CN108309868A - A kind of air cushion BB frosts containing fullerene - Google Patents
A kind of air cushion BB frosts containing fullerene Download PDFInfo
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
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- A—HUMAN NECESSITIES
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/55—Phosphorus compounds
- A61K8/553—Phospholipids, e.g. lecithin
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/678—Tocopherol, i.e. vitamin E
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- A—HUMAN NECESSITIES
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/735—Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/89—Polysiloxanes
- A61K8/891—Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone
- A61K8/894—Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone modified by a polyoxyalkylene group, e.g. cetyl dimethicone copolyol
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
- A61Q1/12—Face or body powders for grooming, adorning or absorbing
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
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- A61K2800/5922—At least two compounds being classified in the same subclass of A61K8/18
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/805—Corresponding aspects not provided for by any of codes A61K2800/81 - A61K2800/95
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Abstract
The invention discloses a kind of, and the air cushion BB containing fullerene is white, which is characterized in that includes following raw material:25 parts of 10 dimethyl silicone polymers of PEG,0.3 0.8 parts of carbonic acid dioctyl ester,5 parts of fuller olefinic carbon 60 .5,0.5 2 parts of trimethyl silicane alkoxy esters of silicon acis,0.5 1 parts of saualane,0.1 2 parts of lecithin,0.1 5 parts of polymethylsilsesquioxane,0.5 5 parts of Sensiva SC50,0.5 2 parts of tocopherol acetate,0.1 1 parts of toner,0.1 2 parts of thickener,5 10 parts of glycerine,15 parts of Sodium Hyaluronate,0.5 1.5 parts of EDETATE SODIUM,0.5 1 parts of Phenoxyethanol,0.1 0.5 parts of methyl hydroxybenzoate,0.01 0.1 parts of essence,0.5 2 parts of Laurocapram,0.5 2 parts of Rabdosia rubescens extract,0.6 4 parts of fiveleaf carpetweet herb extract,13 parts of soulie barberry bark extract,0.05 0.3 parts of citric acid,40 80 parts of water.Air cushion BB of the present invention frost, can reach it is good anti-sweat, the effect for holding adornment for a long time are also notable in anti-aging aspect effect while repair flaw, can while hiding the flaw skin nutrition, use for a long time, another skin water profit gloss.
Description
Technical field
The present invention relates to cosmetic field, more particularly to a kind of air cushion BB frosts containing fullerene.
Background technology
In recent years, with the increase of the continuous development of cosmetics and the demand for the women that likes to be beautiful, BB frosts are increasingly pursued by people
And become fashion trend.Its underlying cause is that BB frosts are not only easy to use, but also has both foundation cream, sun-proof and isolated product
Effect.The women to like to be beautiful need to only use BB frosts that can possess flawless skin quality and skin sense.
However the BB frosts sold currently on the market, makeup is slow, and adornment sense weight hinders skin, and the effect of moisturizing and anti-aging
Difference, endurance is not good enough after makeup, holds adornment effect about 4h, cannot meet consumer demand, therefore, it is necessary to develop a new
BB frost.
Invention content
Inadequate to solve existing BB frosts adornment sense endurance, moisturizing and anti-aging function are inadequate, provide a kind of containing fullerene
Air cushion BB frost, reach while promoting adornment sense endurance, have both moisturizing and anti-aging function.
In order to achieve the above object, it is achieved by following technical solution:
A kind of air cushion BB frosts containing fullerene, including following raw material:2-5 parts of PEG-10 Polydimethylsiloxane, carbonic acid
0.3-0.8 parts of dioctyl ester .5-5 parts of fuller olefinic carbon 60,0.5-2 parts of trimethyl silicane alkoxy esters of silicon acis, 0.5-1 parts of saualane, lecithin
0.1-2 parts of fat, 0.1-5 parts of polymethylsilsesquioxane, 0.5-5 parts of Sensiva SC50,0.5-2 parts of tocopherol acetate, color
0.1-1 parts of powder, 0.1-2 parts of thickener, 5-10 parts of glycerine, 1-5 parts of Sodium Hyaluronate, 0.5-1.5 parts of EDETATE SODIUM, Phenoxyethanol
0.5-1 parts, 0.1-0.5 parts of methyl hydroxybenzoate .1 parts of 0 .01-0 of essence, 0.5-2 parts of Laurocapram, Rabdosia rubescens extract 0.5-
2 parts, 0.6-4 parts of fiveleaf carpetweet herb extract, 1-3 parts of soulie barberry bark extract, 0.05-0.3 parts of citric acid, 40-80 parts of water.
Preferably, the air cushion BB frosts, including following raw material:2-3 parts of PEG-10 Polydimethylsiloxane, carbonic acid
0.3-0.5 parts of dioctyl ester .5-3 parts of fuller olefinic carbon 60,0.5-2 parts of trimethyl silicane alkoxy esters of silicon acis, 0.5-0.8 parts of saualane, ovum
.1-1 parts of phosphatidase 0,1-3 parts of polymethylsilsesquioxane, 1-3 parts of Sensiva SC50,0.5-1.5 parts of tocopherol acetate, color
0.5-1 parts of powder, 0.6-1.5 parts of thickener, 5-8 parts of glycerine, 2-4 parts of Sodium Hyaluronate, 1.0-1.5 parts of EDETATE SODIUM, benzene oxygen second
0.5-0.8 parts of alcohol, 0.1-0.3 parts of methyl hydroxybenzoate, 0.05-0.1 parts of essence, 1-1.5 parts of Laurocapram, Rabdosia rubescens extract 1-
2 parts, 2-4 parts of fiveleaf carpetweet herb extract, 1-2 parts of soulie barberry bark extract, 0.1-0.2 parts of citric acid, 40-60 parts of water.
Preferably, the air cushion BB frosts, including following raw material:2.5 parts of PEG-10 Polydimethylsiloxane, carbonic acid
0.4 part of dioctyl ester, 2 parts of fullerene, 1.5 parts of trimethyl silicane alkoxy esters of silicon acis, 0.6 part of saualane, 0.8 part of lecithin, poly- first
1.5 parts of base silsesquioxane, 2 parts of Sensiva SC50,1.0 parts of tocopherol acetate, 0.8 part of toner, 0.8 part of thickener are sweet
6 parts of oil, 3 parts of Sodium Hyaluronate, 1.2 parts of EDETATE SODIUM, 0.6 part of Phenoxyethanol, 0.2 part of methyl hydroxybenzoate, 0.2 part of essence, bay
1.2 parts of Azone, 2 parts of Rabdosia rubescens extract, 3 parts of fiveleaf carpetweet herb extract, 1.5 parts of soulie barberry bark extract, 0.15 part of citric acid, water
50 parts.
Preferably, the preparation method of the Rabdosia rubescens extract is:
(1)Rabdosia rubescens is crushed;
(2)Gained Rabdosia rubescens powder is placed in extractor, the mass percent that 4-8 times of Rabdosia rubescens powder weight is added is 0.3-0.8%
Citric acid solution, impregnate 1-2 hour, be then heated to 80-90 DEG C, heat 1-3 hour, filter, collection extracting solution;
(3)The water that filtered granulated slag is added to 2-6 times of weight is heated to 55-60 DEG C, and tune ph values are 5.0-5.8, are added
The cellulase of granulated slag water weight 0.5-1.5% digests 2 hours, and enzymolysis liquid is collected in filtering;
(4)Above-mentioned gained extracting solution is merged with enzymolysis liquid, it is neutrality to adjust ph values, is heated to 65-70 DEG C, then refined filtration obtains refined filtration
Liquid;
(5)Gained refined filtration liquid is concentrated under reduced pressure;
(6)Gained concentrate is spray-dried to get Rabdosia rubescens extract.
Preferably, the preparation method of the fiveleaf carpetweet herb extract is:
(1)Fiveleaf carpetweet herb is taken, the salt of a concentration of 0.1-0.5mol/L as extracting solution is added by 1: 1-1: 200g/ml solid-liquid ratio
Acid solution, then at 70-80 DEG C, mixing speed is taken out after being extracted 1-3 hours under the conditions of being 800-1200rpm/min, through filtering
Afterwards, the solution after removal precipitation is obtained;
(2)Ethyl alcohol, which is added, in solution after gained removal precipitation makes polysaccharide precipitation;
(3)Precipitated liquid is filtered processing, removes solution and obtains sediment, sediment absolute ethyl alcohol, propyl alcohol or acetone is anti-
After backwashing is washed for several times, drying to obtain fiveleaf carpetweet herb extract.
Preferably, the preparation method of the soulie barberry bark extract is:
1)It is 1 in mass ratio by soulie barberry bark powder and water:The ratio of 8-10 mixes, and constant temperature stirs 30- in 70-80 DEG C of water-bath
Input to cycle in colloid mill crushes 3-4 time after 60min, and the stator and rotor clearance in colloid mill are controlled at 30-50 microns, glue
The speed of body mill is 3000-4000rpm/min, and soulie barberry bark forms feed liquid after colloid mill;
2)Feed liquid is put into freeze drying box and is freeze-dried, the cryogenic temperature in freeze drying box is -30~-25 DEG C,
Freeze drying box carries out vacuumize process, and vacuum degree 2-4Pa after reaching -30~-25 DEG C, keeps 2.2~2.5h of the temperature,
50-60 DEG C is then heated to, and keeps 45-50min at such a temperature;85-95 DEG C is then heated to, and is kept at such a temperature
1-1.5h;Then it is cooled to 30-40 DEG C, and keeps at such a temperature and keeps 10-15h at such a temperature;Soulie barberry bark is formed to freeze
Dry powder;
3)Soulie barberry bark freeze-dried powder, glycerine, water mix, and the mass ratio of soulie barberry bark freeze-dried powder and glycerol and water mixed liquor is 1:
15~20, it is filtered after constant temperature stirring extraction 1-3h in 60-70 DEG C of water-bath, merges the filtrate extracted twice, wherein glycerine and water
Volume ratio be 1:5-6;
4)By step(3)The filtrate of gained is through being concentrated in vacuo, to get soulie barberry bark extract after drying.
The preparation method of air cushion BB frosts as described above, including following preparation process:
(1)By parts by weight fullerene, PEG-10 Polydimethylsiloxane, carbonic acid dioctyl ester, trimethyl silicane alkoxy esters of silicon acis, ovum
Phosphatide, polymethylsilsesquioxane, Phenoxyethanol, methyl hydroxybenzoate mixing are warming up to 80-90 DEG C, stir evenly, obtain mixture 1;
(2)It is wherein added thickener to mixture, glycerine, Sensiva SC50, toner, essence, water stirs evenly, must mix
Object 2;
(3)Mixture 2 is cooled to 50-60 DEG C, is added water, EDETATE SODIUM, Sodium Hyaluronate, saualane, Laurocapram stirs
It mixes uniformly, obtains mixture 3;
(4)Mixture 3 is cooled to 40-50 DEG C, tocopherol acetate, Rabdosia rubescens extract, fiveleaf carpetweet herb extract, thorn Huang is added
Coptis extract stirs evenly, and PH to 6.5-6.8 is adjusted with citric acid, stirs evenly to get air cushion BB frosts.
Preferably, the thickener is bentonite.
Preferably, step(1)The temperature is 85 DEG C.
Preferably, step(4)The PH is 6.8.
Advantageous effect:Air cushion BB of the present invention frost can reach good while repair flaw, and anti-sweat holds adornment for a long time
Effect, it is also notable in anti-aging aspect effect, can while hiding the flaw skin nutrition, use for a long time, another skin water moistens gloss.
Main active substances Rabdosia rubescens extract in the present invention, fiveleaf carpetweet herb extract, soulie barberry bark extract are to be insulted respectively to the Chinese medicine winter
Three kinds of grass, fiveleaf carpetweet herb, soulie barberry bark Chinese medicines are handled using completely new extracting method, and obtained extract has very strong screening
The flaw, anti-sweat effect, three kinds of Chinese medical extracts are used in combination with fullerene, and the effect of the screening flaw and anti-sweat, which has, to be significantly increased.This
The product is invented, moisturizing 12h can be reached, for a long time the effect of anti-sweat, not de- adornment.
Specific embodiment
A kind of preparation of the air cushion BB frosts containing fullerene of embodiment 1
A kind of air cushion BB frosts containing fullerene, including following raw material:2 parts of PEG-10 Polydimethylsiloxane, carbonic acid two
0.3 part of monooctyl ester .5 parts of fuller olefinic carbon 60,0.5 part of trimethyl silicane alkoxy esters of silicon acis, 0.5 part of saualane, 0.1 part of lecithin, poly- first
0.1 part of base silsesquioxane, 0.5 part of Sensiva SC50,0.5 part of tocopherol acetate, 0.1 part of toner, 0.1 part of thickener,
5 parts of glycerine, 1 part of Sodium Hyaluronate, 0.5 part of EDETATE SODIUM, 0.5 part of Phenoxyethanol, 0.1 part of methyl hydroxybenzoate, 0 .01 parts of essence,
0.5 part of Laurocapram, 0.5 part of Rabdosia rubescens extract, 0.6 part of fiveleaf carpetweet herb extract, 1 part of soulie barberry bark extract, citric acid
0.05 part, 40 parts of water.
The preparation method of the Rabdosia rubescens extract is:
(1)Rabdosia rubescens is crushed;
(2)Gained Rabdosia rubescens powder is placed in extractor, the lemon that the mass percent of 4 times of Rabdosia rubescens powder weight is 0.3% is added
Acid solution impregnates 1 hour, is then heated to 80 DEG C, heats 1 hour, and extracting solution is collected in filtering;
(3)The water that filtered granulated slag is added to 2 times of weight is heated to 55 DEG C, and it is 5.0 to adjust ph values, adds granulated slag water weight
The cellulase of amount 0.5% digests 2 hours, and enzymolysis liquid is collected in filtering;
(4)Above-mentioned gained extracting solution is merged with enzymolysis liquid, it is neutrality to adjust ph values, is heated to 65 DEG C, then refined filtration obtains refined filtration liquid;
(5)Gained refined filtration liquid is concentrated under reduced pressure;
(6)Gained concentrate is spray-dried to get Rabdosia rubescens extract.
The preparation method of the fiveleaf carpetweet herb extract is:
(1)Fiveleaf carpetweet herb is taken, by 1:The hydrochloric acid solution of a concentration of 0.1mol/L as extracting solution is added in the solid-liquid ratio of 1g/ml, so
Afterwards at 70 DEG C, mixing speed is taken out after being extracted 1 hour under the conditions of being 800rpm/min, after filtering, after obtaining removal precipitation
Solution;
(2)Ethyl alcohol, which is added, in solution after gained removal precipitation makes polysaccharide precipitation;
(3)Precipitated liquid is filtered processing, removes solution and obtains sediment, sediment absolute ethyl alcohol, propyl alcohol or acetone is anti-
After backwashing is washed for several times, drying to obtain fiveleaf carpetweet herb extract.
The preparation method of the soulie barberry bark extract is:
1)It is 1 in mass ratio by soulie barberry bark powder and water:8 ratio mixing is put into 70 DEG C of water-baths after constant temperature stirring 30min
It is crushed 3 times to cycle in colloid mill, the stator and rotor clearance control in colloid mill are in 30 microns, the speed of colloid mill
3000rpm/min, soulie barberry bark forms feed liquid after colloid mill;
2)Feed liquid is put into freeze drying box and is freeze-dried, the cryogenic temperature in freeze drying box is -30 DEG C, and freezing is dry
Dry case carries out vacuumize process, and vacuum degree 2Pa after reaching -30 DEG C, keeps temperature 2.2h, then heats to 50-60 DEG C,
And 45min is kept at such a temperature;85 DEG C are then heated to, and keeps 1h at such a temperature;Then 30 DEG C are cooled to, and at this
At a temperature of keep and keep 10h at such a temperature;Form soulie barberry bark freeze-dried powder;
3)Soulie barberry bark freeze-dried powder, glycerine, water mix, and the mass ratio of soulie barberry bark freeze-dried powder and glycerol and water mixed liquor is 1:
15, it is filtered after constant temperature stirring extraction 1h in 60 DEG C of water-baths, merges the filtrate extracted twice, the volume ratio of wherein glycerine and water is
1:5;
4)By step(3)The filtrate of gained is through being concentrated in vacuo, to get soulie barberry bark extract after drying.
The preparation method of air cushion BB frosts as described above, including following preparation process:
(1)By parts by weight fullerene, PEG-10 Polydimethylsiloxane, carbonic acid dioctyl ester, trimethyl silicane alkoxy esters of silicon acis, ovum
Phosphatide, polymethylsilsesquioxane, Phenoxyethanol, methyl hydroxybenzoate mixing are warming up to 80 DEG C, stir evenly, obtain mixture 1;
(2)It is wherein added thickener to mixture, glycerine, Sensiva SC50, toner, essence, water stirs evenly, must mix
Object 2;
(3)Mixture 2 is cooled to 50 DEG C, water, EDETATE SODIUM, Sodium Hyaluronate, saualane, Laurocapram, stirring is added
Uniformly, mixture 3 is obtained;
(4)Mixture 3 is cooled to 40 DEG C, tocopherol acetate, Rabdosia rubescens extract, fiveleaf carpetweet herb extract, soulie barberry bark is added
Extract stirs evenly, and PH to 6.5 is adjusted with citric acid, stirs evenly to get air cushion BB frosts.
A kind of preparation of the air cushion BB frosts containing fullerene of embodiment 2
A kind of air cushion BB frosts containing fullerene, including following raw material:
2.5 parts of PEG-10 Polydimethylsiloxane, 0.4 part of carbonic acid dioctyl ester, 2 parts of fullerene, trimethyl silicane alkoxy esters of silicon acis
1.5 parts, 0.6 part of saualane, 0.8 part of lecithin, 1.5 parts of polymethylsilsesquioxane, 2 parts of Sensiva SC50, tocopherol second
1.0 parts of acid esters, 0.8 part of toner, 0.8 part of thickener, 6 parts of glycerine, 3 parts of Sodium Hyaluronate, 1.2 parts of EDETATE SODIUM, Phenoxyethanol
0.6 part, 0.2 part of methyl hydroxybenzoate, 0.2 part of essence, 1.2 parts of Laurocapram, 2 parts of Rabdosia rubescens extract, fiveleaf carpetweet herb extract 3
Part, 1.5 parts of soulie barberry bark extract, 0.15 part of citric acid, 50 parts of water.
The preparation method of the Rabdosia rubescens extract is:
(1)Rabdosia rubescens is crushed;
(2)Gained Rabdosia rubescens powder is placed in extractor, the lemon that the mass percent of 6 times of Rabdosia rubescens powder weight is 0.6% is added
Acid solution impregnates 1.5 hours, is then heated to 85 DEG C, heats 2 hours, and extracting solution is collected in filtering;
(3)The water that filtered granulated slag is added to 5 times of weight is heated to 55 DEG C, and it is 5.5 to adjust ph values, adds granulated slag water weight
The cellulase of amount 1% digests 2 hours, and enzymolysis liquid is collected in filtering;
(4)Above-mentioned gained extracting solution is merged with enzymolysis liquid, it is neutrality to adjust ph values, is heated to 68 DEG C, then refined filtration obtains refined filtration liquid;
(5)Gained refined filtration liquid is concentrated under reduced pressure;
(6)Gained concentrate is spray-dried to get Rabdosia rubescens extract.
The preparation method of the fiveleaf carpetweet herb extract is:
(1)Fiveleaf carpetweet herb is taken, the hydrochloric acid solution of a concentration of 0.3mol/L as extracting solution is added by 1: 100g/ml solid-liquid ratio,
Then at 75 DEG C, mixing speed is taken out after being extracted 2 hours under the conditions of being 1000rpm/min, after filtering, after obtaining removal precipitation
Solution;
(2)Ethyl alcohol, which is added, in solution after gained removal precipitation makes polysaccharide precipitation;
(3)Precipitated liquid is filtered processing, removes solution and obtains sediment, sediment absolute ethyl alcohol, propyl alcohol or acetone is anti-
After backwashing is washed for several times, drying to obtain fiveleaf carpetweet herb extract.
The preparation method of the soulie barberry bark extract is:
1)It is 1 in mass ratio by soulie barberry bark powder and water:9 ratio mixing is put into 75 DEG C of water-baths after constant temperature stirring 45min
It is crushed 4 times to cycle in colloid mill, the stator and rotor clearance control in colloid mill are in 50 microns, the speed of colloid mill
3500rpm/min, soulie barberry bark forms feed liquid after colloid mill;
2)Feed liquid is put into freeze drying box and is freeze-dried, the cryogenic temperature in freeze drying box is -25 DEG C, and freezing is dry
Dry case carries out vacuumize process, and vacuum degree 3Pa after reaching -25 DEG C, keeps temperature 2.5h, then heats to 55 DEG C, and
45min is kept at such a temperature;90 DEG C are then heated to, and keeps 1h at such a temperature;Then 35 DEG C are cooled to, and in the temperature
Degree is lower to be kept and keeps 12h at such a temperature;Form soulie barberry bark freeze-dried powder;
3)Soulie barberry bark freeze-dried powder, glycerine, water mix, and the mass ratio of soulie barberry bark freeze-dried powder and glycerol and water mixed liquor is 1:
18, it is filtered after constant temperature stirring extraction 2h in 65 DEG C of water-baths, merges the filtrate extracted twice, the volume ratio of wherein glycerine and water is
1:5;
4)By step(3)The filtrate of gained is through being concentrated in vacuo, to get soulie barberry bark extract after drying.
The preparation method of air cushion BB frosts as described above, including following preparation process:
(1)By parts by weight fullerene, PEG-10 Polydimethylsiloxane, carbonic acid dioctyl ester, trimethyl silicane alkoxy esters of silicon acis, ovum
Phosphatide, polymethylsilsesquioxane, Phenoxyethanol, methyl hydroxybenzoate mixing are warming up to 85 DEG C, stir evenly, obtain mixture 1;
(2)It is wherein added bentonite to mixture, glycerine, Sensiva SC50, toner, essence, water stirs evenly, must mix
Object 2;
(3)Mixture 2 is cooled to 55 DEG C, water, EDETATE SODIUM, Sodium Hyaluronate, saualane, Laurocapram, stirring is added
Uniformly, mixture 3 is obtained;
(4)Mixture 3 is cooled to 45 DEG C, tocopherol acetate, Rabdosia rubescens extract, fiveleaf carpetweet herb extract, soulie barberry bark is added
Extract stirs evenly, and PH to 6.8 is adjusted with citric acid, stirs evenly to get air cushion BB frosts.
A kind of air cushion BB frosts containing fullerene of embodiment 3
A kind of air cushion BB frosts containing fullerene, including following raw material:5 parts of PEG-10 Polydimethylsiloxane, carbonic acid two
0.8 part of monooctyl ester, 5 parts of fullerene, 2 parts of trimethyl silicane alkoxy esters of silicon acis, 1 part of saualane, 2 parts of lecithin, poly- methyl silicon sesquialter
5 parts of oxygen alkane, 5 parts of Sensiva SC50,2 parts of tocopherol acetate, 1 part of toner, 2 parts of thickener, 10 parts of glycerine, Sodium Hyaluronate
5 parts, 01.5 part of EDETATE SODIUM, 1 part of Phenoxyethanol, 0.5 part of methyl hydroxybenzoate, 0.1 part of essence, 2 parts of Laurocapram, Rabdosia rubescens carries
Take 2 parts of object, 4 parts of fiveleaf carpetweet herb extract, 3 parts of soulie barberry bark extract, 0.3 part of citric acid, 80 parts of water.
The preparation method of the Rabdosia rubescens extract is:
(1)Rabdosia rubescens is crushed;
(2)Gained Rabdosia rubescens powder is placed in extractor, the lemon that the mass percent of 8 times of Rabdosia rubescens powder weight is 0.8% is added
Acid solution impregnates 2 hours, is then heated to 90 DEG C, heats 3 hours, and extracting solution is collected in filtering;
(3)The water that filtered granulated slag is added to 6 times of weight is heated to 60 DEG C, and it is 5.8 to adjust ph values, adds granulated slag water weight
The cellulase of amount 1.5% digests 2 hours, and enzymolysis liquid is collected in filtering;
(4)Above-mentioned gained extracting solution is merged with enzymolysis liquid, it is neutrality to adjust ph values, is heated to 70 DEG C, then refined filtration obtains refined filtration liquid;
(5)Gained refined filtration liquid is concentrated under reduced pressure;
(6)Gained concentrate is spray-dried to get Rabdosia rubescens extract.
Preferably, the preparation method of the fiveleaf carpetweet herb extract is:
(1)Fiveleaf carpetweet herb is taken, the hydrochloric acid solution of a concentration of 0.5mol/L as extracting solution is added by 1: 200g/ml solid-liquid ratio,
Then at 80 DEG C, mixing speed is taken out after being extracted 3 hours under the conditions of being 1200rpm/min, after filtering, after obtaining removal precipitation
Solution;
(2)Ethyl alcohol, which is added, in solution after gained removal precipitation makes polysaccharide precipitation;
(3)Precipitated liquid is filtered processing, removes solution and obtains sediment, sediment absolute ethyl alcohol, propyl alcohol or acetone is anti-
After backwashing is washed for several times, drying to obtain fiveleaf carpetweet herb extract.
Preferably, the preparation method of the soulie barberry bark extract is:
1)It is 1 in mass ratio by soulie barberry bark powder and water:10 ratio mixing is thrown in 80 DEG C of water-baths after constant temperature stirring 60min
Enter into colloid mill cycle to crush 4 times, the stator and rotor clearance control in colloid mill are in 50 microns, the speed of colloid mill
4000rpm/min, soulie barberry bark forms feed liquid after colloid mill;
2)Feed liquid is put into freeze drying box and is freeze-dried, the cryogenic temperature in freeze drying box is -25 DEG C, and freezing is dry
Dry case carries out vacuumize process, and vacuum degree 4Pa after reaching -25 DEG C, keeps temperature 2.5h, then heats to 60 DEG C, and
50min is kept at such a temperature;95 DEG C are then heated to, and keeps 1.5h at such a temperature;Then 40 DEG C are cooled to, and at this
At a temperature of keep and keep 15h at such a temperature;Form soulie barberry bark freeze-dried powder;
3)Soulie barberry bark freeze-dried powder, glycerine, water mix, and the mass ratio of soulie barberry bark freeze-dried powder and glycerol and water mixed liquor is 1:
20, it is filtered after constant temperature stirring extraction 3h in 70 DEG C of water-baths, merges the filtrate extracted twice, the volume ratio of wherein glycerine and water is
1: 6;
4)By step(3)The filtrate of gained is through being concentrated in vacuo, to get soulie barberry bark extract after drying.
The preparation method of air cushion BB frosts as described above, including following preparation process:
(1)By parts by weight fullerene, PEG-10 Polydimethylsiloxane, carbonic acid dioctyl ester, trimethyl silicane alkoxy esters of silicon acis, ovum
Phosphatide, polymethylsilsesquioxane, Phenoxyethanol, methyl hydroxybenzoate mixing are warming up to 90 DEG C, stir evenly, obtain mixture 1;
(2)It is wherein added thickener to mixture, glycerine, Sensiva SC50, toner, essence, water stirs evenly, must mix
Object 2;
(3)Mixture 2 is cooled to 60 DEG C, water, EDETATE SODIUM, Sodium Hyaluronate, saualane, Laurocapram, stirring is added
Uniformly, mixture 3 is obtained;
(4)Mixture 3 is cooled to 50 DEG C, tocopherol acetate, Rabdosia rubescens extract, fiveleaf carpetweet herb extract, soulie barberry bark is added
Extract stirs evenly, and PH to 6.8 is adjusted with citric acid, stirs evenly to get air cushion BB frosts.
Comparative example 1
Comparative example 1 the difference from example 2 is that, be free of fullerene, preparation method is same as Example 2 with parameter.
Comparative example 2
Comparative example 2 the difference from example 2 is that, be free of Rabdosia rubescens extract, preparation method and parameter with 2 phase of embodiment
Together.
Comparative example 3
Comparative example 3 the difference from example 2 is that, be free of fiveleaf carpetweet herb extract, preparation method and parameter with 2 phase of embodiment
Together.
Comparative example 4
Comparative example 4 the difference from example 2 is that, be free of soulie barberry bark extract, preparation method and parameter with 2 phase of embodiment
Together.
Comparative example 5
For commercially available BB frosts.
Effect experiment:
One, moistening effect is tested
1. given the test agent:Embodiment 1-3 samples, comparative example 1-5 samples.
2. experimental basis:QB/T 4265-2011《Cosmetics moisture-keeping efficacy evaluation guide》
3. subject:It is 25-35 Sui that each product, which respectively looks for 50 female volunteers, age,.
4. experimental method:Double inner forearms mark recipient site everywhere, are randomly assigned as the areas Tu Yang 1, the areas Tu Yang 2, apply
Tested material is smeared in sample area 3 and check plot, the areas Tu Yang, and check plot does not smear any product, and application area 3cmX3cm is smeared
Dosage:6mg/cm2 , subject sits quietly after 20min, (T0) keratoderma water content before test recipient site sample is smeared, so
Prescribed dose to be pressed afterwards smears tested material, the areas Tu Yang 1, the areas Tu Yang 2, the areas Tu Yang 3 are 30 minutes after smearing tested material, 1 hour,
2 hours, 4 hours, 8 hours, 12 hours, recipient site keratoderma water content is tested, with dry before testing
Paper handkerchief wiping removal the remaining product of skin surface, smear sample before and blank control area skin test before also with dry paper
Towel scrape skin is twice.During experiment, the exposure of subject's forearm places in test mode, keeps loosening.
5. Testing index:Moisture content of skin.
Test environment:25 DEG C of temperature, relative humidity 40%-60%.
6. experimental result
Table 1:Moisture content of skin
0h(%) | 30min(%) | 1h(%) | 2h(%) | 4h(%) | 8h(%) | 12h(%) | |
Embodiment 1 | 36.4 | 68.4 | 68.3 | 67.8 | 67.5 | 66.4 | 66.1 |
Embodiment 2 | 36.7 | 75.1 | 75.0 | 74.8 | 74.2 | 73.2 | 73.0 |
Embodiment 3 | 36.9 | 71.6 | 71.2 | 70.6 | 70.2 | 69.8 | 69.3 |
Comparative example 1 | 35.1 | 48.9 | 46.5 | 45.2 | 43.1 | 42.1 | 41.2 |
Comparative example 2 | 35.4 | 55.4 | 53.1 | 52.4 | 51.6 | 50.0 | 49.2 |
Comparative example 3 | 35.8 | 56.3 | 55.3 | 53.1 | 50.4 | 48.3 | 47.6 |
Comparative example 4 | 35.1 | 54.2 | 53.2 | 51.4 | 49.6 | 48.6 | 46.8 |
Comparative example 5 | 36.8 | 45.6 | 42.1 | 40.8 | 36.4 | 35.4 | 34.3 |
By result above it can be proved that the embodiment of the present invention has the moistening effect up to 12 hours, and moistening effect is notable
Better than comparative example product and commercial product.
2. anti-aging effects
It is effect of the verification skin care item of the invention at crease-resistant aspect, selects 160 volunteers to carry out validity experiment, use
Double-dummy design, contrast experiment carry out comparison investigation.160 volunteers are that men and women is unlimited, and healthy population, the age is 40-55 year
Between, 20 one group of people are randomly divided into 8 groups.The use of embodiment 1 ~ 3 is respectively experimental group 1-3, the use of control group 1-4 products is control
Group 1-4 is control group 5 using commercially available BB frosts.Band adornment 8h, application method are to take to be applied to face in right amount to 8 groups of people daily, are reached
Adornment effect.Regular follow-up investigation is carried out to every user, using skinanalysis apparatus (Derma-Expert MC760) to skin
Friction testing, every 10 days primary for stage test, and test position is both sides cheek.
Record each group volunteer tests the mean value (D0) of skin parameters when starting respectively, skin ginseng when testing the 10th day
Several mean values (D10), and skin parameters when experiment the 20th day mean value (D20), and experiment with computing is opened on the 10th day with experiment
When the beginning difference (D0-D10) of skin parameters mean value and experiment the 20th day with test the 20th day when skin parameters mean value difference
(D10-D20).When volunteer's parameters difference >=5, being considered as skin improves crowd.Skin improvement rate=each group skin changes
Philanthropist's number/each group total number of persons.
2 skin friction power test result of table
(D10-D0) | (D20-D10) | Skin improvement rate(%) | |
Control group 1 | -11.5 | -14.5 | 56 |
Control group 2 | -12.4 | -18.1 | 65 |
Control group 3 | -15.6 | -16.3 | 60 |
Control group 4 | -16.4 | -20.7 | 45 |
Control group 5 | -3.1 | -2.3 | 1 |
Experimental group 1 | -61.5 | -60.4 | 95 |
Experimental group 2 | -82.6 | -88.5 | 100 |
Experimental group 3 | -73.9 | -80.4 | 95 |
As seen from the above table, the value of D10-D0, D20-D10 are smaller, and skin is more smooth, and wrinkle is more shallow.The skin of experimental group improves feelings
Condition is apparently higher than control group and commercially available air cushion BB frosts, and with the best results of experimental group 2.
Please as above 180 using after 20 days name volunteer carry out product evaluated after, extremely hold adornment be 5 points, preferably hold adornment be 4
Point, it is 3 points generally to hold adornment, and it is 2 points not hold adornment;It is 5 points extremely to repair flaw, and it is 4 points preferably to repair flaw, and it is 3 points generally to repair flaw,
It is 2 points not repair flaw;Very anti-sweat is 5 points, and preferable anti-sweat is 4 points, and general anti-sweat is 3 points, and not anti-sweat is 2 points.
Experimental result is as shown in table 3 below:
Table 3:
Hold adornment | Repair flaw | Anti- sweat | |
Control group 1 | 3.5 | 3.8 | 3.6 |
Control group 2 | 3.9 | 4.0 | 4.0 |
Control group 3 | 3.7 | 3.8 | 3.8 |
Control group 4 | 3.5 | 3.6 | 3.9 |
Control group 5 | 3.9 | 3.6 | 3.0 |
Experimental group 1 | 4.6 | 4.6 | 4.6 |
Experimental group 2 | 4.9 | 4.9 | 4.8 |
Experimental group 3 | 4.7 | 4.8 | 4.7 |
By upper table data it is found that the air cushion BB frost users of the present invention think very highly, anti-sweat can be reached, flaw is repaiied, holds adornment for a long time
Effect.
It can be that professional and technical personnel in the field realize or use that the above embodiment, which is intended to illustrate the present invention, to above-mentioned
Embodiment, which is modified, will be apparent to those skilled in the art, therefore the present invention includes but not limited to
The above embodiment, it is any to meet the claims or specification description, meet with principles disclosed herein and novelty,
The method of inventive features, technique, product, each fall within protection scope of the present invention.
Claims (10)
1. a kind of air cushion BB frosts containing fullerene, which is characterized in that include following raw material:PEG-10 polydimethylsiloxanes
2-5 parts of alkane, 0.3-0.8 parts of carbonic acid dioctyl ester .5-5 parts of fuller olefinic carbon 60,0.5-2 parts of trimethyl silicane alkoxy esters of silicon acis, saualane
0.5-1 parts, 0.1-2 parts of lecithin, 0.1-5 parts of polymethylsilsesquioxane, 0.5-5 parts of Sensiva SC50, tocopheryl acetate
0.5-2 parts of ester, 0.1-1 parts of toner, 0.1-2 parts of thickener, 5-10 parts of glycerine, 1-5 parts of Sodium Hyaluronate, EDETATE SODIUM 0.5-
1.5 parts, 0.5-1 parts of Phenoxyethanol, 0.1-0.5 parts of methyl hydroxybenzoate .1 parts of 0 .01-0 of essence, 0.5-2 parts of Laurocapram, the winter
Insult careless 0.5-2 parts of extract, 0.6-4 parts of fiveleaf carpetweet herb extract, 1-3 parts of soulie barberry bark extract, 0.05-0.3 parts of citric acid, water
40-80 parts.
2. air cushion BB frosts according to claim 1, which is characterized in that include following raw material:PEG-10 poly dimethyls
2-3 parts of siloxanes, 0.3-0.5 parts of carbonic acid dioctyl ester .5-3 parts of fuller olefinic carbon 60,0.5-2 parts of trimethyl silicane alkoxy esters of silicon acis, angle
0.5-0.8 parts of shark alkane, 0.1-1 parts of lecithin, 1-3 parts of polymethylsilsesquioxane, 1-3 parts of Sensiva SC50, tocopherol second
0.5-1.5 parts of acid esters, 0.5-1 parts of toner, 0.6-1.5 parts of thickener, 5-8 parts of glycerine, 2-4 parts of Sodium Hyaluronate, EDETATE SODIUM
1.0-1.5 parts, 0.5-0.8 parts of Phenoxyethanol, 0.1-0.3 parts of methyl hydroxybenzoate, 0.05-0.1 parts of essence, Laurocapram 1-1.5
Part, 1-2 parts of Rabdosia rubescens extract, 2-4 parts of fiveleaf carpetweet herb extract, 1-2 parts of soulie barberry bark extract, 0.1-0.2 parts of citric acid, water
40-60 parts.
3. air cushion BB frosts according to claim 2, which is characterized in that include following raw material:PEG-10 poly dimethyls
2.5 parts of siloxanes, 0.4 part of carbonic acid dioctyl ester, 2 parts of fullerene, 1.5 parts of trimethyl silicane alkoxy esters of silicon acis, 0.6 part of saualane,
0.8 part of lecithin, 1.5 parts of polymethylsilsesquioxane, 2 parts of Sensiva SC50,1.0 parts of tocopherol acetate, toner 0.8
Part, 0.8 part of thickener, 6 parts of glycerine, 3 parts of Sodium Hyaluronate, 1.2 parts of EDETATE SODIUM, 0.6 part of Phenoxyethanol, methyl hydroxybenzoate 0.2
Part, 0.2 part of essence, 1.2 parts of Laurocapram, 2 parts of Rabdosia rubescens extract, 3 parts of fiveleaf carpetweet herb extract, soulie barberry bark extract 1.5
Part, 0.15 part of citric acid, 50 parts of water.
4. according to any air cushion BB frosts of claim 1-3, which is characterized in that the preparation method of the Rabdosia rubescens extract
For:(1)Rabdosia rubescens is crushed;
(2)Gained Rabdosia rubescens powder is placed in extractor, the mass percent that 4-8 times of Rabdosia rubescens powder weight is added is 0.3-0.8%
Citric acid solution, impregnate 1-2 hour, be then heated to 80-90 DEG C, heat 1-3 hour, filter, collection extracting solution;
(3)The water that filtered granulated slag is added to 2-6 times of weight is heated to 55-60 DEG C, and tune ph values are 5.0-5.8, are added
The cellulase of granulated slag water weight 0.5-1.5% digests 2 hours, and enzymolysis liquid is collected in filtering;
(4)Above-mentioned gained extracting solution is merged with enzymolysis liquid, it is neutrality to adjust ph values, is heated to 65-70 DEG C, then refined filtration obtains refined filtration
Liquid;
(5)Gained refined filtration liquid is concentrated under reduced pressure;
(6)Gained concentrate is spray-dried to get Rabdosia rubescens extract.
5. according to any air cushion BB frosts of claim 1-3, which is characterized in that the preparation method of the fiveleaf carpetweet herb extract
For:
(1)Fiveleaf carpetweet herb is taken, the salt of a concentration of 0.1-0.5mol/L as extracting solution is added by 1: 1-1: 200g/ml solid-liquid ratio
Acid solution, then at 70-80 DEG C, mixing speed is taken out after being extracted 1-3 hours under the conditions of being 800-1200rpm/min, through filtering
Afterwards, the solution after removal precipitation is obtained;
(2)Ethyl alcohol, which is added, in solution after gained removal precipitation makes polysaccharide precipitation;
(3)Precipitated liquid is filtered processing, removes solution and obtains sediment, sediment absolute ethyl alcohol, propyl alcohol or acetone is anti-
After backwashing is washed for several times, drying to obtain fiveleaf carpetweet herb extract.
6. according to any air cushion BB frosts of claim 1-3, which is characterized in that the preparation method of the soulie barberry bark extract
For:
(1)It is 1 in mass ratio by soulie barberry bark powder and water:The ratio of 8-10 mixes, and constant temperature stirs 30- in 70-80 DEG C of water-bath
Input to cycle in colloid mill crushes 3-4 time after 60min, and the stator and rotor clearance in colloid mill are controlled at 30-50 microns, glue
The speed of body mill is 3000-4000rpm/min, and soulie barberry bark forms feed liquid after colloid mill;
(2)Feed liquid is put into freeze drying box and is freeze-dried, the cryogenic temperature in freeze drying box is -30~-25 DEG C,
Freeze drying box carries out vacuumize process, and vacuum degree 2-4Pa after reaching -30~-25 DEG C, keeps temperature 2.2-2.5h,
50-60 DEG C is then heated to, and keeps 45-50min at such a temperature;85-95 DEG C is then heated to, and is kept at such a temperature
1-1.5h;Then it is cooled to 30-40 DEG C, and keeps at such a temperature and keeps 10-15h at such a temperature;Soulie barberry bark is formed to freeze
Dry powder;
(3)Soulie barberry bark freeze-dried powder, glycerine, water mix, and soulie barberry bark freeze-dried powder and the mass ratio of glycerol and water mixed liquor be
1:15~20, filtered after constant temperature stirring extraction 1-3h in 60-70 DEG C of water-bath, merge the filtrate extracted twice, wherein glycerine with
The volume ratio of water is 1:5-6;
(3)By step(3)The filtrate of gained is through being concentrated in vacuo, to get soulie barberry bark extract after drying.
7. the preparation method of any air cushion BB frosts of claim 1-3, which is characterized in that include following preparation process:
(1)By parts by weight fullerene, PEG-10 Polydimethylsiloxane, carbonic acid dioctyl ester, trimethyl silicane alkoxy esters of silicon acis, ovum
Phosphatide, polymethylsilsesquioxane, Phenoxyethanol, methyl hydroxybenzoate mixing are warming up to 80-90 DEG C, stir evenly, obtain mixture 1;
(2)It is wherein added thickener to mixture, glycerine, Sensiva SC50, toner, essence, water stirs evenly, must mix
Object 2;
(3)Mixture 2 is cooled to 50-60 DEG C, is added water, EDETATE SODIUM, Sodium Hyaluronate, saualane, Laurocapram stirs
It mixes uniformly, obtains mixture 3;
(4)Mixture 3 is cooled to 40-50 DEG C, tocopherol acetate, Rabdosia rubescens extract, fiveleaf carpetweet herb extract, thorn Huang is added
Coptis extract stirs evenly, and PH to 6.5-6.8 is adjusted with citric acid, stirs evenly to get air cushion BB frosts.
8. preparation method according to claim 7, which is characterized in that the thickener is bentonite.
9. preparation method according to claim 7, which is characterized in that step(1)The temperature is 85 DEG C.
10. preparation method according to claim 7, which is characterized in that step(4)The PH is 6.8.
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CN108852943B (en) * | 2018-09-06 | 2021-04-16 | 广州艾蓓生物科技有限公司 | Foundation make-up composition without titanium dioxide and preparation method thereof |
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