CN108285713A - A kind of metope water-repellent paint and preparation method thereof - Google Patents
A kind of metope water-repellent paint and preparation method thereof Download PDFInfo
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- CN108285713A CN108285713A CN201810204547.1A CN201810204547A CN108285713A CN 108285713 A CN108285713 A CN 108285713A CN 201810204547 A CN201810204547 A CN 201810204547A CN 108285713 A CN108285713 A CN 108285713A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D133/00—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Coating compositions based on derivatives of such polymers
- C09D133/04—Homopolymers or copolymers of esters
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/004—Reflecting paints; Signal paints
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/14—Paints containing biocides, e.g. fungicides, insecticides or pesticides
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K13/00—Use of mixtures of ingredients not covered by one single of the preceding main groups, each of these compounds being essential
- C08K13/04—Ingredients characterised by their shape and organic or inorganic ingredients
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
- C08K3/20—Oxides; Hydroxides
- C08K3/22—Oxides; Hydroxides of metals
- C08K2003/2237—Oxides; Hydroxides of metals of titanium
- C08K2003/2241—Titanium dioxide
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
- C08K3/24—Acids; Salts thereof
- C08K3/26—Carbonates; Bicarbonates
- C08K2003/265—Calcium, strontium or barium carbonate
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K2201/00—Specific properties of additives
- C08K2201/011—Nanostructured additives
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/34—Silicon-containing compounds
- C08K3/36—Silica
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K5/00—Use of organic ingredients
- C08K5/04—Oxygen-containing compounds
- C08K5/10—Esters; Ether-esters
- C08K5/11—Esters; Ether-esters of acyclic polycarboxylic acids
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K5/00—Use of organic ingredients
- C08K5/04—Oxygen-containing compounds
- C08K5/10—Esters; Ether-esters
- C08K5/12—Esters; Ether-esters of cyclic polycarboxylic acids
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K7/00—Use of ingredients characterised by shape
- C08K7/22—Expanded, porous or hollow particles
- C08K7/24—Expanded, porous or hollow particles inorganic
- C08K7/28—Glass
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Plant Pathology (AREA)
- Paints Or Removers (AREA)
Abstract
The invention discloses a kind of metope water-repellent paints and preparation method thereof, are prepared from the following raw materials in parts by weight：65 85 parts of pure-acrylic emulsion, 8 16 parts of titanium dioxide, 3 10 parts of nano silicon dioxide, 10 20 parts of calcium carbonate, 15 parts of sodium base roc profit soil, 15 parts of hollow glass microbead, 0.5 0.8 parts of curing agent, 0.3 0.7 parts of plasticizer, 0.6 1.4 parts of dispersant, 0.4 1.2 parts of mould inhibitor, 22 44 parts of deionized water.Preparation method：（1）Weigh raw material ball milling mixing；（2）Pure-acrylic emulsion, deionized water mixing is added；（3）Curing agent, plasticizer, dispersant, mould inhibitor is added to get metope high-elastic waterproof coating.The high-elastic waterproof coating of the present invention has preferable water resistance and water proofing property, and has stronger resistance of rainwater washing against performance, good weatherability, and preparation method is simple, is easy to industrialized production.
Description
Technical field
The present invention relates to building material technical fields, more particularly, to a kind of metope water-repellent paint and preparation method thereof.
Background technology
Currently, the decoration of construction wall generally uses traditional coating, most coating is only limited to have elastomeric
Feature, water resistance and water proofing property are poor, and weatherability is poor, it is short using birthday noodle the problems such as.Therefore it is normally only used for interior decoration.It is existing
Increasingly focus on living environment in people, so outdoor decoration is also more and more concerned.But it is outdoor different from interior, in ring
Border pollution is increasingly severe, and the rainwater under outdoor is all acid rain, so light waterproof is not all right, also wants that rain acidification can be prevented to apply
Layer, not so after rain drop erosion its paint film will integrally peel off, rainwater just penetrates into metope, corrodes metope, causes damages.
Invention content
Based on this, the present invention provides a kind of metope water-repellent paint, solve current waterproof material water resistance and water proofing property compared with
The problem of difference, weatherability difference and service life short life.
In order to achieve the above object, the present invention is achieved through the following technical solutions：
A kind of metope water-repellent paint, is prepared from the following raw materials in parts by weight：65-85 parts of pure-acrylic emulsion, 8-16 parts of titanium dioxide,
3-10 parts of nano silicon dioxide, 10-20 parts of calcium carbonate, 1-5 parts of soil of sodium base roc profit, 1-5 parts of hollow glass microbead, curing agent 0.5-
0.8 part, 0.3-0.7 parts of plasticizer, 0.6-1.4 parts of dispersant, 0.4-1.2 parts of mould inhibitor, 22-44 parts of deionized water.
Preferably, being prepared from the following raw materials in parts by weight：70 parts of pure-acrylic emulsion, 12 parts of titanium dioxide, nanometer titanium dioxide
7 parts of silicon, 15 parts of calcium carbonate, 3 parts of sodium base roc profit soil, 3 parts of hollow glass microbead, 0.6 part of curing agent, 0.5 part of plasticizer, dispersant
1 part, 0.8 part of mould inhibitor, 31 parts of deionized water.
Preferably, the titanium dioxide is rutile type nano titanic oxide, and the grain of rutile type nano titanic oxide
Diameter is 50nm-200nm.
Preferably, the density range of the hollow glass microbead is 0.4-0.8g/cm3。
Preferably, the curing agent is selected from calcium chloride, zinc chloride, ammonium chloride, aluminium polychloride, bodied ferric sulfate and gathers
Close one or more of aluminium iron sulfate.
Preferably, the plasticizer is dioctyl phthalate, dibutyl phthalate or dioctyl adipate
Or dioctyl sebacate.
Preferably, the dispersant is selected from waterglass, sodium tripolyphosphate, triethyl group hexyl phosphoric acid, dodecyl sulphate
One or more of sodium and methyl anyl alcohol.
Preferably, the mould inhibitor be octyl-isothiazolinone, bis-benzamide, benzimidazole carbamate or
Ethylene bisdithiocarbamic ammonium.
The present invention also provides a kind of preparation methods of metope water-repellent paint, include the following steps：
（1）In parts by weight, titanium dioxide, nano silicon dioxide, calcium carbonate, sodium base roc profit soil, hollow glass are weighed respectively
Microballon ball milling mixing, obtains powder, spare；
（2）Pure-acrylic emulsion, deionized water are added into reaction kettle, heats while stirring, heating temperature is 30-40 DEG C, is added
Step（1）In powder, be uniformly mixed, obtain mixed slurry；
（3）To step（2）In mixed slurry be added curing agent, plasticizer, dispersant, mould inhibitor, continue heating 50-60 DEG C,
It is uniformly mixed, obtains metope water-repellent paint.
Preferably, the step（1）In ball milling mixing condition：Wet-milling 20-30min on ball mill, drum's speed of rotation
For 250-350r/min.
Compared with prior art, the present invention having following advantageous effect：
（1）The present invention and improves coating height by using pure-acrylic emulsion by using the component and content of restriction as base-material
Strength pull ductility makes coating have preferable fracture elongation, and the infiltration to base and cementitiousness reinforcement, together
When, moisten the fillers such as soil, hollow glass microbead by the way that titanium dioxide, nano silicon dioxide, calcium carbonate, sodium base roc is added, further carries
Its high water resistance and weatherability, enhance the intensity of coating, due to the use of be inorganic environment-friendly material, also reduce environment dirt
Dye.
(2) strong weatherability and strong sun light reflective of the present invention using rutile type nano titanic oxide, by applying
Rutile type nano titanic oxide is added in material, to improve the weatherability of water-repellent paint, even if under the direct projection of sunlight
The weatherability that the water-repellent paint of the present invention has also had.
（3）The present invention further improves the elasticity and fatigue performance of pure-acrylic emulsion by addition plasticizer, and adds
Mould inhibitor prevents mildew attack waterproof layer, increases the validity period of water-repellent paint.
（4）The high-elastic waterproof coating of the present invention is used for metope water-proofing treatment, and construction is simple, surface drying time is short, can shorten work
Phase, while sagging is can effectively avoid, the waste in coating application is reduced, and preparation method is simple, is easy to industrialization production.
Specific implementation mode
Form by the following examples is described in further detail the above of the present invention again, but should not be by this
The range for being interpreted as the above-mentioned theme of the present invention is only limitted to following embodiment, all based on the technology realized belonging to the above of the present invention
It all belongs to the scope of the present invention.
Embodiment 1
A kind of metope water-repellent paint, is prepared from the following raw materials in parts by weight：65 parts of pure-acrylic emulsion, 8 part, nanometer two of titanium dioxide
3 parts of silica, 10 parts of calcium carbonate, 1 part of sodium base roc profit soil, 1 part of hollow glass microbead, 0.5 part of curing agent, plasticizer 0.3 part, point
0.6 part of powder, 0.4 part of mould inhibitor, 22 parts of deionized water.
Wherein, the titanium dioxide is rutile type nano titanic oxide, and the grain size of rutile type nano titanic oxide is
50nm-200nm。
Wherein, the density range of the hollow glass microbead is 0.4-0.8g/cm3。
Wherein, the curing agent is selected from calcium chloride, zinc chloride, ammonium chloride, aluminium polychloride, bodied ferric sulfate and polymerised sulphur
One or more of sour ferro-aluminum.
Wherein, the plasticizer is dioctyl phthalate, dibutyl phthalate or dioctyl adipate or the last of the ten Heavenly stems
Adipate.
Wherein, the dispersant be selected from waterglass, sodium tripolyphosphate, triethyl group hexyl phosphoric acid, lauryl sodium sulfate and
One or more of methyl anyl alcohol.
Wherein, the mould inhibitor is octyl-isothiazolinone, bis-benzamide, benzimidazole carbamate or ethylene
Bisdithiocarbamic ammonium.
The present invention also provides a kind of preparation methods of metope water-repellent paint, include the following steps：
（1）In parts by weight, titanium dioxide, nano silicon dioxide, calcium carbonate, sodium base roc profit soil, hollow glass are weighed respectively
Microballon ball milling mixing, obtains powder, spare；
（2）Pure-acrylic emulsion, deionized water are added into reaction kettle, heats while stirring, heating temperature is 30 DEG C, adds step
（1）In powder, be uniformly mixed, obtain mixed slurry；
（3）To step（2）In mixed slurry be added curing agent, plasticizer, dispersant, mould inhibitor, continue heating 50 DEG C, mixing
Uniformly, metope water-repellent paint is obtained.
Wherein, the step（1）In ball milling mixing condition：Wet-milling 20min on ball mill, drum's speed of rotation 250r/
min。
Embodiment 2
A kind of metope water-repellent paint, is prepared from the following raw materials in parts by weight：85 parts of pure-acrylic emulsion, titanium dioxide 16 part, nanometer
0 part of silica 1,20 parts of calcium carbonate, 5 parts of sodium base roc profit soil, 5 parts of hollow glass microbead, 0.8 part of curing agent, plasticizer 0.7
Part, 1.4 parts of dispersant, 1.2 parts of mould inhibitor, 44 parts of deionized water.
Wherein, the titanium dioxide is rutile type nano titanic oxide, and the grain size of rutile type nano titanic oxide is
50nm-200nm。
Wherein, the density range of the hollow glass microbead is 0.4-0.8g/cm3。
Wherein, the curing agent is selected from calcium chloride, zinc chloride, ammonium chloride, aluminium polychloride, bodied ferric sulfate and polymerised sulphur
One or more of sour ferro-aluminum.
Wherein, the plasticizer is dioctyl phthalate, dibutyl phthalate or dioctyl adipate or the last of the ten Heavenly stems
Adipate.
Wherein, the dispersant be selected from waterglass, sodium tripolyphosphate, triethyl group hexyl phosphoric acid, lauryl sodium sulfate and
One or more of methyl anyl alcohol.
Wherein, the mould inhibitor is octyl-isothiazolinone, bis-benzamide, benzimidazole carbamate or ethylene
Bisdithiocarbamic ammonium.
The present invention also provides a kind of preparation methods of metope water-repellent paint, include the following steps：
（1）In parts by weight, titanium dioxide, nano silicon dioxide, calcium carbonate, sodium base roc profit soil, hollow glass are weighed respectively
Microballon ball milling mixing, obtains powder, spare；
（2）Pure-acrylic emulsion, deionized water are added into reaction kettle, heats while stirring, heating temperature is 40 DEG C, adds step
（1）In powder, be uniformly mixed, obtain mixed slurry；
（3）To step（2）In mixed slurry be added curing agent, plasticizer, dispersant, mould inhibitor, continue heating 60 DEG C, mixing
Uniformly, metope water-repellent paint is obtained.
Wherein, the step（1）In ball milling mixing condition：Wet-milling 30min on ball mill, drum's speed of rotation 350r/
min。
Embodiment 3
A kind of metope water-repellent paint, is prepared from the following raw materials in parts by weight：70 parts of pure-acrylic emulsion, titanium dioxide 12 part, nanometer
7 parts of silica, 15 parts of calcium carbonate, sodium base roc profit soil 3 parts, 3 parts of hollow glass microbead, 0.6 part of curing agent, 0.5 part of plasticizer,
1 part of dispersant, 0.8 part of mould inhibitor, 31 parts of deionized water.
Wherein, the titanium dioxide is rutile type nano titanic oxide, and the grain size of rutile type nano titanic oxide is
50nm-200nm。
Wherein, the density range of the hollow glass microbead is 0.4-0.8g/cm3。
Wherein, the curing agent is selected from calcium chloride, zinc chloride, ammonium chloride, aluminium polychloride, bodied ferric sulfate and polymerised sulphur
One or more of sour ferro-aluminum.
Wherein, the plasticizer is dioctyl phthalate, dibutyl phthalate or dioctyl adipate or the last of the ten Heavenly stems
Adipate.
Wherein, the dispersant be selected from waterglass, sodium tripolyphosphate, triethyl group hexyl phosphoric acid, lauryl sodium sulfate and
One or more of methyl anyl alcohol.
Wherein, the mould inhibitor is octyl-isothiazolinone, bis-benzamide, benzimidazole carbamate or ethylene
Bisdithiocarbamic ammonium.
The present invention also provides a kind of preparation methods of metope water-repellent paint, include the following steps：
（1）In parts by weight, titanium dioxide, nano silicon dioxide, calcium carbonate, sodium base roc profit soil, hollow glass are weighed respectively
Microballon ball milling mixing, obtains powder, spare；
（2）Pure-acrylic emulsion, deionized water are added into reaction kettle, heats while stirring, heating temperature is 35 DEG C, adds step
（1）In powder, be uniformly mixed, obtain mixed slurry；
（3）To step（2）In mixed slurry be added curing agent, plasticizer, dispersant, mould inhibitor, continue heating 55 DEG C, mixing
Uniformly, metope water-repellent paint is obtained.
Wherein, the step（1）In ball milling mixing condition：Wet-milling 25min on ball mill, drum's speed of rotation 300r/
min。
Experimental example
According to polymer emulsion water-repellent paint standard《JC/T864-2000》, take water-repellent paint made from embodiment 1-3 and
Commercially available other two water-repellent paint on the market is tested respectively as control group 1 and control group 2：
Obtain the test result such as table 1：
It can be seen from Table 1 that the requirements of metope water-repellent paint obtained are up to state standards through the invention, and also
Better than national standard, apparent advantage is had more relative to other two comparison control groups.
To sum up, the present invention and is improved by using pure-acrylic emulsion as base-material by using the component and content of restriction
Coating high intensity tensile ductility makes coating have preferable fracture elongation, and adds to the infiltration and cementitiousness of base
By force, meanwhile, moisten the fillers such as soil, hollow glass microbead by the way that titanium dioxide, nano silicon dioxide, calcium carbonate, sodium base roc is added, into one
Step improves its water resistance and weatherability, enhances the intensity of coating, due to the use of be inorganic environment-friendly material, also reduce environment
Pollution.
The foregoing is only a preferred embodiment of the present invention, is not intended to restrict the invention, although with reference to aforementioned reality
Applying example, invention is explained in detail, for those skilled in the art, still can be to aforementioned each implementation
Technical solution recorded in example is modified or equivalent replacement of some of the technical features.All essences in the present invention
With within principle, any modification, equivalent replacement, improvement and so on should all be included in the protection scope of the present invention god.
Claims (10)
1. a kind of metope water-repellent paint, which is characterized in that be prepared from the following raw materials in parts by weight：65-85 parts of pure-acrylic emulsion,
8-16 parts of titanium dioxide, 3-10 parts of nano silicon dioxide, 10-20 parts of calcium carbonate, 1-5 parts of soil of sodium base roc profit, hollow glass microbead 1-5
Part, 0.5-0.8 parts of curing agent, 0.3-0.7 parts of plasticizer, 0.6-1.4 parts of dispersant, 0.4-1.2 parts of mould inhibitor, deionized water
22-44 parts.
2. metope water-repellent paint according to claim 1, which is characterized in that be prepared from the following raw materials in parts by weight：
70 parts of pure-acrylic emulsion, 12 parts of titanium dioxide, 7 parts of nano silicon dioxide, 15 parts of calcium carbonate, sodium base roc profit native 3 parts, hollow glass microbead
3 parts, 0.6 part of curing agent, 0.5 part of plasticizer, 1 part of dispersant, 0.8 part of mould inhibitor, 31 parts of deionized water.
3. metope water-repellent paint according to claim 1, which is characterized in that the titanium dioxide is rutile type nano two
Titanium oxide, and the grain size of rutile type nano titanic oxide is 50nm-200nm.
4. metope water-repellent paint according to claim 1, which is characterized in that the density range of the hollow glass microbead
For 0.4-0.8g/cm3。
5. metope water-repellent paint according to claim 1, which is characterized in that the curing agent is selected from calcium chloride, chlorination
One or more of zinc, ammonium chloride, aluminium polychloride, bodied ferric sulfate and polymeric aluminum sulfate iron.
6. metope water-repellent paint according to claim 1, which is characterized in that the plasticizer is that phthalic acid two is pungent
Ester, dibutyl phthalate or dioctyl adipate or dioctyl sebacate.
7. metope water-repellent paint according to claim 1, which is characterized in that the dispersant is selected from waterglass, trimerization
One or more of sodium phosphate, triethyl group hexyl phosphoric acid, lauryl sodium sulfate and methyl anyl alcohol.
8. metope water-repellent paint according to claim 1, which is characterized in that the mould inhibitor is octyl-isothiazolin
Ketone, bis-benzamide, benzimidazole carbamate or ethylene bisdithiocarbamic ammonium.
9. a kind of preparation method according to claim 1-8 any one of them metope water-repellent paints, which is characterized in that including
Following step：
（1）In parts by weight, titanium dioxide, nano silicon dioxide, calcium carbonate, sodium base roc profit soil, hollow glass are weighed respectively
Microballon ball milling mixing, obtains powder, spare；
（2）Pure-acrylic emulsion, deionized water are added into reaction kettle, heats while stirring, heating temperature is 30-40 DEG C, is added
Step（1）In powder, be uniformly mixed, obtain mixed slurry；
（3）To step（2）In mixed slurry be added curing agent, plasticizer, dispersant, mould inhibitor, continue heating 50-60 DEG C,
It is uniformly mixed, obtains metope water-repellent paint.
10. the preparation method of metope water-repellent paint according to claim 9, which is characterized in that the step（1）In
Ball milling mixing condition：Wet-milling 20-30min on ball mill, drum's speed of rotation 250-350r/min.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810204547.1A CN108285713A (en) | 2018-03-13 | 2018-03-13 | A kind of metope water-repellent paint and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810204547.1A CN108285713A (en) | 2018-03-13 | 2018-03-13 | A kind of metope water-repellent paint and preparation method thereof |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110145039A (en) * | 2019-06-20 | 2019-08-20 | 北京中核北研科技发展股份有限公司 | A kind of acrylate copolymer polyester blank in-place forming macromolecule coiled material and construction method |
| CN110342852A (en) * | 2019-08-14 | 2019-10-18 | 向军辉 | A kind of multi-functional photocatalyst aeroge wall covering and preparation method thereof |
| CN110623376A (en) * | 2019-09-29 | 2019-12-31 | 东莞市瑞翔新型材料科技有限公司 | Waterproof metal zipper and manufacturing process thereof |
-
2018
- 2018-03-13 CN CN201810204547.1A patent/CN108285713A/en not_active Withdrawn
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110145039A (en) * | 2019-06-20 | 2019-08-20 | 北京中核北研科技发展股份有限公司 | A kind of acrylate copolymer polyester blank in-place forming macromolecule coiled material and construction method |
| CN110145039B (en) * | 2019-06-20 | 2021-09-03 | 北京中核北研科技发展股份有限公司 | Acrylic polymer polyester tire on-site forming high-molecular coiled material and construction method |
| CN110342852A (en) * | 2019-08-14 | 2019-10-18 | 向军辉 | A kind of multi-functional photocatalyst aeroge wall covering and preparation method thereof |
| CN110623376A (en) * | 2019-09-29 | 2019-12-31 | 东莞市瑞翔新型材料科技有限公司 | Waterproof metal zipper and manufacturing process thereof |
| CN110623376B (en) * | 2019-09-29 | 2022-06-03 | 东莞市瑞翔新型材料科技有限公司 | Waterproof metal zipper and manufacturing process thereof |
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Application publication date: 20180717 |