted under part；
(5) amber sulfonate is added into the system of step (4), reacts 15min under the conditions of room temperature, 800r/min；
(6) silanes antifoaming agent is added into the system of step (5), reacts 5min under the conditions of room temperature, 300r/min,
Obtain product.
Embodiment 3
The present embodiment discloses a kind of flame-proof antibiotic composite building coating, including following mass fraction raw material prepare and
At：32 parts of aqueous polyurethane, 30 parts of water-based acrylic resin lotion, 5 parts of sodium metasilicate, 3 parts of ammonium polyphosphate, 3 parts of amber sulfonate,
13 parts of gelatin, 3 parts of molybdenum oxide, 3 parts of yttrium oxide, 1.5 parts of nano-silver ionic, 1.5 parts of silanes antifoaming agent, 65 parts of deionized water.
Invention additionally discloses a kind of methods preparing above-mentioned flame-proof antibiotic composite building coating, include the following steps：
(1) at room temperature, aqueous polyurethane, water-based acrylic resin lotion are mixed with deionized water, 330r/min's
Under the conditions of stir 7min；
(2) gelatin is added into the system of step (1), reacts 30min under the conditions of 70 DEG C, 350r/min；
(3) sodium metasilicate, ammonium polyphosphate are added into step (2), react 2min under the conditions of 35 DEG C, 350r/min；
(4) molybdenum oxide, yttrium oxide, nano-silver ionic are added into the system of step (3), in room temperature, 600r/min items
20min is reacted under part；
(5) amber sulfonate is added into the system of step (4), reacts 15min under the conditions of room temperature, 800r/min；
(6) silanes antifoaming agent is added into the system of step (5), reacts 5min under the conditions of room temperature, 300r/min,
Obtain product.
Embodiment 4
The present embodiment discloses a kind of flame-proof antibiotic composite building coating, including following mass fraction raw material prepare and
At：25 parts of aqueous polyurethane, 35 parts of water-based acrylic resin lotion, 5 parts of sodium metasilicate, 4 parts of ammonium polyphosphate, 2 parts of amber sulfonate,
11 parts of gelatin, 2 parts of molybdenum oxide, 2.5 parts of yttrium oxide, 2 parts of nano-silver ionic, 0.5 part of silanes antifoaming agent, 67 parts of deionized water.
Invention additionally discloses a kind of methods preparing above-mentioned flame-proof antibiotic composite building coating, include the following steps：
(1) at room temperature, aqueous polyurethane, water-based acrylic resin lotion are mixed with deionized water, 330r/min's
Under the conditions of stir 7min；
(2) gelatin is added into the system of step (1), reacts 30min under the conditions of 70 DEG C, 350r/min；
(3) sodium metasilicate, ammonium polyphosphate are added into step (2), react 2min under the conditions of 35 DEG C, 350r/min；
(4) molybdenum oxide, yttrium oxide, nano-silver ionic are added into the system of step (3), in room temperature, 600r/min items
20min is reacted under part；
(5) amber sulfonate is added into the system of step (4), reacts 15min under the conditions of room temperature, 800r/min；
(6) silanes antifoaming agent is added into the system of step (5), reacts 5min under the conditions of room temperature, 300r/min,
Obtain product.
Embodiment 5
The present embodiment discloses a kind of flame-proof antibiotic composite building coating, including following mass fraction raw material prepare and
At：35 parts of aqueous polyurethane, 42 parts of water-based acrylic resin lotion, 6 parts of sodium metasilicate, 4 parts of ammonium polyphosphate, 4 parts of amber sulfonate,
15 parts of gelatin, 3 parts of molybdenum oxide, 3 parts of yttrium oxide, 2 parts of nano-silver ionic, 2 parts of silanes antifoaming agent, 70 parts of deionized water.
Invention additionally discloses a kind of methods preparing above-mentioned flame-proof antibiotic composite building coating, include the following steps：
(1) at room temperature, aqueous polyurethane, water-based acrylic resin lotion are mixed with deionized water, 350r/min's
Under the conditions of stir 5min；
(2) gelatin is added into the system of step (1), reacts 30min under the conditions of 90 DEG C, 350r/min；
(3) sodium metasilicate, ammonium polyphosphate are added into step (2), react 3min under the conditions of 35 DEG C, 350r/min；
(4) molybdenum oxide, yttrium oxide, nano-silver ionic are added into the system of step (3), in room temperature, 1800r/min items
30min is reacted under part；
(5) amber sulfonate is added into the system of step (4), reacts 15min under the conditions of room temperature, 1000r/min；
(6) silanes antifoaming agent is added into the system of step (5), reacts 6min under the conditions of room temperature, 300r/min,
Obtain product.
Embodiment 6
The viscosity of each embodiment of the present invention, flame retardant property, staphylococcus aureus anti-microbial property are as shown in table 1.
Table 1
| Sample | Viscosity cp | Resistance to combustion time min | Antibiotic rate % |
| Embodiment 1 | 3402 | 13 | 93.2 |
| Embodiment 2 | 3388 | 11 | 89.6 |
| Embodiment 3 | 3425 | 15 | 91.2 |
| Embodiment 4 | 3403 | 15 | 90.6 |
| Embodiment 5 | 3362 | 13 | 93.5 |
The above embodiments are merely illustrative of the technical solutions of the present invention, rather than its limitations；Although with reference to the foregoing embodiments
Invention is explained in detail, it will be understood by those of ordinary skill in the art that：It still can be to aforementioned each implementation
Technical solution recorded in example is modified or equivalent replacement of some of the technical features；And these modification or
It replaces, the spirit and scope for various embodiments of the present invention technical solution that it does not separate the essence of the corresponding technical solution.
Claims (5)
1. a kind of flame-proof antibiotic composite building coating, which is characterized in that the raw material including following mass fraction is prepared：Water
20~35 parts of polyurethane of property, 17~42 parts of water-based acrylic resin lotion, 3~6 parts of sodium metasilicate, 2~4 parts of ammonium polyphosphate, amber
2~4 parts of sulfonate, 10~15 parts of gelatin, 1~3 part of molybdenum oxide, 2~3 parts of yttrium oxide, 1~2 part of nano-silver ionic, silanes disappear
0.5~2 part of infusion, 50~70 parts of deionized water.
2. flame-proof antibiotic composite building coating according to claim 1, which is characterized in that including following mass fraction
Raw material is prepared：30 parts of aqueous polyurethane, 36 parts of water-based acrylic resin lotion, 4 parts of sodium metasilicate, 2 parts of ammonium polyphosphate, amber
3 parts of sulfonate, 12 parts of gelatin, 2 parts of molybdenum oxide, 2 parts of yttrium oxide, 1 part of nano-silver ionic, 1 part of silanes antifoaming agent, deionized water
60 parts.
3. flame-proof antibiotic composite building coating according to claim 1, which is characterized in that including following mass fraction
Raw material is prepared：32 parts of aqueous polyurethane, 30 parts of water-based acrylic resin lotion, 5 parts of sodium metasilicate, 3 parts of ammonium polyphosphate, amber
3 parts of sulfonate, 13 parts of gelatin, 3 parts of molybdenum oxide, 3 parts of yttrium oxide, 1.5 parts of nano-silver ionic, 1.5 parts of silanes antifoaming agent, go from
65 parts of sub- water.
4. flame-proof antibiotic composite building coating according to claim 1, which is characterized in that including following mass fraction
Raw material is prepared：25 parts of aqueous polyurethane, 35 parts of water-based acrylic resin lotion, 5 parts of sodium metasilicate, 4 parts of ammonium polyphosphate, amber
2 parts of sulfonate, 11 parts of gelatin, 2 parts of molybdenum oxide, 2.5 parts of yttrium oxide, 2 parts of nano-silver ionic, 0.5 part of silanes antifoaming agent, go from
67 parts of sub- water.
5. a kind of method preparing flame-proof antibiotic composite building coating according to any one of claims 1-4, feature exist
In including the following steps：
(1) at room temperature, aqueous polyurethane, water-based acrylic resin lotion are mixed with deionized water, 300~350r/min's
Under the conditions of stir 5min；
(2) gelatin is added into the system of step (1), under the conditions of 60~90 DEG C, 300~350r/min react 20~
30min；
(3) sodium metasilicate, ammonium polyphosphate are added into step (2), under the conditions of 30~35 DEG C, 300~350r/min react 2~
3min；
(4) molybdenum oxide, yttrium oxide, nano-silver ionic are added into the system of step (3), in room temperature, 400~1800r/min
Under the conditions of react 20~30min；
(5) amber sulfonate is added into the system of step (4), under the conditions of room temperature, 600~1000r/min react 10~
15min；
(6) silanes antifoaming agent is added into the system of step (5), under the conditions of room temperature, 200~300r/min react 3~
6min obtains product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711469578.1A CN108329812A (en) | 2017-12-29 | 2017-12-29 | A kind of flame-proof antibiotic composite building coating and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711469578.1A CN108329812A (en) | 2017-12-29 | 2017-12-29 | A kind of flame-proof antibiotic composite building coating and preparation method thereof |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109337571A (en) * | 2018-09-30 | 2019-02-15 | 江苏耀兴安全玻璃有限公司 | A kind of glass fireproof coating and preparation method thereof |
| CN111534167A (en) * | 2019-12-26 | 2020-08-14 | 阜阳师范大学 | Preparation method of yttrium oxide modified water-based acrylic coating |
-
2017
- 2017-12-29 CN CN201711469578.1A patent/CN108329812A/en active Pending
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109337571A (en) * | 2018-09-30 | 2019-02-15 | 江苏耀兴安全玻璃有限公司 | A kind of glass fireproof coating and preparation method thereof |
| CN111534167A (en) * | 2019-12-26 | 2020-08-14 | 阜阳师范大学 | Preparation method of yttrium oxide modified water-based acrylic coating |
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