CN108301205A - 一种抗紫外阻燃耐光窗帘面料的生产工艺 - Google Patents

一种抗紫外阻燃耐光窗帘面料的生产工艺 Download PDF

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CN108301205A
CN108301205A CN201711101975.3A CN201711101975A CN108301205A CN 108301205 A CN108301205 A CN 108301205A CN 201711101975 A CN201711101975 A CN 201711101975A CN 108301205 A CN108301205 A CN 108301205A
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张根法
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Jiangsu Ruida Textile Technology Co Ltd
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Abstract

本发明公开了一种抗紫外阻燃耐光窗帘面料的生产工艺，是将阻燃聚酯纤维、聚丙烯腈纤维、精硫棉、阻燃尼龙混合纺织成纱线，然后将纱线纺织成半成品面料；将上述制得半成品面料放入整理液中进行浸轧，然后干燥冷却得到成品窗帘面料；所述的整理液包含涂料、Gemini阳离子柔软剂、阻燃剂、微纳米氧化物、烷基聚氧乙烯醚丁二酸酯磺酸盐等组分；阻燃剂由三羟甲基丙烷、亚磷酸三甲酯、磷酸三甲酯按照1:1:1的摩尔比合成得到；Gemini阳离子柔软剂由硬脂酰胺丙基二甲基胺与双(2‑氯乙基)醚按照2：1的摩尔比合成得到。上述方法制取得到的窗帘面料具有良好的抗紫外，高耐光，阻燃性能。

Description

一种抗紫外阻燃耐光窗帘面料的生产工艺
技术领域
本发明涉及窗帘面料生产领域，具体涉及一种抗紫外阻燃耐光窗帘面料的生产工艺。
背景技术
窗帘是居室软装饰的重要组成部分，在现代家居环境的美化及环境营造中发挥着很大的作用。民居、办公室、宾馆、会议室等十分强调采光效果，玻璃窗设计得越来越大，窗帘等内装饰织物会因受到阳光的照射、紫外线的作用而褪色和降解。此外，长时间的曝晒，会使房间内的气温升高。特别在夏季，大窗多窗房间中午室内温度可能超过50℃，而夜间的温度下降，湿度增大。这种冷热循环会进一步导致窗帘织物的褪色和降解，影响窗帘的色彩、图案，乃至使用寿命。另外，由于纺织品大多数具有易燃特性，越来越成为引发室内火灾的主要隐患，因此，从安全、美观、实用等各个角度都需要窗帘面料具有防紫外线、高耐光、阻燃等性能。
发明内容
为解决上述问题，本发明提供了一种抗紫外阻燃耐光窗帘面料的生产工艺，其制取得到的窗帘面料具有良好的抗菌、抗螨虫性能，能够有效降低哮喘的发生。
为实现上述目的，本发明采取的技术方案为：
一种抗紫外阻燃耐光窗帘面料的生产工艺，其特征在于：
将3～3.5重量份的阻燃聚酯纤维、4～5重量份的聚丙烯腈纤维、2～2.5重量份的精硫棉、0.2～0.3重量份的阻燃尼龙混合纺织成纱线，然后将纱线纺织成半成品面料；
将上述制得半成品面料放入整理液中进行浸轧，然后干燥冷却得到成品窗帘面料；所述的整理液包含以下组分：
涂料45～55g/L，涂料白FTW2～4g/L，丙烯酸酯粘合剂15～30g/L，尿素10～20g/L，甘油2～3g/L，Gemini阳离子柔软剂35～40g/L，阻燃剂3～4g/L，微纳米氧化物2.5～15g/L，烷基聚氧乙烯醚丁二酸酯磺酸盐1～2g/L，三苄基酚聚氧乙烯醚2～2.5g/L；
阻燃剂由三羟甲基丙烷、亚磷酸三甲酯、磷酸三甲酯按照1:1:1的摩尔比合成得到；Gemini阳离子柔软剂由硬脂酰胺丙基二甲基胺与双(2-氯乙基)醚按照2：1的摩尔比合成得到。
上述方案制得的窗帘面料具有良好的抗紫外线，高耐光，阻燃性能，同时其使用阻燃聚酯纤维制成的丝线，染色性能好，使用Gemini阳离子柔软剂具有极低的临界胶束浓度，因而在达到同样效果的情况下用量极大地降低。氧化物具有较高的折射率，主要通过对入射紫外线反射或折射达到防紫外线辐射的目的。
在实现本发明的基础上，实验发现不同的原料、整理液制得成品窗帘面料的抗紫外线，高耐光，阻燃性能耗时存在一定差异。通过大量实验分析和优化，最终确定按照如下技术方案进行实施，已取得更好的效果，亦即：
纱线由3重量份的阻燃聚酯纤维、5重量份的聚丙烯腈纤维、2重量份的精硫棉、0.3重量份的阻燃尼龙混合纺织制成。
整理液包含以下组分：涂料50g/L，涂料白FTW3g/L，丙烯酸酯粘合剂25g/L，尿素15g/L，甘油2.5g/L，Gemini阳离子柔软剂38g/L，阻燃剂3.5g/L，微纳米氧化物8g/L，烷基聚氧乙烯醚丁二酸酯磺酸盐1.5g/L，三苄基酚聚氧乙烯醚2.5g/L。
干燥操作包括对浸扎后的面料进行初烘和复烘，初烘的温度为85℃，复烘的温度为145℃。阻燃聚酯纤维为不含磷阻燃聚酯纤维。
具体实施方式
为了使本发明的目的及优点更加清楚明白，以下结合实施例对本发明进行进一步详细说明。应当理解，此处所描述的具体实施例仅仅用以解释本发明，并不用于限定本发明。下述实施例1～3中所用的各原料均可由商业途径购买得到，其中阻燃剂由三羟甲基丙烷、亚磷酸三甲酯、磷酸三甲酯按照1:1:1的摩尔比合成得到；Gemini阳离子柔软剂由硬脂酰胺丙基二甲基胺与双(2-氯乙基)醚按照2：1的摩尔比合成得到。
实施例1
将3重量份的不含磷阻燃聚酯纤维、5重量份的聚丙烯腈纤维、2重量份的精硫棉、0.3重量份的阻燃尼龙混合纺织成纱线，然后将纱线纺织成半成品面料；
分别称取各原料，配置成整理液，配置的整理液组分如下：涂料45g/L，涂料白FTW4g/L，丙烯酸酯粘合剂15g/L，尿素20g/L，甘油2g/L，Gemini阳离子柔软剂40g/L，阻燃剂3g/L，微纳米氧化物15g/L，烷基聚氧乙烯醚丁二酸酯磺酸盐1g/L，三苄基酚聚氧乙烯醚2.5g/L；
向上述整理液中加入渗透剂JFC，使得整理液中JFC含量达到1g/L将上述制得半成品面料放入整理液中进行二浸二轧，轧液率75％，85℃烘干2min，145℃复烘2～3min，然后冷却得到成品窗帘面料。
实施例2
将3重量份的不含磷阻燃聚酯纤维、5重量份的聚丙烯腈纤维、2重量份的精硫棉、0.3重量份的阻燃尼龙混合纺织成纱线，然后将纱线纺织成半成品面料；
分别称取各原料，配置成整理液，配置的整理液组分如下：涂料50g/L，涂料白FTW3g/L，丙烯酸酯粘合剂25g/L，尿素15g/L，甘油2.5g/L，Gemini阳离子柔软剂38g/L，阻燃剂3.5g/L，微纳米氧化物8g/L，烷基聚氧乙烯醚丁二酸酯磺酸盐1.5g/L，三苄基酚聚氧乙烯醚2.5g/L；
向上述整理液中加入渗透剂JFC，使得整理液中JFC含量达到1g/L将上述制得半成品面料放入整理液中进行二浸二轧，轧液率75％，85℃烘干2min，145℃复烘2～3min，然后冷却得到成品窗帘面料。
实施例3
将3.5重量份的不含磷阻燃聚酯纤维、4重量份的聚丙烯腈纤维、2重量份的精硫棉、0.3重量份的阻燃尼龙混合纺织成纱线，然后将纱线纺织成半成品面料；
分别称取各原料，配置成整理液，配置的整理液组分如下：涂料55g/L，涂料白FTW2g/L，丙烯酸酯粘合剂30g/L，尿素20g/L，甘油3g/L，Gemini阳离子柔软剂35g/L，阻燃剂4g/L，微纳米氧化物2.5g/L，烷基聚氧乙烯醚丁二酸酯磺酸盐2g/L，三苄基酚聚氧乙烯醚2.5g/L；
向上述整理液中加入渗透剂JFC，使得整理液中JFC含量达到0.5g/L将上述制得半成品面料放入整理液中进行二浸二轧，轧液率75％，85℃烘干2min，145℃复烘2～3min，然后冷却得到成品窗帘面料。
实施例4
按照下述方法对实施例1～3中制得的窗帘布料进行测试：紫外线透过率(T％)和UPF值：按GB/T18830-测试；耐日晒牢度：按GB/T8427-1998《纺织品色牢度试验耐人造光色牢度：氙弧》；阻燃性能：按GB/T5455-1997《纺织品燃烧性能试验垂直法》；极限氧指数测定：按GB/T5454-1997《纺织品燃烧性能试验氧指数法》；干(湿)摩擦色牢度：按照GB/T5712-1997标准，采用摩擦色牢度试验仪进行测定；耐洗色牢度：按照GB/T3921.1-1997标准，采用耐洗色牢度仪进行测定；遮光率的测试：采用美国AATCC-148-79《窗帘材料遮光效应评定方法》；采取光透射的“箱法”来判断窗帘织物的遮光性能。
对测试值计算透射光率：
式中：T-试样织物的透光率％；A-透过试样反映在光度计上的照度值；B-在光源校准时所测试的光度计上的空白照度值。
测试结果如下表所示：
以上所述仅是本发明的优选实施方式，应当指出，对于本技术领域的普通技术人员来说，在不脱离本发明原理的前提下，还可以作出若干改进和润饰，这些改进和润饰也应视为本发明的保护范围。

Claims (5)

1.一种抗紫外阻燃耐光窗帘面料的生产工艺，其特征在于：
将3～3.5重量份的阻燃聚酯纤维、4～5重量份的聚丙烯腈纤维、2～2.5重量份的精硫棉、0.2～0.3重量份的阻燃尼龙混合纺织成纱线，然后将纱线纺织成半成品面料；
将上述制得半成品面料放入整理液中进行浸轧，然后干燥冷却得到成品窗帘面料；所述的整理液包含以下组分：
涂料45～55g/L，涂料白FTW 2～4g/L，丙烯酸酯粘合剂15～30g/L，尿素10～20g/L，甘油2～3g/L，Gemini阳离子柔软剂35～40g/L，阻燃剂3～4g/L，微纳米氧化物2.5～15g/L，烷基聚氧乙烯醚丁二酸酯磺酸盐1～2g/L，三苄基酚聚氧乙烯醚2～2.5g/L；
阻燃剂由三羟甲基丙烷、亚磷酸三甲酯、磷酸三甲酯按照1:1:1的摩尔比合成得到；Gemini阳离子柔软剂由硬脂酰胺丙基二甲基胺与双(2-氯乙基)醚按照2：1的摩尔比合成得到。
2.如权利要求1所述的抗紫外阻燃耐光窗帘面料的生产工艺，其特征在于：纱线由3重量份的阻燃聚酯纤维、5重量份的聚丙烯腈纤维、2重量份的精硫棉、0.3重量份的阻燃尼龙混合纺织制成。
3.如权利要求1所述的抗紫外阻燃耐光窗帘面料的生产工艺，其特征在于，整理液包含以下组分：涂料50g/L，涂料白FTW 3g/L，丙烯酸酯粘合剂25g/L，尿素15g/L，甘油2.5g/L，Gemini阳离子柔软剂38g/L，阻燃剂3.5g/L，微纳米氧化物8g/L，烷基聚氧乙烯醚丁二酸酯磺酸盐1.5g/L，三苄基酚聚氧乙烯醚2.5g/L。
4.如权利要求1所述的抗紫外阻燃耐光窗帘面料的生产工艺，其特征在于：干燥操作包括对浸扎后的面料进行初烘和复烘，初烘的温度为85℃，复烘的温度为145℃。
5.如权利要求1所述的抗紫外阻燃耐光窗帘面料的生产工艺，其特征在于：阻燃聚酯纤维为不含磷阻燃聚酯纤维。
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CN111377967A (zh) * 2020-02-26 2020-07-07 青岛长荣化工科技有限公司 一种环状膦酸酯阻燃剂的制备方法

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111377967A (zh) * 2020-02-26 2020-07-07 青岛长荣化工科技有限公司 一种环状膦酸酯阻燃剂的制备方法

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